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HomeMy WebLinkAboutAppendix H-2 Phase II ESA 900 King Street Property 900 KING STREET, RYE BROOK, NEW YORK Subsurface (Phase II) Investigation AKRF Project Number: 170073 Prepared for: 900 King Street Owner, LLC 200 Madison Avenue New York, NY 10016 Prepared by: 34 South Broadway, Suite 401 White Plains, New York 10601 914-949-7336 JANUARY 2018 AKRF, Inc. Subsurface (Phase II) Investigation 900 King Street Property – 900 King Street, Rye Brook, NY i TABLE OF CONTENTS 1.0 Introduction ...................................................................................................................................... 1 2.0 Site Description ................................................................................................................................ 1 3.0 Previous Investigations .................................................................................................................... 2 4.0 Field Activities ................................................................................................................................. 4 4.1 Geophysical Survey and Utility Mark-Outs ................................................................................ 4 4.2 Soil Sampling .............................................................................................................................. 4 4.3 Groundwater Sampling ................................................................................................................ 5 4.4 Soil Vapor Sampling ................................................................................................................... 6 5.0 Investigation Results ........................................................................................................................ 7 5.1 Geophysical Survey and Utility Mark Outs................................................................................. 7 5.2 Field Observations ....................................................................................................................... 7 5.3 Soil Analytical Results ................................................................................................................ 7 5.4 Groundwater Analytical Results .................................................................................................. 8 5.5 Soil Vapor and Ambient Air Analytical Results ......................................................................... 9 6.0 Conclusions and Recommendations .............................................................................................. 10 6.1 Conclusions ............................................................................................................................... 11 6.2 Recommendations ..................................................................................................................... 11 7.0 Limitations ..................................................................................................................................... 13 8.0 Soil Disposal Issues ....................................................................................................................... 14 9.0 References ...................................................................................................................................... 15 TABLES Table 1 – Soil Analytical Results of Volatile Organic Compounds (VOCs) Table 2 – Soil Analytical Results of Semivolatile Organic Compounds (SVOCs) Table 3 – Soil Analytical Results of Metals Table 4 – Soil Analytical Results of Polychlorinated Biphenyls (PCBs) and Pesticides Table 5 – Groundwater Analytical Results of VOCs Table 6 – Groundwater Analytical Results of SVOCs Table 7 – Soil Vapor and Ambient Air Analytical Results of VOCs FIGURES Figure 1 – Site Location Map Figure 2 – Site Plan APPENDICES Appendix A – Photographic Documentation Appendix B – Geophysical Investigation Report Appendix C – Field Sampling Logs Appendix D – Laboratory Analytical Reports AKRF, Inc. Subsurface (Phase II) Investigation 900 King Street Property – 900 King Street, Rye Brook, NY 1 1.0 INTRODUCTION AKRF, Inc. (AKRF) was retained by 900 King Street Owner, LLC to perform a Subsurface (Phase II) Investigation at the property located at 900 King Street in the Village of Rye Brook, Westchester County, New York (referred to hereafter as the “Property” or the “Site”). The 17.34-acre Property, as shown on Figure 1, is also identified as Tax Map ID No. 129.68-1-13. The Property is bounded by the Rye Brook Village Hall, Police Department, and Firehouse to the north; Arbor Drive followed by Harkness Park and Blind Brook Middle and High Schools to the east; The Arbors residential community to the south; and the Hutchinson River Parkway to the west. At the time of the investigation, the Property consisted of a 200,000-square foot three-story office building and associated asphalt-paved parking lot, and landscaped and natural areas. The field work associated with the Phase II investigation was completed between November 16 and 21, 2017. The objectives of the Phase II investigation were to further assess the Recognized Environmental Conditions (RECs) and other environmental concerns identified during AKRF’s Phase I Environmental Site Assessment (ESA) of the Property, as documented in the Phase I ESA report dated October 2017. The scope of this Phase II investigation included a geophysical survey and a soil boring program to characterize soil, soil vapor, and groundwater in the area of RECs and areas that would be disturbed during the proposed future redevelopment activities at the Property. The Phase II scope of work included the advancement of nine soil borings, installation of one groundwater monitoring well, installation of three temporary soil vapor points, and the collection of soil, groundwater, soil vapor, and ambient air samples for field-screening and laboratory analysis. Two existing groundwater observation wells, previously installed at the Site by AKRF during the geotechnical investigation in October 2017, were also sampled for laboratory analysis. This report describes the methods and results of the Phase II investigation conducted by AKRF. The locations of the soil borings, groundwater wells, and soil vapor points are depicted on Figure 2. A photographic log documenting the field activities is provided as Appendix A. 2.0 SITE DESCRIPTION At the time of the investigation, the Property consisted of a three-story office building of concrete construction and a northwest- and northeast-adjacent asphalt-paved parking lot. Additional parking was available beneath the northeastern portion of the building. Access to the Property was gained by a driveway off of Arbor Drive, and entrances to the building were noted on three sides of the building. The perimeter of the Property was tree-lined and topography sloped down to the southeast. The office building was constructed into the existing topography and tiered with three levels in the northern portion, and two in the southern portion. The soil, groundwater, and soil vapor sampling depths referenced in this report are reported relative to existing ground surface at the corresponding soil boring, groundwater well, and soil vapor point locations. Groundwater is anticipated to flow to the southeast trending with topography of the Property. However, actual groundwater flow at the Property can be affected by many factors including past filling activities, bedrock configuration, underground utilities, and other subsurface openings or obstructions such as basements, and other factors beyond the scope of this study. AKRF, Inc. Subsurface (Phase II) Investigation 900 King Street Property – 900 King Street, Rye Brook, NY 2 3.0 PREVIOUS INVESTIGATIONS Phase I Environmental Site Assessment (ESA), 900 King Street, AKRF, Inc. – October 2017 AKRF conducted a Phase I ESA in October 2017. The objective of the Phase I ESA was to evaluate the Site for RECs and other environmental concerns resulting from past or current uses of the Site and neighboring properties. Based on the findings from the site reconnaissance and historic records review, the following conclusions were presented: On-Site RECs  RCRA databases indicate that the Property was a historic SQG of ignitable waste, corrosive waste, and spent halogenic solvents. Storage and handling of these wastes have the potential to have affected the subsurface.  Potential buried debris from former on-site structures that could contain historic fill of unknown origin and/or abandoned underground storage tanks (USTs). Based on the age of the previous structures on the Property, fuel oil may have historically been used for heating purposes.  According to records received from the municipal building department, an abandoned underground vault and steam tank were discovered in the parking area and removed in 2003. The exact location of the vault and steam tank is unknown; however, the limited information available suggests that it was located on an edge of the current parking area and not associated with the current on-site building. The steam tank was likely used for heating a former on-site building. The fuel source associated with the steam heating system was likely fuel oil situated in either an aboveground or underground storage tank(s), which may have been removed when the former buildings were demolished. Releases from storage tank(s) associated with the heating systems for the former buildings may have affected the subsurface. On-Site de minimis Conditions  Arsenic and insecticide associated with the historic arboretum on the Property may be present in material beneath the building and surrounding parking lot.  Diesel generators were located northwest adjacent to the Site building on a concrete pad. Two had observable base tanks and a third was reported to have a tank located within the generator structure. Although access to the interior generator compartments were not provided to confirm the size of the diesel tanks and secondary containment, if present, no staining or evidence of spills was observed in association with the generator.  Based on building department records, residual hydraulic oil was observed beneath equipment in the elevator machine room during a 2014 inspection. Staining was not observed during the Phase I Site inspection, indicating the condition was properly addressed.  Although the building was reported to be constructed in 1980, fluorescent lights, lighting fixtures, and the hydraulic elevator machinery observed during the Property inspection have the potential to include polychlorinated biphenyl (PCB)- and/or mercury-containing components (including capacitors and potting compounds). Unless there is labeling or test data which indicates that they are not mercury- and/or PCB-containing, if disposal is required, it should be performed in accordance with applicable federal, state, and local regulations and guidelines. AKRF, Inc. Subsurface (Phase II) Investigation 900 King Street Property – 900 King Street, Rye Brook, NY 3 Off-Site RECs  Based on historic dry cleaner listings in the regulatory database, Putnam Services Unlimited, located at 941 King Street in Greenwich Connecticut, approximately 350 feet north-northeast of the Property was listed as a carpet and upholstery cleaner in 1994 and 1995. Although no releases from Putnam Services Unlimited were reported, based on the proximity to the Property, a release could migrate through groundwater onto the subject property. In addition to the on-site and off-site REC’s, and on-site de minimis conditions described above, the Phase I assessment identified on-site environmental concerns for consideration ahead of future redevelopment work, including: the presence of electric and hydraulic equipment that may contain PCB- or mercury-containing components or oils; and suspect asbestos-containing materials (ACM) and lead- based paint associated with the on-site structure. Preliminary Geotechnical Engineering Report, 900 King Street, AKRF, Inc. – November 9, 2017 AKRF completed a preliminary geotechnical investigation at the Property to evaluate subsurface conditions for the proposed redevelopment work. A total of 13 geotechnical borings, designated PB-1 through PB-13, were drilled at the Site between October 2, 2017 and October 10, 2017, under the full- time oversight of an AKRF geotechnical engineer. The borings were advanced to depths ranging from approximately 32 to 55 feet below ground surface (bgs). Two groundwater observation wells, designated OW-1 and OW-2, were installed in completed boreholes PB-8 and PB-4, respectively. Each well was installed to a depth of approximately 20 feet bgs. Well construction consisted of slotted 2-inch diameter PVC well screen from 10 to 20 feet bgs with solid 2- inch diameter PVC riser to bring the well to approximately 6 inches below grade. Each well was completed with a locking plug and flush-mounted manway. Results of the investigation indicated that the Property is underlain by a layer of uncontrolled fill consisting mainly of brown to gray sand with varying amounts of gravel, silt, and other miscellaneous fill including brick, asphalt, concrete, and pieces of tile. The identified fill layer ranged from 4 to 9 feet in thickness. Brown sand was encountered in all borings below the topsoil, asphalt, and fill layers, and ranged in thickness from about 9 feet to 31 feet. Soft rock was encountered beneath the sand layer at depths ranging from approximately 9 feet bgs in PB-13, located in the eastern portion of the Site, to approximately 35 feet bgs in PB-2, located in the southern portion of the Site. Foliated rock was encountered beneath the soft rock layer at depths ranging from approximately 11 feet bgs at PB-13 to approximately 44 feet bgs at PB-6, located in the northern portion of the Site. The AKRF geotechnical engineer gauged groundwater levels in the two observation wells and reported groundwater at depths of approximately 6 feet and 2 feet bgs at OW-1 and OW-2, respectively. AKRF, Inc. Subsurface (Phase II) Investigation 900 King Street Property – 900 King Street, Rye Brook, NY 4 4.0 FIELD ACTIVITIES 4.1 Geophysical Survey and Utility Mark-Outs On November 16, 2017, a geophysical survey was conducted across accessible targeted indoor and outdoor areas of the Site, to the extent feasible, to clear the proposed soil boring locations for subsurface utilities and/or structures, and to search for potential buried storage tanks. Additionally, the geophysical survey was designed to locate, if possible, the reported abandoned steam boiler vault and associated tanks, if any. The geophysical survey included electromagnetic (EM), radio-detection (RD), and ground penetrating radar (GPR) methods. The Geophysical Investigation Report is attached as Appendix B. In addition to the geophysical survey, Craig Drilling Companies, Inc. (Craig), the drilling contractor, notified Dig Safely New York at least 3 days prior to the start of the intrusive investigation work. 4.2 Soil Sampling A total of nine soil borings (SB-1 through SB-9) were advanced at the Property between November 17 and 20, 2017 by Craig at the locations shown on Figure 2. The locations of the soil borings were selected to evaluate subsurface conditions adjacent to RECs that were identified through the Phase 1 ESA. The eight exterior soil borings (SB-1 through SB-7, and SB-9) were advanced with a track-mounted Geoprobe® direct push probe (DPP) unit and the one interior soil boring (SB-8) was advanced with a hand auger after coring through the concrete floor slab. The soil borings were advanced to depths ranging from 2.5 to 20 feet bgs. The locations of the soil borings are summarized in the following table: Soil Boring Locations Soil Boring Location SB-1 Adjacent to the dumpster staging area on the western portion of the property SB-2 SB-3 Adjacent to the diesel generator located inside of the fenced-in mechanical equipment area in the parking lot on the western side of the building SB-4 SB-5 Adjacent to the diesel generator located outside of the entrance to the kitchen area on the western side of the building SB-6 Adjacent to the hydraulic lift gate at the loading area on the western side of the building SB-7 SB-8 Inside the elevator machine room SB-9 Adjacent to geotechnical soil boring/observation well PB-4/OW-2 in the center of the parking lot on the western side of the building Continuous soil samples were collected from soil borings SB-1 through SB- 7, and SB-9 using 5- foot long, 2-inch diameter, macrocore piston rod samplers fitted with dedicated acetate liners. Soil samples from SB-8 were obtained utilizing manual hand auger equipment. Each macrocore sample was split lengthwise and all samples were logged by AKRF field personnel. Logging consisted of: describing the soil according to the modified Burmister Classification System; describing any evidence of contamination (e.g., staining, sheens, odors); and field screening the soil for organic vapors using a calibrated photoionization detector (PID) in 1-foot intervals. Soil boring logs are provided in Appendix C. The PID was calibrated each day prior to on-site use using isobutylene gas in accordance with the manufacturer’s specifications. Based on the field AKRF, Inc. Subsurface (Phase II) Investigation 900 King Street Property – 900 King Street, Rye Brook, NY 5 screening results, a selected interval from the continuous soil samples from soil borings SB-1 through SB-8 was designated for laboratory analysis as follows: Soil Sample Depths Soil Boring Sample Depths (feet bgs) Rational for Selected Interval SB-1 0-2 Evaluate potential surface release(s) from dumpsters and former RCRA hazardous waste, and general subsurface fill conditions SB-2 0-2 SB-3 0-2 Evaluate potential surface release(s) from above grade diesel powered generators and associated ASTs, and general subsurface fill conditions SB-4 0-2 SB-5 0-2 SB-6 5-7 Evaluate potential subsurface release(s) from subgrade hydraulic lift equipment, and general subsurface fill conditions SB-7 5-7 SB-8 1-2.5 Evaluate potential surface release(s) from hydraulic elevator equipment, and general subsurface fill conditions Note: bgs – below ground surface SB-9 was an additional boring beyond the original scope of work, and was drilled for the purpose of installing a monitoring well and confirming the depth to water in OW-2. Samples selected for laboratory analysis were placed in laboratory-supplied containers and a chilled cooler in accordance with EPA protocols and transported via courier with appropriate chain of custody (COC) documentation to Test America Inc., a New York State Department of Health (NYSDOH) Environmental Laboratory Approval Program (ELAP)-certified laboratory, in Edison, New Jersey. The soil samples were analyzed for volatile organic compounds (VOCs) by EPA Method 8260, semi-volatile organic compounds (SVOCs) by EPA Method 8270, PCBs by EPA Method 8082, pesticides by EPA Method 8081, and Target Analyte List (TAL) metals by EPA’s 6000/7000 series Methods. 4.3 Groundwater Sampling Two groundwater samples were collected from the two previously installed geotechnical observation wells (OW-1 and OW-2). Monitoring well OW-2X, located at soil boring SB-9 during this investigation, was installed to provide supplemental geotechnical data to the AKRF geotechnical engineering group only. Sampling of OW-2X was not warranted as it was installed approximately 10 feet southwest of OW-2 and, based on the field screening of the soil samples, would not have yielded statistically significant data. The locations of the groundwater wells that were sampled are depicted on Figure 2. Prior to sampling, each of the groundwater wells was screened for the presence of VOCs using a calibrated PID after removing the well cap. The depth to groundwater and the total well depth were then measured in each well using a multi-parameter interface probe attached to a measuring tape accurate to 0.01 feet. Modified low-flow sampling techniques were utilized to purge the wells prior to sample collection. The purged water was monitored for turbidity and water quality indicators (i.e., pH, temperature, dissolved oxygen, oxidation reduction potential, and specific conductivity) with measurements collected approximately every five minutes. Purging at OW-1 continued until the turbidity was less than 50 Nephelometric Turbidity Units (NTU) for three successive readings and water quality indicators had stabilized to the extent practicable. Turbidity and/or water quality indicators at OW-2 did not stabilize following two consecutive hours and as such, purging was discontinued and samples were collected. Groundwater sampling logs are provided in Appendix C. Groundwater samples were collected in laboratory-supplied glassware and placed in a chilled cooler in accordance with EPA protocols. The samples were transported AKRF, Inc. Subsurface (Phase II) Investigation 900 King Street Property – 900 King Street, Rye Brook, NY 6 via courier with appropriate COC documentation to Test America Inc. The groundwater samples were analyzed for VOCs by EPA Method 8260 and SVOCs by EPA Method 8270. No evidence of light non-aqueous phase liquid (LNAPL) petroleum product and/or petroleum sheen or odors were detected in the groundwater purged from the monitoring wells at the Site. As such, purge water generated during the well sampling was discarded in grassy areas adjacent to the groundwater well locations. 4.4 Soil Vapor Sampling Three soil vapor points (SV-1 through SV-3) were installed within the footprint of the proposed redevelopment area to facilitate the collection of soil vapor samples for laboratory analysis. The soil vapor sample locations, as depicted on Figure 2, were established to evaluate potential contamination from off-site RECs identified in the Phase I ESA, including a former off-site dry cleaner, and to evaluate general subsurface conditions in the vicinity of the future occupied spaces in the redevelopment area. Soil vapor point SV-1 was installed in the parking lot area east of the existing office building, and soil vapor points SV-2 and SV-3 were installed in the parking lot area northeast of the existing office building. The soil vapor sampling points were installed using a track-mounted Geoprobe® DPP unit to advance a 0.75-inch diameter hollow probe rod fitted with an expendable 6-inch long stainless steel screened implant to a depth of 3 feet bgs. Dedicated tubing with threaded fittings was connected to the probe. The hollow probe rod was then removed and the boring was backfilled with clean silica sand to 1 foot above the screen. Hydrated bentonite was used to fill the remaining void around the sampling tubing to ground surface. Prior to sampling, approximately three system volumes were purged from each soil vapor point using a Gillian® GilAir™ Plus low flow sampling pump. During purging, an inverted 5-gallon bucket was placed over the sampling point and helium gas was introduced through a small hole in the bucket to saturate the atmosphere around the sampling point with helium. The purged vapors were collected in 1-liter Tedlar® bags and were field-screened with a portable helium detector to check for short-circuiting by ambient air into the sampling point (to verify the adequacy of the bentonite seal and confirm that vapors sampled were solely from the subsurface). The purged vapors were also field-screened for organic vapors using a calibrated PID. After purging, each probe was connected via Teflon™ tubing to a laboratory-supplied 6-liter SUMMA® canister equipped with a 0.10 liter per minute (L/min) flow regulator. In addition to the soil vapor samples, one ambient air sample (AA-1) was collected at the eastern side of the office building, adjacent to the main entrance, for quality control purposes. The soil vapor and ambient air samples were collected over an approximate 1-hour timeframe. Methodologies used for soil vapor assessment were consistent with the New York State Department of Health (NYSDOH) Final Guidance on Soil Vapor Intrusion, October 2006 and ASTM E 2600-08 Standard Practice for Assessment of Vapor Intrusion into Structures on Property Involved in Real Estate Transactions. The soil vapor and ambient air samples were transported via courier with appropriate COC documentation to Test America Inc. for analysis for VOCs by EPA Method TO-15. Soil vapor and ambient air sampling logs are provided in Appendix C. AKRF, Inc. Subsurface (Phase II) Investigation 900 King Street Property – 900 King Street, Rye Brook, NY 7 5.0 INVESTIGATION RESULTS 5.1 Geophysical Survey and Utility Mark Outs During the geophysical survey, linear anomalies consistent with subsurface utilities were marked out with spray paint prior to drilling and soil boring locations were adjusted accordingly. No evidence of buried tanks was identified in the areas that were scanned during the geophysical survey. Further, no evidence of the reported abandoned steam boiler vault and associated tanks was identified. The Geophysical Investigation Report is attached as Appendix B. During the geophysical survey, evidence of an ongoing hydraulic oil condition was noted on the concrete slab floor in the elevator machine room on the ground floor of the building. Hydraulic oil and sorbent pads were noted on the slab floor adjacent to elevator motors denoted “Car #1” and “Car #2”. 5.2 Field Observations While no definitive evidence of historic fill material (i.e., buried brick, concrete, and/or building materials) was observed in the soil borings advanced during this investigation, the previous geotechnical investigation reported a suspected fill layer ranging between 4 and 9 feet in thickness. Soils encountered during this investigation comprised of varying amounts of sand, silt, and gravel were identified underlying the concrete and asphalt cover layers, extending to approximately 20 feet bgs (the maximum boring depth). No evidence of contamination (i.e., soil staining, odors, and/or elevated PID readings) was noted in the soil borings that were advanced. Soil descriptions, observations, and PID readings are detailed in the soil boring logs provided in Appendix C. The observed depth to groundwater was recorded at 3.73 feet, 1.14 feet, and 0.98 feet below the top of the well casing in observation wells OW-1 and OW-2, and monitoring well OW-2X, respectively. No evidence of LNAPL and/or petroleum sheen or odors was detected in the groundwater wells at the Site. 5.3 Soil Analytical Results The analytical results from the eight soil samples that were submitted to the laboratory from this investigation were compared to the New York State Department of Environmental Conservation (NYSDEC) Part 375 Unrestricted Use Soil Cleanup Objectives (UUSCOs), Restricted Residential Soil Cleanup Objectives (RRSCOs), and Protection of Groundwater Soil Cleanup Objectives (PGWSCOs) presented in Sections 6.8(a) and 6.8(b) of 6 NYCRR Part 375. Soil analytical results are summarized in Tables 1 through 4. The complete laboratory analytical report is provided as Appendix D. The analytical results from the soil sampling are discussed below: Volatile Organic Compounds (VOCs) Six VOCs (acetone, carbon tetrachloride, methylene chloride, trichlorethene, m,p-xylenes, and o- xylenes) were detected in one or more of the soil samples at concentrations ranging from 0.000069 to 0.0046 milligrams per kilogram (mg/kg). None of the detected VOC concentrations were above their respective UUSCOs, RRSCOs, or PGWSCOs. Analytical results for VOCs in soil are summarized in Table 1. Semivolatile Organic Compounds (SVOCs) Fifteen SVOCs [2-methylnaphthalene, benzo[a]anthracene, benzo[a]pyrene, benzo[b]fluoranthene, benzo[g,h,i]perylene, benzo[k]fluoranthene, bis(2-ethylhexyl) phthalate, carbazole, chrysene, dibenz(a,h)anthracene, fluoranthene, indeno[1,2,3-cd]pyrene, naphthalene, AKRF, Inc. Subsurface (Phase II) Investigation 900 King Street Property – 900 King Street, Rye Brook, NY 8 phenanthrene, and pyrene] were detected in one or more of the soil samples, consisting primarily of polycyclic aromatic hydrocarbons (PAHs), a class of compounds commonly found in fill material, ash, asphalt, and petroleum products. The SVOCs were detected at concentrations ranging from 0.011 to 0.17 mg/kg. None of the detected SVOC concentrations were above their respective UUSCOs, RRSCOs, or PGWSCOs. Analytical results for SVOCs in soil are summarized in Table 2. Metals Seventeen metals (aluminum, arsenic, barium, beryllium, calcium, chromium, cobalt, copper, iron, lead, magnesium, manganese, nickel, potassium, sodium, vanadium, and zinc) were detected in one of more of the soil samples. As summarized in the following table, concentrations of chromium and nickel at SB-1 (0-2), barium, chromium, and nickel at SB-2 (0-2), and chromium at SB-5 (0-2) were detected above their respective UUSCOs, but below their RRSCOs and PGWSCOs. Metals Detected in Soil Above the Part 375 SCOs Boring ID Part 375 Part 375 Part 375 SB-1 SB-2 SB-5 Depth (ft bgs) UUSCO RRSCO PGWSCO (0-2) (0-2) (0-2) Date Sampled 11/20/17 11/20/17 11/20/17 Dilution Factor 1/10 ϯ 1/10 ϯ 1/4/10 ϯ Units = mg/kg Barium 350 400 820 228 379 66.3 Chromium 30*** 180*** NS*** 53.8 76.8 39.5 Nickel 30 310 130 30.3 35.9 21.6 Notes: Bold = Exceeds Unrestricted Use SCO (UUSCO) mg/kg = milligram per kilogram ft bgs = feet below ground surface ϯ = Dilution factor varies *** = Standard reflects trivalent, not total chromium standard Based on the field observations and the Property history, these metals detections are likely attributable to the fill material and/or background conditions, and not to a release or other source area. Analytical results for metals in soil are summarized in Table 3. Polychlorinated Biphenyls (PCBs) and Pesticides No PCBs or pesticides were detected above the laboratory detections limits in the soil samples collected during this investigation. Analytical results for PCBs and pesticides in soil are summarized in Table 4. 5.4 Groundwater Analytical Results The groundwater analytical results from the samples collected from the two previously installed groundwater observation wells (OW-1 and OW-2), and the analytical results from the trip blank sample were compared to the NYSDEC Class GA Ambient Water Quality Standards and Guidance Values (AWQVs) as presented in the NYSDEC Division of Water Technical Operational and Guidance Series (TOGS) 1.1.1. The groundwater analytical results are summarized in Tables 5 and 6. The complete laboratory analytical report is provided as Appendix D. The analytical results from the groundwater sampling are discussed below: AKRF, Inc. Subsurface (Phase II) Investigation 900 King Street Property – 900 King Street, Rye Brook, NY 9 VOCs Two VOCs, including acetone, a common laboratory contaminant, and chloroform, were detected in one of more of the samples collected. Acetone was also detected in the laboratory trip blank sample. The VOCs were detected at concentrations ranging from 1.1 to 4.0 micrograms per liter (µg/L). None of the detected VOC concentrations were above their respective AWQVs. Analytical results for VOCs in groundwater are summarized in Table 5. SVOCs No SVOCs were detected above the laboratory detection limits in the groundwater samples collected during this investigation. Analytical results for SVOCs in groundwater are summarized in Table 6. 5.5 Soil Vapor and Ambient Air Analytical Results The analytical results from the three soil vapor samples and ambient air sample were compared to the NYSDOH Soil Vapor Intrusion Air Guidance Values (AGVs) presented in the Final Guidance for Evaluating Soil Vapor Intrusion in the State of New York, dated October 2006, incorporating subsequent 2013, 2015, and 2017 updates. AGVs are intended as a reference for indoor air quality only and have been established for only three VOCs (methylene chloride, TCE, and PCE). Soil vapor and ambient air sampling analytical results are summarized in Table 7. The complete laboratory analytical report is provided as Appendix D. The analytical data from the soil vapor and ambient air sampling is discussed below. VOCs Twenty-three (23) VOCs were detected in the soil vapor samples. VOCs associated with petroleum (including 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, 1,3-butadiene, 2,2,4- trimethylpentane, 4-ethyltoluene, benzene, cumene, cyclohexane, ethylbenzene, m,p-xylene, n- butane, n-heptane, n-hexane, n-propylbenzene, o-xylene, toluene, and total xylenes) were detected in one of more of the soil vapor samples at concentrations ranging from 1.3 to 810 µg/m3. Solvent related VOCs (including acetone, bromodichloromethane, carbon disulfide, carbon tetrachloride, chloroform, and methyl ethyl ketone) were detected in one of more of the soil vapor samples at concentrations ranging from 0.32 to 90 µg/m3. None of the detected VOC concentrations were above their respective AGVs. Analytical results for VOCs in soil vapor are summarized in Table 7. There were no exceedances to applicable guidance values in the ambient air sample that was collected. AKRF, Inc. Subsurface (Phase II) Investigation 900 King Street Property – 900 King Street, Rye Brook, NY 10 6.0 CONCLUSIONS AND RECOMMENDATIONS AKRF conducted a Subsurface (Phase II) Investigation at the property located at 900 King Street in the Village of Rye Brook, Westchester County, New York, as depicted on Figure 1, between November 16 and 21, 2017. The Phase II investigation was conducted to further assess the recognized environmental conditions (RECs) and other environmental concerns identified during AKRF’s October 2017 Phase I Environmental Site Assessment (ESA) of the Property. The scope of this Phase II investigation included a geophysical survey and a soil boring program to characterize soil, soil vapor, and groundwater in the area of RECs and areas that would be disturbed during the proposed future redevelopment activities at the Property. At the time of the investigation, the Property consisted of a three-story office building of concrete construction and a northwest- and northeast-adjacent asphalt-paved parking lot. Additional parking was available beneath the northeastern portion of the building. Access to the Property was gained by a driveway off of Arbor Drive, and entrances to the building were noted on three sides of the building. The perimeter of the Property was tree-lined and topography sloped down to the southeast. The office building was constructed into the existing topography and tiered with three levels in the northern portion, and two in the southern portion. The Phase II scope included: completion of a geophysical investigation, the advancement of nine soil borings, of which one was converted into a groundwater monitoring well; the installation of three temporary soil vapor points; and the collection of eight soil samples, two groundwater samples, three soil vapor samples, and one ambient air sample for laboratory analysis. While no definitive evidence of historic fill material (i.e., buried brick, concrete, and/or building materials) was observed in the soil borings advanced during this investigation, the previous geotechnical investigation reported a suspected fill layer ranging between 4 and 9 feet in thickness. Soils encountered during this investigation composed of varying amounts of sand, silt, and gravel, were identified underlying the concrete and asphalt cover layers, extending to approximately 20 feet below ground surface (bgs), the maximum boring depth. No evidence of contamination (i.e., soil staining, odors, and/or elevated PID readings) was noted in the soil borings that were advanced. The observed depth to groundwater was recorded at 3.73 feet, 1.14 feet, and 0.98 feet below the top of the well casing in observation wells OW-1 and OW-2, and monitoring well OW-2X, respectively. No evidence of light non-aqueous phase liquid (LNAPL) petroleum product and/or petroleum sheen or odors was detected in the groundwater wells at the Site. Based on the topography surrounding the Property, groundwater is anticipated to flow to the southeast. Analytical results from the soil samples identified concentrations of chromium and nickel at SB-1 (0-2), barium, chromium, and nickel at SB-2 (0-2), and chromium at SB-5 (0-2) above the New York State Department of Environmental Conservation (NYSDEC) Part 375 Unrestricted Use Soil Cleanup Objectives (UUSCOs), but below their respective Restricted Residential Soil Cleanup Objectives (RRSCOs) and Protection of Groundwater Soil Cleanup Objectives (PGWSCOs), as presented in Sections 6.8(a) and 6.8(b) of 6 NYCRR Part 375. Based on observed conditions, the detected metals did not appear to be associated with a release of contamination and are likely present due to the fill material. No volatile organic compounds (VOCs) or semivolatile organic compounds (SVOCs) were detected above their respective UUSCOs, RRSCOs, or PGWSCOs, and no polychlorinated biphenyls (PCBs) or pesticides were detected above the laboratory detection limit in any of the soil samples. Analytical results for the groundwater samples indicated that there were no VOCs or SVOCs detected above their respective NYSDEC Class GA Ambient Water Quality Standards and Guidance Values AKRF, Inc. Subsurface (Phase II) Investigation 900 King Street Property – 900 King Street, Rye Brook, NY 11 (AWQVs) as presented in the NYSDEC Division of Water Technical Operational and Guidance Series (TOGS) 1.1.1. Analytical results for the soil vapor and ambient air samples indicated that petroleum and solvent related VOCs were detected at concentrations ranging from 0.32 to 810 µg/m3. There were no VOCs detected above their respective New York State Department of Health (NYSDOH) Soil Vapor Intrusion Air Guidance Values (AGVs) as presented in the Final Guidance for Evaluating Soil Vapor Intrusion in the State of New York, dated October 2006, incorporating subsequent 2013, 2015, and 2017 updates. 6.1 Conclusions Based on the findings of the Phase II investigation, AKRF concludes the following: •The analytical data from the soil, groundwater, and soil vapor sampling indicated that there was no evidence of a release of contamination associated with the RECs or de minimis condition observations identified during AKRF’s October 2017 Phase I ESA. No evidence of hazardous, non-hazardous, and/or petroleum-like releases (e.g., odors, staining, or elevated PID readings) were identified through the soil, groundwater, and soil vapor sampling. •No concentrations of VOCs, SVOCs, PCBs, or pesticides were detected above their respective Part 375 UUSCOs, RRSCOs, or PGWSCOs in the soil samples from this investigation. •Based on the Phase II field observations, the metals detected in soil at levels above their respective Part 375 UUSCOs are likely attributable to contaminants in the shallow fill layer observed at the Site and/or background conditions, and not related to an on-site release or other source area. •No concentrations of VOCs or SVOCs were detected above their respective AWQVs in the groundwater samples from this investigation. •No concentrations of VOCs were detected above their respective AGVs in the soil vapor/ambient air samples from this investigation. •Evidence of an ongoing hydraulic oil condition was noted on the concrete slab floor in the elevator machine room on the ground floor of the building. Hydraulic oil and sorbent pads were noted on the slab floor adjacent to elevator motors denoted “Car #1” and “Car #2”. The findings from the soil sampling in the elevator machine room suggest the condition has not affected subsurface soils. 6.2 Recommendations It is our understanding that 900 King Street Owner, LLC is proposing to demolish the existing office building in conjunction with the redevelopment of the Property. It is understood that the demolition and redevelopment work will require earth movement, excavation, grading, and filling. Based on the conclusions presented above, in conjunction with the scope of the proposed redevelopment work, AKRF recommends the following: •The hydraulic oil condition noted in the elevator machine room should be addressed including cleaning the residual hydraulic oil from the slab floor and properly draining the hydraulic oil reservoirs from the faulty elevator motors until they are properly repaired and/or removed. All oil soaked materials and residual hydraulic oil should be disposed of in accordance with applicable regulations. AKRF, Inc. Subsurface (Phase II) Investigation 900 King Street Property – 900 King Street, Rye Brook, NY 12  Any soil or fill excavated as part of future Site redevelopment activities should be managed in accordance with applicable regulations. All material intended for off-site disposal should be tested in accordance with the requirements of the intended receiving facility. Transportation of all soil leaving for off-site disposal should be in accordance with requirements covering licensing of haulers and trucks, placarding, truck routes, manifesting, etc. Excavation may reveal different or more significant soil contamination in areas not tested as part of this investigation. If discovered, such contamination could require further investigation and/or remediation in accordance with applicable regulations.  If dewatering is required during future construction activities, water must be discharged in accordance with local, county, state, and federal requirements.  No evidence of underground storage tanks (USTs) or other buried tanks was identified during the geophysical survey or the sampling program. However, if any storage tanks or contaminated soil are encountered during redevelopment, such tanks should be registered with NYSDEC and/or the Westchester County Department of Health (WCDOH), if required, and closed and removed along with any contaminated soil in accordance with applicable regulations.  If any USTs and/or petroleum contaminated soil are encountered during the development activities, consideration should be given to installing a vapor barrier below the proposed building foundation. A membrane-type waterproofing product, if used as part of the foundation construction, could also function as a vapor barrier. AKRF, Inc. Subsurface (Phase II) Investigation 900 King Street Property – 900 King Street, Rye Brook, NY 13 7.0 LIMITATIONS The findings set forth in this report are strictly limited in scope and time to the date of the evaluation described herein. The conclusions and recommendations presented in the report are based solely on the services and any limitations described in this report. This report may contain conclusions that are based on the analysis of data collected at the time and locations noted in the report through intrusive or non-intrusive sampling. However, further investigation might reveal additional data or variations of the current data, which may differ from our understanding of the conditions presented in this report and require the enclosed recommendations to be reevaluated or modified. Chemical analyses may have been performed for specific parameters during the course of this investigation, as summarized in the text and tables. It should be noted that additional chemical constituents, not searched for during this investigation, may be present at the Site. Due to the nature of the investigation and the limited data available, no warranty, expressed or implied, shall be construed with respect to undiscovered liabilities. The presence of biological hazards, radioactive materials, lead-based paint and asbestos-containing materials was not investigated, unless specified in the report. Interpretations of the data, including comparison to regulatory standards, guidelines or background values, are not opinions that these comparisons are legally applicable. Furthermore, any conclusions or recommendations should not be construed as legal advice. For such advice, the client is recommended to seek appropriate legal counsel. Disturbance, handling, transportation, storage and disposal of known or potentially contaminated materials is subject to all applicable laws, which may or may not be fully described as part of this report. The analytical data, conclusions, and/or recommendations provided in this report should not be construed in any way as a classification of waste that may be generated during future disturbance of the project site. Waste(s) generated at the Site including excess fill may be considered regulated solid waste and potentially hazardous waste. Requirements for intended disposal facilities should be determined beforehand as the data provided in this report may be insufficient and could vary following additional sampling. This report may be based solely or partially on data collected, conducted, and provided by, AKRF and/or others. No warranty is expressed or implied by usage of such data. Such data may be included in other investigation reports or documentation. In addition, these reports may have been based upon available previous reports, historical records, documentation from federal, state and local government agencies, personal interviews, and geological mapping. This report is subject, at a minimum, to the limitations of the previous reports, historical documents, availability and accuracy of collected documentation, and personal recollection of those persons interviewed. In certain instances, AKRF has been required to assume that the information provided is accurate with limited or no corroboratory evidence. This report is intended for the use solely by 900 King Street Owner, LLC. Reliance by third parties on the information and opinions contained herein is strictly prohibited and requires the written consent of AKRF. AKRF accepts no responsibility for damages incurred by third parties for any decisions or actions taken based on this report. This report must be used, interpreted, and presented in its entirety. AKRF, Inc. Subsurface (Phase II) Investigation 900 King Street Property – 900 King Street, Rye Brook, NY 14 8.0 SOIL DISPOSAL ISSUES In addition to the discussions in the Conclusions, Recommendations, and Limitations Sections (Sections 6.0 and 7.0), the issue of appropriate management of off-site disposal of soil warrants careful consideration. Any material being disposed of off-site is a regulated waste, and disposal must be in accordance with:  Requirements of the specific receiving facility;  Requirements of any agencies overseeing the cleanup/excavation; and  Federal and state requirements (sometimes in both the state where the soil is generated and where disposal will occur). For hazardous wastes and petroleum-contaminated soil (and other ‘clearly contaminated’ materials), the requirements are usually fairly well defined. It is in the situation where contamination is not readily apparent (e.g., so called “historic or urban fill” or “construction and demolition debris” or material that may have been formerly identified as “clean fill”) that present the greatest potential for problems and cost overruns. Even on sites where no contamination requiring remediation is identified, it is common that most of the excavated material is considered “contaminated” for purposes of waste disposal. Concentrations of the various contaminants in historic fill can be highly variable, and upon further testing, the material could contain higher contaminant concentrations than outlined in this investigation. Portions of this material could be classified as hazardous waste. It is important that the intended disposal facility (or facilities) be identified in advance of off-site disposal. Agency approval is sometimes required for disposal, and the facility will frequently require additional testing prior to (and sometimes at the time of) accepting material. Material must conform to a lengthy list of requirements based on both chemical composition and sometimes numerous other parameters (related to size, percentage of liquids, presence of odors, etc.) for acceptance at the facility. Assuming (or allowing a contractor to assume) that all, or even most, of the soil from a site can be disposed of at minimal cost may result in unanticipated and expensive change orders. For these reasons, we recommend that professional advice be sought prior to preparing bid documents and contracts incorporating soil disposal. AKRF, Inc. Subsurface (Phase II) Investigation 900 King Street Property – 900 King Street, Rye Brook, NY 15 9.0 REFERENCES 1. AKRF, Inc., Phase I Environmental Site Assessment, 900 King Street, October 2017. 2. AKRF, Inc., Preliminary Geotechnical Engineering Report, 900 King Street, November 9, 2017 3. U.S. Geological Survey, Rye, Rye, New York Quadrangle, 7.5 Minute Series (Topographic), Scale 1:24,000, 2010. 4. 6 NYCRR Part 375 Soil Cleanup Objectives (SCOs) For Residential Use, December 14, 2006. 5. New York State Department of Environmental Conservation Technical and Operational Guidance Series (1.1.1), Class GA Ambient Water Quality Standards and Guidance Values. 6. New York State Department of Health, Guidance for Evaluating Soil Vapor Intrusion in the State of New York, October 2006, including 2013, 2015, and 2017 updates. TABLES Table 1 900 King Street Rye Brook, NY Phase II Investigation Soil Analytical Results Volatile Organic Compounds Client ID NYSDEC NYSDEC NYSDEC SB-1 (0-2) SB-2 (0-2) SB-3(0-2) SB-4(0-2) Lab Sample ID Part 375 Part 375 Part 375 460-145515-2 460-145515-1 460-145401-4 460-145401-6 Date Sampled Unrestricted Restricted Protection of 11/20/2017 11/20/2017 11/17/2017 11/17/2017 SCO Residential Groundwater SCO SCO Analyte mg/kg mg/kg mg/kg 1,1,1-Trichloroethane 0.68 100 0.68 0.00076 U 0.00072 U 0.00066 U 0.00075 U 1,1,2,2-Tetrachloroethane NS NS 0.6 G 0.00076 U * 0.00072 U * 0.00066 U 0.00075 U 1,1,2-Trichloro-1,2,2-trifluoroethane NS NS 6 G 0.00076 U 0.00072 U 0.00066 U 0.00075 U 1,1,2-Trichloroethane NS NS NS 0.00076 U 0.00072 U 0.00066 U 0.00075 U 1,1-Dichloroethane 0.27 26 0.27 0.00076 U 0.00072 U 0.00066 U 0.00075 U 1,1-Dichloroethene 0.33 100 0.33 0.00076 U 0.00072 U 0.00066 U 0.00075 U 1,2,3-Trichlorobenzene NS NS NS 0.00076 U * 0.00072 U * 0.00066 U 0.00075 U 1,2,4-Trichlorobenzene NS NS 3.4 G 0.00076 U 0.00072 U 0.00066 U 0.00075 U 1,2-Dibromo-3-Chloropropane NS NS NS 0.00076 U * 0.00072 U * 0.00066 U 0.00075 U 1,2-Dichlorobenzene 1.1 100 1.1 0.00076 U 0.00072 U 0.00066 U 0.00075 U 1,2-Dichloroethane 0.02 3.1 0.02 0.00076 U 0.00072 U 0.00066 U 0.00075 U 1,2-Dichloropropane NS NS NS 0.00076 U 0.00072 U 0.00066 U 0.00075 U 1,3-Dichlorobenzene 2.4 49 2.4 0.00076 U 0.00072 U 0.00066 U 0.00075 U 1,4-Dichlorobenzene 1.8 13 1.8 0.00076 U 0.00072 U 0.00066 U 0.00075 U 1,4-Dioxane 0.1 13 0.1 0.015 U 0.014 U 0.013 U 0.015 U 2-Butanone (MEK)0.12 100 0.12 0.0038 U 0.0036 U 0.0033 U 0.0037 U 2-Hexanone NS NS NS 0.0038 U 0.0036 U 0.0033 U 0.0037 U 4-Methyl-2-pentanone (MIBK)NS NS 1.0 G 0.0038 U 0.0036 U 0.0033 U 0.0037 U Acetone 0.05 100 0.05 0.0038 U 0.0036 U 0.0044 0.0037 U Benzene 0.06 4.8 0.06 0.00076 U 0.00072 U 0.00066 U 0.00075 U Bromoform NS NS NS 0.00076 U 0.00072 U 0.00066 U 0.00075 U Bromomethane NS NS NS 0.00076 U 0.00072 U 0.00066 U 0.00075 U Carbon disulfide NS NS 2.7 G 0.00076 U 0.00072 U 0.00066 U 0.00075 U Carbon tetrachloride 0.76 2.4 0.76 0.0013 0.0016 0.00066 U 0.00075 U Chlorobenzene 1.1 100 1.1 0.00076 U 0.00072 U 0.00066 U 0.00075 U Chlorobromomethane NS NS NS 0.00076 U 0.00072 U 0.00066 U 0.00075 U Chlorodibromomethane NS NS NS 0.00076 U 0.00072 U 0.00066 U 0.00075 U Chloroethane NS NS 1.9 G 0.00076 U 0.00072 U 0.00066 U 0.00075 U Chloroform 0.37 49 0.37 0.00076 U 0.00072 U 0.00066 U 0.00075 U Chloromethane NS NS NS 0.00076 U 0.00072 U 0.00066 U 0.00075 U cis-1,2-Dichloroethene 0.25 100 0.25 0.00076 U 0.00072 U 0.00066 U 0.00075 U cis-1,3-Dichloropropene NS NS NS 0.00076 U 0.00072 U 0.00066 U 0.00075 U Cyclohexane NS NS NS 0.00076 U 0.00072 U 0.00066 U 0.00075 U Dichlorobromomethane NS NS NS 0.00076 U 0.00072 U 0.00066 U 0.00075 U Dichlorodifluoromethane NS NS NS 0.00076 U 0.00072 U 0.00066 U 0.00075 U Ethylbenzene 1 41 1 0.00076 U 0.00072 U 0.00066 U 0.00075 U Ethylene Dibromide NS NS NS 0.00076 U 0.00072 U 0.00066 U 0.00075 U Isopropylbenzene NS NS 2.3 G 0.00076 U 0.00072 U 0.00066 U 0.00075 U Methyl acetate NS NS NS 0.0038 U 0.0036 U 0.0033 U 0.0037 U Methyl tert-butyl ether 0.93 100 0.93 0.00076 U 0.00072 U 0.00066 U 0.00075 U Methylcyclohexane NS NS NS 0.00076 U 0.00072 U 0.00066 U 0.00075 U Methylene Chloride 0.05 100 0.05 0.00076 U 0.00072 U 0.00066 U 0.00065 J m-Xylene & p-Xylene 0.26 TS 100 TS 1.6 TS 0.00076 U 0.00072 U 0.00018 J 0.00075 U o-Xylene 0.26 TS 100 TS 1.6 TS 0.00076 U 0.00072 U 0.000069 J 0.00075 U Styrene NS NS NS 0.00076 U 0.00072 U 0.00066 U 0.00075 U Tetrachloroethene 1.3 19 1.3 0.00076 U 0.00072 U 0.00066 U 0.00075 U Toluene 0.7 100 0.7 0.00076 U 0.00072 U 0.00066 U 0.00075 U trans-1,2-Dichloroethene 0.19 100 0.19 0.00076 U 0.00072 U 0.00066 U 0.00075 U trans-1,3-Dichloropropene NS NS NS 0.00076 U 0.00072 U 0.00066 U 0.00075 U Trichloroethene 0.47 21 0.47 0.00028 J 0.00025 J 0.00019 J 0.00023 J Trichlorofluoromethane NS NS NS 0.00076 U 0.00072 U 0.00066 U 0.00075 U Vinyl chloride 0.02 0.9 0.02 0.00076 U 0.00072 U 0.00066 U 0.00075 U Total Conc NS NS NS 0.00158 0.00185 0.00484 0.00088 Page 1 of 10 Table 1 900 King Street Rye Brook, NY Phase II Investigation Soil Analytical Results Volatile Organic Compounds Client ID NYSDEC NYSDEC NYSDEC Lab Sample ID Part 375 Part 375 Part 375 Date Sampled Unrestricted Restricted Protection of SCO Residential Groundwater SCO SCO Analyte mg/kg mg/kg mg/kg 1,1,1-Trichloroethane 0.68 100 0.68 1,1,2,2-Tetrachloroethane NS NS 0.6 G 1,1,2-Trichloro-1,2,2-trifluoroethane NS NS 6 G 1,1,2-Trichloroethane NS NS NS 1,1-Dichloroethane 0.27 26 0.27 1,1-Dichloroethene 0.33 100 0.33 1,2,3-Trichlorobenzene NS NS NS 1,2,4-Trichlorobenzene NS NS 3.4 G 1,2-Dibromo-3-Chloropropane NS NS NS 1,2-Dichlorobenzene 1.1 100 1.1 1,2-Dichloroethane 0.02 3.1 0.02 1,2-Dichloropropane NS NS NS 1,3-Dichlorobenzene 2.4 49 2.4 1,4-Dichlorobenzene 1.8 13 1.8 1,4-Dioxane 0.1 13 0.1 2-Butanone (MEK)0.12 100 0.12 2-Hexanone NS NS NS 4-Methyl-2-pentanone (MIBK)NS NS 1.0 G Acetone 0.05 100 0.05 Benzene 0.06 4.8 0.06 Bromoform NS NS NS Bromomethane NS NS NS Carbon disulfide NS NS 2.7 G Carbon tetrachloride 0.76 2.4 0.76 Chlorobenzene 1.1 100 1.1 Chlorobromomethane NS NS NS Chlorodibromomethane NS NS NS Chloroethane NS NS 1.9 G Chloroform 0.37 49 0.37 Chloromethane NS NS NS cis-1,2-Dichloroethene 0.25 100 0.25 cis-1,3-Dichloropropene NS NS NS Cyclohexane NS NS NS Dichlorobromomethane NS NS NS Dichlorodifluoromethane NS NS NS Ethylbenzene 1 41 1 Ethylene Dibromide NS NS NS Isopropylbenzene NS NS 2.3 G Methyl acetate NS NS NS Methyl tert-butyl ether 0.93 100 0.93 Methylcyclohexane NS NS NS Methylene Chloride 0.05 100 0.05 m-Xylene & p-Xylene 0.26 TS 100 TS 1.6 TS o-Xylene 0.26 TS 100 TS 1.6 TS Styrene NS NS NS Tetrachloroethene 1.3 19 1.3 Toluene 0.7 100 0.7 trans-1,2-Dichloroethene 0.19 100 0.19 trans-1,3-Dichloropropene NS NS NS Trichloroethene 0.47 21 0.47 Trichlorofluoromethane NS NS NS Vinyl chloride 0.02 0.9 0.02 Total Conc NS NS NS SB-5(0-2)SB-6(5-7) SB-7(5-7) SB-8(1-2.5) 460-145401-5 460-145401-3 460-145401-2 460-145401-1 11/17/2017 11/17/2017 11/17/2017 11/17/2017 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.016 U 0.013 U 0.014 U 0.015 U 0.004 U 0.0034 U 0.0035 U 0.0037 U 0.004 U 0.0034 U 0.0035 U 0.0037 U 0.004 U 0.0034 U 0.0035 U 0.0037 U 0.004 U 0.0046 0.0035 U 0.0037 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U * 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.004 U * 0.0034 U 0.0035 U 0.0037 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.00014 J 0.00013 J 0.00014 J 0.00012 J 0.0008 U 0.00067 U 0.00071 U 0.00019 J 0.0008 U 0.00067 U 0.00071 U 0.00012 J 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.00026 J 0.00033 J 0.00027 J 0.00022 J 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0008 U 0.00067 U 0.00071 U 0.00074 U 0.0004 0.00506 0.00041 0.00065 Page 2 of 10 Table 2 900 King Street Rye Brook, NY Phase II Investigation Soil Analytical Results Semivolatile Organic Compounds Client ID NYSDEC NYSDEC NYSDEC SB-1 (0-2) SB-2 (0-2) SB-3(0-2) SB-4(0-2) Lab Sample ID Part 375 Part 375 Part 375 460-145515-2 460-145515-1 460-145401-4 460-145401-6 Date Sampled Unrestricted Restricted Protection of 11/20/2017 11/20/2017 11/17/2017 11/17/2017 SCO Residential Groundwater SCO SCO Analyte mg/kg mg/kg mg/kg 1,2,4-Trichlorobenzene NS NS 3.4 G 0.037 U 0.036 U 0.036 U 0.036 U 1,2-Dichlorobenzene 1.1 100 1.1 0.37 U 0.36 U 0.36 U 0.36 U 1,3-Dichlorobenzene 2.4 49 2.4 0.37 U 0.36 U 0.36 U 0.36 U 1,4-Dichlorobenzene 1.8 13 1.8 0.37 U 0.36 U 0.36 U 0.36 U 2,2'-oxybis[1-chloropropane]NS NS NS 0.37 U 0.36 U 0.36 U 0.36 U 2,4-Dinitrotoluene NS NS NS 0.074 U 0.073 U 0.073 U 0.073 U 2,6-Dinitrotoluene NS NS 1 G 0.074 U 0.073 U 0.073 U 0.073 U 2-Chloronaphthalene NS NS NS 0.37 U 0.36 U 0.36 U 0.36 U 2-Methylnaphthalene NS NS 36.4 G 0.37 U 0.36 U 0.36 U 0.36 U 2-Nitroaniline NS NS 0.4 G 0.37 U 0.36 U 0.36 U 0.36 U 3,3'-Dichlorobenzidine NS NS NS 0.15 U 0.14 U 0.14 U 0.15 U 3-Nitroaniline NS NS 0.5 G 0.37 U 0.36 U 0.36 U 0.36 U 4-Bromophenyl phenyl ether NS NS NS 0.37 U 0.36 U 0.36 U 0.36 U 4-Chloroaniline NS NS 0.22 G 0.37 U 0.36 U 0.36 U 0.36 U 4-Chlorophenyl phenyl ether NS NS NS 0.37 U 0.36 U 0.36 U 0.36 U 4-Nitroaniline NS NS NS 0.37 U 0.36 U 0.36 U 0.36 U Acenaphthene 20 100 98 0.37 U 0.36 U 0.36 U 0.36 U Acenaphthylene 100 100 107 0.37 U 0.36 U 0.36 U 0.36 U Anthracene 100 100 1,000 0.37 U 0.36 U 0.36 U 0.36 U Benzo[a]anthracene 1 1 1 0.037 U 0.036 U 0.036 U 0.036 U Benzo[a]pyrene 1 1 22 0.037 U 0.036 U 0.036 U 0.036 U Benzo[b]fluoranthene 1 1 1.7 0.037 U 0.036 U 0.036 U 0.036 U Benzo[g,h,i]perylene 100 100 1,000 0.37 U 0.36 U 0.36 U 0.36 U Benzo[k]fluoranthene 0.8 3.9 1.7 0.037 U 0.036 U 0.036 U 0.036 U Bis(2-chloroethoxy)methane NS NS NS 0.37 U 0.36 U 0.36 U 0.36 U Bis(2-chloroethyl)ether NS NS NS 0.037 U 0.036 U 0.036 U 0.036 U Bis(2-ethylhexyl) phthalate NS NS 435 G 0.37 U 0.36 U 0.36 U 0.36 U Butyl benzyl phthalate NS NS 122 G 0.37 U 0.36 U 0.36 U 0.36 U Carbazole NS NS NS 0.37 U 0.36 U 0.36 U 0.36 U Chrysene 1 3.9 1 0.37 U 0.36 U 0.36 U 0.36 U Dibenz(a,h)anthracene 0.33 0.33 1,000 0.037 U 0.036 U 0.036 U 0.036 U Dibenzofuran 7 59 210 0.37 U 0.36 U 0.36 U 0.36 U Diethyl phthalate NS NS 7.1 G 0.37 U 0.36 U 0.36 U 0.36 U Dimethyl phthalate NS NS 27 G 0.37 U 0.36 U 0.36 U 0.36 U Di-n-butyl phthalate NS NS 8.1 G 0.37 U 0.36 U 0.36 U 0.36 U Di-n-octyl phthalate NS NS 120 G 0.37 U 0.36 U 0.36 U 0.36 U Fluoranthene 100 100 1,000 0.37 U 0.36 U 0.36 U 0.36 U Fluorene 30 100 386 0.37 U 0.36 U 0.36 U 0.36 U Hexachlorobenzene 0.33 1.2 3.2 0.037 U 0.036 U 0.036 U 0.036 U Hexachlorobutadiene NS NS NS 0.074 U 0.073 U 0.073 U 0.073 U Hexachlorocyclopentadiene NS NS NS 0.37 U 0.36 U 0.36 U 0.36 U Hexachloroethane NS NS NS 0.037 U 0.036 U 0.036 U 0.036 U Indeno[1,2,3-cd]pyrene 0.5 0.5 8.2 0.037 U 0.036 U 0.036 U 0.036 U Isophorone NS NS 4.4 G 0.15 U 0.14 U 0.14 U 0.15 U Naphthalene 12 100 12 0.37 U 0.36 U 0.36 U 0.36 U Nitrobenzene NS 15 G 0.17 G 0.037 U 0.036 U 0.036 U 0.036 U N-Nitrosodi-n-propylamine NS NS NS 0.037 U 0.036 U 0.036 U 0.036 U N-Nitrosodiphenylamine NS NS NS 0.37 U 0.36 U 0.36 U 0.36 U Phenanthrene 100 100 1,000 0.37 U 0.36 U 0.36 U 0.36 U Pyrene 100 100 1,000 0.37 U 0.36 U 0.36 U 0.36 U Total Conc NS NS NS 0 0 0 0 Page 3 of 10 Table 2 900 King Street Rye Brook, NY Phase II Investigation Soil Analytical Results Semivolatile Organic Compounds Client ID NYSDEC NYSDEC NYSDEC Lab Sample ID Part 375 Part 375 Part 375 Date Sampled Unrestricted Restricted Protection of SCO Residential Groundwater SCO SCO Analyte mg/kg mg/kg mg/kg 1,2,4-Trichlorobenzene NS NS 3.4 G 1,2-Dichlorobenzene 1.1 100 1.1 1,3-Dichlorobenzene 2.4 49 2.4 1,4-Dichlorobenzene 1.8 13 1.8 2,2'-oxybis[1-chloropropane]NS NS NS 2,4-Dinitrotoluene NS NS NS 2,6-Dinitrotoluene NS NS 1 G 2-Chloronaphthalene NS NS NS 2-Methylnaphthalene NS NS 36.4 G 2-Nitroaniline NS NS 0.4 G 3,3'-Dichlorobenzidine NS NS NS 3-Nitroaniline NS NS 0.5 G 4-Bromophenyl phenyl ether NS NS NS 4-Chloroaniline NS NS 0.22 G 4-Chlorophenyl phenyl ether NS NS NS 4-Nitroaniline NS NS NS Acenaphthene 20 100 98 Acenaphthylene 100 100 107 Anthracene 100 100 1,000 Benzo[a]anthracene 1 1 1 Benzo[a]pyrene 1 1 22 Benzo[b]fluoranthene 1 1 1.7 Benzo[g,h,i]perylene 100 100 1,000 Benzo[k]fluoranthene 0.8 3.9 1.7 Bis(2-chloroethoxy)methane NS NS NS Bis(2-chloroethyl)ether NS NS NS Bis(2-ethylhexyl) phthalate NS NS 435 G Butyl benzyl phthalate NS NS 122 G Carbazole NS NS NS Chrysene 1 3.9 1 Dibenz(a,h)anthracene 0.33 0.33 1,000 Dibenzofuran 7 59 210 Diethyl phthalate NS NS 7.1 G Dimethyl phthalate NS NS 27 G Di-n-butyl phthalate NS NS 8.1 G Di-n-octyl phthalate NS NS 120 G Fluoranthene 100 100 1,000 Fluorene 30 100 386 Hexachlorobenzene 0.33 1.2 3.2 Hexachlorobutadiene NS NS NS Hexachlorocyclopentadiene NS NS NS Hexachloroethane NS NS NS Indeno[1,2,3-cd]pyrene 0.5 0.5 8.2 Isophorone NS NS 4.4 G Naphthalene 12 100 12 Nitrobenzene NS 15 G 0.17 G N-Nitrosodi-n-propylamine NS NS NS N-Nitrosodiphenylamine NS NS NS Phenanthrene 100 100 1,000 Pyrene 100 100 1,000 Total Conc NS NS NS SB-5(0-2)SB-6(5-7) SB-7(5-7) SB-8(1-2.5) 460-145401-5 460-145401-3 460-145401-2 460-145401-1 11/17/2017 11/17/2017 11/17/2017 11/17/2017 0.037 U 0.036 U 0.035 U 0.037 U 0.37 U 0.36 U 0.35 U 0.37 U 0.37 U 0.36 U 0.35 U 0.37 U 0.37 U 0.36 U 0.35 U 0.37 U 0.37 U 0.36 U 0.35 U 0.37 U 0.075 U 0.073 U 0.072 U 0.075 U 0.075 U 0.073 U 0.072 U 0.075 U 0.37 U 0.36 U 0.35 U 0.37 U 0.37 U 0.011 J 0.023 J 0.041 J 0.37 U 0.36 U 0.35 U 0.37 U 0.15 U 0.14 U 0.14 U 0.15 U 0.37 U 0.36 U 0.35 U 0.37 U 0.37 U 0.36 U 0.35 U 0.37 U 0.37 U 0.36 U 0.35 U 0.37 U 0.37 U 0.36 U 0.35 U 0.37 U 0.37 U 0.36 U 0.35 U 0.37 U 0.37 U 0.36 U 0.35 U 0.37 U 0.37 U 0.36 U 0.35 U 0.37 U 0.37 U 0.36 U 0.35 U 0.37 U 0.037 U 0.036 U 0.035 U 0.095 0.037 U 0.036 U 0.035 U 0.082 0.037 U 0.036 U 0.035 U 0.12 0.37 U 0.36 U 0.35 U 0.06 J 0.037 U 0.036 U 0.035 U 0.048 0.37 U 0.36 U 0.35 U 0.37 U 0.037 U 0.036 U 0.035 U 0.037 U 0.37 U 0.36 U 0.35 U 0.11 J 0.37 U 0.36 U 0.35 U 0.37 U 0.37 U 0.36 U 0.35 U 0.011 J 0.37 U 0.36 U 0.35 U 0.087 J 0.037 U 0.036 U 0.035 U 0.04 0.37 U 0.36 U 0.35 U 0.37 U 0.37 U 0.36 U 0.35 U 0.37 U 0.37 U 0.36 U 0.35 U 0.37 U 0.37 U 0.36 U 0.35 U 0.37 U 0.37 U 0.36 U 0.35 U 0.37 U 0.37 U 0.36 U 0.35 U 0.13 J 0.37 U 0.36 U 0.35 U 0.37 U 0.037 U 0.036 U 0.035 U 0.037 U 0.075 U 0.073 U 0.072 U 0.075 U 0.37 U 0.36 U 0.35 U 0.37 U 0.037 U 0.036 U 0.035 U 0.037 U 0.037 U 0.036 U 0.035 U 0.071 0.15 U 0.14 U 0.14 U 0.15 U 0.37 U 0.36 U 0.35 U 0.012 J 0.037 U 0.036 U 0.035 U 0.037 U 0.037 U 0.036 U 0.035 U 0.037 U 0.37 U 0.36 U 0.35 U 0.37 U 0.37 U 0.36 U 0.35 U 0.082 J 0.37 U 0.36 U 0.35 U 0.17 J 0 0.011 0.023 1.159 Page 4 of 10 Table 3 900 King Street Rye Brook, NY Phase II Investigation Soil Analytical Results Metals Client ID NYSDEC NYSDEC NYSDEC SB-1 (0-2) SB-2 (0-2) SB-3(0-2) SB-4(0-2) SB-5(0-2) SB-6(5-7) SB-7(5-7) SB-8(1-2.5) Lab Sample ID Part 375 Part 375 Part 375 460-145515-2 460-145515-1 460-145401-4 460-145401-6 460-145401-5 460-145401-3 460-145401-2 460-145401-1 Date Sampled Unrestricted Restricted Protection of 11/20/2017 11/20/2017 11/17/2017 11/17/2017 11/17/2017 11/17/2017 11/17/2017 11/17/2017 Dilution SCO Residential Groundwater 1/10 † 1/10 †1/4 †1/4 † 1/4/10 † 1/4 †1/4 †1/4 † SCO SCO Analyte mg/kg mg/kg mg/kg Aluminum NS NS NS 20,500 22,200 7,450 8,450 18,200 9,810 9,370 10,600 Antimony NS NS NS 10.8 U 10 U 4.2 U 4.3 U 10.7 U 4.3 U 4.1 U 4.2 U Arsenic 13 16 16 8.1 U 7.5 U 3.1 U 0.84 J 3.2 U 3.2 U 3.1 U 3.1 U Barium 350 400 820 228 379 84.6 101 66.3 117 101 86.6 Beryllium 7.2 72 47 1.7 1.9 0.57 0.6 1.2 0.75 0.69 0.59 Cadmium 2.5 4.3 7.5 2.2 U 2 U 0.84 U 0.85 U 0.86 U 0.85 U 0.82 U 0.84 U Calcium NS NS NS 2,450 J 15,300 4,310 7,860 3,780 2,260 5,930 2,670 Chromium 30*** 180*** NS***53.8 76.8 19.5 25.8 39.5 25.4 22.1 18.8 Cobalt NS NS NS 13.7 J 14.8 J 5.4 J 6.8 J 10.1 J 7.1 J 7.5 J 6.6 J Copper 50 270 1,720 29.7 26.2 12.8 15.3 27.3 16.7 16.4 19.6 Iron NS NS NS 31,600 32,000 13,100 14,800 27,200 16,600 16,100 17,100 Lead 63 400 450 9.8 8.1 4.3 4.8 5 6.3 4.7 9 Magnesium NS NS NS 8,790 16,900 4,310 4,820 8,600 4,610 5,450 3,520 Manganese 1,600 2,000 2,000 528 633 269 238 365 206 235 336 Mercury 0.18 0.81 0.73 0.018 U 0.019 U 0.019 U 0.018 U 0.018 U 0.018 U 0.018 U 0.018 U Nickel 30 310 130 30.3 35.9 12.2 16.2 21.6 15.8 14.7 15.5 Potassium NS NS NS 7,570 8,950 3,050 3,520 4,100 4,050 3,770 2,840 Selenium 3.9 180 4 10.8 U 10 U 4.2 U 4.3 U 4.3 U 4.3 U 4.1 U 4.2 U Silver 2 180 8.3 5.4 U 5 U 2.1 U 2.1 U 2.1 U 2.1 U 2 U 2.1 U Sodium NS NS NS 2,690 U 2,500 U 571 J 920 J 3,350 238 J 138 J 142 J Thallium NS NS NS 10.8 U 10 U 4.2 U 4.3 U 4.3 U 4.3 U 4.1 U 4.2 U Vanadium NS NS NS 63.2 64 24.5 28.5 60.1 31.1 31.7 27.8 Zinc 109 10,000 2,480 74.8 65.5 29.1 32.3 62 37.5 33.3 39.9 † Dilution factor varies Page 5 of 10 Table 4 900 King Street Rye Brook, NY Phase II Investigation Soil Analytical Results Polychlorinated Biphenyls and Pesticides Client ID NYSDEC NYSDEC NYSDEC SB-1 (0-2) SB-2 (0-2) SB-3(0-2) SB-4(0-2) SB-5(0-2) SB-6(5-7) SB-7(5-7) SB-8(1-2.5) Lab Sample ID Part 375 Part 375 Part 375 460-145515-2 460-145515-1 460-145401-4 460-145401-6 460-145401-5 460-145401-3 460-145401-2 460-145401-1 Date Sampled Unrestricted Restricted Protection of 11/20/2017 11/20/2017 11/17/2017 11/17/2017 11/17/2017 11/17/2017 11/17/2017 11/17/2017 SCO Residential Groundwater SCO SCO PCBs mg/kg mg/kg mg/kg Aroclor 1016 NS NS NS 0.074 U 0.073 U 0.073 U 0.073 U 0.075 U 0.073 U 0.072 U 0.075 U Aroclor 1221 NS NS NS 0.074 U 0.073 U 0.073 U 0.073 U 0.075 U 0.073 U 0.072 U 0.075 U Aroclor 1232 NS NS NS 0.074 U 0.073 U 0.073 U 0.073 U 0.075 U 0.073 U 0.072 U 0.075 U Aroclor 1242 NS NS NS 0.074 U 0.073 U 0.073 U 0.073 U 0.075 U 0.073 U 0.072 U 0.075 U Aroclor 1248 NS NS NS 0.074 U 0.073 U 0.073 U 0.073 U 0.075 U 0.073 U 0.072 U 0.075 U Aroclor 1254 NS NS NS 0.074 U 0.073 U 0.073 U 0.073 U 0.075 U 0.073 U 0.072 U 0.075 U Aroclor 1260 NS NS NS 0.074 U 0.073 U 0.073 U 0.073 U 0.075 U 0.073 U 0.072 U 0.075 U Aroclor 1262 NS NS NS 0.074 U 0.073 U 0.073 U 0.073 U 0.075 U 0.073 U 0.072 U 0.075 U Aroclor 1268 NS NS NS 0.074 U 0.073 U 0.073 U 0.073 U 0.075 U 0.073 U 0.072 U 0.075 U Polychlorinated biphenyls, Total 0.1 1 3.2 0.074 U 0.073 U 0.073 U 0.073 U 0.075 U 0.073 U 0.072 U 0.075 U Pesticides mg/kg mg/kg mg/kg 4,4'-DDD 0.0033 13 14 0.0074 U 0.0073 U 0.0073 U 0.0073 U 0.0075 U 0.0073 U 0.0072 U 0.0075 U 4,4'-DDE 0.0033 8.9 17 0.0074 U 0.0073 U 0.0073 U 0.0073 U 0.0075 U 0.0073 U 0.0072 U 0.0075 U 4,4'-DDT 0.0033 7.9 136 0.0074 U 0.0073 U 0.0073 U 0.0073 U 0.0075 U 0.0073 U 0.0072 U 0.0075 U Aldrin 0.005 0.097 0.19 0.0074 U 0.0073 U 0.0073 U 0.0073 U 0.0075 U 0.0073 U 0.0072 U 0.0075 U alpha-BHC 0.02 0.48 0.02 0.0022 U 0.0022 U 0.0022 U 0.0022 U 0.0022 U 0.0022 U 0.0021 U 0.0022 U beta-BHC 0.036 0.36 0.09 0.0022 U 0.0022 U 0.0022 U 0.0022 U 0.0022 U 0.0022 U 0.0021 U 0.0022 U Chlordane (technical)NS NS NS 0.074 U 0.073 U 0.073 U 0.073 U 0.075 U 0.073 U 0.072 U 0.075 U delta-BHC 0.04 100 0.25 0.0022 U 0.0022 U 0.0022 U 0.0022 U 0.0022 U 0.0022 U 0.0021 U 0.0022 U Dieldrin 0.005 0.2 0.1 0.0022 U 0.0022 U 0.0022 U 0.0022 U 0.0022 U 0.0022 U 0.0021 U 0.0022 U Endosulfan I 2.4 TS 24 TS 102 TS 0.0074 U 0.0073 U 0.0073 U 0.0073 U 0.0075 U 0.0073 U 0.0072 U 0.0075 U Endosulfan II 2.4 TS 24 TS 102 TS 0.0074 U 0.0073 U 0.0073 U 0.0073 U 0.0075 U 0.0073 U 0.0072 U 0.0075 U Endosulfan sulfate 2.4 TS 24 TS 1,000 TS 0.0074 U 0.0073 U 0.0073 U 0.0073 U 0.0075 U 0.0073 U 0.0072 U 0.0075 U Endrin 0.014 11 0.06 0.0074 U 0.0073 U 0.0073 U 0.0073 U 0.0075 U 0.0073 U 0.0072 U 0.0075 U Endrin aldehyde NS NS NS 0.0074 U 0.0073 U 0.0073 U 0.0073 U 0.0075 U 0.0073 U 0.0072 U 0.0075 U Endrin ketone NS NS NS 0.0074 U 0.0073 U 0.0073 U 0.0073 U 0.0075 U 0.0073 U 0.0072 U 0.0075 U gamma-BHC (Lindane)0.1 1.3 0.1 0.0022 U 0.0022 U 0.0022 U 0.0022 U 0.0022 U 0.0022 U 0.0021 U 0.0022 U Heptachlor 0.042 2.1 0.38 0.0074 U 0.0073 U 0.0073 U 0.0073 U 0.0075 U 0.0073 U 0.0072 U 0.0075 U Heptachlor epoxide NS NS 0.02 G 0.0074 U 0.0073 U 0.0073 U 0.0073 U 0.0075 U 0.0073 U 0.0072 U 0.0075 U Methoxychlor NS NS 900 G 0.0074 U 0.0073 U 0.0073 U 0.0073 U 0.0075 U 0.0073 U 0.0072 U 0.0075 U Toxaphene NS NS NS 0.074 U 0.073 U 0.073 U 0.073 U 0.075 U 0.073 U 0.072 U 0.075 U Page 6 of 10 Table 5 900 King Street Rye Brook, NY Phase II Investigation Groundwater Analytical Results Volatile Organic Compounds Client ID NYSDEC OW-1 OW-2 Trip Blank Lab Sample ID Class GA 460-145597-2 460-145597-1 460-145597-3 Date Sampled Ambient 11/21/2017 11/21/2017 11/21/2017 Standard Analyte µg/L 1,1,1-Trichloroethane 5 1 U 1 U 1 U 1,1,2,2-Tetrachloroethane 5 1 U 1 U 1 U 1,1,2-Trichloro-1,2,2-trifluoroethane 5 1 U 1 U 1 U 1,1,2-Trichloroethane 1 1 U 1 U 1 U 1,1-Dichloroethane 5 1 U 1 U 1 U 1,1-Dichloroethene 5 1 U 1 U 1 U 1,2,3-Trichlorobenzene 5 1 U 1 U 1 U 1,2,4-Trichlorobenzene 5 1 U 1 U 1 U 1,2-Dibromo-3-Chloropropane 0.04 1 U 1 U 1 U 1,2-Dichlorobenzene 3 1 U 1 U 1 U 1,2-Dichloroethane 0.6 1 U 1 U 1 U 1,2-Dichloropropane 1 1 U 1 U 1 U 1,3-Dichlorobenzene 3 1 U 1 U 1 U 1,4-Dichlorobenzene 3 1 U 1 U 1 U 1,4-Dioxane NS 50 U 50 U 50 U 2-Butanone (MEK)50 5 U 5 U 5 U 2-Hexanone 50 5 U 5 U 5 U 4-Methyl-2-pentanone (MIBK)NS 5 U 5 U 5 U Acetone 50 1.1 J 4 J 2.9 J Benzene 1 1 U 1 U 1 U Bromoform 50 1 U 1 U 1 U Bromomethane 5 1 U 1 U 1 U Carbon disulfide 60 1 U 1 U 1 U Carbon tetrachloride 5 1 U 1 U 1 U Chlorobenzene 5 1 U 1 U 1 U Chlorobromomethane 5 1 U 1 U 1 U Chlorodibromomethane 50 1 U 1 U 1 U Chloroethane 5 1 U 1 U 1 U Chloroform 7 1 U 1.7 1 U Chloromethane 5 1 U 1 U 1 U cis-1,2-Dichloroethene 5 1 U 1 U 1 U cis-1,3-Dichloropropene 0.4 TS 1 U 1 U 1 U Cyclohexane NS 1 U 1 U 1 U Dichlorobromomethane 50 1 U 1 U 1 U Dichlorodifluoromethane 5 1 U 1 U 1 U Ethylbenzene 5 1 U 1 U 1 U Ethylene Dibromide 0.0006 1 U 1 U 1 U Isopropylbenzene 5 1 U 1 U 1 U Methyl acetate NS 5 U 5 U 5 U Methyl tert-butyl ether 10 1 U 1 U 1 U Methylcyclohexane NS 1 U 1 U 1 U Methylene Chloride 5 1 U 1 U 1 U m-Xylene & p-Xylene 5 1 U 1 U 1 U o-Xylene 5 1 U 1 U 1 U Styrene 5 1 U 1 U 1 U Tetrachloroethene 5 1 U 1 U 1 U Toluene 5 1 U 1 U 1 U trans-1,2-Dichloroethene 5 1 U 1 U 1 U trans-1,3-Dichloropropene 0.4 TS 1 U 1 U 1 U Trichloroethene 5 1 U 1 U 1 U Trichlorofluoromethane 5 1 U 1 U 1 U Vinyl chloride 2 1 U 1 U 1 U Total Conc NS 1.1 5.7 2.9 Page 7 of 10 Table 6 900 King Street Rye Brook, NY Phase II Investigation Groundwater Analytical Results Semivolatile Organic Compounds Client ID NYSDEC OW-1 OW-2 Lab Sample ID Class GA 460-145597-2 460-145597-1 Date Sampled Ambient 11/21/2017 11/21/2017 Standard Analyte µg/L 2,2'-oxybis[1-chloropropane]5 10 U 10 U 1,2,4-Trichlorobenzene 5 1 U 1 U 1,2-Dichlorobenzene 3 10 U 10 U 1,3-Dichlorobenzene 3 10 U 10 U 1,4-Dichlorobenzene 3 10 U 10 U 2,4-Dinitrotoluene 5 2 U 2 U 2,6-Dinitrotoluene 5 2 U 2 U 2-Chloronaphthalene NS 10 U 10 U 2-Methylnaphthalene NS 10 U 10 U 2-Nitroaniline 5 10 U 10 U 3,3'-Dichlorobenzidine 5 10 U 10 U 3-Nitroaniline 5 10 U 10 U 4-Bromophenyl phenyl ether NS 10 U 10 U 4-Chloroaniline 5 10 U 10 U 4-Chlorophenyl phenyl ether NS 10 U 10 U 4-Nitroaniline 5 10 U 10 U Acenaphthene NS 10 U 10 U Acenaphthylene NS 10 U 10 U Anthracene 50 10 U 10 U Benzo[a]anthracene 0.002 1 U 1 U Benzo[a]pyrene ND 1 U 1 U Benzo[b]fluoranthene 0.002 1 U 1 U Benzo[g,h,i]perylene NS 10 U 10 U Benzo[k]fluoranthene 0.002 1 U 1 U Bis(2-chloroethoxy)methane 5 10 U 10 U Bis(2-chloroethyl)ether 1 1 U 1 U Bis(2-ethylhexyl) phthalate 5 2 U 2 U Butyl benzyl phthalate 50 10 U 10 U Carbazole NS 10 U 10 U Chrysene 0.002 2 U 2 U Dibenz(a,h)anthracene NS 1 U 1 U Dibenzofuran NS 10 U 10 U Diethyl phthalate 50 10 U 10 U Dimethyl phthalate 50 10 U 10 U Di-n-butyl phthalate 50 10 U 10 U Di-n-octyl phthalate 50 10 U 10 U Fluoranthene 50 10 U * 10 U * Fluorene 50 10 U 10 U Hexachlorobenzene 0.04 1 U 1 U Hexachlorobutadiene 0.5 1 U 1 U Hexachlorocyclopentadiene 5 10 U 10 U Hexachloroethane 5 1 U 1 U Indeno[1,2,3-cd]pyrene 0.002 1 U 1 U Isophorone 50 10 U 10 U Naphthalene NS 10 U 10 U Nitrobenzene 0.4 1 U 1 U N-Nitrosodi-n-propylamine NS 1 U 1 U N-Nitrosodiphenylamine 50 10 U 10 U Phenanthrene 50 10 U 10 U Pyrene 50 10 U 10 U Total Conc NS 0 0 Page 8 of 10 Table 7 900 King Street Rye Brook, NY Phase II Investigation Soil Vapor Analytical Results Volatile Organic Compounds Client ID NYSDOH 2006 SV-1 SV-2 SV-3 AA-1 Lab Sample ID Soil Vapor 200-41113-3 200-41113-2 200-41113-1 200-41113-4 Date Sampled Intrusion 11/20/2017 11/20/2017 11/20/2017 11/20/2017 Dilution Air Guidance 2.5 2.98 1 1 Value Analyte µg/m3 1,1,1-Trichloroethane NS 2.7 U 3.3 U 1.1 U 1.1 U 1,1,2,2-Tetrachloroethane NS 3.4 U 4.1 U 1.4 U 1.4 U 1,1,2-Trichloroethane NS 2.7 U 3.3 U 1.1 U 1.1 U 1,1-Dichloroethane NS 2 U 2.4 U 0.81 U 0.81 U 1,1-Dichloroethene NS 0.35 U 0.41 U 0.14 U 0.14 U 1,2,4-Trichlorobenzene NS 9.3 U 11 U 3.7 U 3.7 U 1,2,4-Trimethylbenzene NS 4.6 3.7 5.5 0.98 U 1,2-Dibromoethane NS 3.8 U 4.6 U 1.5 U 1.5 U 1,2-Dichlorobenzene NS 3 U 3.6 U 1.2 U 1.2 U 1,2-Dichloroethane NS 2 U 2.4 U 0.81 U 0.81 U 1,2-Dichloroethene, Total NS 4 U 4.7 U 1.6 U 1.6 U 1,2-Dichloropropane NS 2.3 U 2.8 U 0.92 U 0.92 U 1,2-Dichlorotetrafluoroethane NS 3.5 U 4.2 U 1.4 U 1.4 U 1,3,5-Trimethylbenzene NS 2.5 U 2.9 U 1.6 0.98 U 1,3-Butadiene NS 7.3 4.9 4.7 0.44 U 1,3-Dichlorobenzene NS 3 U 3.6 U 1.2 U 1.2 U 1,4-Dichlorobenzene NS 3 U 3.6 U 1.2 U 1.2 U 1,4-Dioxane NS 45 U 54 U 18 U 18 U 2,2,4-Trimethylpentane NS 2.3 U 93 0.93 U 0.93 U 2-Chlorotoluene NS 2.6 U 3.1 U 1 U 1 U 3-Chloropropene NS 3.9 U 4.7 U 1.6 U 1.6 U 4-Ethyltoluene NS 2.5 U 2.9 U 1.8 0.98 U 4-Isopropyltoluene NS 2.7 U 3.3 U 1.1 U 1.1 U Acetone NS 30 U 90 30 12 U Benzene NS 5.1 4.3 4.9 0.64 U Benzyl chloride NS 2.6 U 3.1 U 1 U 1 U Bromodichloromethane NS 3.4 U 4 U 2.5 1.3 U Bromoethene(Vinyl Bromide)NS 2.2 U 2.6 U 0.87 U 0.87 U Bromoform NS 5.2 U 6.2 U 2.1 U 2.1 U Bromomethane NS 1.9 U 2.3 U 0.78 U 0.78 U Carbon disulfide NS 16 16 11 1.6 U Carbon tetrachloride NS 0.55 U 0.66 U 0.32 0.39 Chlorobenzene NS 2.3 U 2.7 U 0.92 U 0.92 U Chloroethane NS 3.3 U 3.9 U 1.3 U 1.3 U Chloroform NS 11 26 25 0.98 U Chloromethane NS 2.6 U 3.1 U 1 U 1 U cis-1,2-Dichloroethene NS 0.35 U 0.41 U 0.14 U 0.14 U cis-1,3-Dichloropropene NS 2.3 U 2.7 U 0.91 U 0.91 U Cumene NS 2.5 U 3.3 0.98 U 0.98 U Cyclohexane NS 2.5 2.1 U 1.2 0.69 U Dibromochloromethane NS 4.3 U 5.1 U 1.7 U 1.7 U Dichlorodifluoromethane NS 6.2 U 7.4 U 2.5 U 2.5 U Ethylbenzene NS 40 160 4.2 0.87 U Freon 22 NS 4.4 U 5.3 U 1.8 U 1.8 U Freon TF NS 3.8 U 4.6 U 1.5 U 1.5 U Hexachlorobutadiene NS 5.3 U 6.4 U 2.1 U 2.1 U Isopropyl alcohol NS 31 U 37 U 12 U 12 U m,p-Xylene NS 150 620 12 2.2 U Methyl Butyl Ketone (2-Hexanone) NS 5.1 U 6.1 U 2 U 2 U Methyl Ethyl Ketone NS 4.2 18 7.5 1.5 U methyl isobutyl ketone NS 5.1 U 6.1 U 2 U 2 U Methyl methacrylate NS 5.1 U 6.1 U 2 U 2 U Methyl tert-butyl ether NS 1.8 U 2.1 U 0.72 U 0.72 U Methylene Chloride 60 4.3 U 5.2 U 1.7 U 1.7 U Naphthalene NS 6.6 U 7.8 U 2.6 U 2.6 U n-Butane NS 110 40 25 1.2 U n-Butylbenzene NS 2.7 U 3.3 U 1.1 U 1.1 U n-Heptane NS 3.1 2.9 2.7 0.82 U n-Hexane NS 5.4 4.5 4.5 0.7 U n-Propylbenzene NS 2.5 U 2.9 U 1.3 0.98 U o-Xylene NS 53 200 4.3 0.87 U sec-Butylbenzene NS 2.7 U 3.3 U 1.1 U 1.1 U Styrene NS 2.1 U 2.5 U 0.85 U 0.85 U tert-Butyl alcohol NS 38 U 45 U 15 U 15 U tert-Butylbenzene NS 2.7 U 3.3 U 1.1 U 1.1 U Tetrachloroethene 30 3.4 U 4 U 1.4 U 1.4 U Tetrahydrofuran NS 37 U 44 U 15 U 15 U Toluene NS 17 19 23 0.75 U trans-1,2-Dichloroethene NS 2 U 2.4 U 0.79 U 0.79 U trans-1,3-Dichloropropene NS 2.3 U 2.7 U 0.91 U 0.91 U Trichloroethene 2 0.47 U 0.56 U 0.19 U 0.19 U Trichlorofluoromethane NS 2.8 U 3.3 U 1.1 U 1.1 U Vinyl chloride NS 0.22 U 0.27 U 0.089 U 0.089 U Xylene (total)NS 210 810 16 3 U Page 9 of 10 Tables 1-7 900 King Street Rye Brook, NY Phase II Investigation Analytical Results Notes GENERAL NS :No standard. U :The analyte was not detected at the indicated concentration. J :The concentration given is an estimated value. *:LCS or LCSD is outside acceptance limits. TS :Value represents a sum total standard. SOIL Part 375 Soil Cleanup Objectives : mg/kg :milligrams per kilogram = parts per million (ppm) G : Metals ***:Standard reflects trivalent, not total, Chromium. Exceedances of Part 375 Unrestricted Soil Cleanup Objectives (UUSCO) are highlighted in bold font. GROUNDWATER µg/L :micrograms per Liter = parts per billion (ppb) ND :The standard is a non-detectable concentration by the approved analytical method. SOIL VAPOR NYSDOH Soil Vapor Intrusion Air Guidance Value : µg/m3 :micrograms per cubic meter of air Soil Cleanup Objectives listed in NYSDEC (New York State Department of Environmental Conservation) "Part 375" Regulations (6 NYCRR Part 375). This standard reflects the Supplemental Soil Clean-up Objectives listed in Table 1 of NYSDEC "CP- 51/Soil Cleanup Guidance." NYSDOH Air Guidance Values (AGVs) presented in the Final Guidance for Evaluating Soil Vapor Intrusion in the State of New York, dated October 2006 (“NYSDOH Vapor Intrusion Guidance Document”), updated September 2013 for change of AGV for PCE and August 2015 for TCE. NYSDEC Class GA Ambient Standard :New York State Department of Environmental Conservation Technical and Operational Guidance Series (1.1.1): Class GA Ambient Water Quality Standards and Guidance Values. Page 10 of 10 FIGURES DATE PROJECT NO. FIGURESITE LOCATION c 20 1 7 A K R F Q: \ P r o j e c t s \ 1 7 0 0 7 3 - 9 0 0 K I N G S T R E E T \ T e c h n i c a l \ G I S a n d G r a p h i c s \ H a z m a t \ 1 7 0 0 7 3 F i g 1 s i t e l o c m a p P H 2 . m x d 1 2 / 1 / 2 0 1 7 9 : 1 7 : 4 5 A M m v e i l l e u x Village of Rye Brook, New York Map Source: USGS Topo base map service from The National Map SITELOCATION 0 800 1,600 SCALE IN FEET 12/1/2017 170073 1 [ NY CT Area of Detail 900 King Street 440 Park Avenue South, New York, NY 10016 Approximate Extent of Proposed Basement SV-1 SB-9/OW-2X OW-1 SB-8 SV-2 SV-3 OW-2 AA-1 SB-7SB-6 SB-3 SB-4 SB-5 SB-2 SB-1 10080400 SCALE IN FEET ©2 0 1 8 A K R F , I n c Q: \ P r o j e c t s \ 1 7 0 0 7 3 - 9 0 0 K I N G S T R E E T \ T e c h n i c a l \ H a z m a t \ C A D \ 1 7 0 0 7 3 F i g 2 S i t e P l a n . d w g l a s t s a v e : m v e i l l e u x 1 / 1 6 / 2 0 1 8 4 : 4 4 P M DATE Vi l l a g e o f R y e B r o o k , N e w Y o r k 90 0 K i n g S t r e e t SI T E P L A N 1/16/2018 PROJECT NO. 170073 FIGURE 2 PROJECT SITE BOUNDARY PROPOSED BUILDING FOOTPRINT SOIL BORING LOCATION SOIL BORING/MONITORING WELL LOCATION GEOTECHNICAL MONITORING WELL LOCATION SOIL VAPOR/AMBIENT AIR SAMPLE LOCATION LEGEND 44 0 P a r k A v e n u e S o u t h , N e w Y o r k , N Y 1 0 0 1 6 Map Source: Topographical Survey Titled "Existing Conditions" Completed by JMC Dated 9/28/2017. APPENDIX A PHOTOGRAPHIC DOCUMENTATION AKRF, Inc. 900 King Street, Rye Brook, New York Photograph 3: Installation of soil boring SB-8 through the concrete slab in the elevator machine room. Photograph 4: Completed soil boring SB-8 location, patched and cleaned. Photograph 1: Main entrance of the Property building, as seen from parking lot. Photograph 2: Hydraulic oil condition observed adjacent to the “Car 1” and “Car 2” motors in elevator machine room. Page 1 of 2 AKRF, Inc. 900 King Street, Rye Brook, New York Photograph 7: Soil vapor purging and helium test setup at soil vapor point SV-1 Photograph 8: Low flow groundwater sampling setup at observation well OW-2. Photograph 5: Geoprobe Direct Push Probe unit staged at soil boring SB-1 location. Photograph 6: Soil cores from soil boring SB-1 staged for field screening and sampling. Page 2 of 2 APPENDIX B GEOPHYSICAL INVESTIGATION REPORT GEOPHYSICAL ENGINEERING SURVEY REPORT Commercial Site 900 King Street Rye Brook, New York 10573 NOVA PROJECT NUMBER 17-0484 DATED November 24, 2017 PREPARED FOR: AKRF, INC. Environmental, Planning, and Engineering Consultants 34 South Broadway, Suite 401 White Plains, NY 10601 PREPARED BY: NOVA GEOPHYSICAL SERVICES SUBSURFACE MAPPING SOLUTIONS 56-01 Marathon Parkway, # 765, Douglaston, New York 11362 Ph. 347-556-7787 Fax. 718-261-1527 www.nova-gsi.com November 24, 2017 Timothy McClintock Environmental Scientist AKRF, INC. 34 South Broadway, Suite 401 White Plains, NY 10601 P) 914.922.2374 C) 914.439.1629 F) 914.949.7559 Re: Geophysical Engineering Survey (GES) Report Commercial Site 900 King Street Rye Brook, New York 10573 Dear Mr. McClintock Nova Geophysical Services (NOVA) is pleased to provide findings of the geophysical engineering survey (GES) at the above referenced project site: 900 King Street , Rye Brook, New York 10573 (the “Site”). Please see attached Site Location and Survey Plan maps for more details. INTRODUCTION TO GEOPHYSICAL ENGINEERING SURVEY (GES) NOVA performed a Geophysical engineering surveys (GES) consisting of a Ground Penetrating Radar (GPR) survey at the site. The purpose of this survey is to locate and identify utilities and other substructures as well as clear boring locations on November 16th, 2017. The equipment selected for this investigation was a Sensors and Software Noggin 250 MHz ground penetrating radar (GPR) shielded antenna, a Radio Detection RD7100 utility locator and a Schonestedt GA-72Cd Magnetometer A GPR system consists of a radar control unit, control cable and a transducer (antenna). The control unit transmits a trigger pulse at a normal repetition rate of 250 MHz. The trigger pulse is sent to the transmitter electronics in the transducer via the control cable. The transmitter electronics amplify the trigger pulses into bipolar pulses that are radiated to the surface. The transformed pulses vary in shape and frequency according to the transducer used. In the subsurface, variations of the signal occur at boundaries where there is a dielectric contrast (void, steel, soil type, etc.). Signal reflections travel back to the control unit and are represented as color graphic images for interpolation. GEOPHYSICAL ENGINEERING SURVEY / GES REPORT Commercial Site 900 King Street Rye Brook, New York 10573 GEOPHYSICAL METHODS The project site was screened using the GPR to search the specified area and inspected for reflections, which could be indicative of substructures and utilities within the subsurface. GPR data profiles were collected for the areas of the Site specified by the client. The surveyed areas consisted of concrete. DAT A PROCESSING In order to improve the quality of the results and to better identify subsurface anomalies NOVA processed the collected data. The processes flow is briefly described in this section. Step 1. Import raw RAMAC data to standard processing format Step 2. Remove instrument noise (dewow) GEOPHYSICAL ENGINEERING SURVEY / GES REPORT Commercial Site 900 King Street Rye Brook, New York 10573 Step 3. Correct for attenuation losses (energy decay function) Step 4. Remove static from bottom of profile (time cut) Step 5. Mute horizontal ringing/noise (subtracting average) The above example shows the significance of data processing. The last image (step 5) has higher resolution than the starting image (raw data – step 1) and describes the subsurface anomalies more accurately. GEOPHYSICAL ENGINEERING SURVEY / GES REPORT Commercial Site 900 King Street Rye Brook, New York 10573 GPR, Magnetics, Electromagnetics, Seismic, Resistivity, Utility Location, Borehole Logging & Camera PHYSICAL SETTINGS NOVA observed following physical conditions at the time of the survey: Weather: Overcast, light rain Temperature: 55 Degrees (F) Surface: Concrete, soil, grass Geophysical Noise Level (GNL): Geophysical Noise Level (GNL) was medium at the site. The noise was the result of being in a suburban environment. RESULTS The results of the geophysical engineering survey (GES) identified following at the project Site: • NOVA conducted a search using ground penetrating radar and a magnetometer around the perimeter of the subject property for an underground vault containing a steam tank that had previously been excavated. NOVA was unable to locate the previous excavation. • NOVA identified gas, water, electrical, and storm sewer lines on the northwestern side of the building as shown in the survey plan. • NOVA did not detect any anomalies characteristic of an underground storage tank. • All detected subsurface anomalies were marked in the onsite mark out. • All cleared boring locations were marked in the onsite mark out. • The Survey Plan portrays the subsurface areas investigated during the GES. If you have any questions, please do not hesitate to contact the undersigned. Sincerely, NOVA Geophysical Services Levent Eskicakit, P.G., E.P. Project Engineer Attachments: Site Location Map Survey Plan Geophysical Images SITE LOCATION MAP LEGEND SITE SITE:Commercial Site 900 King StreetRye Brook, New York 10573 CLIENT:AKRF DATE:November 16, 2017 AUTH:Chris Steinley SURVEY PLAN LEGEND Survey Area Gas Storm Sewer SITE:Commercial Site 900 King Street Rye Brook, New York 10573 CLIENT:AKRF DATE:November 16, 2017 AUTH:Chris Steinley Water Electric Tank Search GEOPHYSICAL IMAGES Commercial Site 900 King Street Rye Brook, New York 10573 November 16, 2017 GEOPHYSICAL IMAGES Commercial Site 900 King Street Rye Brook, New York 10573 November 16, 2017 GEOPHYSICAL IMAGES Commercial Site 900 King Street Rye Brook, New York 10573 November 16, 2017 GEOPHYSICAL IMAGES Commercial Site 900 King Street Rye Brook, New York 10573 November 16, 2017 GEOPHYSICAL IMAGES Commercial Site 900 King Street Rye Brook, New York 10573 November 16, 2017 GEOPHYSICAL IMAGES Commercial Site 900 King Street Rye Brook, New York 10573 November 16, 2017 APPENDIX C FIELD LOGS Drilling Method: Drilling Sampling Method: Driller: Weather:35°F, Partly Cloudy Logged By:T. McClintock, AKRF De p t h ( f e e t ) Re c o v e r y (I n c h e s ) Od o r Mo i s t u r e PI D NA P L Soil Samples Collected for Laboratory Analysis 1 Top 6": CONCRETE.ND DRY ND ND SB-1 (0-2) 2 at 08:20 3 4 Bottom 24": Brown/gray SAND, some Silt, fine Gravel.ND DRY ND ND 5 6 Top 23": Brown SAND, little Silt, fine Gravel. ND DRY ND ND 7 Next 19": Brown SAND, some Silt, little fine Gravel.ND DRY ND ND 8 9 Bottom 4": Black SAND, little fine Gravel, trace Silt.ND DRY ND ND 10 Top 6": Black SAND, little fine Gravel, trace Silt.ND DRY ND ND ND DRY ND ND 12 13 14 15 16 17 18 19 20 Groundwater not encountered during soil boring installation. End of soil boring at 11 feet below grade due to DPP refusal on apparent cobbles. SB-1AKRF Project Number: 170073 440 Park Avenue South, 7th Floor SOIL BORING LOG 900 King Street Sheet 1 of 1 Soil Boring ID: Geoprobe DPP Surface Condition: Concrete New York, NY 10016 Start Time: 07:55 Finish Time: 08:20 Date: 11/20/2017 5' Macrocores Craig Test Boring Soil classifications and descriptions presented are based on the Modified Burmister Classification System. Descriptions were developed for environmental purposes only. PID = photoionization detector NAPL = non-aqueous phase liquid ND = not detected 24 46 Notes: Soil sample analyzed for: Target Compound List (TCL) VOCs (EPA 8260), TCL SVOCs (EPA 8270), PCBs (EPA 8082), Pesticides (EPA 8081), and TAL Metals (EPA 6000/7000 Series) 14 Bottom 6": Brown/black/red SAND, little fine Gravel, trace Silt.11 Drilling Method: Drilling Sampling Method: Driller: Weather:35°F, Partly Cloudy Logged By:T. McClintock, AKRF De p t h ( f e e t ) Re c o v e r y (I n c h e s ) Od o r Mo i s t u r e PI D NA P L Soil Samples Collected for Laboratory Analysis 1 Top 3": ASPHALT and fine GRAVEL.ND DRY ND ND SB-2 (0-2) at 08:00 2 Next 22": Brown SAND, some Silt, little fine Gravel.ND DRY ND ND 3 4 Bottom 9": Brown SAND, little Silt, trace fine Gravel.ND WET at ND ND 4' 5 6 Top 15": Brown SAND, some Silt, little fine Gravel.ND DRY ND ND 7 Next 8": Gray SILT, trace Sand.ND DRY ND ND 8 9 Bottom 13": Brown/black SAND, some fine Gravel, trace Silt. ND DRY ND ND 10 11 12 13 14 15 16 17 18 19 20 Groundwater encountered at approximately 4 feet below grade during soil boring installation. End of soil boring at 9.5 feet below grade due to DPP refusal on apparent cobbles. SOIL BORING LOG 900 King Street Soil Boring ID:SB-2AKRF Project Number: 170073 Sheet 1 of 1 Geoprobe DPP 5' Macrocores Start Time: 07:30 Finish Time: 08:00Craig Test Boring 440 Park Avenue South, 7th Floor Date: 11/20/2017New York, NY 10016 PID = photoionization detector NAPL = non-aqueous phase liquid ND = not detected Soil classifications and descriptions presented are based on the Modified Burmister Classification System. Descriptions were developed for environmental purposes only. Surface Condition: Asphalt 34 Notes: Soil sample analyzed for: Target Compound List (TCL) VOCs (EPA 8260), TCL SVOCs (EPA 8270), PCBs (EPA 8082), Pesticides (EPA 8081), and TAL Metals (EPA 6000/7000 Series) 36 Drilling Method: Drilling Sampling Method: Driller: Weather:40°F, Sunny Logged By:T. McClintock, AKRF De p t h ( f e e t ) Re c o v e r y (I n c h e s ) Od o r Mo i s t u r e PI D NA P L Soil Samples Collected for Laboratory Analysis 1 Top 4": ASPHALT and fine GRAVEL, some Sand.ND DRY ND ND SB-3 (0-2) 2 at 12:50 3 4 Bottom 30": Brown/gray SAND, some Silt, trace fine Gravel. ND DRY ND ND 5 6 Top 23": Brown/gray SAND, some Silt, trace fine Gravel.ND DRY ND ND 7 8 9 Bottom 6": Light brown SAND, trace Silt.ND WET at ND ND 9.5' 10 11 Top 6": Brown/gray SAND, some Silt, fine Gravel.ND DRY ND ND 12 Next 12": Fine GRAVEL, some brown/white Sand, trace Silt. ND DRY ND ND 13 14 Bottom 17": Brown SAND, little Silt, trace fine Gravel.ND DRY ND ND 15 16 17 18 19 20 Groundwater encountered at approximately 9.5 feet below grade during soil boring installation. End of soil boring at 15 feet below grade. SOIL BORING LOG 900 King Street Soil Boring ID:SB-3AKRF Project Number: 170073 Sheet 1 of 1 Geoprobe DDP 5' Macrocores Start Time: 12:25 Finish Time: 12:50Craig Test Boring 440 Park Avenue South, 7th Floor Date: 11/17/2017New York, NY 10016 PID = photoionization detector NAPL = non-aqueous phase liquid ND = not detected Soil classifications and descriptions presented are based on the Modified Burmister Classification System. Descriptions were developed for environmental purposes only. Surface Condition: Asphalt 34 29 35 Notes: Soil sample analyzed for: Target Compound List (TCL) VOCs (EPA 8260), TCL SVOCs (EPA 8270), PCBs (EPA 8082), Pesticides (EPA 8081), and TAL Metals (EPA 6000/7000 Series) Drilling Method: Drilling Sampling Method: Driller: Weather:40°F, Sunny Logged By:T. McClintock, AKRF De p t h ( f e e t ) Re c o v e r y (I n c h e s ) Od o r Mo i s t u r e PID NA P L Soil Samples Collected for Laboratory Analysis 1 Top 4": ASPHALT and fine GRAVEL.ND DRY ND ND SB-4 (0-2) at 14:15 2 Next 4": Brown/Gray SAND, some Silt, little fine Gravel. ND DRY ND ND 3 4 Bottom 18": Brown/Gray SAND, little Silt, fine Gravel.ND DRY ND ND 5 6 Top 4": Fine GRAVEL, trace Silt.ND DRY ND ND 7 8 9 Bottom 24": Brown/Gray SAND, little Silt, fine Gravel.ND DRY ND ND 10 11 Top 13": Brown/Gray SAND, little Silt, fine Gravel.ND DRY ND ND 12 13 Bottom 4": Fine GRAVEL, trace Silt.ND DRY ND ND 14 15 16 17 18 19 20 Groundwater not encountered during soil boring installation. End of soil boring at 14 feet below grade due to DPP refusal on apparent cobbles. SOIL BORING LOG 900 King Street Soil Boring ID:SB-4AKRF Project Number: 170073 Sheet 1 of 1 Geoprobe DPP 5' Macrocores Start Time: 13:35 Finish Time: 14:15Craig Test Boring 440 Park Avenue South, 7th Floor Date: 11/17/2017New York, NY 10016 PID = photoionization detector NAPL = non-aqueous phase liquid ND = not detected Soil classifications and descriptions presented are based on the Modified Burmister Classification System. Descriptions were developed for environmental purposes only. Surface Condition: Asphalt 26 28 Notes: Soil sample analyzed for: Target Compound List (TCL) VOCs (EPA 8260), TCL SVOCs (EPA 8270), PCBs (EPA 8082), Pesticides (EPA 8081), and TAL Metals (EPA 6000/7000 Series) 17 Drilling Method: Drilling Sampling Method: Driller: Weather:40°F, Sunny Logged By:T. McClintock, AKRF De p t h ( f e e t ) Re c o v e r y (I n c h e s ) Od o r Mo i s t u r e PI D NA P L Soil Samples Collected for Laboratory Analysis 1 Top 6": ASPHALT and fine GRAVEL.ND DRY ND ND SB-5 (0-2) at 13:30 2 Next 6": Brown/Gray SAND, some Silt, trace fine Gravel.ND DRY ND ND 3 Next 6": Brown SAND and fine GRAVEL ND DRY ND ND 4 Bottom 10": Brown/Gray SAND, some Silt, trace fine Gravel. ND DRY ND ND 5 6 Top 12": Brown/Gray SAND, some Silt, trace fine Gravel. ND DRY ND ND 7 8 9 Bottom 20": Brown/Gray SAND, little Silt, fine Gravel.ND DRY ND ND 10 11 Top 6": Brown/Gray SAND, little Silt, fine Gravel.ND DRY ND ND 12 Next 16": Brown/Gray SAND, some Silt, little fine Gravel. ND MOIST ND ND 13 11'-13' 14 Bottom 8": Brown/Gray SAND, little Silt, trace fine Gravel. ND DRY ND ND 15 16 Top 12": Brown/Gray SAND, some Silt, trace fine Gravel. ND WET ND ND 15'-16' 17 Bottom 8": Brown/Gray SAND, little Silt, trace fine Gravel. ND DRY ND ND 18 19 20 Groundwater encountered at approximately 15 feet below grade during soil boring installation. End of soil boring at 18 feet below grade due to DPP refusal on apparent cobbles. SOIL BORING LOG 900 King Street Soil Boring ID:SB-5AKRF Project Number: 170073 Sheet 1 of 1 Geoprobe DPP 5' Macrocores Start Time: 13:05 Finish Time: 13:30Craig Test Boring 440 Park Avenue South, 7th Floor Date: 11/17/2017New York, NY 10016 PID = photoionization detector NAPL = non-aqueous phase liquid ND = not detected Soil classifications and descriptions presented are based on the Modified Burmister Classification System. Descriptions were developed for environmental purposes only. Surface Condition: Asphalt 28 32 30 Notes: Soil sample analyzed for: Target Compound List (TCL) VOCs (EPA 8260), TCL SVOCs (EPA 8270), PCBs (EPA 8082), Pesticides (EPA 8081), and TAL Metals (EPA 6000/7000 Series) 24 Drilling Method: Drilling Sampling Method: Driller: Weather:40°F, Sunny Logged By:T. McClintock, AKRF De p t h ( f e e t ) Re c o v e r y (I n c h e s ) Od o r Mo i s t u r e PI D NA P L Soil Samples Collected for Laboratory Analysis 1 Top 6": ASPHALT and fine GRAVEL.ND DRY ND ND 2 Next 6": Brown/Gray SAND, some Silt, little fine Gravel.ND DRY ND ND 3 4 Bottom 24": Brown/Gray SAND, little Silt, fine Gravel. ND DRY ND ND 5 6 Top 8": Brown/Gray SAND, little Silt, fine Gravel. ND DRY ND ND SB-6 (5-7) at 12:15 7 Next 4": Fine GRAVEL.ND DRY ND ND 8 9 Bottom 24": Brown/Gray SAND, little Silt, fine Gravel.ND DRY ND ND 10 11 Top 20": Brown/Gray SAND, some Silt, little fine Gravel.ND MOIST ND ND 12 10'-12' 13 14 Bottom 24": Brown SAND, little Silt, fine Gravel. ND DRY ND ND 15 16 Top 14": Brown SAND, little Silt, fine Gravel. ND DRY ND ND 17 Bottom 20": Brown/Red/Black SAND, some fine Gravel, trace Silt. ND DRY ND ND 18 19 20 Groundwater not encountered during soil boring installation. End of soil boring at 18 feet below grade due to DPP refusal on apparent cobbles. SOIL BORING LOG 900 King Street Soil Boring ID:SB-6AKRF Project Number: 170073 Sheet 1 of 1 Geoprobe DPP 5' Macrocores Start Time: 11:30 Finish Time: 12:15Craig Test Boring 440 Park Avenue South, 7th Floor Date: 11/17/2017New York, NY 10016 PID = photoionization detector NAPL = non-aqueous phase liquid ND = not detected Soil classifications and descriptions presented are based on the Modified Burmister Classification System. Descriptions were developed for environmental purposes only. Surface Condition: Asphalt 36 36 44 Notes: Soil sample analyzed for: Target Compound List (TCL) VOCs (EPA 8260), TCL SVOCs (EPA 8270), PCBs (EPA 8082), Pesticides (EPA 8081), and TAL Metals (EPA 6000/7000 Series) 34 Drilling Method: Drilling Sampling Method: Driller: Weather:40°F, Sunny Logged By:T. McClintock, AKRF De p t h ( f e e t ) Re c o v e r y (I n c h e s ) Od o r Mo i s t u r e PI D NA P L Soil Samples Collected for Laboratory Analysis 1 Top 6": ASPHALT and fine GRAVEL.ND DRY ND ND 2 3 4 Bottom 20": Brown/Gray SAND, little Silt, fine Gravel.ND DRY ND ND 5 6 Top 6": Fine GRAVEL, some Brown Sand.ND DRY ND ND SB-7 (5-7) 7 at 10:50 8 9 Bottom 49": Brown/Gray SAND, some Silt, little fine Gravel.ND DRY ND ND 10 11 Top 21": Brown/Gray SAND, some Silt, fine Gravel.ND MOIST ND ND 10'-12' 12 Next 6": Fine GRAVEL.ND DRY ND ND 13 14 Bottom 13": Brown SAND, little Silt, fine Gravel.ND DRY ND ND 15 16 Top 12": Brown SAND, little Silt, fine Gravel.ND DRY ND ND 17 Next 6": Fine GRAVEL. ND DRY ND ND 18 19 Bottom 37": Brown/Red/Black SAND, some fine Gravel, trace Silt. ND DRY ND ND 20 Groundwater not encountered during soil boring installation. End of soil boring at 20 feet below grade. SOIL BORING LOG 900 King Street Soil Boring ID:SB-7AKRF Project Number: 170073 Sheet 1 of 1 Geoprobe DPP 5' Macrocores Start Time: 10:10 Finish Time: 10:50Craig Test Boring 440 Park Avenue South, 7th Floor Date: 11/17/2017New York, NY 10016 PID = photoionization detector NAPL = non-aqueous phase liquid ND = not detected Soil classifications and descriptions presented are based on the Modified Burmister Classification System. Descriptions were developed for environmental purposes only. Surface Condition: Asphalt 26 55 40 55 Notes: Soil sample analyzed for: Target Compound List (TCL) VOCs (EPA 8260), TCL SVOCs (EPA 8270), PCBs (EPA 8082), Pesticides (EPA 8081), and TAL Metals (EPA 6000/7000 Series) Drilling Method: Drilling Sampling Method: Driller: Weather:40°F, Sunny Logged By:T. McClintock, AKRF De p t h ( f e e t ) Re c o v e r y (I n c h e s ) Od o r Mo i s t u r e PID NA P L Soil Samples Collected for Laboratory Analysis Top 8": CONCRETE (slab 8" thick).ND DRY ND ND SB-8 (1-2.5) 1 at 09:45 Next 4": Gray SAND, some Silt, fine Gravel.ND DRY ND ND 2 Bottom 18": Brown SAND, some Silt, fine Gravel.ND DRY ND ND 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 Groundwater not encountered during soil boring installation. End of soil boring at 30 inches below grade due to hand auger refusal on apparent cobbles. SOIL BORING LOG 900 King Street Soil Boring ID:SB-8AKRF Project Number: 170073 Sheet 1 of 1 Hand Auger Hand Auger Start Time: 08:30 Finish Time: 09:45Craig Test Boring 440 Park Avenue South, 7th Floor Date: 11/17/2017New York, NY 10016 PID = photoionization detector NAPL = non-aqueous phase liquid ND = not detected Soil classifications and descriptions presented are based on the Modified Burmister Classification System. Descriptions were developed for environmental purposes only. Surface Condition: Concrete Notes: Soil sample analyzed for: Target Compound List (TCL) VOCs (EPA 8260), TCL SVOCs (EPA 8270), PCBs (EPA 8082), Pesticides (EPA 8081), and TAL Metals (EPA 6000/7000 Series) 30 Driller: Weather:35°F, Partly Cloudy Logged by:T. McClintock, AKRF De p t h ( f e e t ) Re c o v e r y (I n c h e s ) Od o r Mo i s t u r e PI D NA P L Soil Samples Collected for Laboratory Analysis Locking Flush Mount 1 Top 4": ASPHALT and fine GRAVEL. ND DRY ND ND 2 Bentonite Seal: 0.5' - 5'Next 6": White SAND and fine GRAVEL. ND DRY ND ND 3 Next 14": Brown/gray SAND, some Silt, ND DRY ND ND little fine Gravel. 4 2" Diameter PVC well riser: 0.5' - 7' Bottom 6": Fine Gravel, some white Sand, ND DRY ND ND 5 trace Silt. 6 Top 14": Brown SAND, some Silt, little ND DRY ND ND Gravel. 7 Next 12": Brown SAND, some silt, trace ND DRY ND ND 8 Gravel. 9 Morie #1 Sand Filter Pack: 5' - 17'Bottom 10": Brown/Red/Black SAND, some ND DRY ND ND 10 Gravel, trace Silt. 11 12 2" Diameter, 0.01 Slot PVC well Bown/Red/Black SAND, some Gravel, ND DRY ND ND 13 Screen: 7' - 17'trace Silt. 14 15 Top 4": Fine GRAVEL, little brown Sand, ND DRY ND ND 16 trace Silt. Bottom 16": Brown/gray SAND, some silt, ND MOIST ND ND 17 fine Gravel.15.5'-17' 18 19 20 Notes:Soil samples analyzed for: Target Compound List (TCL) VOCs (EPA 8260), TCL SVOCs (EPA 8270), Groundwater sampling/analysis not conducted. PCBs (EPA 8082), Pesticides (EPA 8081), and TAL Metals (EPA 6000/7000 Series) Groundwater monitoring well installed to 17 feet below grade.End of soil boring at 17 feet below grade due to DPP refusal on apparent cobbles. Soil classifications and descriptions presented are based on the Modified Burmister Classification System. Descriptions were developed for environmental purposes only. PID = photoionization detector NAPL = non-aqueous phase liquid ND = not detected 30 36 Groundwater measured at 1.2 feet below grade. 42 Groundwater Depth Indicator Groundwater encountered at approximately 1.2 feet below grade in monitoring well OW-2X. 20 Soil Boring Log Soil Boring ID:SB-9OW-2X Groundwater Monitoring Well ID: Sheet 1 of 1 Date: 11/20/2017 Well Construction Surface Condition: Geoprobe DPP 5' Macrocores Sampling Method: 440 Park Avenue South, 7th Floor New York, NY 10016 Craig Test Boring SOIL BORING AND WELL INSTALLATION LOG 900 King Street AKRF Project Number: 170073 Drilling Method: Finish Time: 09:00Start Time: 08:15 Drilling Well Sampling Log Job No: 170073 Client: 900 King St. Owners LLC Well No: Project Location: 900 King St., Rye Brook, NY Sampled By: T. McClintock, AKRF Date: 11/21/2017 Sampling Time:12:20 PID at surface: ND Total Depth:18.73 ft. below top of casing Water Column (WC): 15 feet *= 0.163 * WC for 2" wells Depth to Water:3.73 ft. below top of casing Well Volume*:2.45 gallons *= 0.653 * WC for 4" wells Depth to Product:ND ft. below top of casing Volume Purged:1 gallon *= 1.469 * WC for 6" wells Depth to top of screen:10 ft. below top of casing Well Diam.:2 inches Depth to bottom of screen:20 ft. below top of casing Purging Device (pump type): Approx. Pump Intake:14 ft. below top of casing Depth to Water Purge Rate Temp Conductivity DO ORP Turbidity (Ft.)(ml/min)(oC) (mS/cm) (mg/L)(mV)(NTU) 11:50 4.11 100 13.8 0.488 10.32 8.81 165.7 8.6 11:55 4.23 100 13.7 0.485 10.26 8.79 174.9 10.5 12:00 4.31 100 13.6 0.486 10.25 8.77 185.2 9.1 12:05 4.29 100 13.6 0.487 10.23 8.76 190.4 9.1 12:10 4.25 100 13.8 0.489 10.21 8.75 193.8 10.3 12:15 4.32 100 13.6 0.487 10.21 8.75 194.5 10.6 12:30 4.15 100 14.3 0.497 10.31 8.72 208.6 8.4 +/- 3 mS/cm +/- 0.3 mg/L +/- 0.1 pH units +/- 10 mV <50 NTU Comments (problems, odor, sheen) Groundwater samples analyzed for: Target Compound List (TCL) VOCs (EPA 8260) and TCL SVOCs (EPA 8270) PID = photoionization detector ND = non-detect DO = dissolved oxygen ORP = oxidation-reduction potential No odor or sheen Stabilization Criteria: If water quality parameters do not stabilize and/or turbidity is greater than 50 NTU within two hours, discontinue purging and collect sample. OW-1 Target maximum flow rate is 100 ml/minGeopump Peristaltic Pump Time pH Page 1 of 3 Well Sampling Log Job No: 170073 Client: 900 King St. Owners LLC Well No: Project Location: 900 King St., Rye Brook, NY Sampled By: T. McClintock, AKRF Date: 11/21/2017 Sampling Time:11:05 PID at surface: ND Total Depth:21.94 ft. below top of casing Water Column (WC): 20.8 feet *= 0.163 * WC for 2" wells Depth to Water:1.14 ft. below top of casing Well Volume*:3.39 gallons *= 0.653 * WC for 4" wells Depth to Product:ND ft. below top of casing Volume Purged:4 gallons *= 1.469 * WC for 6" wells Depth to top of screen:10 ft. below top of casing Well Diam.:2 inches Depth to bottom of screen:20 ft. below top of casing Purging Device (pump type): Approx. Pump Intake:15 ft. below top of casing Depth to Water Purge Rate Temp Conductivity DO ORP Turbidity (Ft.)(ml/min)(oC) (mS/cm) (mg/L)(mV)(NTU) 9:00 1.84 100 16.5 1.154 1.12 6.81 227.1 15.5 9:05 1.86 100 16.0 1.157 0.87 6.95 219.3 85.1 9:10 1.86 100 17.3 1.161 0.73 6.96 209.2 98.0 9:15 1.86 100 17.1 1.161 0.67 6.96 202.1 180.1 9:20 1.92 100 17.8 1.159 0.58 6.96 188.0 51.0 9:25 1.97 100 17.9 1.160 0.55 6.96 179.9 38.3 9:30 2.06 100 17.6 1.163 0.52 6.96 166.4 7.6 9:35 1.99 100 17.0 1.163 0.47 6.96 157.3 12.9 9:40 2.02 100 18.1 1.164 0.43 6.95 148.2 22.2 9:45 2.04 100 18.1 1.163 0.40 6.96 144.9 37.8 9:50 2.05 100 18.3 1.166 0.37 6.96 135.6 43.3 9:55 2.07 100 18.3 1.169 0.36 6.96 131.8 53.9 10:00 2.10 100 18.3 1.171 0.35 6.97 128.8 84.3 10:05 2.03 100 17.7 1.170 0.35 6.97 128.2 118.5 10:10 2.00 100 17.8 1.171 0.35 6.96 124.5 127.3 +/- 3 mS/cm +/- 0.3 mg/L +/- 0.1 pH units +/- 10 mV <50 NTU Comments (problems, odor, sheen) Groundwater samples analyzed for: Target Compound List (TCL) VOCs (EPA 8260) and TCL SVOCs (EPA 8270) No odor or sheen Stabilization Criteria: If water quality parameters do not stabilize and/or turbidity is greater than 50 NTU within two hours, discontinue purging and collect sample. PID = photoionization detector ND = non-detect DO = dissolved oxygen ORP = oxidation-reduction potential OW-2 Target maximum flow rate is 100 ml/minGeopump Peristaltic Pump Time pH Page 2 of 3 Well Sampling Log Job No: 170073 Client: 900 King St. Owners LLC Well No: Project Location: 900 King St., Rye Brook, NY Sampled By: T. McClintock, AKRF Date: 11/21/2017 Sampling Time:11:05 PID at surface: ND Total Depth:21.94 ft. below top of casing Water Column (WC): 20.8 feet *= 0.163 * WC for 2" wells Depth to Water:1.14 ft. below top of casing Well Volume*:3.39 gallons *= 0.653 * WC for 4" wells Depth to Product:ND ft. below top of casing Volume Purged:4 gallons *= 1.469 * WC for 6" wells Depth to top of screen:10 ft. below top of casing Well Diam.:2 inches Depth to bottom of screen:20 ft. below top of casing Purging Device (pump type): Approx. Pump Intake:15 ft. below top of casing Depth to Water Purge Rate Temp Conductivity DO ORP Turbidity (Ft.)(ml/min)(oC) (mS/cm) (mg/L)(mV)(NTU) 10:15 1.97 100 17.9 1.173 0.33 6.96 122.0 149.5 10:20 1.99 100 17.9 1.175 0.33 6.97 121.5 148.8 10:25 2.01 100 18.4 1.171 0.31 6.96 118.8 189.6 10:30 2.05 100 18.3 1.173 0.31 6.96 118.0 121.4 10:35 2.06 100 18.3 1.174 0.30 6.96 118.1 167.1 10:40 2.06 100 18.2 1.175 0.29 6.96 114.6 188.1 10:45 2.07 100 18.3 1.168 0.28 6.96 113.0 196.4 10:50 1.98 100 17.9 1.168 0.28 6.97 115.2 222.5 10:55 1.99 100 18.1 1.166 0.27 6.96 114.7 239.1 11:00 1.95 100 18.1 1.169 0.26 6.97 114.0 249.6 11:15 1.98 100 18.1 1.176 0.47 6.94 118.4 67.3 +/- 3 mS/cm +/- 0.3 mg/L +/- 0.1 pH units +/- 10 mV <50 NTU Comments (problems, odor, sheen) Groundwater samples analyzed for: Target Compound List (TCL) VOCs (EPA 8260) and TCL SVOCs (EPA 8270) No odor or sheen Stabilization Criteria: If water quality parameters do not stabilize and/or turbidity is greater than 50 NTU within two hours, discontinue purging and collect sample. PID = photoionization detector ND = non-detect DO = dissolved oxygen ORP = oxidation-reduction potential OW-2 Target maximum flow rate is 100 ml/minPeristaltic Time pH Page 3 of 3 Soil Vapor Sample Log Point Installed By: Installation Method: Sampled By: Weather: 36 Inches Total Time of Purge: 2.95 In3 Purge Volume: Purged Vapor PID:1.8 ppm 0.2 L/min Helium Concentration:0 % SUMMA® Canister ID: Soil Vapor Sample ID: Background PID Soil vapor sample SV-1 collected in a 6-L SUMMA® canister using a 1-hour flow controller. ND = non-detect ppm = parts per million L/min = Liters per minute *Purge flow rate not to exceed 0.2 L/min. Vacuum (in/Hg)Notes 14 minutes Soil Vapor Point ID: Notes: ND -16.5 -6.0 Geoprobe DPP GilAir Plus Time Halfway: Time Stopped: Time Started:13:58 Purging Pump: 2 LTubing Volume: 14:55 AKRF Project No: Project Location: Client: Vapor Point Depth: N/A T. McClintock 40°F, Clear 3999 4335 SV-1 SV-1 Sample Identification Flow Controller ID: N/AND Time 14:29 -30.0 Sample Collection Pump Flow Rate*: Date: ND N/A Craig Test Boring170073 900 King St., Rye Brook, NY 900 King St. Owners LLC 11/20/2017 Sample Setup Page 1 of 4 Soil Vapor Sample Log Point Installed By: Installation Method: Sampled By: Weather: 36 Inches Total Time of Purge: 2.95 In3 Purge Volume: Purged Vapor PID:1.7 ppm 0.2 L/min Helium Concentration:0 % SUMMA® Canister ID: Soil Vapor Sample ID: Background PID Soil vapor sample SV-2 collected in a 6-L SUMMA® canister using a 1-hour flow controller. Notes: *Purge flow rate not to exceed 0.2 L/min. ND = non-detect ppm = parts per million L/min = Liters per minute Time Halfway:13:13 -15.5 ND N/A Time Stopped:13:34 -6.0 ND N/A Sample Collection Time Vacuum (in/Hg)Notes Time Started:12:44 -29.5 ND N/A Pump Flow Rate*: Sample Identification Soil Vapor Point ID:SV-2 4803 Flow Controller ID:4188 SV-2 Sample Setup Vapor Point Depth:13 minutes Tubing Volume:2 L Purging Pump:GilAir Plus Client: 900 King St. Owners LLC T. McClintock Date:11/20/2017 40°F, Clear AKRF Project No:170073 Craig Test Boring Project Location: 900 King St., Rye Brook, NY Geoprobe DPP Page 2 of 4 Soil Vapor Sample Log Point Installed By: Installation Method: Sampled By: Weather: 36 Inches Total Time of Purge: 2.95 In3 Purge Volume: Purged Vapor PID:1.4 ppm 0.2 L/min Helium Concentration:0 % SUMMA® Canister ID: Soil Vapor Sample ID: Background PID Soil vapor sample SV-3 collected in a 6-L SUMMA® canister using a 1-hour flow controller. Notes: *Purge flow rate not to exceed 0.2 L/min. ND = non-detect ppm = parts per million L/min = Liters per minute Time Halfway:12:52 -17.5 ND N/A Time Stopped:13:18 -5.0 ND N/A Sample Collection Time Vacuum (in/Hg)Notes Time Started:12:16 -30.0 ND N/A Pump Flow Rate*: Sample Identification Soil Vapor Point ID:SV-3 3010 Flow Controller ID:3993 SV-3 Sample Setup Vapor Point Depth:15 minutes Tubing Volume:2 L Purging Pump:GilAir Plus Client: 900 King St. Owners LLC T. McClintock Date:11/20/2017 40°F, Clear AKRF Project No:170073 Craig Test Boring Project Location: 900 King St., Rye Brook, NY Geoprobe DPP Page 3 of 4 Ambient Air Sample Log Client: Sampled By: Weather: SUMMA® Canister ID: Ambient Air Sample ID: Background PID Ambient air sample AA-1 collected in a 6-L SUMMA® canister using a 8-hour flow controller. Time Stopped:14:51 -6.00 ND Vehicle Notes:ND = non-detect ppm = parts per million L/min = Liters per minute Time Halfway:14:31 -15.00 ND Vehicle Time: 14:46 -9.00 ND Vehicle Time Started:13:53 -30.00 ND Vehicle Time: 14:23 -18.00 ND Vehicle Flow Controller ID:5201 AA-1 Sample Collection Time Vacuum (in/Hg)Potential VOC Sources/Notes Date:11/20/2017 40°F, Clear Sample Setup Sample Identification On-Site Location:Outside Main Entrance to Building 2537 AKRF Project No:170073 900 King St. Owners LLC Project Location: 900 King St. Rye Brook, NY T. McClintock Page 4 of 4 APPENDIX D LABORATORY ANALYTICAL REPORTS ANALYTICAL REPORT Job Number: 460-145401-1 Job Description: 900 King Street; #170073 For: AKRF Inc 34 South Broadway Suite 314 White Plains, NY 10601 Attention: Mr. Bryan Zieroff _____________________________________________ Approved for release. Thomas A Chupela Project Management Assistant I 11/29/2017 2:00 PM Designee for Melissa Haas, Project Manager I 777 New Durham Road, Edison, NJ, 08817 (203)944-1310 melissa.haas@testamericainc.com 11/29/2017 The test results in this report meet all NELAP requirements unless specified within the case narrative. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory. All questions regarding this report should be directed to the TestAmerica Edison Project Manager. TestAmerica Edison Certifications and Approvals: Connecticut: CTDOH #PH-0200, New Jersey: NJDEP (NELAP) #12028, New York: NYDOH (NELAP) #11452, NYDOH (ELAP) #11452, Pennsylvania: PADEP (NELAP) 68-00522 and Rhode Island: RIDOH LAO00132 TestAmerica Laboratories, Inc. TestAmerica Edison 777 New Durham Road, Edison, NJ 08817 Tel (732) 549-3900 Fax (732) 549-3679 www.testamericainc.com Page 1 of 194 CASE NARRATIVE Client: AKRF Inc Project: 900 King Street; #170073 Report Number: 460-145401-1 This case narrative is in the form of an exception report, where only the anomalies related to this report, method specific performance and/or QA/QC issues are discussed. If there are no issues to report, this narrative will include a statement that documents that there are no relevant data issues. It should be noted that samples with elevated Reporting Limits (RLs) as a result of a dilution may not be able to satisfy customer reporting limits in some cases. Such increases in the RLs are unavoidable but acceptable consequence of sample dilution that enables quantification of target analytes or interferences which exceed the calibration range of the instrument. Calculations are performed before rounding to avoid round-off errors in calculated results. All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below. RECEIPT The samples were received on 11/17/2017 8:40 PM, 11/20/2017 7:50 PM and 11/21/2017 6:25 PM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperatures of the 3 coolers at receipt time were 1.9º C, 3.6º C and 4.4º C. Note: All samples which require thermal preservation are considered acceptable if the arrival temperature is within 2C of the required temperature or method specified range. For samples with a specified temperature of 4C, samples with a temperature ranging from just above freezing temperature of water to 6C shall be acceptable. Samples that are hand delivered immediately following collection may not meet these criteria, however they will be deemed acceptable according to NELAC standards, if there is evidence that the chilling process has begun, such as arrival on ice, etc. VOLATILE ORGANIC COMPOUNDS (GC-MS) Samples SB-8(1-2.5) (460-145401-1), SB-2 (0-2) (460-145515-1), SB-7(5-7) (460-145401-2), SB-1 (0-2) (460-145515-2), SB-6(5-7) (460-145401-3), SB-3(0-2) (460-145401-4), SB-5(0-2) (460-145401-5) and SB-4(0-2) (460-145401-6) were analyzed for Volatile organic compounds (GC-MS) in accordance with EPA SW-846 Method 8260C. The samples were prepared on 11/18/2017 and 11/21/2017 and analyzed on 11/24/2017 and 11/25/2017. Surrogate Toluene-d8 (Surr) recovery for the following LCSD was outside control limits: (LCSD 460-479876/6). The other three system monitoring compounds were within control limits; therefore, re-analysis was not performed. The continuing calibration verification (CCV) analyzed in batch 460-479876 was outside the method criteria for the following analyte: Bromoform. A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte is considered estimated. The laboratory control sample duplicate (LCSD) for batch 479876 recovered outside control limits for the following analytes: Chloromethane and Methyl acetate. These analytes were biased high in the LCSD and were not detected in the associated samples; therefore, the data have been reported. The continuing calibration verification (CCV) associated with batch 460-479706 recovered above the upper control limit for Vinyl chloride, 1,1,2,2-Tetrachloroethane, Acrolein and Methyl acetate. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported. The laboratory control sample (LCS) and / or laboratory control sample duplicate (LCSD) for batch 479706 recovered outside control limits for the following analytes: 1,1,2,2-Tetrachloroethane, 1,2-Dibromo-3-Chloropropane, Acrolein and 1,2,3-Trichlorobenzene. These analytes were biased high in the LCS/LCSD and were not detected in the associated samples; therefore, the data have been reported. Carbon tetrachloride was detected above the reporting limit (RL) in the holding blank associated with: SB-2 (0-2) (460-145515-1) and SB-1 (0-2) (460-145515-2). Refer to the QC report for details. No other difficulties were encountered during the volatiles analysis. All other quality control parameters were within the acceptance limits. Page 2 of 194 VOLATILE ORGANIC COMPOUNDS (GC-MS) Samples OW-2 (460-145597-1), OW-1 (460-145597-2) and Trip Blank (460-145597-3) were analyzed for Volatile organic compounds (GC-MS) in accordance with EPA SW-846 Methods 8260C. The samples were analyzed on 11/26/2017. The continuing calibration verification (CCV) analyzed in batch 460-479912 was outside the method criteria for the following analyte(s): Dichlorodifluoromethane. A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte(s) is considered estimated. Refer to the QC report for details. No other difficulties were encountered during the volatiles analysis. All other quality control parameters were within the acceptance limits. SEMIVOLATILE ORGANIC COMPOUNDS (GC/MS) Samples OW-2 (460-145597-1) and OW-1 (460-145597-2) were analyzed for semivolatile organic compounds (GC/MS) in accordance with EPA SW-846 Method 8270D. The samples were prepared on 11/22/2017 and analyzed on 11/24/2017. The laboratory control sample duplicate (LCSD) for preparation batch 460-479363 and analytical batch 460-479531 recovered outside control limits for the following analyte: Fluoranthene. This analyte was biased high in the LCSD and was not detected in the associated samples; therefore, the data have been reported. Refer to the QC report for details. No other difficulties were encountered during the semivolatiles analysis. All other quality control parameters were within the acceptance limits. PESTICIDES Samples SB-8(1-2.5) (460-145401-1), SB-2 (0-2) (460-145515-1), SB-7(5-7) (460-145401-2), SB-1 (0-2) (460-145515-2), SB-6(5-7) (460-145401-3), SB-3(0-2) (460-145401-4), SB-5(0-2) (460-145401-5) and SB-4(0-2) (460-145401-6) were analyzed for Pesticides in accordance with EPA SW-846 Methods 8081B. The samples were prepared and analyzed on 11/21/2017 and 11/22/2017. No difficulties were encountered during the Pesticides analysis. All quality control parameters were within the acceptance limits. POLYCHLORINATED BIPHENYLS Samples SB-8(1-2.5) (460-145401-1), SB-2 (0-2) (460-145515-1), SB-7(5-7) (460-145401-2), SB-1 (0-2) (460-145515-2), SB-6(5-7) (460-145401-3), SB-3(0-2) (460-145401-4), SB-5(0-2) (460-145401-5) and SB-4(0-2) (460-145401-6) were analyzed for polychlorinated biphenyls in accordance with EPA SW-846 Method 8082A. The samples were prepared and analyzed on 11/21/2017 and 11/22/2017. The continuing calibration verification (CCV) for TCMX surrogate associated with batch 478953 recovered outside the lower control limit on the primary column. The samples associated with this CCV were non-detected; therefore, the data have been reported. (CCVIS 460-478953/20) Refer to the QC report for details. No difficulties were encountered during the PCBs analysis. All quality control parameters were within the acceptance limits. SEMIVOLATILE ORGANIC COMPOUNDS (GC-MS) Samples SB-8(1-2.5) (460-145401-1), SB-2 (0-2) (460-145515-1), SB-7(5-7) (460-145401-2), SB-1 (0-2) (460-145515-2), SB-6(5-7) (460-145401-3), SB-3(0-2) (460-145401-4), SB-5(0-2) (460-145401-5) and SB-4(0-2) (460-145401-6) were analyzed for semivolatile organic compounds (GC-MS) in accordance with EPA SW-846 Method 8270D. The samples were prepared on 11/19/2017 and 11/22/2017 and analyzed on 11/20/2017 and 11/27/2017. The continuing calibration verification (CCV) analyzed in 460-478549 was outside the method criteria for the following analyte(s): 2,2'-oxybis[1-chloropropane], 2-Nitroaniline, 3-Nitroaniline, 4-Nitrophenol, Dibenz(a,h)anthracene and Indeno[1,2,3-cd]pyrene. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte(s) is considered estimated. The continuing calibration verification (CCV) analyzed in batch 460-478510 was outside the method criteria for the following analyte(s): Indeno[1,2,3-cd]pyrene, Hexachlorobenzene, 4-Bromophenyl phenyl ether and 4-Nitroaniline. A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte(s) is considered estimated. Page 3 of 194 The continuing calibration verification (CCV) analyzed in batch 460-479517 was outside the method criteria for the following analyte(s): 2,2'-oxybis[1-chloropropane] and 2-Nitroaniline. A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte(s) is considered estimated. The following laboratory control sample (LCS) associated with batch 460-479261 contained one acid/base surrogate outside acceptance limits:(LCS 460-479261/2-A). The laboratory’s SOP allows one acid and/or one base surrogate to be outside acceptance limits; therefore, re-extraction/re-analysis was not performed. These results have been reported and qualified. The continuing calibration verification (CCV) analyzed in batch 460-480050 was outside the method criteria for the following analyte(s): 2,2'-oxybis[1-chloropropane], Hexachlorocyclopentadiene and 2-Nitroaniline. A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte(s) is considered estimated. Several analytes failed the recovery criteria low for the Matrix Spike/Matrix Spike Duplicate (MS/MSD) of sample 460-145381-5 in batch 460-478510. Several analytes failed the recovery criteria low for the MS/MSD of sample 460-145556-1 in batch 460-479517. Refer to the QC report for details. No other difficulties were encountered during the semivolatiles analysis. All other quality control parameters were within the acceptance limits. TOTAL METALS (ICP) Samples SB-8(1-2.5) (460-145401-1), SB-2 (0-2) (460-145515-1), SB-7(5-7) (460-145401-2), SB-1 (0-2) (460-145515-2), SB-6(5-7) (460-145401-3), SB-3(0-2) (460-145401-4), SB-5(0-2) (460-145401-5) and SB-4(0-2) (460-145401-6) were analyzed for Total Metals (ICP) in accordance with EPA SW-846 Methods 6010C. The samples were prepared on 11/20/2017 and 11/22/2017 and analyzed on 11/22/2017 and 11/24/2017. Aluminum, Magnesium and Potassium failed the recovery criteria low for the MS of sample 460-145281-1 in batch 460-479312. Iron failed the recovery criteria high. Several analytes failed the recovery criteria low for the MS of sample 460-145501-1 in batch 460-479312. Aluminum failed the recovery criteria high. Potassium exceeded the RPD limit for the duplicate of sample 460-145281-1. The presence of the '4' qualifier in the data indicates analytes where the concentration in the unspiked sample exceeded four times the spiking amount. Refer to the QC report for details. Samples SB-2 (0-2) (460-145515-1)[10X], SB-8(1-2.5) (460-145515-1)[4X], SB-1 (0-2) (460-145515-2)[10X], SB-7(5-7) (460-145515-2) [4X], SB-6(5-7) (460-145515-3)[4X], SB-3(0-2) (460-145515-4)[4X], SB-5(0-2) (460-145515-5)[10X], SB-5(0-2) (460-145515-5)[4X] and SB-4(0-2) (460-145515-6)[4X] required dilution prior to analysis. The reporting limits have been adjusted accordingly. No other difficulties were encountered during the Total Metals (ICP) analysis. All other quality control parameters were within the acceptance limits. TOTAL MERCURY Samples SB-8(1-2.5) (460-145401-1), SB-2 (0-2) (460-145515-1), SB-7(5-7) (460-145401-2), SB-1 (0-2) (460-145515-2), SB-6(5-7) (460-145401-3), SB-3(0-2) (460-145401-4), SB-5(0-2) (460-145401-5) and SB-4(0-2) (460-145401-6) were analyzed for total mercury in accordance with EPA SW-846 Method 7471B. The samples were prepared and analyzed on 11/20/2017 and 11/22/2017. No difficulties were encountered during the Hg analysis. All quality control parameters were within the acceptance limits. PERCENT SOLIDS/PERCENT MOISTURE Samples SB-8(1-2.5) (460-145401-1), SB-2 (0-2) (460-145515-1), SB-7(5-7) (460-145401-2), SB-1 (0-2) (460-145515-2), SB-6(5-7) (460-145401-3), SB-3(0-2) (460-145401-4), SB-5(0-2) (460-145401-5) and SB-4(0-2) (460-145401-6) were analyzed for percent solids/percent moisture in accordance with EPA Method CLPISM01.2 (Exhibit D) Modified. The samples were analyzed on 11/21/2017 and 11/22/2017. No difficulties were encountered during the %solids/moisture analysis. Page 4 of 194 All quality control parameters were within the acceptance limits. Page 5 of 194 EXECUTIVE SUMMARY - Detections Client: AKRF Inc Job Number: 460-145401-1 Analyte Result Reporting Limit Units Method Lab Sample ID Client Sample ID Qualifier 460-145401-1 SB-8(1-2.5) 0.00074 mg/Kg 8260C0.00012 JMethylene Chloride 0.00074 mg/Kg 8260C0.00019 Jm-Xylene & p-Xylene 0.00074 mg/Kg 8260C0.00012 Jo-Xylene 0.00074 mg/Kg 8260C0.00022 JTrichloroethene 0.37 mg/Kg 8270D0.041 J2-Methylnaphthalene 0.037 mg/Kg 8270D0.095Benzo[a]anthracene 0.037 mg/Kg 8270D0.082Benzo[a]pyrene 0.037 mg/Kg 8270D0.12Benzo[b]fluoranthene 0.37 mg/Kg 8270D0.060 JBenzo[g,h,i]perylene 0.037 mg/Kg 8270D0.048Benzo[k]fluoranthene 0.37 mg/Kg 8270D0.11 JBis(2-ethylhexyl) phthalate 0.37 mg/Kg 8270D0.011 JCarbazole 0.37 mg/Kg 8270D0.087 JChrysene 0.037 mg/Kg 8270D0.040Dibenz(a,h)anthracene 0.37 mg/Kg 8270D0.13 JFluoranthene 0.037 mg/Kg 8270D0.071Indeno[1,2,3-cd]pyrene 0.37 mg/Kg 8270D0.012 JNaphthalene 0.37 mg/Kg 8270D0.082 JPhenanthrene 0.37 mg/Kg 8270D0.17 JPyrene 41.8 mg/Kg 6010C10600Aluminum 41.8 mg/Kg 6010C86.6Barium 0.42 mg/Kg 6010C0.59Beryllium 1050 mg/Kg 6010C2670Calcium 2.1 mg/Kg 6010C18.8Chromium 10.5 mg/Kg 6010C6.6 JCobalt 5.2 mg/Kg 6010C19.6Copper 31.4 mg/Kg 6010C17100Iron 2.1 mg/Kg 6010C9.0Lead 1050 mg/Kg 6010C3520Magnesium 3.1 mg/Kg 6010C336Manganese 8.4 mg/Kg 6010C15.5Nickel 1050 mg/Kg 6010C2840Potassium 1050 mg/Kg 6010C142 JSodium 10.5 mg/Kg 6010C27.8Vanadium 6.3 mg/Kg 6010C39.9Zinc 1.0 %Moisture10.6Percent Moisture 1.0 %Moisture89.4Percent Solids TestAmerica Edison Page 6 of 194 EXECUTIVE SUMMARY - Detections Client: AKRF Inc Job Number: 460-145401-1 Analyte Result Reporting Limit Units Method Lab Sample ID Client Sample ID Qualifier 460-145401-2 SB-7(5-7) 0.00071 mg/Kg 8260C0.00014 JMethylene Chloride 0.00071 mg/Kg 8260C0.00027 JTrichloroethene 0.35 mg/Kg 8270D0.023 J2-Methylnaphthalene 40.9 mg/Kg 6010C9370Aluminum 40.9 mg/Kg 6010C101Barium 0.41 mg/Kg 6010C0.69Beryllium 1020 mg/Kg 6010C5930Calcium 2.0 mg/Kg 6010C22.1Chromium 10.2 mg/Kg 6010C7.5 JCobalt 5.1 mg/Kg 6010C16.4Copper 30.7 mg/Kg 6010C16100Iron 2.0 mg/Kg 6010C4.7Lead 1020 mg/Kg 6010C5450Magnesium 3.1 mg/Kg 6010C235Manganese 8.2 mg/Kg 6010C14.7Nickel 1020 mg/Kg 6010C3770Potassium 1020 mg/Kg 6010C138 JSodium 10.2 mg/Kg 6010C31.7Vanadium 6.1 mg/Kg 6010C33.3Zinc 1.0 %Moisture6.8Percent Moisture 1.0 %Moisture93.2Percent Solids TestAmerica Edison Page 7 of 194 EXECUTIVE SUMMARY - Detections Client: AKRF Inc Job Number: 460-145401-1 Analyte Result Reporting Limit Units Method Lab Sample ID Client Sample ID Qualifier 460-145401-3 SB-6(5-7) 0.0034 mg/Kg 8260C0.0046Acetone 0.00067 mg/Kg 8260C0.00013 JMethylene Chloride 0.00067 mg/Kg 8260C0.00033 JTrichloroethene 0.36 mg/Kg 8270D0.011 J2-Methylnaphthalene 42.7 mg/Kg 6010C9810Aluminum 42.7 mg/Kg 6010C117Barium 0.43 mg/Kg 6010C0.75Beryllium 1070 mg/Kg 6010C2260Calcium 2.1 mg/Kg 6010C25.4Chromium 10.7 mg/Kg 6010C7.1 JCobalt 5.3 mg/Kg 6010C16.7Copper 32.0 mg/Kg 6010C16600Iron 2.1 mg/Kg 6010C6.3Lead 1070 mg/Kg 6010C4610Magnesium 3.2 mg/Kg 6010C206Manganese 8.5 mg/Kg 6010C15.8Nickel 1070 mg/Kg 6010C4050Potassium 1070 mg/Kg 6010C238 JSodium 10.7 mg/Kg 6010C31.1Vanadium 6.4 mg/Kg 6010C37.5Zinc 1.0 %Moisture8.1Percent Moisture 1.0 %Moisture91.9Percent Solids TestAmerica Edison Page 8 of 194 EXECUTIVE SUMMARY - Detections Client: AKRF Inc Job Number: 460-145401-1 Analyte Result Reporting Limit Units Method Lab Sample ID Client Sample ID Qualifier 460-145401-4 SB-3(0-2) 0.0033 mg/Kg 8260C0.0044Acetone 0.00066 mg/Kg 8260C0.00018 Jm-Xylene & p-Xylene 0.00066 mg/Kg 8260C0.000069 Jo-Xylene 0.00066 mg/Kg 8260C0.00019 JTrichloroethene 41.9 mg/Kg 6010C7450Aluminum 41.9 mg/Kg 6010C84.6Barium 0.42 mg/Kg 6010C0.57Beryllium 1050 mg/Kg 6010C4310Calcium 2.1 mg/Kg 6010C19.5Chromium 10.5 mg/Kg 6010C5.4 JCobalt 5.2 mg/Kg 6010C12.8Copper 31.4 mg/Kg 6010C13100Iron 2.1 mg/Kg 6010C4.3Lead 1050 mg/Kg 6010C4310Magnesium 3.1 mg/Kg 6010C269Manganese 8.4 mg/Kg 6010C12.2Nickel 1050 mg/Kg 6010C3050Potassium 1050 mg/Kg 6010C571 JSodium 10.5 mg/Kg 6010C24.5Vanadium 6.3 mg/Kg 6010C29.1Zinc 1.0 %Moisture8.3Percent Moisture 1.0 %Moisture91.7Percent Solids 460-145401-5 SB-5(0-2) 0.00080 mg/Kg 8260C0.00014 JMethylene Chloride 0.00080 mg/Kg 8260C0.00026 JTrichloroethene 43.0 mg/Kg 6010C18200Aluminum 43.0 mg/Kg 6010C66.3Barium 0.43 mg/Kg 6010C1.2Beryllium 1070 mg/Kg 6010C3780Calcium 2.1 mg/Kg 6010C39.5Chromium 10.7 mg/Kg 6010C10.1 JCobalt 5.4 mg/Kg 6010C27.3Copper 32.2 mg/Kg 6010C27200Iron 2.1 mg/Kg 6010C5.0Lead 1070 mg/Kg 6010C8600Magnesium 3.2 mg/Kg 6010C365Manganese 8.6 mg/Kg 6010C21.6Nickel 1070 mg/Kg 6010C4100Potassium 1070 mg/Kg 6010C3350Sodium 10.7 mg/Kg 6010C60.1Vanadium 6.4 mg/Kg 6010C62.0Zinc 1.0 %Moisture10.5Percent Moisture 1.0 %Moisture89.5Percent Solids TestAmerica Edison Page 9 of 194 EXECUTIVE SUMMARY - Detections Client: AKRF Inc Job Number: 460-145401-1 Analyte Result Reporting Limit Units Method Lab Sample ID Client Sample ID Qualifier 460-145401-6 SB-4(0-2) 0.00075 mg/Kg 8260C0.00065 JMethylene Chloride 0.00075 mg/Kg 8260C0.00023 JTrichloroethene 42.6 mg/Kg 6010C8450Aluminum 3.2 mg/Kg 6010C0.84 JArsenic 42.6 mg/Kg 6010C101Barium 0.43 mg/Kg 6010C0.60Beryllium 1060 mg/Kg 6010C7860Calcium 2.1 mg/Kg 6010C25.8Chromium 10.6 mg/Kg 6010C6.8 JCobalt 5.3 mg/Kg 6010C15.3Copper 31.9 mg/Kg 6010C14800Iron 2.1 mg/Kg 6010C4.8Lead 1060 mg/Kg 6010C4820Magnesium 3.2 mg/Kg 6010C238Manganese 8.5 mg/Kg 6010C16.2Nickel 1060 mg/Kg 6010C3520Potassium 1060 mg/Kg 6010C920 JSodium 10.6 mg/Kg 6010C28.5Vanadium 6.4 mg/Kg 6010C32.3Zinc 1.0 %Moisture8.8Percent Moisture 1.0 %Moisture91.2Percent Solids 460-145515-1 SB-2 (0-2) 0.00072 mg/Kg 8260C0.0016Carbon tetrachloride 0.00072 mg/Kg 8260C0.00025 JTrichloroethene 100 mg/Kg 6010C22200Aluminum 100 mg/Kg 6010C379Barium 1.0 mg/Kg 6010C1.9Beryllium 2500 mg/Kg 6010C15300Calcium 5.0 mg/Kg 6010C76.8Chromium 25.0 mg/Kg 6010C14.8 JCobalt 12.5 mg/Kg 6010C26.2Copper 75.0 mg/Kg 6010C32000Iron 5.0 mg/Kg 6010C8.1Lead 2500 mg/Kg 6010C16900Magnesium 7.5 mg/Kg 6010C633Manganese 20.0 mg/Kg 6010C35.9Nickel 2500 mg/Kg 6010C8950Potassium 25.0 mg/Kg 6010C64.0Vanadium 15.0 mg/Kg 6010C65.5Zinc 1.0 %Moisture8.3Percent Moisture 1.0 %Moisture91.7Percent Solids TestAmerica Edison Page 10 of 194 EXECUTIVE SUMMARY - Detections Client: AKRF Inc Job Number: 460-145401-1 Analyte Result Reporting Limit Units Method Lab Sample ID Client Sample ID Qualifier 460-145515-2 SB-1 (0-2) 0.00076 mg/Kg 8260C0.0013Carbon tetrachloride 0.00076 mg/Kg 8260C0.00028 JTrichloroethene 108 mg/Kg 6010C20500Aluminum 108 mg/Kg 6010C228Barium 1.1 mg/Kg 6010C1.7Beryllium 2690 mg/Kg 6010C2450 JCalcium 5.4 mg/Kg 6010C53.8Chromium 26.9 mg/Kg 6010C13.7 JCobalt 13.5 mg/Kg 6010C29.7Copper 80.8 mg/Kg 6010C31600Iron 5.4 mg/Kg 6010C9.8Lead 2690 mg/Kg 6010C8790Magnesium 8.1 mg/Kg 6010C528Manganese 21.6 mg/Kg 6010C30.3Nickel 2690 mg/Kg 6010C7570Potassium 26.9 mg/Kg 6010C63.2Vanadium 16.2 mg/Kg 6010C74.8Zinc 1.0 %Moisture9.9Percent Moisture 1.0 %Moisture90.1Percent Solids 460-145597-1 OW-2 5.0 ug/L 8260C4.0 JAcetone 1.0 ug/L 8260C1.7Chloroform 460-145597-2 OW-1 5.0 ug/L 8260C1.1 JAcetone 460-145597-3TB TRIP BLANK 5.0 ug/L 8260C2.9 JAcetone TestAmerica Edison Page 11 of 194 METHOD SUMMARY Client: AKRF Inc Job Number: 460-145401-1 Preparation MethodMethodLab LocationDescription Matrix:Solid Volatile Organic Compounds by GC/MS TAL EDI SW846 8260C Closed System Purge and Trap TAL EDI SW846 5035 Semivolatile Organic Compounds (GC/MS)TAL EDI SW846 8270D Microwave Extraction TAL EDI SW846 3546 Organochlorine Pesticides (GC)TAL EDI SW846 8081B Microwave Extraction TAL EDI SW846 3546 Polychlorinated Biphenyls (PCBs) by Gas Chromatography TAL EDI SW846 8082A Microwave Extraction TAL EDI SW846 3546 Metals (ICP)TAL EDI SW846 6010C Preparation, Metals TAL EDI SW846 3050B Mercury (CVAA)TAL EDI SW846 7471B Preparation, Mercury TAL EDI SW846 7471B Percent Moisture TAL EDI EPA Moisture Matrix:Water Volatile Organic Compounds by GC/MS TAL EDI SW846 8260C Purge and Trap TAL EDI SW846 5030C Semivolatile Organic Compounds (GC/MS)TAL EDI SW846 8270D Liquid-Liquid Extraction (Separatory Funnel)TAL EDI SW846 3510C Lab References: TAL EDI = TestAmerica Edison Method References: EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. TestAmerica Edison Page 12 of 194 METHOD / ANALYST SUMMARY Client: AKRF Inc Job Number: 460-145401-1 Method Analyst Analyst ID Chu, Jia-min X JXCSW846 8260C Desai, Saurab SZDSW846 8260C Sarmiento, Daniel DASSW846 8260C Tupayachi, Audberto AATSW846 8260C Khlungprakhon, Sukanya SKSW846 8270D Nimer, Diaa DANSW846 8270D Kapoor, Sita SAKSW846 8081B Dalangin, Catalina CDCSW846 8082A Patel, Jignesh JHPSW846 8082A Chang, Churn Der CDCSW846 6010C Staib, Thomas TJSSW846 7471B Potts, Brandon J BJPEPA Moisture TestAmerica Edison Page 13 of 194 SAMPLE SUMMARY Client: AKRF Inc Job Number: 460-145401-1 Client Sample IDLab Sample ID Client Matrix Sampled Received Date/Time Date/Time 460-145401-1 SB-8(1-2.5)Solid 11/17/2017 0945 11/17/2017 2040 460-145401-2 SB-7(5-7)Solid 11/17/2017 1050 11/17/2017 2040 460-145401-3 SB-6(5-7)Solid 11/17/2017 1215 11/17/2017 2040 460-145401-4 SB-3(0-2)Solid 11/17/2017 1250 11/17/2017 2040 460-145401-5 SB-5(0-2)Solid 11/17/2017 1330 11/17/2017 2040 460-145401-6 SB-4(0-2)Solid 11/17/2017 1415 11/17/2017 2040 460-145515-1 SB-2 (0-2)Solid 11/20/2017 0800 11/20/2017 1950 460-145515-2 SB-1 (0-2)Solid 11/20/2017 0820 11/20/2017 1950 460-145597-1 OW-2 Water 11/21/2017 1105 11/21/2017 1825 460-145597-2 OW-1 Water 11/21/2017 1220 11/21/2017 1825 460-145597-3TB Trip Blank Water 11/21/2017 1255 11/21/2017 1825 TestAmerica Edison Page 14 of 194 SAMPLE RESULTS TestAmerica Edison Page 15 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-8(1-2.5) Client Matrix:% Moisture:10.6 460-145401-1 Solid Date Sampled: 11/17/2017 0945 Date Received: 11/17/2017 2040 8260C Volatile Organic Compounds by GC/MS Dilution: 11/18/2017 1358 11/24/2017 1931 1.0 8260C Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: D44672.D 7.589 g 5 mL 5035 CVOAMS4 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479592 460-478326 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.00074 U 0.000740.000171,1,1-Trichloroethane 0.00074 U 0.000740.000161,1,2,2-Tetrachloroethane 0.00074 U 0.000740.000221,1,2-Trichloro-1,2,2-trifluoroethane 0.00074 U 0.000740.000131,1,2-Trichloroethane 0.00074 U 0.000740.000151,1-Dichloroethane 0.00074 U 0.000740.000171,1-Dichloroethene 0.00074 U 0.000740.000131,2,3-Trichlorobenzene 0.00074 U 0.000740.0000681,2,4-Trichlorobenzene 0.00074 U 0.000740.000341,2-Dibromo-3-Chloropropane 0.00074 U 0.000740.000111,2-Dichlorobenzene 0.00074 U 0.000740.000221,2-Dichloroethane 0.00074 U 0.000740.000311,2-Dichloropropane 0.00074 U 0.000740.000121,3-Dichlorobenzene 0.00074 U 0.000740.0000741,4-Dichlorobenzene 0.015 U 0.0150.00681,4-Dioxane 0.0037 U 0.00370.000822-Butanone (MEK) 0.0037 U 0.00370.000572-Hexanone 0.0037 U 0.00370.000494-Methyl-2-pentanone (MIBK) 0.0037 U 0.00370.0028Acetone 0.00074 U 0.000740.00019Benzene 0.00074 U 0.000740.00031Bromoform 0.00074 U 0.000740.00035Bromomethane 0.00074 U 0.000740.00020Carbon disulfide 0.00074 U 0.000740.00013Carbon tetrachloride 0.00074 U 0.000740.00013Chlorobenzene 0.00074 U 0.000740.00021Chlorobromomethane 0.00074 U 0.000740.00014Chlorodibromomethane 0.00074 U 0.000740.00038Chloroethane 0.00074 U 0.000740.00024Chloroform 0.00074 U 0.000740.00032Chloromethane 0.00074 U 0.000740.00011cis-1,2-Dichloroethene 0.00074 U 0.000740.00020cis-1,3-Dichloropropene 0.00074 U 0.000740.00016Cyclohexane 0.00074 U 0.000740.00019Dichlorobromomethane 0.00074 U 0.000740.00025Dichlorodifluoromethane 0.00074 U 0.000740.00015Ethylbenzene 0.00074 U 0.000740.00013Ethylene Dibromide 0.00074 U 0.000740.000093Isopropylbenzene 0.0037 U 0.00370.0032Methyl acetate 0.00074 U 0.000740.000092Methyl tert-butyl ether 0.00074 U 0.000740.00012Methylcyclohexane 0.00012 J 0.000740.00012Methylene Chloride 0.00019 J 0.000740.00013m-Xylene & p-Xylene 0.00012 J 0.000740.000070o-Xylene 0.00074 U 0.000740.000091Styrene 0.00074 U 0.000740.00011Tetrachloroethene TestAmerica Edison Page 16 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-8(1-2.5) Client Matrix:% Moisture:10.6 460-145401-1 Solid Date Sampled: 11/17/2017 0945 Date Received: 11/17/2017 2040 8260C Volatile Organic Compounds by GC/MS Dilution: 11/18/2017 1358 11/24/2017 1931 1.0 8260C Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: D44672.D 7.589 g 5 mL 5035 CVOAMS4 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479592 460-478326 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.00074 U 0.000740.00046Toluene 0.00074 U 0.000740.00018trans-1,2-Dichloroethene 0.00074 U 0.000740.00020trans-1,3-Dichloropropene 0.00022 J 0.000740.00011Trichloroethene 0.00074 U 0.000740.00030Trichlorofluoromethane 0.00074 U 0.000740.00040Vinyl chloride Surrogate %Rec Acceptance LimitsQualifier 110 78 - 1351,2-Dichloroethane-d4 (Surr) 98 67 - 1264-Bromofluorobenzene 104 61 - 149Dibromofluoromethane (Surr) 107 73 - 121Toluene-d8 (Surr) TestAmerica Edison Page 17 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-7(5-7) Client Matrix:% Moisture:6.8 460-145401-2 Solid Date Sampled: 11/17/2017 1050 Date Received: 11/17/2017 2040 8260C Volatile Organic Compounds by GC/MS Dilution: 11/18/2017 1358 11/24/2017 1956 1.0 8260C Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: D44673.D 7.59 g 5 mL 5035 CVOAMS4 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479592 460-478326 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.00071 U 0.000710.000161,1,1-Trichloroethane 0.00071 U 0.000710.000151,1,2,2-Tetrachloroethane 0.00071 U 0.000710.000211,1,2-Trichloro-1,2,2-trifluoroethane 0.00071 U 0.000710.000131,1,2-Trichloroethane 0.00071 U 0.000710.000151,1-Dichloroethane 0.00071 U 0.000710.000161,1-Dichloroethene 0.00071 U 0.000710.000131,2,3-Trichlorobenzene 0.00071 U 0.000710.0000651,2,4-Trichlorobenzene 0.00071 U 0.000710.000331,2-Dibromo-3-Chloropropane 0.00071 U 0.000710.000101,2-Dichlorobenzene 0.00071 U 0.000710.000211,2-Dichloroethane 0.00071 U 0.000710.000301,2-Dichloropropane 0.00071 U 0.000710.000111,3-Dichlorobenzene 0.00071 U 0.000710.0000711,4-Dichlorobenzene 0.014 U 0.0140.00651,4-Dioxane 0.0035 U 0.00350.000782-Butanone (MEK) 0.0035 U 0.00350.000552-Hexanone 0.0035 U 0.00350.000474-Methyl-2-pentanone (MIBK) 0.0035 U 0.00350.0027Acetone 0.00071 U 0.000710.00018Benzene 0.00071 U 0.000710.00030Bromoform 0.00071 U 0.000710.00034Bromomethane 0.00071 U 0.000710.00019Carbon disulfide 0.00071 U 0.000710.00013Carbon tetrachloride 0.00071 U 0.000710.00013Chlorobenzene 0.00071 U 0.000710.00020Chlorobromomethane 0.00071 U 0.000710.00014Chlorodibromomethane 0.00071 U 0.000710.00037Chloroethane 0.00071 U 0.000710.00023Chloroform 0.00071 U 0.000710.00031Chloromethane 0.00071 U 0.000710.00011cis-1,2-Dichloroethene 0.00071 U 0.000710.00019cis-1,3-Dichloropropene 0.00071 U 0.000710.00016Cyclohexane 0.00071 U 0.000710.00018Dichlorobromomethane 0.00071 U 0.000710.00024Dichlorodifluoromethane 0.00071 U 0.000710.00014Ethylbenzene 0.00071 U 0.000710.00013Ethylene Dibromide 0.00071 U 0.000710.000089Isopropylbenzene 0.0035 U 0.00350.0030Methyl acetate 0.00071 U 0.000710.000088Methyl tert-butyl ether 0.00071 U 0.000710.00011Methylcyclohexane 0.00014 J 0.000710.00012Methylene Chloride 0.00071 U 0.000710.00012m-Xylene & p-Xylene 0.00071 U 0.000710.000067o-Xylene 0.00071 U 0.000710.000087Styrene 0.00071 U 0.000710.00010Tetrachloroethene TestAmerica Edison Page 18 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-7(5-7) Client Matrix:% Moisture:6.8 460-145401-2 Solid Date Sampled: 11/17/2017 1050 Date Received: 11/17/2017 2040 8260C Volatile Organic Compounds by GC/MS Dilution: 11/18/2017 1358 11/24/2017 1956 1.0 8260C Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: D44673.D 7.59 g 5 mL 5035 CVOAMS4 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479592 460-478326 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.00071 U 0.000710.00044Toluene 0.00071 U 0.000710.00017trans-1,2-Dichloroethene 0.00071 U 0.000710.00019trans-1,3-Dichloropropene 0.00027 J 0.000710.00010Trichloroethene 0.00071 U 0.000710.00029Trichlorofluoromethane 0.00071 U 0.000710.00039Vinyl chloride Surrogate %Rec Acceptance LimitsQualifier 103 78 - 1351,2-Dichloroethane-d4 (Surr) 91 67 - 1264-Bromofluorobenzene 98 61 - 149Dibromofluoromethane (Surr) 99 73 - 121Toluene-d8 (Surr) TestAmerica Edison Page 19 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-6(5-7) Client Matrix:% Moisture:8.1 460-145401-3 Solid Date Sampled: 11/17/2017 1215 Date Received: 11/17/2017 2040 8260C Volatile Organic Compounds by GC/MS Dilution: 11/18/2017 1358 11/24/2017 2020 1.0 8260C Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: D44674.D 8.101 g 5 mL 5035 CVOAMS4 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479592 460-478326 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.00067 U 0.000670.000161,1,1-Trichloroethane 0.00067 U 0.000670.000141,1,2,2-Tetrachloroethane 0.00067 U 0.000670.000201,1,2-Trichloro-1,2,2-trifluoroethane 0.00067 U 0.000670.000121,1,2-Trichloroethane 0.00067 U 0.000670.000141,1-Dichloroethane 0.00067 U 0.000670.000151,1-Dichloroethene 0.00067 U 0.000670.000121,2,3-Trichlorobenzene 0.00067 U 0.000670.0000621,2,4-Trichlorobenzene 0.00067 U 0.000670.000311,2-Dibromo-3-Chloropropane 0.00067 U 0.000670.0000971,2-Dichlorobenzene 0.00067 U 0.000670.000201,2-Dichloroethane 0.00067 U 0.000670.000281,2-Dichloropropane 0.00067 U 0.000670.000111,3-Dichlorobenzene 0.00067 U 0.000670.0000671,4-Dichlorobenzene 0.013 U 0.0130.00621,4-Dioxane 0.0034 U 0.00340.000752-Butanone (MEK) 0.0034 U 0.00340.000522-Hexanone 0.0034 U 0.00340.000454-Methyl-2-pentanone (MIBK) 0.0046 0.00340.0025Acetone 0.00067 U 0.000670.00017Benzene 0.00067 U 0.000670.00029Bromoform 0.00067 U 0.000670.00032Bromomethane 0.00067 U 0.000670.00018Carbon disulfide 0.00067 U 0.000670.00012Carbon tetrachloride 0.00067 U 0.000670.00012Chlorobenzene 0.00067 U 0.000670.00019Chlorobromomethane 0.00067 U 0.000670.00013Chlorodibromomethane 0.00067 U 0.000670.00035Chloroethane 0.00067 U 0.000670.00021Chloroform 0.00067 U 0.000670.00029Chloromethane 0.00067 U 0.000670.00010cis-1,2-Dichloroethene 0.00067 U 0.000670.00018cis-1,3-Dichloropropene 0.00067 U 0.000670.00015Cyclohexane 0.00067 U 0.000670.00017Dichlorobromomethane 0.00067 U 0.000670.00023Dichlorodifluoromethane 0.00067 U 0.000670.00013Ethylbenzene 0.00067 U 0.000670.00012Ethylene Dibromide 0.00067 U 0.000670.000085Isopropylbenzene 0.0034 U 0.00340.0029Methyl acetate 0.00067 U 0.000670.000084Methyl tert-butyl ether 0.00067 U 0.000670.00011Methylcyclohexane 0.00013 J 0.000670.00011Methylene Chloride 0.00067 U 0.000670.00012m-Xylene & p-Xylene 0.00067 U 0.000670.000064o-Xylene 0.00067 U 0.000670.000083Styrene 0.00067 U 0.000670.000096Tetrachloroethene TestAmerica Edison Page 20 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-6(5-7) Client Matrix:% Moisture:8.1 460-145401-3 Solid Date Sampled: 11/17/2017 1215 Date Received: 11/17/2017 2040 8260C Volatile Organic Compounds by GC/MS Dilution: 11/18/2017 1358 11/24/2017 2020 1.0 8260C Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: D44674.D 8.101 g 5 mL 5035 CVOAMS4 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479592 460-478326 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.00067 U 0.000670.00042Toluene 0.00067 U 0.000670.00017trans-1,2-Dichloroethene 0.00067 U 0.000670.00018trans-1,3-Dichloropropene 0.00033 J 0.000670.000097Trichloroethene 0.00067 U 0.000670.00027Trichlorofluoromethane 0.00067 U 0.000670.00037Vinyl chloride Surrogate %Rec Acceptance LimitsQualifier 118 78 - 1351,2-Dichloroethane-d4 (Surr) 101 67 - 1264-Bromofluorobenzene 111 61 - 149Dibromofluoromethane (Surr) 115 73 - 121Toluene-d8 (Surr) TestAmerica Edison Page 21 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-3(0-2) Client Matrix:% Moisture:8.3 460-145401-4 Solid Date Sampled: 11/17/2017 1250 Date Received: 11/17/2017 2040 8260C Volatile Organic Compounds by GC/MS Dilution: 11/18/2017 1359 11/24/2017 2045 1.0 8260C Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: D44675.D 8.3 g 5 mL 5035 CVOAMS4 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479592 460-478326 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.00066 U 0.000660.000151,1,1-Trichloroethane 0.00066 U 0.000660.000141,1,2,2-Tetrachloroethane 0.00066 U 0.000660.000201,1,2-Trichloro-1,2,2-trifluoroethane 0.00066 U 0.000660.000121,1,2-Trichloroethane 0.00066 U 0.000660.000141,1-Dichloroethane 0.00066 U 0.000660.000151,1-Dichloroethene 0.00066 U 0.000660.000121,2,3-Trichlorobenzene 0.00066 U 0.000660.0000601,2,4-Trichlorobenzene 0.00066 U 0.000660.000301,2-Dibromo-3-Chloropropane 0.00066 U 0.000660.0000951,2-Dichlorobenzene 0.00066 U 0.000660.000191,2-Dichloroethane 0.00066 U 0.000660.000281,2-Dichloropropane 0.00066 U 0.000660.000101,3-Dichlorobenzene 0.00066 U 0.000660.0000661,4-Dichlorobenzene 0.013 U 0.0130.00601,4-Dioxane 0.0033 U 0.00330.000732-Butanone (MEK) 0.0033 U 0.00330.000512-Hexanone 0.0033 U 0.00330.000444-Methyl-2-pentanone (MIBK) 0.0044 0.00330.0025Acetone 0.00066 U 0.000660.00017Benzene 0.00066 U 0.000660.00028Bromoform 0.00066 U 0.000660.00031Bromomethane 0.00066 U 0.000660.00017Carbon disulfide 0.00066 U 0.000660.00012Carbon tetrachloride 0.00066 U 0.000660.00012Chlorobenzene 0.00066 U 0.000660.00018Chlorobromomethane 0.00066 U 0.000660.00013Chlorodibromomethane 0.00066 U 0.000660.00034Chloroethane 0.00066 U 0.000660.00021Chloroform 0.00066 U 0.000660.00029Chloromethane 0.00066 U 0.000660.00010cis-1,2-Dichloroethene 0.00066 U 0.000660.00018cis-1,3-Dichloropropene 0.00066 U 0.000660.00015Cyclohexane 0.00066 U 0.000660.00017Dichlorobromomethane 0.00066 U 0.000660.00022Dichlorodifluoromethane 0.00066 U 0.000660.00013Ethylbenzene 0.00066 U 0.000660.00012Ethylene Dibromide 0.00066 U 0.000660.000083Isopropylbenzene 0.0033 U 0.00330.0028Methyl acetate 0.00066 U 0.000660.000082Methyl tert-butyl ether 0.00066 U 0.000660.00011Methylcyclohexane 0.00066 U 0.000660.00011Methylene Chloride 0.00018 J 0.000660.00011m-Xylene & p-Xylene 0.000069 J 0.000660.000062o-Xylene 0.00066 U 0.000660.000081Styrene 0.00066 U 0.000660.000094Tetrachloroethene TestAmerica Edison Page 22 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-3(0-2) Client Matrix:% Moisture:8.3 460-145401-4 Solid Date Sampled: 11/17/2017 1250 Date Received: 11/17/2017 2040 8260C Volatile Organic Compounds by GC/MS Dilution: 11/18/2017 1359 11/24/2017 2045 1.0 8260C Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: D44675.D 8.3 g 5 mL 5035 CVOAMS4 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479592 460-478326 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.00066 U 0.000660.00041Toluene 0.00066 U 0.000660.00016trans-1,2-Dichloroethene 0.00066 U 0.000660.00017trans-1,3-Dichloropropene 0.00019 J 0.000660.000095Trichloroethene 0.00066 U 0.000660.00027Trichlorofluoromethane 0.00066 U 0.000660.00036Vinyl chloride Surrogate %Rec Acceptance LimitsQualifier 112 78 - 1351,2-Dichloroethane-d4 (Surr) 103 67 - 1264-Bromofluorobenzene 108 61 - 149Dibromofluoromethane (Surr) 113 73 - 121Toluene-d8 (Surr) TestAmerica Edison Page 23 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-5(0-2) Client Matrix:% Moisture:10.5 460-145401-5 Solid Date Sampled: 11/17/2017 1330 Date Received: 11/17/2017 2040 8260C Volatile Organic Compounds by GC/MS Dilution: 11/18/2017 1359 11/25/2017 2147 1.0 8260C Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: D44721.D 6.979 g 5 mL 5035 CVOAMS4 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479876 460-478326 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.00080 U 0.000800.000191,1,1-Trichloroethane 0.00080 U 0.000800.000171,1,2,2-Tetrachloroethane 0.00080 U 0.000800.000241,1,2-Trichloro-1,2,2-trifluoroethane 0.00080 U 0.000800.000141,1,2-Trichloroethane 0.00080 U 0.000800.000161,1-Dichloroethane 0.00080 U 0.000800.000181,1-Dichloroethene 0.00080 U 0.000800.000141,2,3-Trichlorobenzene 0.00080 U 0.000800.0000741,2,4-Trichlorobenzene 0.00080 U 0.000800.000371,2-Dibromo-3-Chloropropane 0.00080 U 0.000800.000121,2-Dichlorobenzene 0.00080 U 0.000800.000241,2-Dichloroethane 0.00080 U 0.000800.000341,2-Dichloropropane 0.00080 U 0.000800.000131,3-Dichlorobenzene 0.00080 U 0.000800.0000801,4-Dichlorobenzene 0.016 U 0.0160.00731,4-Dioxane 0.0040 U 0.00400.000892-Butanone (MEK) 0.0040 U 0.00400.000622-Hexanone 0.0040 U 0.00400.000534-Methyl-2-pentanone (MIBK) 0.0040 U 0.00400.0030Acetone 0.00080 U 0.000800.00021Benzene 0.00080 U 0.000800.00034Bromoform 0.00080 U 0.000800.00038Bromomethane 0.00080 U 0.000800.00021Carbon disulfide 0.00080 U 0.000800.00014Carbon tetrachloride 0.00080 U 0.000800.00014Chlorobenzene 0.00080 U 0.000800.00022Chlorobromomethane 0.00080 U 0.000800.00016Chlorodibromomethane 0.00080 U 0.000800.00042Chloroethane 0.00080 U 0.000800.00026Chloroform 0.00080 U *0.000800.00035Chloromethane 0.00080 U 0.000800.00012cis-1,2-Dichloroethene 0.00080 U 0.000800.00022cis-1,3-Dichloropropene 0.00080 U 0.000800.00018Cyclohexane 0.00080 U 0.000800.00021Dichlorobromomethane 0.00080 U 0.000800.00027Dichlorodifluoromethane 0.00080 U 0.000800.00016Ethylbenzene 0.00080 U 0.000800.00014Ethylene Dibromide 0.00080 U 0.000800.00010Isopropylbenzene 0.0040 U *0.00400.0034Methyl acetate 0.00080 U 0.000800.00010Methyl tert-butyl ether 0.00080 U 0.000800.00013Methylcyclohexane 0.00014 J 0.000800.00013Methylene Chloride 0.00080 U 0.000800.00014m-Xylene & p-Xylene 0.00080 U 0.000800.000076o-Xylene 0.00080 U 0.000800.000098Styrene 0.00080 U 0.000800.00011Tetrachloroethene TestAmerica Edison Page 24 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-5(0-2) Client Matrix:% Moisture:10.5 460-145401-5 Solid Date Sampled: 11/17/2017 1330 Date Received: 11/17/2017 2040 8260C Volatile Organic Compounds by GC/MS Dilution: 11/18/2017 1359 11/25/2017 2147 1.0 8260C Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: D44721.D 6.979 g 5 mL 5035 CVOAMS4 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479876 460-478326 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.00080 U 0.000800.00050Toluene 0.00080 U 0.000800.00020trans-1,2-Dichloroethene 0.00080 U 0.000800.00021trans-1,3-Dichloropropene 0.00026 J 0.000800.00012Trichloroethene 0.00080 U 0.000800.00033Trichlorofluoromethane 0.00080 U 0.000800.00044Vinyl chloride Surrogate %Rec Acceptance LimitsQualifier 103 78 - 1351,2-Dichloroethane-d4 (Surr) 90 67 - 1264-Bromofluorobenzene 97 61 - 149Dibromofluoromethane (Surr) 102 73 - 121Toluene-d8 (Surr) TestAmerica Edison Page 25 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-4(0-2) Client Matrix:% Moisture:8.8 460-145401-6 Solid Date Sampled: 11/17/2017 1415 Date Received: 11/17/2017 2040 8260C Volatile Organic Compounds by GC/MS Dilution: 11/18/2017 1359 11/24/2017 2133 1.0 8260C Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: D44677.D 7.342 g 5 mL 5035 CVOAMS4 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479592 460-478326 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.00075 U 0.000750.000171,1,1-Trichloroethane 0.00075 U 0.000750.000161,1,2,2-Tetrachloroethane 0.00075 U 0.000750.000221,1,2-Trichloro-1,2,2-trifluoroethane 0.00075 U 0.000750.000131,1,2-Trichloroethane 0.00075 U 0.000750.000151,1-Dichloroethane 0.00075 U 0.000750.000171,1-Dichloroethene 0.00075 U 0.000750.000141,2,3-Trichlorobenzene 0.00075 U 0.000750.0000691,2,4-Trichlorobenzene 0.00075 U 0.000750.000341,2-Dibromo-3-Chloropropane 0.00075 U 0.000750.000111,2-Dichlorobenzene 0.00075 U 0.000750.000221,2-Dichloroethane 0.00075 U 0.000750.000321,2-Dichloropropane 0.00075 U 0.000750.000121,3-Dichlorobenzene 0.00075 U 0.000750.0000751,4-Dichlorobenzene 0.015 U 0.0150.00691,4-Dioxane 0.0037 U 0.00370.000832-Butanone (MEK) 0.0037 U 0.00370.000582-Hexanone 0.0037 U 0.00370.000504-Methyl-2-pentanone (MIBK) 0.0037 U 0.00370.0028Acetone 0.00075 U 0.000750.00019Benzene 0.00075 U 0.000750.00032Bromoform 0.00075 U 0.000750.00035Bromomethane 0.00075 U 0.000750.00020Carbon disulfide 0.00075 U 0.000750.00014Carbon tetrachloride 0.00075 U 0.000750.00013Chlorobenzene 0.00075 U 0.000750.00021Chlorobromomethane 0.00075 U 0.000750.00014Chlorodibromomethane 0.00075 U 0.000750.00039Chloroethane 0.00075 U 0.000750.00024Chloroform 0.00075 U 0.000750.00032Chloromethane 0.00075 U 0.000750.00011cis-1,2-Dichloroethene 0.00075 U 0.000750.00020cis-1,3-Dichloropropene 0.00075 U 0.000750.00017Cyclohexane 0.00075 U 0.000750.00019Dichlorobromomethane 0.00075 U 0.000750.00025Dichlorodifluoromethane 0.00075 U 0.000750.00015Ethylbenzene 0.00075 U 0.000750.00013Ethylene Dibromide 0.00075 U 0.000750.000094Isopropylbenzene 0.0037 U 0.00370.0032Methyl acetate 0.00075 U 0.000750.000093Methyl tert-butyl ether 0.00075 U 0.000750.00012Methylcyclohexane 0.00065 J 0.000750.00012Methylene Chloride 0.00075 U 0.000750.00013m-Xylene & p-Xylene 0.00075 U 0.000750.000071o-Xylene 0.00075 U 0.000750.000092Styrene 0.00075 U 0.000750.00011Tetrachloroethene TestAmerica Edison Page 26 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-4(0-2) Client Matrix:% Moisture:8.8 460-145401-6 Solid Date Sampled: 11/17/2017 1415 Date Received: 11/17/2017 2040 8260C Volatile Organic Compounds by GC/MS Dilution: 11/18/2017 1359 11/24/2017 2133 1.0 8260C Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: D44677.D 7.342 g 5 mL 5035 CVOAMS4 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479592 460-478326 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.00075 U 0.000750.00047Toluene 0.00075 U 0.000750.00018trans-1,2-Dichloroethene 0.00075 U 0.000750.00020trans-1,3-Dichloropropene 0.00023 J 0.000750.00011Trichloroethene 0.00075 U 0.000750.00030Trichlorofluoromethane 0.00075 U 0.000750.00041Vinyl chloride Surrogate %Rec Acceptance LimitsQualifier 101 78 - 1351,2-Dichloroethane-d4 (Surr) 89 67 - 1264-Bromofluorobenzene 95 61 - 149Dibromofluoromethane (Surr) 99 73 - 121Toluene-d8 (Surr) TestAmerica Edison Page 27 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-2 (0-2) Client Matrix:% Moisture:8.3 460-145515-1 Solid Date Sampled: 11/20/2017 0800 Date Received: 11/20/2017 1950 8260C Volatile Organic Compounds by GC/MS Dilution: 11/21/2017 1026 11/24/2017 2352 1.0 8260C Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: B23993.D 7.549 g 5 mL 5035 CVOAMS2 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479706 460-478957 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.00072 U 0.000720.000171,1,1-Trichloroethane 0.00072 U *0.000720.000151,1,2,2-Tetrachloroethane 0.00072 U 0.000720.000221,1,2-Trichloro-1,2,2-trifluoroethane 0.00072 U 0.000720.000131,1,2-Trichloroethane 0.00072 U 0.000720.000151,1-Dichloroethane 0.00072 U 0.000720.000161,1-Dichloroethene 0.00072 U *0.000720.000131,2,3-Trichlorobenzene 0.00072 U 0.000720.0000661,2,4-Trichlorobenzene 0.00072 U *0.000720.000331,2-Dibromo-3-Chloropropane 0.00072 U 0.000720.000101,2-Dichlorobenzene 0.00072 U 0.000720.000211,2-Dichloroethane 0.00072 U 0.000720.000311,2-Dichloropropane 0.00072 U 0.000720.000111,3-Dichlorobenzene 0.00072 U 0.000720.0000721,4-Dichlorobenzene 0.014 U 0.0140.00661,4-Dioxane 0.0036 U 0.00360.000802-Butanone (MEK) 0.0036 U 0.00360.000562-Hexanone 0.0036 U 0.00360.000484-Methyl-2-pentanone (MIBK) 0.0036 U 0.00360.0027Acetone 0.00072 U 0.000720.00019Benzene 0.00072 U 0.000720.00031Bromoform 0.00072 U 0.000720.00034Bromomethane 0.00072 U 0.000720.00019Carbon disulfide 0.0016 0.000720.00013Carbon tetrachloride 0.00072 U 0.000720.00013Chlorobenzene 0.00072 U 0.000720.00020Chlorobromomethane 0.00072 U 0.000720.00014Chlorodibromomethane 0.00072 U 0.000720.00038Chloroethane 0.00072 U 0.000720.00023Chloroform 0.00072 U 0.000720.00031Chloromethane 0.00072 U 0.000720.00011cis-1,2-Dichloroethene 0.00072 U 0.000720.00020cis-1,3-Dichloropropene 0.00072 U 0.000720.00016Cyclohexane 0.00072 U 0.000720.00019Dichlorobromomethane 0.00072 U 0.000720.00024Dichlorodifluoromethane 0.00072 U 0.000720.00014Ethylbenzene 0.00072 U 0.000720.00013Ethylene Dibromide 0.00072 U 0.000720.000091Isopropylbenzene 0.0036 U 0.00360.0031Methyl acetate 0.00072 U 0.000720.000090Methyl tert-butyl ether 0.00072 U 0.000720.00012Methylcyclohexane 0.00072 U 0.000720.00012Methylene Chloride 0.00072 U 0.000720.00013m-Xylene & p-Xylene 0.00072 U 0.000720.000069o-Xylene 0.00072 U 0.000720.000089Styrene 0.00072 U 0.000720.00010Tetrachloroethene TestAmerica Edison Page 28 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-2 (0-2) Client Matrix:% Moisture:8.3 460-145515-1 Solid Date Sampled: 11/20/2017 0800 Date Received: 11/20/2017 1950 8260C Volatile Organic Compounds by GC/MS Dilution: 11/21/2017 1026 11/24/2017 2352 1.0 8260C Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: B23993.D 7.549 g 5 mL 5035 CVOAMS2 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479706 460-478957 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.00072 U 0.000720.00045Toluene 0.00072 U 0.000720.00018trans-1,2-Dichloroethene 0.00072 U 0.000720.00019trans-1,3-Dichloropropene 0.00025 J 0.000720.00010Trichloroethene 0.00072 U 0.000720.00029Trichlorofluoromethane 0.00072 U 0.000720.00039Vinyl chloride Surrogate %Rec Acceptance LimitsQualifier 109 78 - 1351,2-Dichloroethane-d4 (Surr) 87 67 - 1264-Bromofluorobenzene 98 61 - 149Dibromofluoromethane (Surr) 85 73 - 121Toluene-d8 (Surr) TestAmerica Edison Page 29 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-1 (0-2) Client Matrix:% Moisture:9.9 460-145515-2 Solid Date Sampled: 11/20/2017 0820 Date Received: 11/20/2017 1950 8260C Volatile Organic Compounds by GC/MS Dilution: 11/21/2017 1027 11/25/2017 0016 1.0 8260C Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: B23994.D 7.308 g 5 mL 5035 CVOAMS2 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479706 460-478957 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.00076 U 0.000760.000181,1,1-Trichloroethane 0.00076 U *0.000760.000161,1,2,2-Tetrachloroethane 0.00076 U 0.000760.000231,1,2-Trichloro-1,2,2-trifluoroethane 0.00076 U 0.000760.000141,1,2-Trichloroethane 0.00076 U 0.000760.000161,1-Dichloroethane 0.00076 U 0.000760.000171,1-Dichloroethene 0.00076 U *0.000760.000141,2,3-Trichlorobenzene 0.00076 U 0.000760.0000701,2,4-Trichlorobenzene 0.00076 U *0.000760.000351,2-Dibromo-3-Chloropropane 0.00076 U 0.000760.000111,2-Dichlorobenzene 0.00076 U 0.000760.000221,2-Dichloroethane 0.00076 U 0.000760.000321,2-Dichloropropane 0.00076 U 0.000760.000121,3-Dichlorobenzene 0.00076 U 0.000760.0000761,4-Dichlorobenzene 0.015 U 0.0150.00701,4-Dioxane 0.0038 U 0.00380.000842-Butanone (MEK) 0.0038 U 0.00380.000592-Hexanone 0.0038 U 0.00380.000504-Methyl-2-pentanone (MIBK) 0.0038 U 0.00380.0029Acetone 0.00076 U 0.000760.00020Benzene 0.00076 U 0.000760.00032Bromoform 0.00076 U 0.000760.00036Bromomethane 0.00076 U 0.000760.00020Carbon disulfide 0.0013 0.000760.00014Carbon tetrachloride 0.00076 U 0.000760.00013Chlorobenzene 0.00076 U 0.000760.00021Chlorobromomethane 0.00076 U 0.000760.00015Chlorodibromomethane 0.00076 U 0.000760.00040Chloroethane 0.00076 U 0.000760.00024Chloroform 0.00076 U 0.000760.00033Chloromethane 0.00076 U 0.000760.00012cis-1,2-Dichloroethene 0.00076 U 0.000760.00021cis-1,3-Dichloropropene 0.00076 U 0.000760.00017Cyclohexane 0.00076 U 0.000760.00020Dichlorobromomethane 0.00076 U 0.000760.00026Dichlorodifluoromethane 0.00076 U 0.000760.00015Ethylbenzene 0.00076 U 0.000760.00014Ethylene Dibromide 0.00076 U 0.000760.000096Isopropylbenzene 0.0038 U 0.00380.0033Methyl acetate 0.00076 U 0.000760.000095Methyl tert-butyl ether 0.00076 U 0.000760.00012Methylcyclohexane 0.00076 U 0.000760.00012Methylene Chloride 0.00076 U 0.000760.00013m-Xylene & p-Xylene 0.00076 U 0.000760.000072o-Xylene 0.00076 U 0.000760.000093Styrene 0.00076 U 0.000760.00011Tetrachloroethene TestAmerica Edison Page 30 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-1 (0-2) Client Matrix:% Moisture:9.9 460-145515-2 Solid Date Sampled: 11/20/2017 0820 Date Received: 11/20/2017 1950 8260C Volatile Organic Compounds by GC/MS Dilution: 11/21/2017 1027 11/25/2017 0016 1.0 8260C Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: B23994.D 7.308 g 5 mL 5035 CVOAMS2 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479706 460-478957 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.00076 U 0.000760.00047Toluene 0.00076 U 0.000760.00019trans-1,2-Dichloroethene 0.00076 U 0.000760.00020trans-1,3-Dichloropropene 0.00028 J 0.000760.00011Trichloroethene 0.00076 U 0.000760.00031Trichlorofluoromethane 0.00076 U 0.000760.00041Vinyl chloride Surrogate %Rec Acceptance LimitsQualifier 105 78 - 1351,2-Dichloroethane-d4 (Surr) 89 67 - 1264-Bromofluorobenzene 95 61 - 149Dibromofluoromethane (Surr) 87 73 - 121Toluene-d8 (Surr) TestAmerica Edison Page 31 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: OW-2 Client Matrix: 460-145597-1 Water Date Sampled: 11/21/2017 1105 Date Received: 11/21/2017 1825 8260C Volatile Organic Compounds by GC/MS Dilution: 11/26/2017 1450 11/26/2017 1450 1.0 8260C Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: P37900.D 5 mL 5 mL 5030C CVOAMS13 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479912 N/A Analysis Method: Prep Method: Analyte Result (ug/L)Qualifier MDL RL 1.0 U 1.00.281,1,1-Trichloroethane 1.0 U 1.00.191,1,2,2-Tetrachloroethane 1.0 U 1.00.341,1,2-Trichloro-1,2,2-trifluoroethane 1.0 U 1.00.0801,1,2-Trichloroethane 1.0 U 1.00.241,1-Dichloroethane 1.0 U 1.00.341,1-Dichloroethene 1.0 U 1.00.351,2,3-Trichlorobenzene 1.0 U 1.00.271,2,4-Trichlorobenzene 1.0 U 1.00.231,2-Dibromo-3-Chloropropane 1.0 U 1.00.221,2-Dichlorobenzene 1.0 U 1.00.251,2-Dichloroethane 1.0 U 1.00.181,2-Dichloropropane 1.0 U 1.00.331,3-Dichlorobenzene 1.0 U 1.00.331,4-Dichlorobenzene 50 U 508.71,4-Dioxane 5.0 U 5.02.22-Butanone (MEK) 5.0 U 5.00.722-Hexanone 5.0 U 5.00.634-Methyl-2-pentanone (MIBK) 4.0 J 5.01.1Acetone 1.0 U 1.00.090Benzene 1.0 U 1.00.18Bromoform 1.0 U 1.00.18Bromomethane 1.0 U 1.00.22Carbon disulfide 1.0 U 1.00.33Carbon tetrachloride 1.0 U 1.00.24Chlorobenzene 1.0 U 1.00.30Chlorobromomethane 1.0 U 1.00.22Chlorodibromomethane 1.0 U 1.00.37Chloroethane 1.7 1.00.22Chloroform 1.0 U 1.00.22Chloromethane 1.0 U 1.00.26cis-1,2-Dichloroethene 1.0 U 1.00.16cis-1,3-Dichloropropene 1.0 U 1.00.26Cyclohexane 1.0 U 1.00.15Dichlorobromomethane 1.0 U 1.00.14Dichlorodifluoromethane 1.0 U 1.00.30Ethylbenzene 1.0 U 1.00.19Ethylene Dibromide 1.0 U 1.00.32Isopropylbenzene 5.0 U 5.00.58Methyl acetate 1.0 U 1.00.13Methyl tert-butyl ether 1.0 U 1.00.22Methylcyclohexane 1.0 U 1.00.21Methylene Chloride 1.0 U 1.00.28m-Xylene & p-Xylene 1.0 U 1.00.32o-Xylene 1.0 U 1.00.17Styrene 1.0 U 1.00.12Tetrachloroethene TestAmerica Edison Page 32 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: OW-2 Client Matrix: 460-145597-1 Water Date Sampled: 11/21/2017 1105 Date Received: 11/21/2017 1825 8260C Volatile Organic Compounds by GC/MS Dilution: 11/26/2017 1450 11/26/2017 1450 1.0 8260C Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: P37900.D 5 mL 5 mL 5030C CVOAMS13 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479912 N/A Analysis Method: Prep Method: Analyte Result (ug/L)Qualifier MDL RL 1.0 U 1.00.25Toluene 1.0 U 1.00.18trans-1,2-Dichloroethene 1.0 U 1.00.19trans-1,3-Dichloropropene 1.0 U 1.00.22Trichloroethene 1.0 U 1.00.15Trichlorofluoromethane 1.0 U 1.00.060Vinyl chloride Surrogate %Rec Acceptance LimitsQualifier 101 74 - 1321,2-Dichloroethane-d4 (Surr) 91 77 - 1244-Bromofluorobenzene 105 72 - 131Dibromofluoromethane (Surr) 100 80 - 120Toluene-d8 (Surr) TestAmerica Edison Page 33 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: OW-1 Client Matrix: 460-145597-2 Water Date Sampled: 11/21/2017 1220 Date Received: 11/21/2017 1825 8260C Volatile Organic Compounds by GC/MS Dilution: 11/26/2017 1515 11/26/2017 1515 1.0 8260C Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: P37901.D 5 mL 5 mL 5030C CVOAMS13 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479912 N/A Analysis Method: Prep Method: Analyte Result (ug/L)Qualifier MDL RL 1.0 U 1.00.281,1,1-Trichloroethane 1.0 U 1.00.191,1,2,2-Tetrachloroethane 1.0 U 1.00.341,1,2-Trichloro-1,2,2-trifluoroethane 1.0 U 1.00.0801,1,2-Trichloroethane 1.0 U 1.00.241,1-Dichloroethane 1.0 U 1.00.341,1-Dichloroethene 1.0 U 1.00.351,2,3-Trichlorobenzene 1.0 U 1.00.271,2,4-Trichlorobenzene 1.0 U 1.00.231,2-Dibromo-3-Chloropropane 1.0 U 1.00.221,2-Dichlorobenzene 1.0 U 1.00.251,2-Dichloroethane 1.0 U 1.00.181,2-Dichloropropane 1.0 U 1.00.331,3-Dichlorobenzene 1.0 U 1.00.331,4-Dichlorobenzene 50 U 508.71,4-Dioxane 5.0 U 5.02.22-Butanone (MEK) 5.0 U 5.00.722-Hexanone 5.0 U 5.00.634-Methyl-2-pentanone (MIBK) 1.1 J 5.01.1Acetone 1.0 U 1.00.090Benzene 1.0 U 1.00.18Bromoform 1.0 U 1.00.18Bromomethane 1.0 U 1.00.22Carbon disulfide 1.0 U 1.00.33Carbon tetrachloride 1.0 U 1.00.24Chlorobenzene 1.0 U 1.00.30Chlorobromomethane 1.0 U 1.00.22Chlorodibromomethane 1.0 U 1.00.37Chloroethane 1.0 U 1.00.22Chloroform 1.0 U 1.00.22Chloromethane 1.0 U 1.00.26cis-1,2-Dichloroethene 1.0 U 1.00.16cis-1,3-Dichloropropene 1.0 U 1.00.26Cyclohexane 1.0 U 1.00.15Dichlorobromomethane 1.0 U 1.00.14Dichlorodifluoromethane 1.0 U 1.00.30Ethylbenzene 1.0 U 1.00.19Ethylene Dibromide 1.0 U 1.00.32Isopropylbenzene 5.0 U 5.00.58Methyl acetate 1.0 U 1.00.13Methyl tert-butyl ether 1.0 U 1.00.22Methylcyclohexane 1.0 U 1.00.21Methylene Chloride 1.0 U 1.00.28m-Xylene & p-Xylene 1.0 U 1.00.32o-Xylene 1.0 U 1.00.17Styrene 1.0 U 1.00.12Tetrachloroethene TestAmerica Edison Page 34 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: OW-1 Client Matrix: 460-145597-2 Water Date Sampled: 11/21/2017 1220 Date Received: 11/21/2017 1825 8260C Volatile Organic Compounds by GC/MS Dilution: 11/26/2017 1515 11/26/2017 1515 1.0 8260C Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: P37901.D 5 mL 5 mL 5030C CVOAMS13 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479912 N/A Analysis Method: Prep Method: Analyte Result (ug/L)Qualifier MDL RL 1.0 U 1.00.25Toluene 1.0 U 1.00.18trans-1,2-Dichloroethene 1.0 U 1.00.19trans-1,3-Dichloropropene 1.0 U 1.00.22Trichloroethene 1.0 U 1.00.15Trichlorofluoromethane 1.0 U 1.00.060Vinyl chloride Surrogate %Rec Acceptance LimitsQualifier 103 74 - 1321,2-Dichloroethane-d4 (Surr) 92 77 - 1244-Bromofluorobenzene 107 72 - 131Dibromofluoromethane (Surr) 102 80 - 120Toluene-d8 (Surr) TestAmerica Edison Page 35 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: Trip Blank Client Matrix: 460-145597-3TB Water Date Sampled: 11/21/2017 1255 Date Received: 11/21/2017 1825 8260C Volatile Organic Compounds by GC/MS Dilution: 11/26/2017 1334 11/26/2017 1334 1.0 8260C Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: P37897.D 5 mL 5 mL 5030C CVOAMS13 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479912 N/A Analysis Method: Prep Method: Analyte Result (ug/L)Qualifier MDL RL 1.0 U 1.00.281,1,1-Trichloroethane 1.0 U 1.00.191,1,2,2-Tetrachloroethane 1.0 U 1.00.341,1,2-Trichloro-1,2,2-trifluoroethane 1.0 U 1.00.0801,1,2-Trichloroethane 1.0 U 1.00.241,1-Dichloroethane 1.0 U 1.00.341,1-Dichloroethene 1.0 U 1.00.351,2,3-Trichlorobenzene 1.0 U 1.00.271,2,4-Trichlorobenzene 1.0 U 1.00.231,2-Dibromo-3-Chloropropane 1.0 U 1.00.221,2-Dichlorobenzene 1.0 U 1.00.251,2-Dichloroethane 1.0 U 1.00.181,2-Dichloropropane 1.0 U 1.00.331,3-Dichlorobenzene 1.0 U 1.00.331,4-Dichlorobenzene 50 U 508.71,4-Dioxane 5.0 U 5.02.22-Butanone (MEK) 5.0 U 5.00.722-Hexanone 5.0 U 5.00.634-Methyl-2-pentanone (MIBK) 2.9 J 5.01.1Acetone 1.0 U 1.00.090Benzene 1.0 U 1.00.18Bromoform 1.0 U 1.00.18Bromomethane 1.0 U 1.00.22Carbon disulfide 1.0 U 1.00.33Carbon tetrachloride 1.0 U 1.00.24Chlorobenzene 1.0 U 1.00.30Chlorobromomethane 1.0 U 1.00.22Chlorodibromomethane 1.0 U 1.00.37Chloroethane 1.0 U 1.00.22Chloroform 1.0 U 1.00.22Chloromethane 1.0 U 1.00.26cis-1,2-Dichloroethene 1.0 U 1.00.16cis-1,3-Dichloropropene 1.0 U 1.00.26Cyclohexane 1.0 U 1.00.15Dichlorobromomethane 1.0 U 1.00.14Dichlorodifluoromethane 1.0 U 1.00.30Ethylbenzene 1.0 U 1.00.19Ethylene Dibromide 1.0 U 1.00.32Isopropylbenzene 5.0 U 5.00.58Methyl acetate 1.0 U 1.00.13Methyl tert-butyl ether 1.0 U 1.00.22Methylcyclohexane 1.0 U 1.00.21Methylene Chloride 1.0 U 1.00.28m-Xylene & p-Xylene 1.0 U 1.00.32o-Xylene 1.0 U 1.00.17Styrene 1.0 U 1.00.12Tetrachloroethene TestAmerica Edison Page 36 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: Trip Blank Client Matrix: 460-145597-3TB Water Date Sampled: 11/21/2017 1255 Date Received: 11/21/2017 1825 8260C Volatile Organic Compounds by GC/MS Dilution: 11/26/2017 1334 11/26/2017 1334 1.0 8260C Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: P37897.D 5 mL 5 mL 5030C CVOAMS13 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479912 N/A Analysis Method: Prep Method: Analyte Result (ug/L)Qualifier MDL RL 1.0 U 1.00.25Toluene 1.0 U 1.00.18trans-1,2-Dichloroethene 1.0 U 1.00.19trans-1,3-Dichloropropene 1.0 U 1.00.22Trichloroethene 1.0 U 1.00.15Trichlorofluoromethane 1.0 U 1.00.060Vinyl chloride Surrogate %Rec Acceptance LimitsQualifier 98 74 - 1321,2-Dichloroethane-d4 (Surr) 90 77 - 1244-Bromofluorobenzene 103 72 - 131Dibromofluoromethane (Surr) 100 80 - 120Toluene-d8 (Surr) TestAmerica Edison Page 37 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-8(1-2.5) Client Matrix:% Moisture:10.6 460-145401-1 Solid Date Sampled: 11/17/2017 0945 Date Received: 11/17/2017 2040 8270D Semivolatile Organic Compounds (GC/MS) Dilution: 11/19/2017 0938 11/20/2017 0252 1.0 8270D Injection Volume: Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: L205279.D 15.0418 g 1 mL 1 uL 3546 CBNAMS12 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-478510 460-478451 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.037 U 0.0370.00811,2,4-Trichlorobenzene 0.37 U 0.370.0121,2-Dichlorobenzene 0.37 U 0.370.0291,3-Dichlorobenzene 0.37 U 0.370.0291,4-Dichlorobenzene 0.37 U 0.370.0152,2'-oxybis[1-chloropropane] 0.075 U 0.0750.0152,4-Dinitrotoluene 0.075 U 0.0750.0202,6-Dinitrotoluene 0.37 U 0.370.00842-Chloronaphthalene 0.041 J 0.370.00812-Methylnaphthalene 0.37 U 0.370.0122-Nitroaniline 0.15 U 0.150.0413,3'-Dichlorobenzidine 0.37 U 0.370.0113-Nitroaniline 0.37 U 0.370.0124-Bromophenyl phenyl ether 0.37 U 0.370.00954-Chloroaniline 0.37 U 0.370.0114-Chlorophenyl phenyl ether 0.37 U 0.370.0144-Nitroaniline 0.37 U 0.370.0089Acenaphthene 0.37 U 0.370.0095Acenaphthylene 0.37 U 0.370.035Anthracene 0.095 0.0370.031Benzo[a]anthracene 0.082 0.0370.011Benzo[a]pyrene 0.12 0.0370.014Benzo[b]fluoranthene 0.060 J 0.370.021Benzo[g,h,i]perylene 0.048 0.0370.016Benzo[k]fluoranthene 0.37 U 0.370.011Bis(2-chloroethoxy)methane 0.037 U 0.0370.0087Bis(2-chloroethyl)ether 0.11 J 0.370.014Bis(2-ethylhexyl) phthalate 0.37 U 0.370.011Butyl benzyl phthalate 0.011 J 0.370.0091Carbazole 0.087 J 0.370.010Chrysene 0.040 0.0370.019Dibenz(a,h)anthracene 0.37 U 0.370.011Dibenzofuran 0.37 U 0.370.010Diethyl phthalate 0.37 U 0.370.011Dimethyl phthalate 0.37 U 0.370.011Di-n-butyl phthalate 0.37 U 0.370.019Di-n-octyl phthalate 0.13 J 0.370.011Fluoranthene 0.37 U 0.370.0080Fluorene 0.037 U 0.0370.015Hexachlorobenzene 0.075 U 0.0750.010Hexachlorobutadiene 0.37 U 0.370.023Hexachlorocyclopentadiene 0.037 U 0.0370.013Hexachloroethane 0.071 0.0370.025Indeno[1,2,3-cd]pyrene 0.15 U 0.150.0079Isophorone 0.012 J 0.370.0094Naphthalene 0.037 U 0.0370.012Nitrobenzene TestAmerica Edison Page 38 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-8(1-2.5) Client Matrix:% Moisture:10.6 460-145401-1 Solid Date Sampled: 11/17/2017 0945 Date Received: 11/17/2017 2040 8270D Semivolatile Organic Compounds (GC/MS) Dilution: 11/19/2017 0938 11/20/2017 0252 1.0 8270D Injection Volume: Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: L205279.D 15.0418 g 1 mL 1 uL 3546 CBNAMS12 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-478510 460-478451 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.037 U 0.0370.012N-Nitrosodi-n-propylamine 0.37 U 0.370.033N-Nitrosodiphenylamine 0.082 J 0.370.0098Phenanthrene 0.17 J 0.370.017Pyrene Surrogate %Rec Acceptance LimitsQualifier 50 38 - 952-Fluorobiphenyl 45 37 - 94Nitrobenzene-d5 (Surr) 68 24 - 109Terphenyl-d14 (Surr) TestAmerica Edison Page 39 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-7(5-7) Client Matrix:% Moisture:6.8 460-145401-2 Solid Date Sampled: 11/17/2017 1050 Date Received: 11/17/2017 2040 8270D Semivolatile Organic Compounds (GC/MS) Dilution: 11/19/2017 0938 11/20/2017 0314 1.0 8270D Injection Volume: Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: L205280.D 15.0326 g 1 mL 1 uL 3546 CBNAMS12 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-478510 460-478451 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.035 U 0.0350.00781,2,4-Trichlorobenzene 0.35 U 0.350.0121,2-Dichlorobenzene 0.35 U 0.350.0271,3-Dichlorobenzene 0.35 U 0.350.0281,4-Dichlorobenzene 0.35 U 0.350.0152,2'-oxybis[1-chloropropane] 0.072 U 0.0720.0142,4-Dinitrotoluene 0.072 U 0.0720.0192,6-Dinitrotoluene 0.35 U 0.350.00802-Chloronaphthalene 0.023 J 0.350.00782-Methylnaphthalene 0.35 U 0.350.0122-Nitroaniline 0.14 U 0.140.0403,3'-Dichlorobenzidine 0.35 U 0.350.0103-Nitroaniline 0.35 U 0.350.0114-Bromophenyl phenyl ether 0.35 U 0.350.00914-Chloroaniline 0.35 U 0.350.0114-Chlorophenyl phenyl ether 0.35 U 0.350.0134-Nitroaniline 0.35 U 0.350.0086Acenaphthene 0.35 U 0.350.0091Acenaphthylene 0.35 U 0.350.034Anthracene 0.035 U 0.0350.030Benzo[a]anthracene 0.035 U 0.0350.011Benzo[a]pyrene 0.035 U 0.0350.014Benzo[b]fluoranthene 0.35 U 0.350.020Benzo[g,h,i]perylene 0.035 U 0.0350.015Benzo[k]fluoranthene 0.35 U 0.350.011Bis(2-chloroethoxy)methane 0.035 U 0.0350.0084Bis(2-chloroethyl)ether 0.35 U 0.350.014Bis(2-ethylhexyl) phthalate 0.35 U 0.350.011Butyl benzyl phthalate 0.35 U 0.350.0088Carbazole 0.35 U 0.350.0096Chrysene 0.035 U 0.0350.018Dibenz(a,h)anthracene 0.35 U 0.350.011Dibenzofuran 0.35 U 0.350.010Diethyl phthalate 0.35 U 0.350.010Dimethyl phthalate 0.35 U 0.350.011Di-n-butyl phthalate 0.35 U 0.350.018Di-n-octyl phthalate 0.35 U 0.350.010Fluoranthene 0.35 U 0.350.0077Fluorene 0.035 U 0.0350.014Hexachlorobenzene 0.072 U 0.0720.010Hexachlorobutadiene 0.35 U 0.350.022Hexachlorocyclopentadiene 0.035 U 0.0350.013Hexachloroethane 0.035 U 0.0350.024Indeno[1,2,3-cd]pyrene 0.14 U 0.140.0076Isophorone 0.35 U 0.350.0090Naphthalene 0.035 U 0.0350.011Nitrobenzene TestAmerica Edison Page 40 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-7(5-7) Client Matrix:% Moisture:6.8 460-145401-2 Solid Date Sampled: 11/17/2017 1050 Date Received: 11/17/2017 2040 8270D Semivolatile Organic Compounds (GC/MS) Dilution: 11/19/2017 0938 11/20/2017 0314 1.0 8270D Injection Volume: Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: L205280.D 15.0326 g 1 mL 1 uL 3546 CBNAMS12 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-478510 460-478451 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.035 U 0.0350.012N-Nitrosodi-n-propylamine 0.35 U 0.350.032N-Nitrosodiphenylamine 0.35 U 0.350.0094Phenanthrene 0.35 U 0.350.016Pyrene Surrogate %Rec Acceptance LimitsQualifier 56 38 - 952-Fluorobiphenyl 52 37 - 94Nitrobenzene-d5 (Surr) 81 24 - 109Terphenyl-d14 (Surr) TestAmerica Edison Page 41 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-6(5-7) Client Matrix:% Moisture:8.1 460-145401-3 Solid Date Sampled: 11/17/2017 1215 Date Received: 11/17/2017 2040 8270D Semivolatile Organic Compounds (GC/MS) Dilution: 11/19/2017 0938 11/20/2017 0336 1.0 8270D Injection Volume: Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: L205281.D 15.0418 g 1 mL 1 uL 3546 CBNAMS12 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-478510 460-478451 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.036 U 0.0360.00791,2,4-Trichlorobenzene 0.36 U 0.360.0121,2-Dichlorobenzene 0.36 U 0.360.0281,3-Dichlorobenzene 0.36 U 0.360.0281,4-Dichlorobenzene 0.36 U 0.360.0152,2'-oxybis[1-chloropropane] 0.073 U 0.0730.0142,4-Dinitrotoluene 0.073 U 0.0730.0192,6-Dinitrotoluene 0.36 U 0.360.00812-Chloronaphthalene 0.011 J 0.360.00792-Methylnaphthalene 0.36 U 0.360.0122-Nitroaniline 0.14 U 0.140.0403,3'-Dichlorobenzidine 0.36 U 0.360.0113-Nitroaniline 0.36 U 0.360.0114-Bromophenyl phenyl ether 0.36 U 0.360.00924-Chloroaniline 0.36 U 0.360.0114-Chlorophenyl phenyl ether 0.36 U 0.360.0144-Nitroaniline 0.36 U 0.360.0087Acenaphthene 0.36 U 0.360.0092Acenaphthylene 0.36 U 0.360.034Anthracene 0.036 U 0.0360.030Benzo[a]anthracene 0.036 U 0.0360.011Benzo[a]pyrene 0.036 U 0.0360.014Benzo[b]fluoranthene 0.36 U 0.360.021Benzo[g,h,i]perylene 0.036 U 0.0360.016Benzo[k]fluoranthene 0.36 U 0.360.011Bis(2-chloroethoxy)methane 0.036 U 0.0360.0085Bis(2-chloroethyl)ether 0.36 U 0.360.014Bis(2-ethylhexyl) phthalate 0.36 U 0.360.011Butyl benzyl phthalate 0.36 U 0.360.0089Carbazole 0.36 U 0.360.0098Chrysene 0.036 U 0.0360.019Dibenz(a,h)anthracene 0.36 U 0.360.011Dibenzofuran 0.36 U 0.360.010Diethyl phthalate 0.36 U 0.360.010Dimethyl phthalate 0.36 U 0.360.011Di-n-butyl phthalate 0.36 U 0.360.018Di-n-octyl phthalate 0.36 U 0.360.011Fluoranthene 0.36 U 0.360.0078Fluorene 0.036 U 0.0360.015Hexachlorobenzene 0.073 U 0.0730.010Hexachlorobutadiene 0.36 U 0.360.022Hexachlorocyclopentadiene 0.036 U 0.0360.013Hexachloroethane 0.036 U 0.0360.024Indeno[1,2,3-cd]pyrene 0.14 U 0.140.0077Isophorone 0.36 U 0.360.0091Naphthalene 0.036 U 0.0360.011Nitrobenzene TestAmerica Edison Page 42 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-6(5-7) Client Matrix:% Moisture:8.1 460-145401-3 Solid Date Sampled: 11/17/2017 1215 Date Received: 11/17/2017 2040 8270D Semivolatile Organic Compounds (GC/MS) Dilution: 11/19/2017 0938 11/20/2017 0336 1.0 8270D Injection Volume: Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: L205281.D 15.0418 g 1 mL 1 uL 3546 CBNAMS12 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-478510 460-478451 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.036 U 0.0360.012N-Nitrosodi-n-propylamine 0.36 U 0.360.033N-Nitrosodiphenylamine 0.36 U 0.360.0095Phenanthrene 0.36 U 0.360.016Pyrene Surrogate %Rec Acceptance LimitsQualifier 60 38 - 952-Fluorobiphenyl 54 37 - 94Nitrobenzene-d5 (Surr) 90 24 - 109Terphenyl-d14 (Surr) TestAmerica Edison Page 43 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-3(0-2) Client Matrix:% Moisture:8.3 460-145401-4 Solid Date Sampled: 11/17/2017 1250 Date Received: 11/17/2017 2040 8270D Semivolatile Organic Compounds (GC/MS) Dilution: 11/19/2017 0938 11/20/2017 0358 1.0 8270D Injection Volume: Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: L205282.D 15.0419 g 1 mL 1 uL 3546 CBNAMS12 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-478510 460-478451 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.036 U 0.0360.00791,2,4-Trichlorobenzene 0.36 U 0.360.0121,2-Dichlorobenzene 0.36 U 0.360.0281,3-Dichlorobenzene 0.36 U 0.360.0281,4-Dichlorobenzene 0.36 U 0.360.0152,2'-oxybis[1-chloropropane] 0.073 U 0.0730.0142,4-Dinitrotoluene 0.073 U 0.0730.0192,6-Dinitrotoluene 0.36 U 0.360.00822-Chloronaphthalene 0.36 U 0.360.00792-Methylnaphthalene 0.36 U 0.360.0122-Nitroaniline 0.14 U 0.140.0403,3'-Dichlorobenzidine 0.36 U 0.360.0113-Nitroaniline 0.36 U 0.360.0114-Bromophenyl phenyl ether 0.36 U 0.360.00924-Chloroaniline 0.36 U 0.360.0114-Chlorophenyl phenyl ether 0.36 U 0.360.0144-Nitroaniline 0.36 U 0.360.0087Acenaphthene 0.36 U 0.360.0092Acenaphthylene 0.36 U 0.360.034Anthracene 0.036 U 0.0360.030Benzo[a]anthracene 0.036 U 0.0360.011Benzo[a]pyrene 0.036 U 0.0360.014Benzo[b]fluoranthene 0.36 U 0.360.021Benzo[g,h,i]perylene 0.036 U 0.0360.016Benzo[k]fluoranthene 0.36 U 0.360.011Bis(2-chloroethoxy)methane 0.036 U 0.0360.0085Bis(2-chloroethyl)ether 0.36 U 0.360.014Bis(2-ethylhexyl) phthalate 0.36 U 0.360.011Butyl benzyl phthalate 0.36 U 0.360.0089Carbazole 0.36 U 0.360.0098Chrysene 0.036 U 0.0360.019Dibenz(a,h)anthracene 0.36 U 0.360.011Dibenzofuran 0.36 U 0.360.010Diethyl phthalate 0.36 U 0.360.010Dimethyl phthalate 0.36 U 0.360.011Di-n-butyl phthalate 0.36 U 0.360.018Di-n-octyl phthalate 0.36 U 0.360.011Fluoranthene 0.36 U 0.360.0078Fluorene 0.036 U 0.0360.015Hexachlorobenzene 0.073 U 0.0730.010Hexachlorobutadiene 0.36 U 0.360.022Hexachlorocyclopentadiene 0.036 U 0.0360.013Hexachloroethane 0.036 U 0.0360.024Indeno[1,2,3-cd]pyrene 0.14 U 0.140.0077Isophorone 0.36 U 0.360.0091Naphthalene 0.036 U 0.0360.011Nitrobenzene TestAmerica Edison Page 44 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-3(0-2) Client Matrix:% Moisture:8.3 460-145401-4 Solid Date Sampled: 11/17/2017 1250 Date Received: 11/17/2017 2040 8270D Semivolatile Organic Compounds (GC/MS) Dilution: 11/19/2017 0938 11/20/2017 0358 1.0 8270D Injection Volume: Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: L205282.D 15.0419 g 1 mL 1 uL 3546 CBNAMS12 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-478510 460-478451 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.036 U 0.0360.012N-Nitrosodi-n-propylamine 0.36 U 0.360.033N-Nitrosodiphenylamine 0.36 U 0.360.0096Phenanthrene 0.36 U 0.360.016Pyrene Surrogate %Rec Acceptance LimitsQualifier 55 38 - 952-Fluorobiphenyl 50 37 - 94Nitrobenzene-d5 (Surr) 77 24 - 109Terphenyl-d14 (Surr) TestAmerica Edison Page 45 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-5(0-2) Client Matrix:% Moisture:10.5 460-145401-5 Solid Date Sampled: 11/17/2017 1330 Date Received: 11/17/2017 2040 8270D Semivolatile Organic Compounds (GC/MS) Dilution: 11/19/2017 0938 11/20/2017 0421 1.0 8270D Injection Volume: Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: L205283.D 15.0326 g 1 mL 1 uL 3546 CBNAMS12 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-478510 460-478451 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.037 U 0.0370.00811,2,4-Trichlorobenzene 0.37 U 0.370.0121,2-Dichlorobenzene 0.37 U 0.370.0291,3-Dichlorobenzene 0.37 U 0.370.0291,4-Dichlorobenzene 0.37 U 0.370.0152,2'-oxybis[1-chloropropane] 0.075 U 0.0750.0152,4-Dinitrotoluene 0.075 U 0.0750.0202,6-Dinitrotoluene 0.37 U 0.370.00842-Chloronaphthalene 0.37 U 0.370.00812-Methylnaphthalene 0.37 U 0.370.0122-Nitroaniline 0.15 U 0.150.0413,3'-Dichlorobenzidine 0.37 U 0.370.0113-Nitroaniline 0.37 U 0.370.0124-Bromophenyl phenyl ether 0.37 U 0.370.00954-Chloroaniline 0.37 U 0.370.0114-Chlorophenyl phenyl ether 0.37 U 0.370.0144-Nitroaniline 0.37 U 0.370.0089Acenaphthene 0.37 U 0.370.0095Acenaphthylene 0.37 U 0.370.035Anthracene 0.037 U 0.0370.031Benzo[a]anthracene 0.037 U 0.0370.011Benzo[a]pyrene 0.037 U 0.0370.014Benzo[b]fluoranthene 0.37 U 0.370.021Benzo[g,h,i]perylene 0.037 U 0.0370.016Benzo[k]fluoranthene 0.37 U 0.370.011Bis(2-chloroethoxy)methane 0.037 U 0.0370.0087Bis(2-chloroethyl)ether 0.37 U 0.370.014Bis(2-ethylhexyl) phthalate 0.37 U 0.370.011Butyl benzyl phthalate 0.37 U 0.370.0091Carbazole 0.37 U 0.370.010Chrysene 0.037 U 0.0370.019Dibenz(a,h)anthracene 0.37 U 0.370.011Dibenzofuran 0.37 U 0.370.010Diethyl phthalate 0.37 U 0.370.011Dimethyl phthalate 0.37 U 0.370.011Di-n-butyl phthalate 0.37 U 0.370.019Di-n-octyl phthalate 0.37 U 0.370.011Fluoranthene 0.37 U 0.370.0080Fluorene 0.037 U 0.0370.015Hexachlorobenzene 0.075 U 0.0750.010Hexachlorobutadiene 0.37 U 0.370.023Hexachlorocyclopentadiene 0.037 U 0.0370.013Hexachloroethane 0.037 U 0.0370.025Indeno[1,2,3-cd]pyrene 0.15 U 0.150.0079Isophorone 0.37 U 0.370.0094Naphthalene 0.037 U 0.0370.012Nitrobenzene TestAmerica Edison Page 46 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-5(0-2) Client Matrix:% Moisture:10.5 460-145401-5 Solid Date Sampled: 11/17/2017 1330 Date Received: 11/17/2017 2040 8270D Semivolatile Organic Compounds (GC/MS) Dilution: 11/19/2017 0938 11/20/2017 0421 1.0 8270D Injection Volume: Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: L205283.D 15.0326 g 1 mL 1 uL 3546 CBNAMS12 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-478510 460-478451 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.037 U 0.0370.012N-Nitrosodi-n-propylamine 0.37 U 0.370.033N-Nitrosodiphenylamine 0.37 U 0.370.0098Phenanthrene 0.37 U 0.370.017Pyrene Surrogate %Rec Acceptance LimitsQualifier 52 38 - 952-Fluorobiphenyl 47 37 - 94Nitrobenzene-d5 (Surr) 83 24 - 109Terphenyl-d14 (Surr) TestAmerica Edison Page 47 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-4(0-2) Client Matrix:% Moisture:8.8 460-145401-6 Solid Date Sampled: 11/17/2017 1415 Date Received: 11/17/2017 2040 8270D Semivolatile Organic Compounds (GC/MS) Dilution: 11/19/2017 0938 11/20/2017 0443 1.0 8270D Injection Volume: Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: L205284.D 15.0418 g 1 mL 1 uL 3546 CBNAMS12 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-478510 460-478451 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.036 U 0.0360.00801,2,4-Trichlorobenzene 0.36 U 0.360.0121,2-Dichlorobenzene 0.36 U 0.360.0281,3-Dichlorobenzene 0.36 U 0.360.0281,4-Dichlorobenzene 0.36 U 0.360.0152,2'-oxybis[1-chloropropane] 0.073 U 0.0730.0142,4-Dinitrotoluene 0.073 U 0.0730.0192,6-Dinitrotoluene 0.36 U 0.360.00822-Chloronaphthalene 0.36 U 0.360.00802-Methylnaphthalene 0.36 U 0.360.0122-Nitroaniline 0.15 U 0.150.0403,3'-Dichlorobenzidine 0.36 U 0.360.0113-Nitroaniline 0.36 U 0.360.0114-Bromophenyl phenyl ether 0.36 U 0.360.00934-Chloroaniline 0.36 U 0.360.0114-Chlorophenyl phenyl ether 0.36 U 0.360.0144-Nitroaniline 0.36 U 0.360.0087Acenaphthene 0.36 U 0.360.0093Acenaphthylene 0.36 U 0.360.034Anthracene 0.036 U 0.0360.030Benzo[a]anthracene 0.036 U 0.0360.011Benzo[a]pyrene 0.036 U 0.0360.014Benzo[b]fluoranthene 0.36 U 0.360.021Benzo[g,h,i]perylene 0.036 U 0.0360.016Benzo[k]fluoranthene 0.36 U 0.360.011Bis(2-chloroethoxy)methane 0.036 U 0.0360.0085Bis(2-chloroethyl)ether 0.36 U 0.360.014Bis(2-ethylhexyl) phthalate 0.36 U 0.360.011Butyl benzyl phthalate 0.36 U 0.360.0090Carbazole 0.36 U 0.360.0098Chrysene 0.036 U 0.0360.019Dibenz(a,h)anthracene 0.36 U 0.360.011Dibenzofuran 0.36 U 0.360.010Diethyl phthalate 0.36 U 0.360.010Dimethyl phthalate 0.36 U 0.360.011Di-n-butyl phthalate 0.36 U 0.360.018Di-n-octyl phthalate 0.36 U 0.360.011Fluoranthene 0.36 U 0.360.0079Fluorene 0.036 U 0.0360.015Hexachlorobenzene 0.073 U 0.0730.010Hexachlorobutadiene 0.36 U 0.360.023Hexachlorocyclopentadiene 0.036 U 0.0360.013Hexachloroethane 0.036 U 0.0360.024Indeno[1,2,3-cd]pyrene 0.15 U 0.150.0078Isophorone 0.36 U 0.360.0092Naphthalene 0.036 U 0.0360.011Nitrobenzene TestAmerica Edison Page 48 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-4(0-2) Client Matrix:% Moisture:8.8 460-145401-6 Solid Date Sampled: 11/17/2017 1415 Date Received: 11/17/2017 2040 8270D Semivolatile Organic Compounds (GC/MS) Dilution: 11/19/2017 0938 11/20/2017 0443 1.0 8270D Injection Volume: Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: L205284.D 15.0418 g 1 mL 1 uL 3546 CBNAMS12 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-478510 460-478451 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.036 U 0.0360.012N-Nitrosodi-n-propylamine 0.36 U 0.360.033N-Nitrosodiphenylamine 0.36 U 0.360.0096Phenanthrene 0.36 U 0.360.016Pyrene Surrogate %Rec Acceptance LimitsQualifier 59 38 - 952-Fluorobiphenyl 54 37 - 94Nitrobenzene-d5 (Surr) 83 24 - 109Terphenyl-d14 (Surr) TestAmerica Edison Page 49 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-2 (0-2) Client Matrix:% Moisture:8.3 460-145515-1 Solid Date Sampled: 11/20/2017 0800 Date Received: 11/20/2017 1950 8270D Semivolatile Organic Compounds (GC/MS) Dilution: 11/22/2017 0851 11/27/2017 1558 1.0 8270D Injection Volume: Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: f38764.D 15.0167 g 1 mL 1 uL 3546 CBNAMS15 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-480050 460-479261 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.036 U 0.0360.00801,2,4-Trichlorobenzene 0.36 U 0.360.0121,2-Dichlorobenzene 0.36 U 0.360.0281,3-Dichlorobenzene 0.36 U 0.360.0281,4-Dichlorobenzene 0.36 U 0.360.0152,2'-oxybis[1-chloropropane] 0.073 U 0.0730.0142,4-Dinitrotoluene 0.073 U 0.0730.0192,6-Dinitrotoluene 0.36 U 0.360.00822-Chloronaphthalene 0.36 U 0.360.00802-Methylnaphthalene 0.36 U 0.360.0122-Nitroaniline 0.14 U 0.140.0403,3'-Dichlorobenzidine 0.36 U 0.360.0113-Nitroaniline 0.36 U 0.360.0114-Bromophenyl phenyl ether 0.36 U 0.360.00934-Chloroaniline 0.36 U 0.360.0114-Chlorophenyl phenyl ether 0.36 U 0.360.0144-Nitroaniline 0.36 U 0.360.0087Acenaphthene 0.36 U 0.360.0093Acenaphthylene 0.36 U 0.360.034Anthracene 0.036 U 0.0360.030Benzo[a]anthracene 0.036 U 0.0360.011Benzo[a]pyrene 0.036 U 0.0360.014Benzo[b]fluoranthene 0.36 U 0.360.021Benzo[g,h,i]perylene 0.036 U 0.0360.016Benzo[k]fluoranthene 0.36 U 0.360.011Bis(2-chloroethoxy)methane 0.036 U 0.0360.0085Bis(2-chloroethyl)ether 0.36 U 0.360.014Bis(2-ethylhexyl) phthalate 0.36 U 0.360.011Butyl benzyl phthalate 0.36 U 0.360.0089Carbazole 0.36 U 0.360.0098Chrysene 0.036 U 0.0360.019Dibenz(a,h)anthracene 0.36 U 0.360.011Dibenzofuran 0.36 U 0.360.010Diethyl phthalate 0.36 U 0.360.010Dimethyl phthalate 0.36 U 0.360.011Di-n-butyl phthalate 0.36 U 0.360.018Di-n-octyl phthalate 0.36 U 0.360.011Fluoranthene 0.36 U 0.360.0078Fluorene 0.036 U 0.0360.015Hexachlorobenzene 0.073 U 0.0730.010Hexachlorobutadiene 0.36 U 0.360.022Hexachlorocyclopentadiene 0.036 U 0.0360.013Hexachloroethane 0.036 U 0.0360.024Indeno[1,2,3-cd]pyrene 0.14 U 0.140.0077Isophorone 0.36 U 0.360.0091Naphthalene 0.036 U 0.0360.011Nitrobenzene TestAmerica Edison Page 50 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-2 (0-2) Client Matrix:% Moisture:8.3 460-145515-1 Solid Date Sampled: 11/20/2017 0800 Date Received: 11/20/2017 1950 8270D Semivolatile Organic Compounds (GC/MS) Dilution: 11/22/2017 0851 11/27/2017 1558 1.0 8270D Injection Volume: Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: f38764.D 15.0167 g 1 mL 1 uL 3546 CBNAMS15 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-480050 460-479261 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.036 U 0.0360.012N-Nitrosodi-n-propylamine 0.36 U 0.360.033N-Nitrosodiphenylamine 0.36 U 0.360.0096Phenanthrene 0.36 U 0.360.016Pyrene Surrogate %Rec Acceptance LimitsQualifier 78 38 - 952-Fluorobiphenyl 69 37 - 94Nitrobenzene-d5 (Surr) 80 24 - 109Terphenyl-d14 (Surr) TestAmerica Edison Page 51 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-1 (0-2) Client Matrix:% Moisture:9.9 460-145515-2 Solid Date Sampled: 11/20/2017 0820 Date Received: 11/20/2017 1950 8270D Semivolatile Organic Compounds (GC/MS) Dilution: 11/22/2017 0851 11/27/2017 1620 1.0 8270D Injection Volume: Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: f38765.D 15.0350 g 1 mL 1 uL 3546 CBNAMS15 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-480050 460-479261 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.037 U 0.0370.00811,2,4-Trichlorobenzene 0.37 U 0.370.0121,2-Dichlorobenzene 0.37 U 0.370.0281,3-Dichlorobenzene 0.37 U 0.370.0291,4-Dichlorobenzene 0.37 U 0.370.0152,2'-oxybis[1-chloropropane] 0.074 U 0.0740.0152,4-Dinitrotoluene 0.074 U 0.0740.0192,6-Dinitrotoluene 0.37 U 0.370.00832-Chloronaphthalene 0.37 U 0.370.00812-Methylnaphthalene 0.37 U 0.370.0122-Nitroaniline 0.15 U 0.150.0413,3'-Dichlorobenzidine 0.37 U 0.370.0113-Nitroaniline 0.37 U 0.370.0124-Bromophenyl phenyl ether 0.37 U 0.370.00944-Chloroaniline 0.37 U 0.370.0114-Chlorophenyl phenyl ether 0.37 U 0.370.0144-Nitroaniline 0.37 U 0.370.0089Acenaphthene 0.37 U 0.370.0094Acenaphthylene 0.37 U 0.370.035Anthracene 0.037 U 0.0370.031Benzo[a]anthracene 0.037 U 0.0370.011Benzo[a]pyrene 0.037 U 0.0370.014Benzo[b]fluoranthene 0.37 U 0.370.021Benzo[g,h,i]perylene 0.037 U 0.0370.016Benzo[k]fluoranthene 0.37 U 0.370.011Bis(2-chloroethoxy)methane 0.037 U 0.0370.0086Bis(2-chloroethyl)ether 0.37 U 0.370.014Bis(2-ethylhexyl) phthalate 0.37 U 0.370.011Butyl benzyl phthalate 0.37 U 0.370.0091Carbazole 0.37 U 0.370.010Chrysene 0.037 U 0.0370.019Dibenz(a,h)anthracene 0.37 U 0.370.011Dibenzofuran 0.37 U 0.370.010Diethyl phthalate 0.37 U 0.370.011Dimethyl phthalate 0.37 U 0.370.011Di-n-butyl phthalate 0.37 U 0.370.019Di-n-octyl phthalate 0.37 U 0.370.011Fluoranthene 0.37 U 0.370.0080Fluorene 0.037 U 0.0370.015Hexachlorobenzene 0.074 U 0.0740.010Hexachlorobutadiene 0.37 U 0.370.023Hexachlorocyclopentadiene 0.037 U 0.0370.013Hexachloroethane 0.037 U 0.0370.024Indeno[1,2,3-cd]pyrene 0.15 U 0.150.0079Isophorone 0.37 U 0.370.0093Naphthalene 0.037 U 0.0370.012Nitrobenzene TestAmerica Edison Page 52 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-1 (0-2) Client Matrix:% Moisture:9.9 460-145515-2 Solid Date Sampled: 11/20/2017 0820 Date Received: 11/20/2017 1950 8270D Semivolatile Organic Compounds (GC/MS) Dilution: 11/22/2017 0851 11/27/2017 1620 1.0 8270D Injection Volume: Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: f38765.D 15.0350 g 1 mL 1 uL 3546 CBNAMS15 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-480050 460-479261 Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.037 U 0.0370.012N-Nitrosodi-n-propylamine 0.37 U 0.370.033N-Nitrosodiphenylamine 0.37 U 0.370.0097Phenanthrene 0.37 U 0.370.017Pyrene Surrogate %Rec Acceptance LimitsQualifier 68 38 - 952-Fluorobiphenyl 60 37 - 94Nitrobenzene-d5 (Surr) 72 24 - 109Terphenyl-d14 (Surr) TestAmerica Edison Page 53 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: OW-2 Client Matrix: 460-145597-1 Water Date Sampled: 11/21/2017 1105 Date Received: 11/21/2017 1825 8270D Semivolatile Organic Compounds (GC/MS) Dilution: 11/22/2017 1439 11/24/2017 1251 1.0 8270D Injection Volume: Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: A111391.D 245 mL 2 mL 5 uL 3510C CBNAMS16 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479531 460-479363 Analysis Method: Prep Method: Analyte Result (ug/L)Qualifier MDL RL 1.0 U 1.00.621,2,4-Trichlorobenzene 10 U 100.851,2-Dichlorobenzene 10 U 101.11,3-Dichlorobenzene 10 U 100.671,4-Dichlorobenzene 10 U 100.952,2'-oxybis[1-chloropropane] 2.0 U 2.01.12,4-Dinitrotoluene 2.0 U 2.00.902,6-Dinitrotoluene 10 U 100.622-Chloronaphthalene 10 U 100.902-Methylnaphthalene 10 U 100.662-Nitroaniline 10 U 101.13,3'-Dichlorobenzidine 10 U 100.843-Nitroaniline 10 U 101.04-Bromophenyl phenyl ether 10 U 100.744-Chloroaniline 10 U 100.984-Chlorophenyl phenyl ether 10 U 100.494-Nitroaniline 10 U 100.90Acenaphthene 10 U 100.66Acenaphthylene 10 U 100.58Anthracene 1.0 U 1.00.56Benzo[a]anthracene 1.0 U 1.00.16Benzo[a]pyrene 1.0 U 1.00.45Benzo[b]fluoranthene 10 U 100.77Benzo[g,h,i]perylene 1.0 U 1.00.18Benzo[k]fluoranthene 10 U 100.70Bis(2-chloroethoxy)methane 1.0 U 1.00.12Bis(2-chloroethyl)ether 2.0 U 2.00.73Bis(2-ethylhexyl) phthalate 10 U 100.61Butyl benzyl phthalate 10 U 100.87Carbazole 2.0 U 2.00.68Chrysene 1.0 U 1.00.092Dibenz(a,h)anthracene 10 U 100.87Dibenzofuran 10 U 101.0Diethyl phthalate 10 U 101.0Dimethyl phthalate 10 U 100.84Di-n-butyl phthalate 10 U 100.70Di-n-octyl phthalate 10 U *100.73Fluoranthene 10 U 100.82Fluorene 1.0 U 1.00.48Hexachlorobenzene 1.0 U 1.00.78Hexachlorobutadiene 10 U 100.62Hexachlorocyclopentadiene 1.0 U 1.00.092Hexachloroethane 1.0 U 1.00.21Indeno[1,2,3-cd]pyrene 10 U 100.68Isophorone 10 U 100.82Naphthalene 1.0 U 1.00.50Nitrobenzene TestAmerica Edison Page 54 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: OW-2 Client Matrix: 460-145597-1 Water Date Sampled: 11/21/2017 1105 Date Received: 11/21/2017 1825 8270D Semivolatile Organic Compounds (GC/MS) Dilution: 11/22/2017 1439 11/24/2017 1251 1.0 8270D Injection Volume: Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: A111391.D 245 mL 2 mL 5 uL 3510C CBNAMS16 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479531 460-479363 Analysis Method: Prep Method: Analyte Result (ug/L)Qualifier MDL RL 1.0 U 1.00.85N-Nitrosodi-n-propylamine 10 U 100.76N-Nitrosodiphenylamine 10 U 100.66Phenanthrene 10 U 100.85Pyrene Surrogate %Rec Acceptance LimitsQualifier 74 45 - 1072-Fluorobiphenyl 85 51 - 108Nitrobenzene-d5 (Surr) 79 40 - 148Terphenyl-d14 (Surr) TestAmerica Edison Page 55 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: OW-1 Client Matrix: 460-145597-2 Water Date Sampled: 11/21/2017 1220 Date Received: 11/21/2017 1825 8270D Semivolatile Organic Compounds (GC/MS) Dilution: 11/22/2017 1439 11/24/2017 1311 1.0 8270D Injection Volume: Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: A111392.D 246 mL 2 mL 5 uL 3510C CBNAMS16 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479531 460-479363 Analysis Method: Prep Method: Analyte Result (ug/L)Qualifier MDL RL 1.0 U 1.00.621,2,4-Trichlorobenzene 10 U 100.841,2-Dichlorobenzene 10 U 101.11,3-Dichlorobenzene 10 U 100.671,4-Dichlorobenzene 10 U 100.952,2'-oxybis[1-chloropropane] 2.0 U 2.01.12,4-Dinitrotoluene 2.0 U 2.00.892,6-Dinitrotoluene 10 U 100.622-Chloronaphthalene 10 U 100.892-Methylnaphthalene 10 U 100.662-Nitroaniline 10 U 101.13,3'-Dichlorobenzidine 10 U 100.833-Nitroaniline 10 U 101.04-Bromophenyl phenyl ether 10 U 100.744-Chloroaniline 10 U 100.984-Chlorophenyl phenyl ether 10 U 100.494-Nitroaniline 10 U 100.89Acenaphthene 10 U 100.66Acenaphthylene 10 U 100.58Anthracene 1.0 U 1.00.56Benzo[a]anthracene 1.0 U 1.00.16Benzo[a]pyrene 1.0 U 1.00.45Benzo[b]fluoranthene 10 U 100.76Benzo[g,h,i]perylene 1.0 U 1.00.18Benzo[k]fluoranthene 10 U 100.70Bis(2-chloroethoxy)methane 1.0 U 1.00.12Bis(2-chloroethyl)ether 2.0 U 2.00.73Bis(2-ethylhexyl) phthalate 10 U 100.61Butyl benzyl phthalate 10 U 100.86Carbazole 2.0 U 2.00.68Chrysene 1.0 U 1.00.091Dibenz(a,h)anthracene 10 U 100.86Dibenzofuran 10 U 101.0Diethyl phthalate 10 U 101.0Dimethyl phthalate 10 U 100.83Di-n-butyl phthalate 10 U 100.70Di-n-octyl phthalate 10 U *100.73Fluoranthene 10 U 100.81Fluorene 1.0 U 1.00.48Hexachlorobenzene 1.0 U 1.00.77Hexachlorobutadiene 10 U 100.62Hexachlorocyclopentadiene 1.0 U 1.00.091Hexachloroethane 1.0 U 1.00.21Indeno[1,2,3-cd]pyrene 10 U 100.68Isophorone 10 U 100.81Naphthalene 1.0 U 1.00.50Nitrobenzene TestAmerica Edison Page 56 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: OW-1 Client Matrix: 460-145597-2 Water Date Sampled: 11/21/2017 1220 Date Received: 11/21/2017 1825 8270D Semivolatile Organic Compounds (GC/MS) Dilution: 11/22/2017 1439 11/24/2017 1311 1.0 8270D Injection Volume: Final Weight/Volume: Initial Weight/Volume: Lab File ID: Instrument ID: A111392.D 246 mL 2 mL 5 uL 3510C CBNAMS16 Analysis Date: Prep Date: Analysis Batch: Prep Batch: 460-479531 460-479363 Analysis Method: Prep Method: Analyte Result (ug/L)Qualifier MDL RL 1.0 U 1.00.84N-Nitrosodi-n-propylamine 10 U 100.75N-Nitrosodiphenylamine 10 U 100.66Phenanthrene 10 U 100.84Pyrene Surrogate %Rec Acceptance LimitsQualifier 76 45 - 1072-Fluorobiphenyl 81 51 - 108Nitrobenzene-d5 (Surr) 79 40 - 148Terphenyl-d14 (Surr) TestAmerica Edison Page 57 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-8(1-2.5) Client Matrix:% Moisture:10.6 460-145401-1 Solid Date Sampled: 11/17/2017 0945 Date Received: 11/17/2017 2040 8081B Organochlorine Pesticides (GC) Dilution: 8081B 3546 1.0 11/21/2017 2206 11/21/2017 0040 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:PRIMARY +15.0017 g 10 mL 1 uL CPESTGC4 Analysis Date: Prep Date: Analysis Batch: 460-479079 460-478818Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.0075 U 0.00750.00134,4'-DDD 0.0075 U 0.00750.000884,4'-DDE 0.0075 U 0.00750.00144,4'-DDT 0.0075 U 0.00750.0011Aldrin 0.0022 U 0.00220.00076alpha-BHC 0.0022 U 0.00220.00084beta-BHC 0.075 U 0.0750.018Chlordane (technical) 0.0022 U 0.00220.00046delta-BHC 0.0022 U 0.00220.00097Dieldrin 0.0075 U 0.00750.0011Endosulfan I 0.0075 U 0.00750.0019Endosulfan II 0.0075 U 0.00750.00094Endosulfan sulfate 0.0075 U 0.00750.0011Endrin 0.0075 U 0.00750.0018Endrin aldehyde 0.0075 U 0.00750.0015Endrin ketone 0.0022 U 0.00220.00069gamma-BHC (Lindane) 0.0075 U 0.00750.00088Heptachlor 0.0075 U 0.00750.0011Heptachlor epoxide 0.0075 U 0.00750.0017Methoxychlor 0.075 U 0.0750.027Toxaphene Surrogate %Rec Acceptance LimitsQualifier 119 50 - 150DCB Decachlorobiphenyl 123 47 - 150Tetrachloro-m-xylene TestAmerica Edison Page 58 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-8(1-2.5) Client Matrix:% Moisture:10.6 460-145401-1 Solid Date Sampled: 11/17/2017 0945 Date Received: 11/17/2017 2040 8081B Organochlorine Pesticides (GC) Dilution: 8081B 3546 1.0 11/21/2017 2206 11/21/2017 0040 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:SECONDARY +15.0017 g 10 mL 1 uL CPESTGC4 Analysis Date: Prep Date: Analysis Batch: 460-479079 460-478818Prep Batch: Analysis Method: Prep Method: Surrogate %Rec Acceptance LimitsQualifier 112 50 - 150DCB Decachlorobiphenyl 118 47 - 150Tetrachloro-m-xylene TestAmerica Edison Page 59 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-7(5-7) Client Matrix:% Moisture:6.8 460-145401-2 Solid Date Sampled: 11/17/2017 1050 Date Received: 11/17/2017 2040 8081B Organochlorine Pesticides (GC) Dilution: 8081B 3546 1.0 11/21/2017 2219 11/21/2017 0040 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:PRIMARY +15.0090 g 10 mL 1 uL CPESTGC4 Analysis Date: Prep Date: Analysis Batch: 460-479079 460-478818Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.0072 U 0.00720.00124,4'-DDD 0.0072 U 0.00720.000854,4'-DDE 0.0072 U 0.00720.00134,4'-DDT 0.0072 U 0.00720.0011Aldrin 0.0021 U 0.00210.00073alpha-BHC 0.0021 U 0.00210.00080beta-BHC 0.072 U 0.0720.017Chlordane (technical) 0.0021 U 0.00210.00044delta-BHC 0.0021 U 0.00210.00093Dieldrin 0.0072 U 0.00720.0011Endosulfan I 0.0072 U 0.00720.0018Endosulfan II 0.0072 U 0.00720.00090Endosulfan sulfate 0.0072 U 0.00720.0010Endrin 0.0072 U 0.00720.0017Endrin aldehyde 0.0072 U 0.00720.0014Endrin ketone 0.0021 U 0.00210.00066gamma-BHC (Lindane) 0.0072 U 0.00720.00085Heptachlor 0.0072 U 0.00720.0011Heptachlor epoxide 0.0072 U 0.00720.0016Methoxychlor 0.072 U 0.0720.026Toxaphene Surrogate %Rec Acceptance LimitsQualifier 113 50 - 150DCB Decachlorobiphenyl 117 47 - 150Tetrachloro-m-xylene TestAmerica Edison Page 60 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-7(5-7) Client Matrix:% Moisture:6.8 460-145401-2 Solid Date Sampled: 11/17/2017 1050 Date Received: 11/17/2017 2040 8081B Organochlorine Pesticides (GC) Dilution: 8081B 3546 1.0 11/21/2017 2219 11/21/2017 0040 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:SECONDARY +15.0090 g 10 mL 1 uL CPESTGC4 Analysis Date: Prep Date: Analysis Batch: 460-479079 460-478818Prep Batch: Analysis Method: Prep Method: Surrogate %Rec Acceptance LimitsQualifier 111 50 - 150DCB Decachlorobiphenyl 114 47 - 150Tetrachloro-m-xylene TestAmerica Edison Page 61 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-6(5-7) Client Matrix:% Moisture:8.1 460-145401-3 Solid Date Sampled: 11/17/2017 1215 Date Received: 11/17/2017 2040 8081B Organochlorine Pesticides (GC) Dilution: 8081B 3546 1.0 11/21/2017 2230 11/21/2017 0040 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:PRIMARY +15.0035 g 10 mL 1 uL CPESTGC4 Analysis Date: Prep Date: Analysis Batch: 460-479079 460-478818Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.0073 U 0.00730.00124,4'-DDD 0.0073 U 0.00730.000864,4'-DDE 0.0073 U 0.00730.00134,4'-DDT 0.0073 U 0.00730.0011Aldrin 0.0022 U 0.00220.00074alpha-BHC 0.0022 U 0.00220.00082beta-BHC 0.073 U 0.0730.018Chlordane (technical) 0.0022 U 0.00220.00045delta-BHC 0.0022 U 0.00220.00095Dieldrin 0.0073 U 0.00730.0011Endosulfan I 0.0073 U 0.00730.0019Endosulfan II 0.0073 U 0.00730.00091Endosulfan sulfate 0.0073 U 0.00730.0010Endrin 0.0073 U 0.00730.0017Endrin aldehyde 0.0073 U 0.00730.0014Endrin ketone 0.0022 U 0.00220.00067gamma-BHC (Lindane) 0.0073 U 0.00730.00086Heptachlor 0.0073 U 0.00730.0011Heptachlor epoxide 0.0073 U 0.00730.0017Methoxychlor 0.073 U 0.0730.026Toxaphene Surrogate %Rec Acceptance LimitsQualifier 99 50 - 150DCB Decachlorobiphenyl 102 47 - 150Tetrachloro-m-xylene TestAmerica Edison Page 62 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-6(5-7) Client Matrix:% Moisture:8.1 460-145401-3 Solid Date Sampled: 11/17/2017 1215 Date Received: 11/17/2017 2040 8081B Organochlorine Pesticides (GC) Dilution: 8081B 3546 1.0 11/21/2017 2230 11/21/2017 0040 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:SECONDARY +15.0035 g 10 mL 1 uL CPESTGC4 Analysis Date: Prep Date: Analysis Batch: 460-479079 460-478818Prep Batch: Analysis Method: Prep Method: Surrogate %Rec Acceptance LimitsQualifier 99 50 - 150DCB Decachlorobiphenyl 102 47 - 150Tetrachloro-m-xylene TestAmerica Edison Page 63 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-3(0-2) Client Matrix:% Moisture:8.3 460-145401-4 Solid Date Sampled: 11/17/2017 1250 Date Received: 11/17/2017 2040 8081B Organochlorine Pesticides (GC) Dilution: 8081B 3546 1.0 11/21/2017 2242 11/21/2017 0040 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:PRIMARY +15.0113 g 10 mL 1 uL CPESTGC4 Analysis Date: Prep Date: Analysis Batch: 460-479079 460-478818Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.0073 U 0.00730.00124,4'-DDD 0.0073 U 0.00730.000864,4'-DDE 0.0073 U 0.00730.00134,4'-DDT 0.0073 U 0.00730.0011Aldrin 0.0022 U 0.00220.00074alpha-BHC 0.0022 U 0.00220.00082beta-BHC 0.073 U 0.0730.018Chlordane (technical) 0.0022 U 0.00220.00045delta-BHC 0.0022 U 0.00220.00095Dieldrin 0.0073 U 0.00730.0011Endosulfan I 0.0073 U 0.00730.0019Endosulfan II 0.0073 U 0.00730.00091Endosulfan sulfate 0.0073 U 0.00730.0010Endrin 0.0073 U 0.00730.0017Endrin aldehyde 0.0073 U 0.00730.0014Endrin ketone 0.0022 U 0.00220.00068gamma-BHC (Lindane) 0.0073 U 0.00730.00086Heptachlor 0.0073 U 0.00730.0011Heptachlor epoxide 0.0073 U 0.00730.0017Methoxychlor 0.073 U 0.0730.026Toxaphene Surrogate %Rec Acceptance LimitsQualifier 117 50 - 150DCB Decachlorobiphenyl 116 47 - 150Tetrachloro-m-xylene TestAmerica Edison Page 64 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-3(0-2) Client Matrix:% Moisture:8.3 460-145401-4 Solid Date Sampled: 11/17/2017 1250 Date Received: 11/17/2017 2040 8081B Organochlorine Pesticides (GC) Dilution: 8081B 3546 1.0 11/21/2017 2242 11/21/2017 0040 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:SECONDARY +15.0113 g 10 mL 1 uL CPESTGC4 Analysis Date: Prep Date: Analysis Batch: 460-479079 460-478818Prep Batch: Analysis Method: Prep Method: Surrogate %Rec Acceptance LimitsQualifier 116 50 - 150DCB Decachlorobiphenyl 115 47 - 150Tetrachloro-m-xylene TestAmerica Edison Page 65 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-5(0-2) Client Matrix:% Moisture:10.5 460-145401-5 Solid Date Sampled: 11/17/2017 1330 Date Received: 11/17/2017 2040 8081B Organochlorine Pesticides (GC) Dilution: 8081B 3546 1.0 11/21/2017 2253 11/21/2017 0040 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:PRIMARY +15.0005 g 10 mL 1 uL CPESTGC4 Analysis Date: Prep Date: Analysis Batch: 460-479079 460-478818Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.0075 U 0.00750.00134,4'-DDD 0.0075 U 0.00750.000884,4'-DDE 0.0075 U 0.00750.00144,4'-DDT 0.0075 U 0.00750.0011Aldrin 0.0022 U 0.00220.00076alpha-BHC 0.0022 U 0.00220.00084beta-BHC 0.075 U 0.0750.018Chlordane (technical) 0.0022 U 0.00220.00046delta-BHC 0.0022 U 0.00220.00097Dieldrin 0.0075 U 0.00750.0011Endosulfan I 0.0075 U 0.00750.0019Endosulfan II 0.0075 U 0.00750.00094Endosulfan sulfate 0.0075 U 0.00750.0011Endrin 0.0075 U 0.00750.0018Endrin aldehyde 0.0075 U 0.00750.0015Endrin ketone 0.0022 U 0.00220.00069gamma-BHC (Lindane) 0.0075 U 0.00750.00088Heptachlor 0.0075 U 0.00750.0011Heptachlor epoxide 0.0075 U 0.00750.0017Methoxychlor 0.075 U 0.0750.027Toxaphene Surrogate %Rec Acceptance LimitsQualifier 127 50 - 150DCB Decachlorobiphenyl 127 47 - 150Tetrachloro-m-xylene TestAmerica Edison Page 66 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-5(0-2) Client Matrix:% Moisture:10.5 460-145401-5 Solid Date Sampled: 11/17/2017 1330 Date Received: 11/17/2017 2040 8081B Organochlorine Pesticides (GC) Dilution: 8081B 3546 1.0 11/21/2017 2253 11/21/2017 0040 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:SECONDARY +15.0005 g 10 mL 1 uL CPESTGC4 Analysis Date: Prep Date: Analysis Batch: 460-479079 460-478818Prep Batch: Analysis Method: Prep Method: Surrogate %Rec Acceptance LimitsQualifier 118 50 - 150DCB Decachlorobiphenyl 118 47 - 150Tetrachloro-m-xylene TestAmerica Edison Page 67 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-4(0-2) Client Matrix:% Moisture:8.8 460-145401-6 Solid Date Sampled: 11/17/2017 1415 Date Received: 11/17/2017 2040 8081B Organochlorine Pesticides (GC) Dilution: 8081B 3546 1.0 11/21/2017 2306 11/21/2017 0040 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:PRIMARY +15.0075 g 10 mL 1 uL CPESTGC4 Analysis Date: Prep Date: Analysis Batch: 460-479079 460-478818Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.0073 U 0.00730.00124,4'-DDD 0.0073 U 0.00730.000874,4'-DDE 0.0073 U 0.00730.00134,4'-DDT 0.0073 U 0.00730.0011Aldrin 0.0022 U 0.00220.00075alpha-BHC 0.0022 U 0.00220.00082beta-BHC 0.073 U 0.0730.018Chlordane (technical) 0.0022 U 0.00220.00045delta-BHC 0.0022 U 0.00220.00095Dieldrin 0.0073 U 0.00730.0011Endosulfan I 0.0073 U 0.00730.0019Endosulfan II 0.0073 U 0.00730.00092Endosulfan sulfate 0.0073 U 0.00730.0011Endrin 0.0073 U 0.00730.0017Endrin aldehyde 0.0073 U 0.00730.0014Endrin ketone 0.0022 U 0.00220.00068gamma-BHC (Lindane) 0.0073 U 0.00730.00087Heptachlor 0.0073 U 0.00730.0011Heptachlor epoxide 0.0073 U 0.00730.0017Methoxychlor 0.073 U 0.0730.027Toxaphene Surrogate %Rec Acceptance LimitsQualifier 118 50 - 150DCB Decachlorobiphenyl 118 47 - 150Tetrachloro-m-xylene TestAmerica Edison Page 68 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-4(0-2) Client Matrix:% Moisture:8.8 460-145401-6 Solid Date Sampled: 11/17/2017 1415 Date Received: 11/17/2017 2040 8081B Organochlorine Pesticides (GC) Dilution: 8081B 3546 1.0 11/21/2017 2306 11/21/2017 0040 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:SECONDARY +15.0075 g 10 mL 1 uL CPESTGC4 Analysis Date: Prep Date: Analysis Batch: 460-479079 460-478818Prep Batch: Analysis Method: Prep Method: Surrogate %Rec Acceptance LimitsQualifier 111 50 - 150DCB Decachlorobiphenyl 111 47 - 150Tetrachloro-m-xylene TestAmerica Edison Page 69 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-2 (0-2) Client Matrix:% Moisture:8.3 460-145515-1 Solid Date Sampled: 11/20/2017 0800 Date Received: 11/20/2017 1950 8081B Organochlorine Pesticides (GC) Dilution: 8081B 3546 1.0 11/22/2017 1152 11/22/2017 0001 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:PRIMARY +15.0050 g 10 mL 1 uL CPESTGC5 Analysis Date: Prep Date: Analysis Batch: 460-479228 460-479140Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.0073 U 0.00730.00124,4'-DDD 0.0073 U 0.00730.000864,4'-DDE 0.0073 U 0.00730.00134,4'-DDT 0.0073 U 0.00730.0011Aldrin 0.0022 U 0.00220.00074alpha-BHC 0.0022 U 0.00220.00082beta-BHC 0.073 U 0.0730.018Chlordane (technical) 0.0022 U 0.00220.00045delta-BHC 0.0022 U 0.00220.00095Dieldrin 0.0073 U 0.00730.0011Endosulfan I 0.0073 U 0.00730.0019Endosulfan II 0.0073 U 0.00730.00092Endosulfan sulfate 0.0073 U 0.00730.0010Endrin 0.0073 U 0.00730.0017Endrin aldehyde 0.0073 U 0.00730.0014Endrin ketone 0.0022 U 0.00220.00068gamma-BHC (Lindane) 0.0073 U 0.00730.00086Heptachlor 0.0073 U 0.00730.0011Heptachlor epoxide 0.0073 U 0.00730.0017Methoxychlor 0.073 U 0.0730.026Toxaphene Surrogate %Rec Acceptance LimitsQualifier 106 50 - 150DCB Decachlorobiphenyl 114 47 - 150Tetrachloro-m-xylene TestAmerica Edison Page 70 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-2 (0-2) Client Matrix:% Moisture:8.3 460-145515-1 Solid Date Sampled: 11/20/2017 0800 Date Received: 11/20/2017 1950 8081B Organochlorine Pesticides (GC) Dilution: 8081B 3546 1.0 11/22/2017 1152 11/22/2017 0001 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:SECONDARY +15.0050 g 10 mL 1 uL CPESTGC5 Analysis Date: Prep Date: Analysis Batch: 460-479228 460-479140Prep Batch: Analysis Method: Prep Method: Surrogate %Rec Acceptance LimitsQualifier 106 50 - 150DCB Decachlorobiphenyl 114 47 - 150Tetrachloro-m-xylene TestAmerica Edison Page 71 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-1 (0-2) Client Matrix:% Moisture:9.9 460-145515-2 Solid Date Sampled: 11/20/2017 0820 Date Received: 11/20/2017 1950 8081B Organochlorine Pesticides (GC) Dilution: 8081B 3546 1.0 11/22/2017 1205 11/22/2017 0001 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:PRIMARY +15.0062 g 10 mL 1 uL CPESTGC5 Analysis Date: Prep Date: Analysis Batch: 460-479228 460-479140Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.0074 U 0.00740.00134,4'-DDD 0.0074 U 0.00740.000884,4'-DDE 0.0074 U 0.00740.00144,4'-DDT 0.0074 U 0.00740.0011Aldrin 0.0022 U 0.00220.00075alpha-BHC 0.0022 U 0.00220.00083beta-BHC 0.074 U 0.0740.018Chlordane (technical) 0.0022 U 0.00220.00045delta-BHC 0.0022 U 0.00220.00097Dieldrin 0.0074 U 0.00740.0011Endosulfan I 0.0074 U 0.00740.0019Endosulfan II 0.0074 U 0.00740.00093Endosulfan sulfate 0.0074 U 0.00740.0011Endrin 0.0074 U 0.00740.0018Endrin aldehyde 0.0074 U 0.00740.0014Endrin ketone 0.0022 U 0.00220.00069gamma-BHC (Lindane) 0.0074 U 0.00740.00088Heptachlor 0.0074 U 0.00740.0011Heptachlor epoxide 0.0074 U 0.00740.0017Methoxychlor 0.074 U 0.0740.027Toxaphene Surrogate %Rec Acceptance LimitsQualifier 110 50 - 150DCB Decachlorobiphenyl 116 47 - 150Tetrachloro-m-xylene TestAmerica Edison Page 72 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-1 (0-2) Client Matrix:% Moisture:9.9 460-145515-2 Solid Date Sampled: 11/20/2017 0820 Date Received: 11/20/2017 1950 8081B Organochlorine Pesticides (GC) Dilution: 8081B 3546 1.0 11/22/2017 1205 11/22/2017 0001 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:SECONDARY +15.0062 g 10 mL 1 uL CPESTGC5 Analysis Date: Prep Date: Analysis Batch: 460-479228 460-479140Prep Batch: Analysis Method: Prep Method: Surrogate %Rec Acceptance LimitsQualifier 109 50 - 150DCB Decachlorobiphenyl 116 47 - 150Tetrachloro-m-xylene TestAmerica Edison Page 73 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-8(1-2.5) Client Matrix:% Moisture:10.6 460-145401-1 Solid Date Sampled: 11/17/2017 0945 Date Received: 11/17/2017 2040 8082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography Dilution: 8082A 3546 1.0 11/21/2017 1649 11/21/2017 0049 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:PRIMARY +15.0017 g 10 mL 1 uL CPESTGC11 Analysis Date: Prep Date: Analysis Batch: 460-478940 460-478820Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.075 U 0.0750.010Aroclor 1016 0.075 U 0.0750.010Aroclor 1221 0.075 U 0.0750.010Aroclor 1232 0.075 U 0.0750.010Aroclor 1242 0.075 U 0.0750.010Aroclor 1248 0.075 U 0.0750.010Aroclor 1254 0.075 U 0.0750.010Aroclor 1260 0.075 U 0.0750.010Aroclor-1262 0.075 U 0.0750.010Aroclor 1268 0.075 U 0.0750.010Polychlorinated biphenyls, Total Surrogate %Rec Acceptance LimitsQualifier 114 35 - 150DCB Decachlorobiphenyl TestAmerica Edison Page 74 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-8(1-2.5) Client Matrix:% Moisture:10.6 460-145401-1 Solid Date Sampled: 11/17/2017 0945 Date Received: 11/17/2017 2040 8082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography Dilution: 8082A 3546 1.0 11/21/2017 1649 11/21/2017 0049 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:SECONDARY +15.0017 g 10 mL 1 uL CPESTGC11 Analysis Date: Prep Date: Analysis Batch: 460-478940 460-478820Prep Batch: Analysis Method: Prep Method: Surrogate %Rec Acceptance LimitsQualifier 100 35 - 150DCB Decachlorobiphenyl TestAmerica Edison Page 75 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-7(5-7) Client Matrix:% Moisture:6.8 460-145401-2 Solid Date Sampled: 11/17/2017 1050 Date Received: 11/17/2017 2040 8082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography Dilution: 8082A 3546 1.0 11/21/2017 1703 11/21/2017 0049 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:PRIMARY +15.0090 g 10 mL 1 uL CPESTGC11 Analysis Date: Prep Date: Analysis Batch: 460-478940 460-478820Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.072 U 0.0720.0095Aroclor 1016 0.072 U 0.0720.0095Aroclor 1221 0.072 U 0.0720.0095Aroclor 1232 0.072 U 0.0720.0095Aroclor 1242 0.072 U 0.0720.0095Aroclor 1248 0.072 U 0.0720.0099Aroclor 1254 0.072 U 0.0720.0099Aroclor 1260 0.072 U 0.0720.0099Aroclor-1262 0.072 U 0.0720.0099Aroclor 1268 0.072 U 0.0720.0099Polychlorinated biphenyls, Total Surrogate %Rec Acceptance LimitsQualifier 120 35 - 150DCB Decachlorobiphenyl TestAmerica Edison Page 76 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-7(5-7) Client Matrix:% Moisture:6.8 460-145401-2 Solid Date Sampled: 11/17/2017 1050 Date Received: 11/17/2017 2040 8082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography Dilution: 8082A 3546 1.0 11/21/2017 1703 11/21/2017 0049 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:SECONDARY +15.0090 g 10 mL 1 uL CPESTGC11 Analysis Date: Prep Date: Analysis Batch: 460-478940 460-478820Prep Batch: Analysis Method: Prep Method: Surrogate %Rec Acceptance LimitsQualifier 104 35 - 150DCB Decachlorobiphenyl TestAmerica Edison Page 77 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-6(5-7) Client Matrix:% Moisture:8.1 460-145401-3 Solid Date Sampled: 11/17/2017 1215 Date Received: 11/17/2017 2040 8082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography Dilution: 8082A 3546 1.0 11/21/2017 1635 11/21/2017 0049 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:PRIMARY +15.0035 g 10 mL 1 uL CPESTGC8 Analysis Date: Prep Date: Analysis Batch: 460-478953 460-478820Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.073 U 0.0730.0097Aroclor 1016 0.073 U 0.0730.0097Aroclor 1221 0.073 U 0.0730.0097Aroclor 1232 0.073 U 0.0730.0097Aroclor 1242 0.073 U 0.0730.0097Aroclor 1248 0.073 U 0.0730.010Aroclor 1254 0.073 U 0.0730.010Aroclor 1260 0.073 U 0.0730.010Aroclor-1262 0.073 U 0.0730.010Aroclor 1268 0.073 U 0.0730.010Polychlorinated biphenyls, Total Surrogate %Rec Acceptance LimitsQualifier 116 35 - 150DCB Decachlorobiphenyl TestAmerica Edison Page 78 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-6(5-7) Client Matrix:% Moisture:8.1 460-145401-3 Solid Date Sampled: 11/17/2017 1215 Date Received: 11/17/2017 2040 8082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography Dilution: 8082A 3546 1.0 11/21/2017 1635 11/21/2017 0049 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:SECONDARY +15.0035 g 10 mL 1 uL CPESTGC8 Analysis Date: Prep Date: Analysis Batch: 460-478953 460-478820Prep Batch: Analysis Method: Prep Method: Surrogate %Rec Acceptance LimitsQualifier 86 35 - 150DCB Decachlorobiphenyl TestAmerica Edison Page 79 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-3(0-2) Client Matrix:% Moisture:8.3 460-145401-4 Solid Date Sampled: 11/17/2017 1250 Date Received: 11/17/2017 2040 8082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography Dilution: 8082A 3546 1.0 11/21/2017 1653 11/21/2017 0049 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:PRIMARY +15.0113 g 10 mL 1 uL CPESTGC8 Analysis Date: Prep Date: Analysis Batch: 460-478953 460-478820Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.073 U 0.0730.0097Aroclor 1016 0.073 U 0.0730.0097Aroclor 1221 0.073 U 0.0730.0097Aroclor 1232 0.073 U 0.0730.0097Aroclor 1242 0.073 U 0.0730.0097Aroclor 1248 0.073 U 0.0730.010Aroclor 1254 0.073 U 0.0730.010Aroclor 1260 0.073 U 0.0730.010Aroclor-1262 0.073 U 0.0730.010Aroclor 1268 0.073 U 0.0730.010Polychlorinated biphenyls, Total Surrogate %Rec Acceptance LimitsQualifier 136 35 - 150DCB Decachlorobiphenyl TestAmerica Edison Page 80 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-3(0-2) Client Matrix:% Moisture:8.3 460-145401-4 Solid Date Sampled: 11/17/2017 1250 Date Received: 11/17/2017 2040 8082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography Dilution: 8082A 3546 1.0 11/21/2017 1653 11/21/2017 0049 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:SECONDARY +15.0113 g 10 mL 1 uL CPESTGC8 Analysis Date: Prep Date: Analysis Batch: 460-478953 460-478820Prep Batch: Analysis Method: Prep Method: Surrogate %Rec Acceptance LimitsQualifier 92 35 - 150DCB Decachlorobiphenyl TestAmerica Edison Page 81 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-5(0-2) Client Matrix:% Moisture:10.5 460-145401-5 Solid Date Sampled: 11/17/2017 1330 Date Received: 11/17/2017 2040 8082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography Dilution: 8082A 3546 1.0 11/21/2017 1710 11/21/2017 0049 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:PRIMARY +15.0005 g 10 mL 1 uL CPESTGC8 Analysis Date: Prep Date: Analysis Batch: 460-478953 460-478820Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.075 U 0.0750.0099Aroclor 1016 0.075 U 0.0750.0099Aroclor 1221 0.075 U 0.0750.0099Aroclor 1232 0.075 U 0.0750.0099Aroclor 1242 0.075 U 0.0750.0099Aroclor 1248 0.075 U 0.0750.010Aroclor 1254 0.075 U 0.0750.010Aroclor 1260 0.075 U 0.0750.010Aroclor-1262 0.075 U 0.0750.010Aroclor 1268 0.075 U 0.0750.010Polychlorinated biphenyls, Total Surrogate %Rec Acceptance LimitsQualifier 123 35 - 150DCB Decachlorobiphenyl TestAmerica Edison Page 82 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-5(0-2) Client Matrix:% Moisture:10.5 460-145401-5 Solid Date Sampled: 11/17/2017 1330 Date Received: 11/17/2017 2040 8082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography Dilution: 8082A 3546 1.0 11/21/2017 1710 11/21/2017 0049 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:SECONDARY +15.0005 g 10 mL 1 uL CPESTGC8 Analysis Date: Prep Date: Analysis Batch: 460-478953 460-478820Prep Batch: Analysis Method: Prep Method: Surrogate %Rec Acceptance LimitsQualifier 87 35 - 150DCB Decachlorobiphenyl TestAmerica Edison Page 83 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-4(0-2) Client Matrix:% Moisture:8.8 460-145401-6 Solid Date Sampled: 11/17/2017 1415 Date Received: 11/17/2017 2040 8082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography Dilution: 8082A 3546 1.0 11/21/2017 1728 11/21/2017 0049 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:PRIMARY +15.0075 g 10 mL 1 uL CPESTGC8 Analysis Date: Prep Date: Analysis Batch: 460-478953 460-478820Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.073 U 0.0730.0098Aroclor 1016 0.073 U 0.0730.0098Aroclor 1221 0.073 U 0.0730.0098Aroclor 1232 0.073 U 0.0730.0098Aroclor 1242 0.073 U 0.0730.0098Aroclor 1248 0.073 U 0.0730.010Aroclor 1254 0.073 U 0.0730.010Aroclor 1260 0.073 U 0.0730.010Aroclor-1262 0.073 U 0.0730.010Aroclor 1268 0.073 U 0.0730.010Polychlorinated biphenyls, Total Surrogate %Rec Acceptance LimitsQualifier 140 35 - 150DCB Decachlorobiphenyl TestAmerica Edison Page 84 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-4(0-2) Client Matrix:% Moisture:8.8 460-145401-6 Solid Date Sampled: 11/17/2017 1415 Date Received: 11/17/2017 2040 8082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography Dilution: 8082A 3546 1.0 11/21/2017 1728 11/21/2017 0049 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:SECONDARY +15.0075 g 10 mL 1 uL CPESTGC8 Analysis Date: Prep Date: Analysis Batch: 460-478953 460-478820Prep Batch: Analysis Method: Prep Method: Surrogate %Rec Acceptance LimitsQualifier 98 35 - 150DCB Decachlorobiphenyl TestAmerica Edison Page 85 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-2 (0-2) Client Matrix:% Moisture:8.3 460-145515-1 Solid Date Sampled: 11/20/2017 0800 Date Received: 11/20/2017 1950 8082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography Dilution: 8082A 3546 1.0 11/22/2017 1253 11/22/2017 0008 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:PRIMARY +15.0050 g 10 mL 1 uL CPESTGC7 Analysis Date: Prep Date: Analysis Batch: 460-479278 460-479142Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.073 U 0.0730.0097Aroclor 1016 0.073 U 0.0730.0097Aroclor 1221 0.073 U 0.0730.0097Aroclor 1232 0.073 U 0.0730.0097Aroclor 1242 0.073 U 0.0730.0097Aroclor 1248 0.073 U 0.0730.010Aroclor 1254 0.073 U 0.0730.010Aroclor 1260 0.073 U 0.0730.010Aroclor-1262 0.073 U 0.0730.010Aroclor 1268 0.073 U 0.0730.010Polychlorinated biphenyls, Total Surrogate %Rec Acceptance LimitsQualifier 122 35 - 150DCB Decachlorobiphenyl TestAmerica Edison Page 86 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-2 (0-2) Client Matrix:% Moisture:8.3 460-145515-1 Solid Date Sampled: 11/20/2017 0800 Date Received: 11/20/2017 1950 8082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography Dilution: 8082A 3546 1.0 11/22/2017 1253 11/22/2017 0008 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:SECONDARY +15.0050 g 10 mL 1 uL CPESTGC7 Analysis Date: Prep Date: Analysis Batch: 460-479278 460-479142Prep Batch: Analysis Method: Prep Method: Surrogate %Rec Acceptance LimitsQualifier 111 35 - 150DCB Decachlorobiphenyl TestAmerica Edison Page 87 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-1 (0-2) Client Matrix:% Moisture:9.9 460-145515-2 Solid Date Sampled: 11/20/2017 0820 Date Received: 11/20/2017 1950 8082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography Dilution: 8082A 3546 1.0 11/22/2017 1229 11/22/2017 0008 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:PRIMARY +15.0062 g 10 mL 1 uL CPESTGC7 Analysis Date: Prep Date: Analysis Batch: 460-479278 460-479142Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.074 U 0.0740.0099Aroclor 1016 0.074 U 0.0740.0099Aroclor 1221 0.074 U 0.0740.0099Aroclor 1232 0.074 U 0.0740.0099Aroclor 1242 0.074 U 0.0740.0099Aroclor 1248 0.074 U 0.0740.010Aroclor 1254 0.074 U 0.0740.010Aroclor 1260 0.074 U 0.0740.010Aroclor-1262 0.074 U 0.0740.010Aroclor 1268 0.074 U 0.0740.010Polychlorinated biphenyls, Total Surrogate %Rec Acceptance LimitsQualifier 139 35 - 150DCB Decachlorobiphenyl TestAmerica Edison Page 88 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-1 (0-2) Client Matrix:% Moisture:9.9 460-145515-2 Solid Date Sampled: 11/20/2017 0820 Date Received: 11/20/2017 1950 8082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography Dilution: 8082A 3546 1.0 11/22/2017 1229 11/22/2017 0008 Instrument ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Result Type:SECONDARY +15.0062 g 10 mL 1 uL CPESTGC7 Analysis Date: Prep Date: Analysis Batch: 460-479278 460-479142Prep Batch: Analysis Method: Prep Method: Surrogate %Rec Acceptance LimitsQualifier 124 35 - 150DCB Decachlorobiphenyl TestAmerica Edison Page 89 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-8(1-2.5) Client Matrix:% Moisture:10.6 460-145401-1 Solid Date Sampled: 11/17/2017 0945 Date Received: 11/17/2017 2040 6010C Metals (ICP) 6010C Instrument ID: Lab File ID:479166D1.asc Dilution:4.0 Initial Weight/Volume:1.07 g 11/22/2017 1707 Final Weight/Volume:50 mL 11/20/2017 0237 3050B ICP5 Analysis Date: Prep Date: Analysis Batch: 460-479312 460-478536Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 10600 41.88.6Aluminum 4.2 U 4.20.50Antimony 3.1 U 3.10.77Arsenic 86.6 41.83.4Barium 0.59 0.420.048Beryllium 0.84 U 0.840.12Cadmium 2670 1050107Calcium 18.8 2.10.58Chromium 6.6 J 10.51.2Cobalt 19.6 5.21.2Copper 17100 31.45.6Iron 9.0 2.10.63Lead 3520 105080.6Magnesium 336 3.10.32Manganese 15.5 8.40.79Nickel 2840 105055.6Potassium 4.2 U 4.21.3Selenium 2.1 U 2.10.32Silver 142 J 105080.5Sodium 4.2 U 4.21.2Thallium 27.8 10.51.2Vanadium 39.9 6.30.54Zinc 7471B Mercury (CVAA) 7471B Instrument ID: Lab File ID:478540HG1.CSV Dilution:1.0 Initial Weight/Volume:0.63 g 11/20/2017 1047 Final Weight/Volume:50 mL 11/20/2017 0511 7471B LEEMAN7 Analysis Date: Prep Date: Analysis Batch: 460-478647 460-478547Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.018 U 0.0180.012Mercury TestAmerica Edison Page 90 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-7(5-7) Client Matrix:% Moisture:6.8 460-145401-2 Solid Date Sampled: 11/17/2017 1050 Date Received: 11/17/2017 2040 6010C Metals (ICP) 6010C Instrument ID: Lab File ID:479166D1.asc Dilution:4.0 Initial Weight/Volume:1.05 g 11/22/2017 1710 Final Weight/Volume:50 mL 11/20/2017 0237 3050B ICP5 Analysis Date: Prep Date: Analysis Batch: 460-479312 460-478536Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 9370 40.98.4Aluminum 4.1 U 4.10.49Antimony 3.1 U 3.10.76Arsenic 101 40.93.3Barium 0.69 0.410.047Beryllium 0.82 U 0.820.12Cadmium 5930 1020104Calcium 22.1 2.00.57Chromium 7.5 J 10.21.2Cobalt 16.4 5.11.2Copper 16100 30.75.5Iron 4.7 2.00.62Lead 5450 102078.8Magnesium 235 3.10.32Manganese 14.7 8.20.78Nickel 3770 102054.4Potassium 4.1 U 4.11.2Selenium 2.0 U 2.00.31Silver 138 J 102078.7Sodium 4.1 U 4.11.2Thallium 31.7 10.21.2Vanadium 33.3 6.10.53Zinc 7471B Mercury (CVAA) 7471B Instrument ID: Lab File ID:478540HG1.CSV Dilution:1.0 Initial Weight/Volume:0.62 g 11/20/2017 1052 Final Weight/Volume:50 mL 11/20/2017 0511 7471B LEEMAN7 Analysis Date: Prep Date: Analysis Batch: 460-478647 460-478547Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.018 U 0.0180.011Mercury TestAmerica Edison Page 91 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-6(5-7) Client Matrix:% Moisture:8.1 460-145401-3 Solid Date Sampled: 11/17/2017 1215 Date Received: 11/17/2017 2040 6010C Metals (ICP) 6010C Instrument ID: Lab File ID:479166D1.asc Dilution:4.0 Initial Weight/Volume:1.02 g 11/22/2017 1714 Final Weight/Volume:50 mL 11/20/2017 0237 3050B ICP5 Analysis Date: Prep Date: Analysis Batch: 460-479312 460-478536Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 9810 42.78.7Aluminum 4.3 U 4.30.51Antimony 3.2 U 3.20.79Arsenic 117 42.73.5Barium 0.75 0.430.049Beryllium 0.85 U 0.850.13Cadmium 2260 1070109Calcium 25.4 2.10.59Chromium 7.1 J 10.71.2Cobalt 16.7 5.31.2Copper 16600 32.05.8Iron 6.3 2.10.64Lead 4610 107082.2Magnesium 206 3.20.33Manganese 15.8 8.50.81Nickel 4050 107056.7Potassium 4.3 U 4.31.3Selenium 2.1 U 2.10.33Silver 238 J 107082.1Sodium 4.3 U 4.31.3Thallium 31.1 10.71.3Vanadium 37.5 6.40.55Zinc 7471B Mercury (CVAA) 7471B Instrument ID: Lab File ID:478540HG1.CSV Dilution:1.0 Initial Weight/Volume:0.61 g 11/20/2017 1054 Final Weight/Volume:50 mL 11/20/2017 0511 7471B LEEMAN7 Analysis Date: Prep Date: Analysis Batch: 460-478647 460-478547Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.018 U 0.0180.012Mercury TestAmerica Edison Page 92 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-3(0-2) Client Matrix:% Moisture:8.3 460-145401-4 Solid Date Sampled: 11/17/2017 1250 Date Received: 11/17/2017 2040 6010C Metals (ICP) 6010C Instrument ID: Lab File ID:479166D1.asc Dilution:4.0 Initial Weight/Volume:1.04 g 11/22/2017 1718 Final Weight/Volume:50 mL 11/20/2017 0237 3050B ICP5 Analysis Date: Prep Date: Analysis Batch: 460-479312 460-478536Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 7450 41.98.6Aluminum 4.2 U 4.20.50Antimony 3.1 U 3.10.78Arsenic 84.6 41.93.4Barium 0.57 0.420.048Beryllium 0.84 U 0.840.12Cadmium 4310 1050107Calcium 19.5 2.10.58Chromium 5.4 J 10.51.2Cobalt 12.8 5.21.2Copper 13100 31.45.7Iron 4.3 2.10.63Lead 4310 105080.8Magnesium 269 3.10.32Manganese 12.2 8.40.80Nickel 3050 105055.8Potassium 4.2 U 4.21.3Selenium 2.1 U 2.10.32Silver 571 J 105080.7Sodium 4.2 U 4.21.2Thallium 24.5 10.51.2Vanadium 29.1 6.30.54Zinc 7471B Mercury (CVAA) 7471B Instrument ID: Lab File ID:478540HG1.CSV Dilution:1.0 Initial Weight/Volume:0.60 g 11/20/2017 1056 Final Weight/Volume:50 mL 11/20/2017 0511 7471B LEEMAN7 Analysis Date: Prep Date: Analysis Batch: 460-478647 460-478547Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.019 U 0.0190.012Mercury TestAmerica Edison Page 93 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-5(0-2) Client Matrix:% Moisture:10.5 460-145401-5 Solid Date Sampled: 11/17/2017 1330 Date Received: 11/17/2017 2040 6010C Metals (ICP) 6010C Instrument ID: Lab File ID:479166D1.asc Dilution:4.0 Initial Weight/Volume:1.04 g 11/22/2017 1722 Final Weight/Volume:50 mL 11/20/2017 0237 3050B ICP5 Analysis Date: Prep Date: Analysis Batch: 460-479312 460-478536Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 18200 43.08.8Aluminum 3.2 U 3.20.80Arsenic 66.3 43.03.5Barium 1.2 0.430.049Beryllium 0.86 U 0.860.13Cadmium 3780 1070110Calcium 39.5 2.10.60Chromium 10.1 J 10.71.2Cobalt 27.3 5.41.2Copper 27200 32.25.8Iron 5.0 2.10.65Lead 8600 107082.8Magnesium 365 3.20.33Manganese 21.6 8.60.82Nickel 4100 107057.2Potassium 4.3 U 4.31.3Selenium 2.1 U 2.10.33Silver 3350 107082.7Sodium 4.3 U 4.31.3Thallium 60.1 10.71.3Vanadium 62.0 6.40.56Zinc 6010C Instrument ID: Lab File ID:479488D1.asc Dilution:10 Initial Weight/Volume:1.04 g 11/24/2017 0948 Final Weight/Volume:50 mL 11/20/2017 0237 3050B ICP5 Analysis Date: Prep Date: Analysis Batch: 460-479612 460-478536Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 10.7 U 10.71.3Antimony 7471B Mercury (CVAA) 7471B Instrument ID: Lab File ID:478540HG1.CSV Dilution:1.0 Initial Weight/Volume:0.64 g 11/20/2017 1057 Final Weight/Volume:50 mL 11/20/2017 0511 7471B LEEMAN7 Analysis Date: Prep Date: Analysis Batch: 460-478647 460-478547Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.018 U 0.0180.012Mercury TestAmerica Edison Page 94 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-4(0-2) Client Matrix:% Moisture:8.8 460-145401-6 Solid Date Sampled: 11/17/2017 1415 Date Received: 11/17/2017 2040 6010C Metals (ICP) 6010C Instrument ID: Lab File ID:479166D1.asc Dilution:4.0 Initial Weight/Volume:1.03 g 11/22/2017 1726 Final Weight/Volume:50 mL 11/20/2017 0237 3050B ICP5 Analysis Date: Prep Date: Analysis Batch: 460-479312 460-478536Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 8450 42.68.7Aluminum 4.3 U 4.30.51Antimony 0.84 J 3.20.79Arsenic 101 42.63.4Barium 0.60 0.430.049Beryllium 0.85 U 0.850.13Cadmium 7860 1060109Calcium 25.8 2.10.59Chromium 6.8 J 10.61.2Cobalt 15.3 5.31.2Copper 14800 31.95.7Iron 4.8 2.10.64Lead 4820 106082.1Magnesium 238 3.20.33Manganese 16.2 8.50.81Nickel 3520 106056.6Potassium 4.3 U 4.31.3Selenium 2.1 U 2.10.32Silver 920 J 106082.0Sodium 4.3 U 4.31.3Thallium 28.5 10.61.3Vanadium 32.3 6.40.55Zinc 7471B Mercury (CVAA) 7471B Instrument ID: Lab File ID:478540HG1.CSV Dilution:1.0 Initial Weight/Volume:0.62 g 11/20/2017 1059 Final Weight/Volume:50 mL 11/20/2017 0511 7471B LEEMAN7 Analysis Date: Prep Date: Analysis Batch: 460-478647 460-478547Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.018 U 0.0180.012Mercury TestAmerica Edison Page 95 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-2 (0-2) Client Matrix:% Moisture:8.3 460-145515-1 Solid Date Sampled: 11/20/2017 0800 Date Received: 11/20/2017 1950 6010C Metals (ICP) 6010C Instrument ID: Lab File ID:479488D1.asc Dilution:10 Initial Weight/Volume:1.09 g 11/24/2017 0940 Final Weight/Volume:50 mL 11/22/2017 0239 3050B ICP5 Analysis Date: Prep Date: Analysis Batch: 460-479612 460-479166Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 22200 10020.5Aluminum 10.0 U 10.01.2Antimony 7.5 U 7.51.9Arsenic 379 1008.1Barium 1.9 1.00.12Beryllium 2.0 U 2.00.30Cadmium 15300 2500255Calcium 76.8 5.01.4Chromium 14.8 J 25.02.9Cobalt 26.2 12.52.8Copper 32000 75.013.5Iron 8.1 5.01.5Lead 16900 2500193Magnesium 633 7.50.78Manganese 35.9 20.01.9Nickel 8950 2500133Potassium 10.0 U 10.03.0Selenium 5.0 U 5.00.76Silver 2500 U 2500193Sodium 10.0 U 10.03.0Thallium 64.0 25.03.0Vanadium 65.5 15.01.3Zinc 7471B Mercury (CVAA) 7471B Instrument ID: Lab File ID:479171HG1.CSV Dilution:1.0 Initial Weight/Volume:0.60 g 11/22/2017 0923 Final Weight/Volume:50 mL 11/22/2017 0402 7471B LEEMAN7 Analysis Date: Prep Date: Analysis Batch: 460-479302 460-479171Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.019 U 0.0190.012Mercury TestAmerica Edison Page 96 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 Client Sample ID: Lab Sample ID: SB-1 (0-2) Client Matrix:% Moisture:9.9 460-145515-2 Solid Date Sampled: 11/20/2017 0820 Date Received: 11/20/2017 1950 6010C Metals (ICP) 6010C Instrument ID: Lab File ID:479488D1.asc Dilution:10 Initial Weight/Volume:1.03 g 11/24/2017 0944 Final Weight/Volume:50 mL 11/22/2017 0239 3050B ICP5 Analysis Date: Prep Date: Analysis Batch: 460-479612 460-479166Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 20500 10822.1Aluminum 10.8 U 10.81.3Antimony 8.1 U 8.12.0Arsenic 228 1088.7Barium 1.7 1.10.12Beryllium 2.2 U 2.20.32Cadmium 2450 J 2690275Calcium 53.8 5.41.5Chromium 13.7 J 26.93.1Cobalt 29.7 13.53.0Copper 31600 80.814.5Iron 9.8 5.41.6Lead 8790 2690208Magnesium 528 8.10.84Manganese 30.3 21.62.0Nickel 7570 2690143Potassium 10.8 U 10.83.3Selenium 5.4 U 5.40.82Silver 2690 U 2690207Sodium 10.8 U 10.83.2Thallium 63.2 26.93.2Vanadium 74.8 16.21.4Zinc 7471B Mercury (CVAA) 7471B Instrument ID: Lab File ID:479171HG1.CSV Dilution:1.0 Initial Weight/Volume:0.62 g 11/22/2017 0924 Final Weight/Volume:50 mL 11/22/2017 0402 7471B LEEMAN7 Analysis Date: Prep Date: Analysis Batch: 460-479302 460-479171Prep Batch: Analysis Method: Prep Method: Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL 0.018 U 0.0180.012Mercury TestAmerica Edison Page 97 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 General Chemistry Client Sample ID: Lab Sample ID: SB-8(1-2.5) Client Matrix: 460-145401-1 Solid Date Sampled: 11/17/2017 0945 Date Received: 11/17/2017 2040 Analyte Result Qual Units RL RL Dil Method Percent Moisture 10.6 %1.0 1.0 1.0 Moisture DryWt Corrected: NAnalysis Date: 11/21/2017 1112Analysis Batch: 460-478966 Percent Solids 89.4 %1.0 1.0 1.0 Moisture DryWt Corrected: NAnalysis Date: 11/21/2017 1112Analysis Batch: 460-478966 TestAmerica Edison Page 98 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 General Chemistry Client Sample ID: Lab Sample ID: SB-7(5-7) Client Matrix: 460-145401-2 Solid Date Sampled: 11/17/2017 1050 Date Received: 11/17/2017 2040 Analyte Result Qual Units RL RL Dil Method Percent Moisture 6.8 %1.0 1.0 1.0 Moisture DryWt Corrected: NAnalysis Date: 11/21/2017 1112Analysis Batch: 460-478966 Percent Solids 93.2 %1.0 1.0 1.0 Moisture DryWt Corrected: NAnalysis Date: 11/21/2017 1112Analysis Batch: 460-478966 TestAmerica Edison Page 99 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 General Chemistry Client Sample ID: Lab Sample ID: SB-6(5-7) Client Matrix: 460-145401-3 Solid Date Sampled: 11/17/2017 1215 Date Received: 11/17/2017 2040 Analyte Result Qual Units RL RL Dil Method Percent Moisture 8.1 %1.0 1.0 1.0 Moisture DryWt Corrected: NAnalysis Date: 11/21/2017 1112Analysis Batch: 460-478966 Percent Solids 91.9 %1.0 1.0 1.0 Moisture DryWt Corrected: NAnalysis Date: 11/21/2017 1112Analysis Batch: 460-478966 TestAmerica Edison Page 100 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 General Chemistry Client Sample ID: Lab Sample ID: SB-3(0-2) Client Matrix: 460-145401-4 Solid Date Sampled: 11/17/2017 1250 Date Received: 11/17/2017 2040 Analyte Result Qual Units RL RL Dil Method Percent Moisture 8.3 %1.0 1.0 1.0 Moisture DryWt Corrected: NAnalysis Date: 11/21/2017 1130Analysis Batch: 460-478972 Percent Solids 91.7 %1.0 1.0 1.0 Moisture DryWt Corrected: NAnalysis Date: 11/21/2017 1130Analysis Batch: 460-478972 TestAmerica Edison Page 101 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 General Chemistry Client Sample ID: Lab Sample ID: SB-5(0-2) Client Matrix: 460-145401-5 Solid Date Sampled: 11/17/2017 1330 Date Received: 11/17/2017 2040 Analyte Result Qual Units RL RL Dil Method Percent Moisture 10.5 %1.0 1.0 1.0 Moisture DryWt Corrected: NAnalysis Date: 11/21/2017 1130Analysis Batch: 460-478972 Percent Solids 89.5 %1.0 1.0 1.0 Moisture DryWt Corrected: NAnalysis Date: 11/21/2017 1130Analysis Batch: 460-478972 TestAmerica Edison Page 102 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 General Chemistry Client Sample ID: Lab Sample ID: SB-4(0-2) Client Matrix: 460-145401-6 Solid Date Sampled: 11/17/2017 1415 Date Received: 11/17/2017 2040 Analyte Result Qual Units RL RL Dil Method Percent Moisture 8.8 %1.0 1.0 1.0 Moisture DryWt Corrected: NAnalysis Date: 11/21/2017 1130Analysis Batch: 460-478972 Percent Solids 91.2 %1.0 1.0 1.0 Moisture DryWt Corrected: NAnalysis Date: 11/21/2017 1130Analysis Batch: 460-478972 TestAmerica Edison Page 103 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 General Chemistry Client Sample ID: Lab Sample ID: SB-2 (0-2) Client Matrix: 460-145515-1 Solid Date Sampled: 11/20/2017 0800 Date Received: 11/20/2017 1950 Analyte Result Qual Units RL RL Dil Method Percent Moisture 8.3 %1.0 1.0 1.0 Moisture DryWt Corrected: NAnalysis Date: 11/22/2017 1538Analysis Batch: 460-479372 Percent Solids 91.7 %1.0 1.0 1.0 Moisture DryWt Corrected: NAnalysis Date: 11/22/2017 1538Analysis Batch: 460-479372 TestAmerica Edison Page 104 of 194 Analytical Data Client: AKRF Inc Job Number: 460-145401-1 General Chemistry Client Sample ID: Lab Sample ID: SB-1 (0-2) Client Matrix: 460-145515-2 Solid Date Sampled: 11/20/2017 0820 Date Received: 11/20/2017 1950 Analyte Result Qual Units RL RL Dil Method Percent Moisture 9.9 %1.0 1.0 1.0 Moisture DryWt Corrected: NAnalysis Date: 11/22/2017 1538Analysis Batch: 460-479372 Percent Solids 90.1 %1.0 1.0 1.0 Moisture DryWt Corrected: NAnalysis Date: 11/22/2017 1538Analysis Batch: 460-479372 TestAmerica Edison Page 105 of 194 DATA REPORTING QUALIFIERS Client: AKRF Inc Job Number: 460-145401-1 Lab Section Qualifier Description GC/MS VOA Analyzed for but not detected.U Indicates an estimated value.J LCS or LCSD is outside acceptance limits.* Surrogate is outside acceptance limits.* GC/MS Semi VOA Analyzed for but not detected.U Indicates an estimated value.J LCS or LCSD is outside acceptance limits.* MS or MSD is outside acceptance limits.* Surrogate is outside acceptance limits.* GC Semi VOA Analyzed for but not detected.U Metals Duplicate analysis not within control limits.* Indicates analyzed for but not detected.U MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not applicable. 4 Sample result is greater than the MDL but below the CRDLJ Spiked sample recovery is not within control limits.N TestAmerica Edison Page 106 of 194 QUALITY CONTROL RESULTS TestAmerica Edison Page 107 of 194 Quality Control Results Client: AKRF Inc Job Number: 460-145401-1 QC Association Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis GC/MS VOA Prep Batch: 460-478326 SolidSB-8(1-2.5)5035460-145401-1 T SolidSB-7(5-7)5035460-145401-2 T SolidSB-6(5-7)5035460-145401-3 T SolidSB-3(0-2)5035460-145401-4 T SolidSB-5(0-2)5035460-145401-5 T SolidSB-4(0-2)5035460-145401-6 T Prep Batch: 460-478957 SolidSB-2 (0-2)5035460-145515-1 T SolidSB-1 (0-2)5035460-145515-2 T Analysis Batch:460-479592 Lab Control Sample Solid 8260CLCS 460-479592/4 T Lab Control Sample Duplicate Solid 8260CLCSD 460-479592/5 T Method Blank Solid 8260CMB 460-479592/8 T Solid 460-478326SB-8(1-2.5)8260C460-145401-1 T Solid 460-478326SB-7(5-7)8260C460-145401-2 T Solid 460-478326SB-6(5-7)8260C460-145401-3 T Solid 460-478326SB-3(0-2)8260C460-145401-4 T Solid 460-478326SB-4(0-2)8260C460-145401-6 T Analysis Batch:460-479706 Lab Control Sample Solid 8260CLCS 460-479706/3 T Lab Control Sample Duplicate Solid 8260CLCSD 460-479706/4 T Method Blank Solid 8260CMB 460-479706/7 T Solid 460-478957SB-2 (0-2)8260C460-145515-1 T Solid 460-478957SB-1 (0-2)8260C460-145515-2 T Analysis Batch:460-479876 Lab Control Sample Solid 8260CLCS 460-479876/5 T Lab Control Sample Duplicate Solid 8260CLCSD 460-479876/6 T Method Blank Solid 8260CMB 460-479876/9 T Solid 460-478326SB-5(0-2)8260C460-145401-5 T Analysis Batch:460-479912 Lab Control Sample Water 8260CLCS 460-479912/3 T Lab Control Sample Duplicate Water 8260CLCSD 460-479912/4 T Method Blank Water 8260CMB 460-479912/6 T WaterOW-2 8260C460-145597-1 T WaterOW-1 8260C460-145597-2 T WaterTrip Blank 8260C460-145597-3TB T Report Basis T = Total TestAmerica Edison Page 108 of 194 Quality Control Results Client: AKRF Inc Job Number: 460-145401-1 QC Association Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis GC/MS Semi VOA Prep Batch: 460-478451 Lab Control Sample Solid 3546LCS 460-478451/2-A T Method Blank Solid 3546MB 460-478451/1-A T Matrix Spike Solid 3546460-145381-C-5-D MS T Matrix Spike Duplicate Solid 3546460-145381-C-5-E MSD T SolidSB-8(1-2.5)3546460-145401-1 T SolidSB-7(5-7)3546460-145401-2 T SolidSB-6(5-7)3546460-145401-3 T SolidSB-3(0-2)3546460-145401-4 T SolidSB-5(0-2)3546460-145401-5 T SolidSB-4(0-2)3546460-145401-6 T Analysis Batch:460-478510 Method Blank Solid 460-4784518270DMB 460-478451/1-A T Matrix Spike Solid 460-4784518270D460-145381-C-5-D MS T Matrix Spike Duplicate Solid 460-4784518270D460-145381-C-5-E MSD T Solid 460-478451SB-8(1-2.5)8270D460-145401-1 T Solid 460-478451SB-7(5-7)8270D460-145401-2 T Solid 460-478451SB-6(5-7)8270D460-145401-3 T Solid 460-478451SB-3(0-2)8270D460-145401-4 T Solid 460-478451SB-5(0-2)8270D460-145401-5 T Solid 460-478451SB-4(0-2)8270D460-145401-6 T Analysis Batch:460-478549 Lab Control Sample Solid 460-4784518270DLCS 460-478451/2-A T Prep Batch: 460-479261 Lab Control Sample Solid 3546LCS 460-479261/2-A T Method Blank Solid 3546MB 460-479261/1-A T SolidSB-2 (0-2)3546460-145515-1 T SolidSB-1 (0-2)3546460-145515-2 T Matrix Spike Solid 3546460-145556-A-1-B MS T Matrix Spike Duplicate Solid 3546460-145556-A-1-C MSD T Prep Batch: 460-479363 Lab Control Sample Water 3510CLCS 460-479363/2-A T Lab Control Sample Duplicate Water 3510CLCSD 460-479363/3-A T Method Blank Water 3510CMB 460-479363/1-A T WaterOW-2 3510C460-145597-1 T WaterOW-1 3510C460-145597-2 T Analysis Batch:460-479517 Lab Control Sample Solid 460-4792618270DLCS 460-479261/2-A T Method Blank Solid 460-4792618270DMB 460-479261/1-A T Matrix Spike Solid 460-4792618270D460-145556-A-1-B MS T Matrix Spike Duplicate Solid 460-4792618270D460-145556-A-1-C MSD T TestAmerica Edison Page 109 of 194 Quality Control Results Client: AKRF Inc Job Number: 460-145401-1 QC Association Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis GC/MS Semi VOA Analysis Batch:460-479531 Lab Control Sample Water 460-4793638270DLCS 460-479363/2-A T Lab Control Sample Duplicate Water 460-4793638270DLCSD 460-479363/3-A T Method Blank Water 460-4793638270DMB 460-479363/1-A T Water 460-479363OW-2 8270D460-145597-1 T Water 460-479363OW-1 8270D460-145597-2 T Analysis Batch:460-480050 Solid 460-479261SB-2 (0-2)8270D460-145515-1 T Solid 460-479261SB-1 (0-2)8270D460-145515-2 T Report Basis T = Total TestAmerica Edison Page 110 of 194 Quality Control Results Client: AKRF Inc Job Number: 460-145401-1 QC Association Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis GC Semi VOA Prep Batch: 460-478818 Lab Control Sample Solid 3546LCS 460-478818/2-A T Method Blank Solid 3546MB 460-478818/1-A T Matrix Spike Solid 3546460-145399-E-1-C MS T Matrix Spike Duplicate Solid 3546460-145399-E-1-D MSD T SolidSB-8(1-2.5)3546460-145401-1 T SolidSB-7(5-7)3546460-145401-2 T SolidSB-6(5-7)3546460-145401-3 T SolidSB-3(0-2)3546460-145401-4 T SolidSB-5(0-2)3546460-145401-5 T SolidSB-4(0-2)3546460-145401-6 T Prep Batch: 460-478820 Lab Control Sample Solid 3546LCS 460-478820/2-A T Method Blank Solid 3546MB 460-478820/1-A T SolidSB-8(1-2.5)3546460-145401-1 T SolidSB-7(5-7)3546460-145401-2 T SolidSB-6(5-7)3546460-145401-3 T SolidSB-3(0-2)3546460-145401-4 T SolidSB-5(0-2)3546460-145401-5 T SolidSB-4(0-2)3546460-145401-6 T Matrix Spike Solid 3546460-145455-A-6-D MS T Matrix Spike Duplicate Solid 3546460-145455-A-6-E MSD T Analysis Batch:460-478940 Lab Control Sample Solid 460-4788208082ALCS 460-478820/2-A T Method Blank Solid 460-4788208082AMB 460-478820/1-A T Solid 460-478820SB-8(1-2.5)8082A460-145401-1 T Solid 460-478820SB-7(5-7)8082A460-145401-2 T Matrix Spike Solid 460-4788208082A460-145455-A-6-D MS T Matrix Spike Duplicate Solid 460-4788208082A460-145455-A-6-E MSD T Analysis Batch:460-478953 Solid 460-478820SB-6(5-7)8082A460-145401-3 T Solid 460-478820SB-3(0-2)8082A460-145401-4 T Solid 460-478820SB-5(0-2)8082A460-145401-5 T Solid 460-478820SB-4(0-2)8082A460-145401-6 T TestAmerica Edison Page 111 of 194 Quality Control Results Client: AKRF Inc Job Number: 460-145401-1 QC Association Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis GC Semi VOA Analysis Batch:460-479079 Lab Control Sample Solid 460-4788188081BLCS 460-478818/2-A T Method Blank Solid 460-4788188081BMB 460-478818/1-A T Solid 460-478818SB-8(1-2.5)8081B460-145401-1 T Solid 460-478818SB-7(5-7)8081B460-145401-2 T Solid 460-478818SB-6(5-7)8081B460-145401-3 T Solid 460-478818SB-3(0-2)8081B460-145401-4 T Solid 460-478818SB-5(0-2)8081B460-145401-5 T Solid 460-478818SB-4(0-2)8081B460-145401-6 T Prep Batch: 460-479140 Lab Control Sample Solid 3546LCS 460-479140/2-A T Method Blank Solid 3546MB 460-479140/1-A T Matrix Spike Solid 3546460-145501-A-1-E MS T Matrix Spike Duplicate Solid 3546460-145501-A-1-F MSD T SolidSB-2 (0-2)3546460-145515-1 T SolidSB-1 (0-2)3546460-145515-2 T Prep Batch: 460-479142 Lab Control Sample Solid 3546LCS 460-479142/2-A T Method Blank Solid 3546MB 460-479142/1-A T Matrix Spike Solid 3546460-145501-A-1-H MS T Matrix Spike Duplicate Solid 3546460-145501-A-1-I MSD T SolidSB-2 (0-2)3546460-145515-1 T SolidSB-1 (0-2)3546460-145515-2 T Analysis Batch:460-479228 Lab Control Sample Solid 460-4791408081BLCS 460-479140/2-A T Method Blank Solid 460-4791408081BMB 460-479140/1-A T Matrix Spike Solid 460-4791408081B460-145501-A-1-E MS T Matrix Spike Duplicate Solid 460-4791408081B460-145501-A-1-F MSD T Solid 460-479140SB-2 (0-2)8081B460-145515-1 T Solid 460-479140SB-1 (0-2)8081B460-145515-2 T Analysis Batch:460-479230 Matrix Spike Solid 460-4788188081B460-145399-E-1-C MS T Matrix Spike Duplicate Solid 460-4788188081B460-145399-E-1-D MSD T Analysis Batch:460-479233 Lab Control Sample Solid 460-4791428082ALCS 460-479142/2-A T Method Blank Solid 460-4791428082AMB 460-479142/1-A T Matrix Spike Solid 460-4791428082A460-145501-A-1-H MS T Matrix Spike Duplicate Solid 460-4791428082A460-145501-A-1-I MSD T TestAmerica Edison Page 112 of 194 Quality Control Results Client: AKRF Inc Job Number: 460-145401-1 QC Association Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis GC Semi VOA Analysis Batch:460-479278 Solid 460-479142SB-2 (0-2)8082A460-145515-1 T Solid 460-479142SB-1 (0-2)8082A460-145515-2 T Report Basis T = Total TestAmerica Edison Page 113 of 194 Quality Control Results Client: AKRF Inc Job Number: 460-145401-1 QC Association Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis Metals Prep Batch: 460-478536 LCS-Certified Reference Material Solid 3050BLCSSRM 460-478536/2-A ^4 T Method Blank Solid 3050BMB 460-478536/1-A ^2 T Duplicate Solid 3050B460-145281-A-1-B DU ^4 T Matrix Spike Solid 3050B460-145281-A-1-C MS ^4 T SolidSB-8(1-2.5)3050B460-145401-1 T SolidSB-7(5-7)3050B460-145401-2 T SolidSB-6(5-7)3050B460-145401-3 T SolidSB-3(0-2)3050B460-145401-4 T SolidSB-5(0-2)3050B460-145401-5 T SolidSB-4(0-2)3050B460-145401-6 T Prep Batch: 460-478547 LCS-Certified Reference Material Solid 7471BLCSSRM 460-478547/2-A ^40 T Method Blank Solid 7471BMB 460-478547/1-A T Duplicate Solid 7471B460-145378-E-1-D DU T Matrix Spike Solid 7471B460-145378-E-1-E MS T SolidSB-8(1-2.5)7471B460-145401-1 T SolidSB-7(5-7)7471B460-145401-2 T SolidSB-6(5-7)7471B460-145401-3 T SolidSB-3(0-2)7471B460-145401-4 T SolidSB-5(0-2)7471B460-145401-5 T SolidSB-4(0-2)7471B460-145401-6 T Analysis Batch:460-478647 LCS-Certified Reference Material Solid 460-4785477471BLCSSRM 460-478547/2-A ^40 T Method Blank Solid 460-4785477471BMB 460-478547/1-A T Duplicate Solid 460-4785477471B460-145378-E-1-D DU T Matrix Spike Solid 460-4785477471B460-145378-E-1-E MS T Solid 460-478547SB-8(1-2.5)7471B460-145401-1 T Solid 460-478547SB-7(5-7)7471B460-145401-2 T Solid 460-478547SB-6(5-7)7471B460-145401-3 T Solid 460-478547SB-3(0-2)7471B460-145401-4 T Solid 460-478547SB-5(0-2)7471B460-145401-5 T Solid 460-478547SB-4(0-2)7471B460-145401-6 T Prep Batch: 460-479166 LCS-Certified Reference Material Solid 3050BLCSSRM 460-479166/2-A ^4 T Method Blank Solid 3050BMB 460-479166/1-A ^2 T Duplicate Solid 3050B460-145501-B-1-C DU ^4 T Matrix Spike Solid 3050B460-145501-B-1-D MS ^4 T SolidSB-2 (0-2)3050B460-145515-1 T SolidSB-1 (0-2)3050B460-145515-2 T TestAmerica Edison Page 114 of 194 Quality Control Results Client: AKRF Inc Job Number: 460-145401-1 QC Association Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis Metals Prep Batch: 460-479171 LCS-Certified Reference Material Solid 7471BLCSSRM 460-479171/11-A ^40 T Method Blank Solid 7471BMB 460-479171/10-A T Duplicate Solid 7471B460-144734-A-6-C DU T Matrix Spike Solid 7471B460-144734-A-6-D MS T SolidSB-2 (0-2)7471B460-145515-1 T SolidSB-1 (0-2)7471B460-145515-2 T Analysis Batch:460-479302 LCS-Certified Reference Material Solid 460-4791717471BLCSSRM 460-479171/11-A ^40 T Method Blank Solid 460-4791717471BMB 460-479171/10-A T Duplicate Solid 460-4791717471B460-144734-A-6-C DU T Matrix Spike Solid 460-4791717471B460-144734-A-6-D MS T Solid 460-479171SB-2 (0-2)7471B460-145515-1 T Solid 460-479171SB-1 (0-2)7471B460-145515-2 T Analysis Batch:460-479312 LCS-Certified Reference Material Solid 460-4785366010CLCSSRM 460-478536/2-A ^4 T Method Blank Solid 460-4785366010CMB 460-478536/1-A ^2 T LCS-Certified Reference Material Solid 460-4791666010CLCSSRM 460-479166/2-A ^4 T Method Blank Solid 460-4791666010CMB 460-479166/1-A ^2 T Duplicate Solid 460-4785366010C460-145281-A-1-B DU ^4 T Matrix Spike Solid 460-4785366010C460-145281-A-1-C MS ^4 T Solid 460-478536SB-8(1-2.5)6010C460-145401-1 T Solid 460-478536SB-7(5-7)6010C460-145401-2 T Solid 460-478536SB-6(5-7)6010C460-145401-3 T Solid 460-478536SB-3(0-2)6010C460-145401-4 T Solid 460-478536SB-5(0-2)6010C460-145401-5 T Solid 460-478536SB-4(0-2)6010C460-145401-6 T Duplicate Solid 460-4791666010C460-145501-B-1-C DU ^4 T Matrix Spike Solid 460-4791666010C460-145501-B-1-D MS ^4 T Solid 460-479166SB-2 (0-2)6010C460-145515-1 T Solid 460-479166SB-1 (0-2)6010C460-145515-2 T Analysis Batch:460-479612 Solid 460-478536SB-5(0-2)6010C460-145401-5 T Solid 460-479166SB-2 (0-2)6010C460-145515-1 T Solid 460-479166SB-1 (0-2)6010C460-145515-2 T Report Basis T = Total TestAmerica Edison Page 115 of 194 Quality Control Results Client: AKRF Inc Job Number: 460-145401-1 QC Association Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis General Chemistry Analysis Batch:460-478966 SolidSB-8(1-2.5)Moisture460-145401-1 T SolidSB-7(5-7)Moisture460-145401-2 T SolidSB-6(5-7)Moisture460-145401-3 T Duplicate Solid Moisture460-145401-3DU T Analysis Batch:460-478972 SolidSB-3(0-2)Moisture460-145401-4 T SolidSB-5(0-2)Moisture460-145401-5 T SolidSB-4(0-2)Moisture460-145401-6 T Duplicate Solid Moisture460-145407-B-8 DU T Analysis Batch:460-479372 SolidSB-2 (0-2)Moisture460-145515-1 T SolidSB-1 (0-2)Moisture460-145515-2 T Duplicate Solid Moisture460-145555-E-1 DU T Report Basis T = Total TestAmerica Edison Page 116 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Surrogate Recovery Report 8260C Volatile Organic Compounds by GC/MS Client Matrix: Solid Lab Sample ID Client Sample ID DCA BFB DBFM TOL %Rec %Rec %Rec %Rec 460-145401-1 SB-8(1-2.5)110 98 104 107 460-145401-2 SB-7(5-7)103 91 98 99 460-145401-3 SB-6(5-7)118 101 111 115 460-145401-4 SB-3(0-2)112 103 108 113 460-145401-5 SB-5(0-2)103 90 97 102 460-145401-6 SB-4(0-2)101 89 95 99 460-145515-1 SB-2 (0-2)109 87 98 85 460-145515-2 SB-1 (0-2)105 89 95 87 MB 460-479592/8 105 98 102 110 MB 460-479706/7 103 91 90 84 MB 460-479876/9 97 89 93 101 LCS 460-479592/4 104 96 105 106 LCS 460-479706/3 94 89 89 86 LCS 460-479876/5 102 93 101 101 LCSD 460-479592/5 103 95 104 105 LCSD 460-479706/4 95 89 91 86 LCSD 460-479876/6 121 112 119 124* Surrogate Acceptance Limits DCA = 1,2-Dichloroethane-d4 (Surr)78-135 BFB = 4-Bromofluorobenzene 67-126 DBFM = Dibromofluoromethane (Surr)61-149 TOL = Toluene-d8 (Surr)73-121 TestAmerica Edison Page 117 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Surrogate Recovery Report 8260C Volatile Organic Compounds by GC/MS Client Matrix: Water Lab Sample ID Client Sample ID DCA BFB DBFM TOL %Rec %Rec %Rec %Rec 460-145597-1 OW-2 101 91 105 100 460-145597-2 OW-1 103 92 107 102 460-145597-3 Trip Blank 98 90 103 100 MB 460-479912/6 103 93 106 103 LCS 460-479912/3 102 101 106 104 LCSD 460-479912/4 100 96 102 100 Surrogate Acceptance Limits DCA = 1,2-Dichloroethane-d4 (Surr)74-132 BFB = 4-Bromofluorobenzene 77-124 DBFM = Dibromofluoromethane (Surr)72-131 TOL = Toluene-d8 (Surr)80-120 TestAmerica Edison Page 118 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Surrogate Recovery Report 8270D Semivolatile Organic Compounds (GC/MS) Client Matrix: Solid Lab Sample ID Client Sample ID FBP NBZ TPHL %Rec %Rec %Rec 460-145401-1 SB-8(1-2.5)50 45 68 460-145401-2 SB-7(5-7)56 52 81 460-145401-3 SB-6(5-7)60 54 90 460-145401-4 SB-3(0-2)55 50 77 460-145401-5 SB-5(0-2)52 47 83 460-145401-6 SB-4(0-2)59 54 83 460-145515-1 SB-2 (0-2)78 69 80 460-145515-2 SB-1 (0-2)68 60 72 MB 460-478451/1-A 69 65 97 MB 460-479261/1-A 102* 83 71 LCS 460-478451/2-A 68 73 68 LCS 460-479261/2-A 100* 88 70 460-145381-C-5-D MS 65 60 76 460-145556-A-1-B MS 79 65 56 460-145381-C-5-E MSD 65 56 72 460-145556-A-1-C MSD 84 70 56 Surrogate Acceptance Limits FBP = 2-Fluorobiphenyl 38-95 NBZ = Nitrobenzene-d5 (Surr)37-94 TPHL = Terphenyl-d14 (Surr)24-109 TestAmerica Edison Page 119 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Surrogate Recovery Report 8270D Semivolatile Organic Compounds (GC/MS) Client Matrix: Water Lab Sample ID Client Sample ID FBP NBZ TPHL %Rec %Rec %Rec 460-145597-1 OW-2 74 85 79 460-145597-2 OW-1 76 81 79 MB 460-479363/1-A 75 79 76 LCS 460-479363/2-A 79 85 80 LCSD 460-479363/3-A 85 90 83 Surrogate Acceptance Limits FBP = 2-Fluorobiphenyl 45-107 NBZ = Nitrobenzene-d5 (Surr)51-108 TPHL = Terphenyl-d14 (Surr)40-148 TestAmerica Edison Page 120 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Surrogate Recovery Report 8081B Organochlorine Pesticides (GC) Client Matrix: Solid Lab Sample ID Client Sample ID DCBP1 DCBP2 TCX1 TCX2 %Rec %Rec %Rec %Rec 460-145401-1 SB-8(1-2.5)112 119 118 123 460-145401-2 SB-7(5-7)111 113 114 117 460-145401-3 SB-6(5-7)99 99 102 102 460-145401-4 SB-3(0-2)116 117 115 116 460-145401-5 SB-5(0-2)118 127 118 127 460-145401-6 SB-4(0-2)111 118 111 118 460-145515-1 SB-2 (0-2)106 106 114 114 460-145515-2 SB-1 (0-2)109 110 116 116 MB 460-478818/1-A 113 119 114 119 MB 460-479140/1-A 95 99 109 107 LCS 460-478818/2-A 108 112 113 112 LCS 460-479140/2-A 98 99 111 102 460-145399-E-1-C MS 113 113 113 115 460-145501-A-1-E MS 102 118 123 109 460-145399-E-1-D MSD 106 107 105 107 460-145501-A-1-F MSD 99 114 119 109 Surrogate Acceptance Limits DCBP = DCB Decachlorobiphenyl 50-150 TCX = Tetrachloro-m-xylene 47-150 TestAmerica Edison Page 121 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Surrogate Recovery Report 8082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography Client Matrix: Solid Lab Sample ID Client Sample ID DCBP1 DCBP2 %Rec %Rec 460-145401-1 SB-8(1-2.5)100 114 460-145401-2 SB-7(5-7)104 120 460-145401-3 SB-6(5-7)86 116 460-145401-4 SB-3(0-2)92 136 460-145401-5 SB-5(0-2)87 123 460-145401-6 SB-4(0-2)98 140 460-145515-1 SB-2 (0-2)122 111 460-145515-2 SB-1 (0-2)139 124 MB 460-478820/1-A 108 125 MB 460-479142/1-A 93 92 LCS 460-478820/2-A 106 126 LCS 460-479142/2-A 131 132 460-145455-A-6-D MS 104 123 460-145501-A-1-H MS 105 103 460-145455-A-6-E MSD 102 119 460-145501-A-1-I MSD 104 110 Surrogate Acceptance Limits DCBP = DCB Decachlorobiphenyl 35-150 TestAmerica Edison Page 122 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc SolidClient Matrix: 1.0Dilution: Lab Sample ID: 11/24/2017 1317 Method Blank - Batch: 460-479592 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: D44657.D 5 mL 5 mLUnits:mg/Kg Method: 8260C Preparation: N/A CVOAMS4MB 460-479592/8 Analysis Date: Analysis Batch: Prep Batch: Leach Batch: 460-479592 N/A N/A Prep Date: Leach Date: N/A N/A Analyte Result Qual MDL RL 0.0010 U 0.00100.000231,1,1-Trichloroethane 0.0010 U 0.00100.000211,1,2,2-Tetrachloroethane 0.0010 U 0.00100.000301,1,2-Trichloro-1,2,2-trifluoroethane 0.0010 U 0.00100.000181,1,2-Trichloroethane 0.0010 U 0.00100.000211,1-Dichloroethane 0.0010 U 0.00100.000231,1-Dichloroethene 0.0010 U 0.00100.000181,2,3-Trichlorobenzene 0.0010 U 0.00100.0000921,2,4-Trichlorobenzene 0.0010 U 0.00100.000461,2-Dibromo-3-Chloropropane 0.0010 U 0.00100.000141,2-Dichlorobenzene 0.0010 U 0.00100.000301,2-Dichloroethane 0.0010 U 0.00100.000421,2-Dichloropropane 0.0010 U 0.00100.000161,3-Dichlorobenzene 0.0010 U 0.00100.000101,4-Dichlorobenzene 0.020 U 0.0200.00921,4-Dioxane 0.0050 U 0.00500.00112-Butanone (MEK) 0.0050 U 0.00500.000782-Hexanone 0.0050 U 0.00500.000664-Methyl-2-pentanone (MIBK) 0.0050 U 0.00500.0038Acetone 0.0010 U 0.00100.00026Benzene 0.0010 U 0.00100.00043Bromoform 0.0010 U 0.00100.00047Bromomethane 0.0010 U 0.00100.00027Carbon disulfide 0.0010 U 0.00100.00018Carbon tetrachloride 0.0010 U 0.00100.00018Chlorobenzene 0.0010 U 0.00100.00028Chlorobromomethane 0.0010 U 0.00100.00019Chlorodibromomethane 0.0010 U 0.00100.00052Chloroethane 0.0010 U 0.00100.00032Chloroform 0.0010 U 0.00100.00044Chloromethane 0.0010 U 0.00100.00015cis-1,2-Dichloroethene 0.0010 U 0.00100.00027cis-1,3-Dichloropropene 0.0010 U 0.00100.00022Cyclohexane 0.0010 U 0.00100.00026Dichlorobromomethane 0.0010 U 0.00100.00034Dichlorodifluoromethane 0.0010 U 0.00100.00020Ethylbenzene 0.0010 U 0.00100.00018Ethylene Dibromide 0.0010 U 0.00100.00013Isopropylbenzene 0.0050 U 0.00500.0043Methyl acetate 0.0010 U 0.00100.00013Methyl tert-butyl ether 0.0010 U 0.00100.00016Methylcyclohexane 0.0010 U 0.00100.00016Methylene Chloride 0.0010 U 0.00100.00017m-Xylene & p-Xylene 0.0010 U 0.00100.000095o-Xylene 0.0010 U 0.00100.00012Styrene TestAmerica Edison Page 123 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc SolidClient Matrix: 1.0Dilution: Lab Sample ID: 11/24/2017 1317 Method Blank - Batch: 460-479592 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: D44657.D 5 mL 5 mLUnits:mg/Kg Method: 8260C Preparation: N/A CVOAMS4MB 460-479592/8 Analysis Date: Analysis Batch: Prep Batch: Leach Batch: 460-479592 N/A N/A Prep Date: Leach Date: N/A N/A Analyte Result Qual MDL RL 0.0010 U 0.00100.00014Tetrachloroethene 0.0010 U 0.00100.00063Toluene 0.0010 U 0.00100.00025trans-1,2-Dichloroethene 0.0010 U 0.00100.00027trans-1,3-Dichloropropene 0.0010 U 0.00100.00014Trichloroethene 0.0010 U 0.00100.00041Trichlorofluoromethane 0.0010 U 0.00100.00055Vinyl chloride Surrogate % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr)105 78 - 135 4-Bromofluorobenzene 98 67 - 126 Dibromofluoromethane (Surr)102 61 - 149 Toluene-d8 (Surr)110 73 - 121 TestAmerica Edison Page 124 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Dilution: Dilution: 11/24/2017 1204 Lab Control Sample/ Lab Control Sample Duplicate Recovery Report - Batch: 460-479592 1.0 1.0 Solid LCS Lab Sample ID: LCSD Lab Sample ID: Client Matrix: Units: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Client Matrix:Solid Units: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: mg/Kg N/A D44653.D 5 mL 5 mL 5 mL D44654.D 5 mL 5 mL 5 mL mg/Kg Method: 8260C Preparation: N/A N/A CVOAMS4 CVOAMS4 LCS 460-479592/4 LCSD 460-479592/5 Analysis Date: Prep Date: Leach Date: 11/24/2017 1140 Analysis Batch: Prep Batch: Leach Batch: 460-479592 Analysis Date: Prep Date: Leach Date: Analysis Batch: Prep Batch: Leach Batch: 460-479592 N/A N/A N/A N/A N/A N/A Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS % Rec. 9897 80 - 125 1 301,1,1-Trichloroethane 107112 72 - 131 5 301,1,2,2-Tetrachloroethane 9995 78 - 132 4 301,1,2-Trichloro-1,2,2-trifluoroethane 102107 76 - 124 4 301,1,2-Trichloroethane 104105 80 - 124 1 301,1-Dichloroethane 9795 79 - 132 2 301,1-Dichloroethene 9598 75 - 123 4 301,2,3-Trichlorobenzene 9296 74 - 124 5 301,2,4-Trichlorobenzene 9195 65 - 129 5 301,2-Dibromo-3-Chloropropane 100103 80 - 121 2 301,2-Dichlorobenzene 104106 68 - 120 2 301,2-Dichloroethane 108108 77 - 124 0 301,2-Dichloropropane 100103 79 - 124 3 301,3-Dichlorobenzene 98102 79 - 121 4 301,4-Dichlorobenzene 97100 67 - 150 3 301,4-Dioxane 10096 61 - 140 4 302-Butanone (MEK) 10097 78 - 120 3 302-Hexanone 10199 80 - 120 2 304-Methyl-2-pentanone (MIBK) 9695 75 - 120 1 30Acetone 99100 75 - 127 1 30Benzene 8790 19 - 150 4 30Bromoform 107109 59 - 136 2 30Bromomethane 9997 74 - 130 2 30Carbon disulfide 9794 77 - 138 3 30Carbon tetrachloride 101102 80 - 120 2 30Chlorobenzene 103104 80 - 125 1 30Chlorobromomethane 98100 67 - 143 3 30Chlorodibromomethane 97100 50 - 139 3 30Chloroethane 103103 80 - 122 0 30Chloroform 116118 66 - 128 2 30Chloromethane 100100 80 - 123 1 30cis-1,2-Dichloroethene 98102 75 - 124 5 30cis-1,3-Dichloropropene 10097 67 - 135 3 30Cyclohexane 9899 76 - 129 1 30Dichlorobromomethane 9188 72 - 127 3 30Dichlorodifluoromethane TestAmerica Edison Page 125 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Dilution: Dilution: 11/24/2017 1204 Lab Control Sample/ Lab Control Sample Duplicate Recovery Report - Batch: 460-479592 1.0 1.0 Solid LCS Lab Sample ID: LCSD Lab Sample ID: Client Matrix: Units: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Client Matrix:Solid Units: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: mg/Kg N/A D44653.D 5 mL 5 mL 5 mL D44654.D 5 mL 5 mL 5 mL mg/Kg Method: 8260C Preparation: N/A N/A CVOAMS4 CVOAMS4 LCS 460-479592/4 LCSD 460-479592/5 Analysis Date: Prep Date: Leach Date: 11/24/2017 1140 Analysis Batch: Prep Batch: Leach Batch: 460-479592 Analysis Date: Prep Date: Leach Date: Analysis Batch: Prep Batch: Leach Batch: 460-479592 N/A N/A N/A N/A N/A N/A Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS % Rec. 99103 79 - 124 3 30Ethylbenzene 99101 80 - 122 2 30Ethylene Dibromide 100102 80 - 125 2 30Isopropylbenzene 106110 73 - 123 4 30Methyl acetate 101104 80 - 120 3 30Methyl tert-butyl ether 104100 71 - 137 3 30Methylcyclohexane 104106 79 - 128 2 30Methylene Chloride 97100 79 - 121 3 30m-Xylene & p-Xylene 100103 79 - 123 2 30o-Xylene 97101 78 - 123 5 30Styrene 9493 73 - 130 1 30Tetrachloroethene 9195 75 - 122 4 30Toluene 100100 80 - 129 1 30trans-1,2-Dichloroethene 9596 72 - 121 1 30trans-1,3-Dichloropropene 9695 79 - 122 1 30Trichloroethene 8889 68 - 136 1 30Trichlorofluoromethane 116121 70 - 134 4 30Vinyl chloride Surrogate LCS % Rec LCSD % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr)104 103 78 - 135 4-Bromofluorobenzene 96 95 67 - 126 Dibromofluoromethane (Surr)105 104 61 - 149 Toluene-d8 (Surr)106 105 73 - 121 TestAmerica Edison Page 126 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc SolidClient Matrix: 1.0Dilution: Lab Sample ID: 11/24/2017 2153 Method Blank - Batch: 460-479706 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: B23988.D 5 mL 5 mLUnits:mg/Kg Method: 8260C Preparation: N/A CVOAMS2MB 460-479706/7 Analysis Date: Analysis Batch: Prep Batch: Leach Batch: 460-479706 N/A N/A Prep Date: Leach Date: N/A N/A Analyte Result Qual MDL RL 0.0010 U 0.00100.000231,1,1-Trichloroethane 0.0010 U 0.00100.000211,1,2,2-Tetrachloroethane 0.0010 U 0.00100.000301,1,2-Trichloro-1,2,2-trifluoroethane 0.0010 U 0.00100.000181,1,2-Trichloroethane 0.0010 U 0.00100.000211,1-Dichloroethane 0.0010 U 0.00100.000231,1-Dichloroethene 0.0010 U 0.00100.000181,2,3-Trichlorobenzene 0.0010 U 0.00100.0000921,2,4-Trichlorobenzene 0.0010 U 0.00100.000461,2-Dibromo-3-Chloropropane 0.0010 U 0.00100.000141,2-Dichlorobenzene 0.0010 U 0.00100.000301,2-Dichloroethane 0.0010 U 0.00100.000421,2-Dichloropropane 0.0010 U 0.00100.000161,3-Dichlorobenzene 0.0010 U 0.00100.000101,4-Dichlorobenzene 0.020 U 0.0200.00921,4-Dioxane 0.0050 U 0.00500.00112-Butanone (MEK) 0.0050 U 0.00500.000782-Hexanone 0.0050 U 0.00500.000664-Methyl-2-pentanone (MIBK) 0.0050 U 0.00500.0038Acetone 0.0010 U 0.00100.00026Benzene 0.0010 U 0.00100.00043Bromoform 0.0010 U 0.00100.00047Bromomethane 0.0010 U 0.00100.00027Carbon disulfide 0.0010 U 0.00100.00018Carbon tetrachloride 0.0010 U 0.00100.00018Chlorobenzene 0.0010 U 0.00100.00028Chlorobromomethane 0.0010 U 0.00100.00019Chlorodibromomethane 0.0010 U 0.00100.00052Chloroethane 0.0010 U 0.00100.00032Chloroform 0.0010 U 0.00100.00044Chloromethane 0.0010 U 0.00100.00015cis-1,2-Dichloroethene 0.0010 U 0.00100.00027cis-1,3-Dichloropropene 0.0010 U 0.00100.00022Cyclohexane 0.0010 U 0.00100.00026Dichlorobromomethane 0.0010 U 0.00100.00034Dichlorodifluoromethane 0.0010 U 0.00100.00020Ethylbenzene 0.0010 U 0.00100.00018Ethylene Dibromide 0.0010 U 0.00100.00013Isopropylbenzene 0.0050 U 0.00500.0043Methyl acetate 0.0010 U 0.00100.00013Methyl tert-butyl ether 0.0010 U 0.00100.00016Methylcyclohexane 0.0010 U 0.00100.00016Methylene Chloride 0.0010 U 0.00100.00017m-Xylene & p-Xylene 0.0010 U 0.00100.000095o-Xylene 0.0010 U 0.00100.00012Styrene TestAmerica Edison Page 127 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc SolidClient Matrix: 1.0Dilution: Lab Sample ID: 11/24/2017 2153 Method Blank - Batch: 460-479706 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: B23988.D 5 mL 5 mLUnits:mg/Kg Method: 8260C Preparation: N/A CVOAMS2MB 460-479706/7 Analysis Date: Analysis Batch: Prep Batch: Leach Batch: 460-479706 N/A N/A Prep Date: Leach Date: N/A N/A Analyte Result Qual MDL RL 0.0010 U 0.00100.00014Tetrachloroethene 0.0010 U 0.00100.00063Toluene 0.0010 U 0.00100.00025trans-1,2-Dichloroethene 0.0010 U 0.00100.00027trans-1,3-Dichloropropene 0.0010 U 0.00100.00014Trichloroethene 0.0010 U 0.00100.00041Trichlorofluoromethane 0.0010 U 0.00100.00055Vinyl chloride Surrogate % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr)103 78 - 135 4-Bromofluorobenzene 91 67 - 126 Dibromofluoromethane (Surr)90 61 - 149 Toluene-d8 (Surr)84 73 - 121 TestAmerica Edison Page 128 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Dilution: Dilution: 11/24/2017 2040 Lab Control Sample/ Lab Control Sample Duplicate Recovery Report - Batch: 460-479706 1.0 1.0 Solid LCS Lab Sample ID: LCSD Lab Sample ID: Client Matrix: Units: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Client Matrix:Solid Units: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: mg/Kg N/A B23984.D 5 mL 5 mL 5 mL B23985.D 5 mL 5 mL 5 mL mg/Kg Method: 8260C Preparation: N/A N/A CVOAMS2 CVOAMS2 LCS 460-479706/3 LCSD 460-479706/4 Analysis Date: Prep Date: Leach Date: 11/24/2017 2016 Analysis Batch: Prep Batch: Leach Batch: 460-479706 Analysis Date: Prep Date: Leach Date: Analysis Batch: Prep Batch: Leach Batch: 460-479706 N/A N/A N/A N/A N/A N/A Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS % Rec. 105107 80 - 125 1 301,1,1-Trichloroethane 123134 72 - 131 9 30 *1,1,2,2-Tetrachloroethane 9797 78 - 132 0 301,1,2-Trichloro-1,2,2-trifluoroethane 9799 76 - 124 2 301,1,2-Trichloroethane 99103 80 - 124 4 301,1-Dichloroethane 8989 79 - 132 1 301,1-Dichloroethene 116126 75 - 123 8 30 *1,2,3-Trichlorobenzene 113115 74 - 124 2 301,2,4-Trichlorobenzene 134156 65 - 129 15 30 **1,2-Dibromo-3-Chloropropane 99105 80 - 121 6 301,2-Dichlorobenzene 100104 68 - 120 4 301,2-Dichloroethane 98100 77 - 124 2 301,2-Dichloropropane 103103 79 - 124 1 301,3-Dichlorobenzene 9599 79 - 121 5 301,4-Dichlorobenzene 106110 67 - 150 4 301,4-Dioxane 7876 61 - 140 2 302-Butanone (MEK) 8390 78 - 120 8 302-Hexanone 8889 80 - 120 2 304-Methyl-2-pentanone (MIBK) 8284 75 - 120 3 30Acetone 9395 75 - 127 2 30Benzene 92104 19 - 150 12 30Bromoform 129123 59 - 136 5 30Bromomethane 9293 74 - 130 1 30Carbon disulfide 109109 77 - 138 0 30Carbon tetrachloride 9294 80 - 120 3 30Chlorobenzene 8995 80 - 125 6 30Chlorobromomethane 90103 67 - 143 14 30Chlorodibromomethane 112108 50 - 139 4 30Chloroethane 9998 80 - 122 1 30Chloroform 10195 66 - 128 6 30Chloromethane 9087 80 - 123 3 30cis-1,2-Dichloroethene 97104 75 - 124 7 30cis-1,3-Dichloropropene 9696 67 - 135 0 30Cyclohexane 97103 76 - 129 6 30Dichlorobromomethane 8383 72 - 127 1 30Dichlorodifluoromethane TestAmerica Edison Page 129 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Dilution: Dilution: 11/24/2017 2040 Lab Control Sample/ Lab Control Sample Duplicate Recovery Report - Batch: 460-479706 1.0 1.0 Solid LCS Lab Sample ID: LCSD Lab Sample ID: Client Matrix: Units: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Client Matrix:Solid Units: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: mg/Kg N/A B23984.D 5 mL 5 mL 5 mL B23985.D 5 mL 5 mL 5 mL mg/Kg Method: 8260C Preparation: N/A N/A CVOAMS2 CVOAMS2 LCS 460-479706/3 LCSD 460-479706/4 Analysis Date: Prep Date: Leach Date: 11/24/2017 2016 Analysis Batch: Prep Batch: Leach Batch: 460-479706 Analysis Date: Prep Date: Leach Date: Analysis Batch: Prep Batch: Leach Batch: 460-479706 N/A N/A N/A N/A N/A N/A Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS % Rec. 9191 79 - 124 0 30Ethylbenzene 8999 80 - 122 11 30Ethylene Dibromide 99100 80 - 125 2 30Isopropylbenzene 107123 73 - 123 14 30Methyl acetate 94100 80 - 120 6 30Methyl tert-butyl ether 97100 71 - 137 3 30Methylcyclohexane 8790 79 - 128 3 30Methylene Chloride 8990 79 - 121 2 30m-Xylene & p-Xylene 8993 79 - 123 4 30o-Xylene 9494 78 - 123 0 30Styrene 96101 73 - 130 5 30Tetrachloroethene 8892 75 - 122 5 30Toluene 9292 80 - 129 0 30trans-1,2-Dichloroethene 95107 72 - 121 12 30trans-1,3-Dichloropropene 8486 79 - 122 2 30Trichloroethene 9486 68 - 136 8 30Trichlorofluoromethane 119115 70 - 134 3 30Vinyl chloride Surrogate LCS % Rec LCSD % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr)94 95 78 - 135 4-Bromofluorobenzene 89 89 67 - 126 Dibromofluoromethane (Surr)89 91 61 - 149 Toluene-d8 (Surr)86 86 73 - 121 TestAmerica Edison Page 130 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc SolidClient Matrix: 1.0Dilution: Lab Sample ID: 11/25/2017 2033 Method Blank - Batch: 460-479876 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: D44718.D 5 mL 5 mLUnits:mg/Kg Method: 8260C Preparation: N/A CVOAMS4MB 460-479876/9 Analysis Date: Analysis Batch: Prep Batch: Leach Batch: 460-479876 N/A N/A Prep Date: Leach Date: N/A N/A Analyte Result Qual MDL RL 0.0010 U 0.00100.000231,1,1-Trichloroethane 0.0010 U 0.00100.000211,1,2,2-Tetrachloroethane 0.0010 U 0.00100.000301,1,2-Trichloro-1,2,2-trifluoroethane 0.0010 U 0.00100.000181,1,2-Trichloroethane 0.0010 U 0.00100.000211,1-Dichloroethane 0.0010 U 0.00100.000231,1-Dichloroethene 0.0010 U 0.00100.000181,2,3-Trichlorobenzene 0.0010 U 0.00100.0000921,2,4-Trichlorobenzene 0.0010 U 0.00100.000461,2-Dibromo-3-Chloropropane 0.0010 U 0.00100.000141,2-Dichlorobenzene 0.0010 U 0.00100.000301,2-Dichloroethane 0.0010 U 0.00100.000421,2-Dichloropropane 0.0010 U 0.00100.000161,3-Dichlorobenzene 0.0010 U 0.00100.000101,4-Dichlorobenzene 0.020 U 0.0200.00921,4-Dioxane 0.0050 U 0.00500.00112-Butanone (MEK) 0.0050 U 0.00500.000782-Hexanone 0.0050 U 0.00500.000664-Methyl-2-pentanone (MIBK) 0.0050 U 0.00500.0038Acetone 0.0010 U 0.00100.00026Benzene 0.0010 U 0.00100.00043Bromoform 0.0010 U 0.00100.00047Bromomethane 0.0010 U 0.00100.00027Carbon disulfide 0.0010 U 0.00100.00018Carbon tetrachloride 0.0010 U 0.00100.00018Chlorobenzene 0.0010 U 0.00100.00028Chlorobromomethane 0.0010 U 0.00100.00019Chlorodibromomethane 0.0010 U 0.00100.00052Chloroethane 0.0010 U 0.00100.00032Chloroform 0.0010 U 0.00100.00044Chloromethane 0.0010 U 0.00100.00015cis-1,2-Dichloroethene 0.0010 U 0.00100.00027cis-1,3-Dichloropropene 0.0010 U 0.00100.00022Cyclohexane 0.0010 U 0.00100.00026Dichlorobromomethane 0.0010 U 0.00100.00034Dichlorodifluoromethane 0.0010 U 0.00100.00020Ethylbenzene 0.0010 U 0.00100.00018Ethylene Dibromide 0.0010 U 0.00100.00013Isopropylbenzene 0.0050 U 0.00500.0043Methyl acetate 0.0010 U 0.00100.00013Methyl tert-butyl ether 0.0010 U 0.00100.00016Methylcyclohexane 0.0010 U 0.00100.00016Methylene Chloride 0.0010 U 0.00100.00017m-Xylene & p-Xylene 0.0010 U 0.00100.000095o-Xylene 0.0010 U 0.00100.00012Styrene TestAmerica Edison Page 131 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc SolidClient Matrix: 1.0Dilution: Lab Sample ID: 11/25/2017 2033 Method Blank - Batch: 460-479876 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: D44718.D 5 mL 5 mLUnits:mg/Kg Method: 8260C Preparation: N/A CVOAMS4MB 460-479876/9 Analysis Date: Analysis Batch: Prep Batch: Leach Batch: 460-479876 N/A N/A Prep Date: Leach Date: N/A N/A Analyte Result Qual MDL RL 0.0010 U 0.00100.00014Tetrachloroethene 0.0010 U 0.00100.00063Toluene 0.0010 U 0.00100.00025trans-1,2-Dichloroethene 0.0010 U 0.00100.00027trans-1,3-Dichloropropene 0.0010 U 0.00100.00014Trichloroethene 0.0010 U 0.00100.00041Trichlorofluoromethane 0.0010 U 0.00100.00055Vinyl chloride Surrogate % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr)97 78 - 135 4-Bromofluorobenzene 89 67 - 126 Dibromofluoromethane (Surr)93 61 - 149 Toluene-d8 (Surr)101 73 - 121 TestAmerica Edison Page 132 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Dilution: Dilution: 11/25/2017 1904 Lab Control Sample/ Lab Control Sample Duplicate Recovery Report - Batch: 460-479876 1.0 1.0 Solid LCS Lab Sample ID: LCSD Lab Sample ID: Client Matrix: Units: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Client Matrix:Solid Units: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: mg/Kg N/A D44714.D 5 mL 5 mL 5 mL D44715.D 5 mL 5 mL 5 mL mg/Kg Method: 8260C Preparation: N/A N/A CVOAMS4 CVOAMS4 LCS 460-479876/5 LCSD 460-479876/6 Analysis Date: Prep Date: Leach Date: 11/25/2017 1839 Analysis Batch: Prep Batch: Leach Batch: 460-479876 Analysis Date: Prep Date: Leach Date: Analysis Batch: Prep Batch: Leach Batch: 460-479876 N/A N/A N/A N/A N/A N/A Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS % Rec. 11195 80 - 125 15 301,1,1-Trichloroethane 124107 72 - 131 15 301,1,2,2-Tetrachloroethane 10893 78 - 132 15 301,1,2-Trichloro-1,2,2-trifluoroethane 118100 76 - 124 16 301,1,2-Trichloroethane 123106 80 - 124 14 301,1-Dichloroethane 11294 79 - 132 17 301,1-Dichloroethene 10893 75 - 123 15 301,2,3-Trichlorobenzene 10391 74 - 124 12 301,2,4-Trichlorobenzene 10187 65 - 129 15 301,2-Dibromo-3-Chloropropane 11399 80 - 121 13 301,2-Dichlorobenzene 120106 68 - 120 13 301,2-Dichloroethane 123110 77 - 124 12 301,2-Dichloropropane 11298 79 - 124 13 301,3-Dichlorobenzene 11297 79 - 121 14 301,4-Dichlorobenzene 113101 67 - 150 11 301,4-Dioxane 11296 61 - 140 15 302-Butanone (MEK) 11198 78 - 120 12 302-Hexanone 114100 80 - 120 13 304-Methyl-2-pentanone (MIBK) 10894 75 - 120 14 30Acetone 11496 75 - 127 17 30Benzene 9884 19 - 150 15 30Bromoform 125107 59 - 136 16 30Bromomethane 10891 74 - 130 17 30Carbon disulfide 10792 77 - 138 15 30Carbon tetrachloride 11698 80 - 120 17 30Chlorobenzene 119104 80 - 125 14 30Chlorobromomethane 11193 67 - 143 17 30Chlorodibromomethane 11499 50 - 139 15 30Chloroethane 119103 80 - 122 14 30Chloroform 132115 66 - 128 14 30 *Chloromethane 114100 80 - 123 13 30cis-1,2-Dichloroethene 11194 75 - 124 17 30cis-1,3-Dichloropropene 11497 67 - 135 16 30Cyclohexane 11396 76 - 129 16 30Dichlorobromomethane 10591 72 - 127 14 30Dichlorodifluoromethane TestAmerica Edison Page 133 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Dilution: Dilution: 11/25/2017 1904 Lab Control Sample/ Lab Control Sample Duplicate Recovery Report - Batch: 460-479876 1.0 1.0 Solid LCS Lab Sample ID: LCSD Lab Sample ID: Client Matrix: Units: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Client Matrix:Solid Units: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: mg/Kg N/A D44714.D 5 mL 5 mL 5 mL D44715.D 5 mL 5 mL 5 mL mg/Kg Method: 8260C Preparation: N/A N/A CVOAMS4 CVOAMS4 LCS 460-479876/5 LCSD 460-479876/6 Analysis Date: Prep Date: Leach Date: 11/25/2017 1839 Analysis Batch: Prep Batch: Leach Batch: 460-479876 Analysis Date: Prep Date: Leach Date: Analysis Batch: Prep Batch: Leach Batch: 460-479876 N/A N/A N/A N/A N/A N/A Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS % Rec. 11598 79 - 124 16 30Ethylbenzene 11697 80 - 122 17 30Ethylene Dibromide 11599 80 - 125 15 30Isopropylbenzene 127110 73 - 123 15 30 *Methyl acetate 117103 80 - 120 13 30Methyl tert-butyl ether 11599 71 - 137 15 30Methylcyclohexane 120104 79 - 128 14 30Methylene Chloride 11296 79 - 121 16 30m-Xylene & p-Xylene 11499 79 - 123 14 30o-Xylene 11499 78 - 123 14 30Styrene 10689 73 - 130 18 30Tetrachloroethene 10690 75 - 122 16 30Toluene 11499 80 - 129 14 30trans-1,2-Dichloroethene 10691 72 - 121 15 30trans-1,3-Dichloropropene 10895 79 - 122 14 30Trichloroethene 10491 68 - 136 14 30Trichlorofluoromethane 127114 70 - 134 11 30Vinyl chloride Surrogate LCS % Rec LCSD % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr)102 121 78 - 135 4-Bromofluorobenzene 93 112 67 - 126 Dibromofluoromethane (Surr)101 119 61 - 149 Toluene-d8 (Surr)101 124 73 - 121* TestAmerica Edison Page 134 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc WaterClient Matrix: 1.0Dilution: Lab Sample ID: 11/26/2017 1051 Method Blank - Batch: 460-479912 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: P37891.D 5 mL 5 mLUnits:ug/L Method: 8260C Preparation: 5030C CVOAMS13MB 460-479912/6 Analysis Date: Analysis Batch: Prep Batch: Leach Batch: 460-479912 N/A N/A Prep Date: 11/26/2017 1051 Leach Date:N/A Analyte Result Qual MDL RL 1.0 U 1.00.281,1,1-Trichloroethane 1.0 U 1.00.191,1,2,2-Tetrachloroethane 1.0 U 1.00.341,1,2-Trichloro-1,2,2-trifluoroethane 1.0 U 1.00.0801,1,2-Trichloroethane 1.0 U 1.00.241,1-Dichloroethane 1.0 U 1.00.341,1-Dichloroethene 1.0 U 1.00.351,2,3-Trichlorobenzene 1.0 U 1.00.271,2,4-Trichlorobenzene 1.0 U 1.00.231,2-Dibromo-3-Chloropropane 1.0 U 1.00.221,2-Dichlorobenzene 1.0 U 1.00.251,2-Dichloroethane 1.0 U 1.00.181,2-Dichloropropane 1.0 U 1.00.331,3-Dichlorobenzene 1.0 U 1.00.331,4-Dichlorobenzene 50 U 508.71,4-Dioxane 5.0 U 5.02.22-Butanone (MEK) 5.0 U 5.00.722-Hexanone 5.0 U 5.00.634-Methyl-2-pentanone (MIBK) 5.0 U 5.01.1Acetone 1.0 U 1.00.090Benzene 1.0 U 1.00.18Bromoform 1.0 U 1.00.18Bromomethane 1.0 U 1.00.22Carbon disulfide 1.0 U 1.00.33Carbon tetrachloride 1.0 U 1.00.24Chlorobenzene 1.0 U 1.00.30Chlorobromomethane 1.0 U 1.00.22Chlorodibromomethane 1.0 U 1.00.37Chloroethane 1.0 U 1.00.22Chloroform 1.0 U 1.00.22Chloromethane 1.0 U 1.00.26cis-1,2-Dichloroethene 1.0 U 1.00.16cis-1,3-Dichloropropene 1.0 U 1.00.26Cyclohexane 1.0 U 1.00.15Dichlorobromomethane 1.0 U 1.00.14Dichlorodifluoromethane 1.0 U 1.00.30Ethylbenzene 1.0 U 1.00.19Ethylene Dibromide 1.0 U 1.00.32Isopropylbenzene 5.0 U 5.00.58Methyl acetate 1.0 U 1.00.13Methyl tert-butyl ether 1.0 U 1.00.22Methylcyclohexane 1.0 U 1.00.21Methylene Chloride 1.0 U 1.00.28m-Xylene & p-Xylene 1.0 U 1.00.32o-Xylene 1.0 U 1.00.17Styrene TestAmerica Edison Page 135 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc WaterClient Matrix: 1.0Dilution: Lab Sample ID: 11/26/2017 1051 Method Blank - Batch: 460-479912 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: P37891.D 5 mL 5 mLUnits:ug/L Method: 8260C Preparation: 5030C CVOAMS13MB 460-479912/6 Analysis Date: Analysis Batch: Prep Batch: Leach Batch: 460-479912 N/A N/A Prep Date: 11/26/2017 1051 Leach Date:N/A Analyte Result Qual MDL RL 1.0 U 1.00.12Tetrachloroethene 1.0 U 1.00.25Toluene 1.0 U 1.00.18trans-1,2-Dichloroethene 1.0 U 1.00.19trans-1,3-Dichloropropene 1.0 U 1.00.22Trichloroethene 1.0 U 1.00.15Trichlorofluoromethane 1.0 U 1.00.060Vinyl chloride Surrogate % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr)103 74 - 132 4-Bromofluorobenzene 93 77 - 124 Dibromofluoromethane (Surr)106 72 - 131 Toluene-d8 (Surr)103 80 - 120 TestAmerica Edison Page 136 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Dilution: Dilution: 11/26/2017 0937 Lab Control Sample/ Lab Control Sample Duplicate Recovery Report - Batch: 460-479912 1.0 1.0 Water LCS Lab Sample ID: LCSD Lab Sample ID: Client Matrix: Units: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Client Matrix:Water Units: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: ug/L P37888.D 5 mL 5 mL 5 mL P37889.D 5 mL 5 mL 5 mL ug/L 11/26/2017 0937 Method: 8260C Preparation: 5030C CVOAMS13 CVOAMS13 LCS 460-479912/3 LCSD 460-479912/4 Analysis Date: Prep Date: Leach Date: 11/26/2017 0902 11/26/2017 0902 Analysis Batch: Prep Batch: Leach Batch: 460-479912 Analysis Date: Prep Date: Leach Date: Analysis Batch: Prep Batch: Leach Batch: 460-479912 N/A N/A N/A N/A N/A N/A Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS % Rec. 99103 75 - 125 4 301,1,1-Trichloroethane 100103 74 - 120 3 301,1,2,2-Tetrachloroethane 8590 59 - 150 5 301,1,2-Trichloro-1,2,2-trifluoroethane 100102 78 - 120 3 301,1,2-Trichloroethane 105109 77 - 123 5 301,1-Dichloroethane 98102 74 - 123 3 301,1-Dichloroethene 98103 78 - 131 5 301,2,3-Trichlorobenzene 98100 80 - 124 3 301,2,4-Trichlorobenzene 8689 55 - 134 3 301,2-Dibromo-3-Chloropropane 104109 80 - 120 4 301,2-Dichlorobenzene 99102 76 - 121 3 301,2-Dichloroethane 106110 77 - 123 4 301,2-Dichloropropane 104107 80 - 120 4 301,3-Dichlorobenzene 103105 80 - 120 2 301,4-Dichlorobenzene 100106 10 - 150 5 301,4-Dioxane 8993 64 - 120 4 302-Butanone (MEK) 100103 71 - 125 3 302-Hexanone 103107 78 - 124 4 304-Methyl-2-pentanone (MIBK) 9292 39 - 150 0 30Acetone 103106 77 - 121 2 30Benzene 96100 53 - 120 3 30Bromoform 9190 10 - 150 1 30Bromomethane 103106 69 - 133 3 30Carbon disulfide 97101 70 - 132 4 30Carbon tetrachloride 102105 80 - 120 3 30Chlorobenzene 104108 77 - 127 4 30Chlorobromomethane 100103 73 - 120 3 30Chlorodibromomethane 135142 52 - 150 5 30Chloroethane 102105 80 - 120 3 30Chloroform 8789 56 - 131 3 30Chloromethane 103105 80 - 120 2 30cis-1,2-Dichloroethene 101103 77 - 120 2 30cis-1,3-Dichloropropene 9092 56 - 150 2 30Cyclohexane 101104 76 - 120 4 30Dichlorobromomethane 6067 50 - 131 12 30Dichlorodifluoromethane TestAmerica Edison Page 137 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Dilution: Dilution: 11/26/2017 0937 Lab Control Sample/ Lab Control Sample Duplicate Recovery Report - Batch: 460-479912 1.0 1.0 Water LCS Lab Sample ID: LCSD Lab Sample ID: Client Matrix: Units: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Client Matrix:Water Units: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: ug/L P37888.D 5 mL 5 mL 5 mL P37889.D 5 mL 5 mL 5 mL ug/L 11/26/2017 0937 Method: 8260C Preparation: 5030C CVOAMS13 CVOAMS13 LCS 460-479912/3 LCSD 460-479912/4 Analysis Date: Prep Date: Leach Date: 11/26/2017 0902 11/26/2017 0902 Analysis Batch: Prep Batch: Leach Batch: 460-479912 Analysis Date: Prep Date: Leach Date: Analysis Batch: Prep Batch: Leach Batch: 460-479912 N/A N/A N/A N/A N/A N/A Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS % Rec. 102105 80 - 120 3 30Ethylbenzene 97101 80 - 120 4 30Ethylene Dibromide 103107 80 - 123 4 30Isopropylbenzene 110115 66 - 144 4 30Methyl acetate 100102 79 - 122 2 30Methyl tert-butyl ether 8891 61 - 145 4 30Methylcyclohexane 103106 77 - 123 3 30Methylene Chloride 102105 80 - 120 4 30m-Xylene & p-Xylene 99103 80 - 120 4 30o-Xylene 101104 80 - 120 3 30Styrene 101102 78 - 122 2 30Tetrachloroethene 102105 80 - 120 3 30Toluene 102105 79 - 120 3 30trans-1,2-Dichloroethene 102104 76 - 120 2 30trans-1,3-Dichloropropene 102106 77 - 120 4 30Trichloroethene 9193 71 - 143 2 30Trichlorofluoromethane 8691 62 - 138 6 30Vinyl chloride Surrogate LCS % Rec LCSD % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr)102 100 74 - 132 4-Bromofluorobenzene 101 96 77 - 124 Dibromofluoromethane (Surr)106 102 72 - 131 Toluene-d8 (Surr)104 100 80 - 120 TestAmerica Edison Page 138 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc SolidClient Matrix: 1.0Dilution: Lab Sample ID: 11/19/2017 2226 Method Blank - Batch: 460-478451 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: L205267.D 15.0000 g 1 mLUnits:mg/Kg Method: 8270D Preparation: 3546 CBNAMS12MB 460-478451/1-A Analysis Date: Analysis Batch: Prep Batch: Leach Batch: 460-478510 460-478451 N/A Prep Date:Injection Volume:11/19/2017 0938 1 uL Leach Date:N/A Analyte Result Qual MDL RL 0.033 U 0.0330.00731,2,4-Trichlorobenzene 0.33 U 0.330.0111,2-Dichlorobenzene 0.33 U 0.330.0261,3-Dichlorobenzene 0.33 U 0.330.0261,4-Dichlorobenzene 0.33 U 0.330.0142,2'-oxybis[1-chloropropane] 0.067 U 0.0670.0132,4-Dinitrotoluene 0.067 U 0.0670.0182,6-Dinitrotoluene 0.33 U 0.330.00752-Chloronaphthalene 0.33 U 0.330.00732-Methylnaphthalene 0.33 U 0.330.0112-Nitroaniline 0.13 U 0.130.0373,3'-Dichlorobenzidine 0.33 U 0.330.00983-Nitroaniline 0.33 U 0.330.0104-Bromophenyl phenyl ether 0.33 U 0.330.00854-Chloroaniline 0.33 U 0.330.00994-Chlorophenyl phenyl ether 0.33 U 0.330.0134-Nitroaniline 0.33 U 0.330.0080Acenaphthene 0.33 U 0.330.0085Acenaphthylene 0.33 U 0.330.031Anthracene 0.033 U 0.0330.028Benzo[a]anthracene 0.033 U 0.0330.010Benzo[a]pyrene 0.033 U 0.0330.013Benzo[b]fluoranthene 0.33 U 0.330.019Benzo[g,h,i]perylene 0.033 U 0.0330.014Benzo[k]fluoranthene 0.33 U 0.330.010Bis(2-chloroethoxy)methane 0.033 U 0.0330.0078Bis(2-chloroethyl)ether 0.33 U 0.330.013Bis(2-ethylhexyl) phthalate 0.33 U 0.330.010Butyl benzyl phthalate 0.33 U 0.330.0082Carbazole 0.33 U 0.330.0090Chrysene 0.033 U 0.0330.017Dibenz(a,h)anthracene 0.33 U 0.330.010Dibenzofuran 0.33 U 0.330.0094Diethyl phthalate 0.33 U 0.330.0096Dimethyl phthalate 0.33 U 0.330.0099Di-n-butyl phthalate 0.33 U 0.330.017Di-n-octyl phthalate 0.33 U 0.330.0098Fluoranthene 0.33 U 0.330.0072Fluorene 0.033 U 0.0330.013Hexachlorobenzene 0.067 U 0.0670.0093Hexachlorobutadiene 0.33 U 0.330.021Hexachlorocyclopentadiene 0.033 U 0.0330.012Hexachloroethane 0.033 U 0.0330.022Indeno[1,2,3-cd]pyrene 0.13 U 0.130.0071Isophorone 0.33 U 0.330.0084Naphthalene TestAmerica Edison Page 139 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc SolidClient Matrix: 1.0Dilution: Lab Sample ID: 11/19/2017 2226 Method Blank - Batch: 460-478451 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: L205267.D 15.0000 g 1 mLUnits:mg/Kg Method: 8270D Preparation: 3546 CBNAMS12MB 460-478451/1-A Analysis Date: Analysis Batch: Prep Batch: Leach Batch: 460-478510 460-478451 N/A Prep Date:Injection Volume:11/19/2017 0938 1 uL Leach Date:N/A Analyte Result Qual MDL RL 0.033 U 0.0330.010Nitrobenzene 0.033 U 0.0330.011N-Nitrosodi-n-propylamine 0.33 U 0.330.030N-Nitrosodiphenylamine 0.33 U 0.330.0088Phenanthrene 0.33 U 0.330.015Pyrene Surrogate % Rec Acceptance Limits 2-Fluorobiphenyl 69 38 - 95 Nitrobenzene-d5 (Surr)65 37 - 94 Terphenyl-d14 (Surr)97 24 - 109 TestAmerica Edison Page 140 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Solid 1.0 Lab Control Sample - Batch: 460-478451 Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Z483637.D 15.0000 g 1 mLUnits:mg/Kg Method: 8270D Preparation: 3546 CBNAMS11LCS 460-478451/2-A Analysis Date: 11/20/2017 0925 Analysis Batch: Prep Batch: Leach Batch: 460-478549 460-478451 N/A Prep Date:Injection Volume:1 uL Leach Date: 11/19/2017 0938 N/A Analyte QualLimit% Rec.ResultSpike Amount 3.33 2.29 69 62 - 1041,2,4-Trichlorobenzene 3.33 2.30 69 64 - 981,2-Dichlorobenzene 3.33 2.26 68 62 - 961,3-Dichlorobenzene 3.33 2.31 69 63 - 971,4-Dichlorobenzene 3.33 3.37 101 39 - 1222,2'-oxybis[1-chloropropane] 3.33 2.76 83 66 - 1222,4-Dinitrotoluene 3.33 2.63 79 70 - 1142,6-Dinitrotoluene 3.33 2.38 71 63 - 1072-Chloronaphthalene 3.33 2.44 73 65 - 1042-Methylnaphthalene 3.33 2.94 88 57 - 1142-Nitroaniline 3.33 1.40 42 18 - 883,3'-Dichlorobenzidine 3.33 1.70 51 30 - 943-Nitroaniline 3.33 2.25 68 59 - 1224-Bromophenyl phenyl ether 3.33 1.03 31 18 - 944-Chloroaniline 3.33 2.46 74 66 - 1104-Chlorophenyl phenyl ether 3.33 2.46 74 49 - 1184-Nitroaniline 3.33 2.44 73 62 - 108Acenaphthene 3.33 2.37 71 67 - 107Acenaphthylene 3.33 2.52 76 69 - 111Anthracene 3.33 2.46 74 68 - 110Benzo[a]anthracene 3.33 2.65 80 72 - 115Benzo[a]pyrene 3.33 2.63 79 69 - 119Benzo[b]fluoranthene 3.33 2.44 73 54 - 128Benzo[g,h,i]perylene 3.33 2.51 75 70 - 115Benzo[k]fluoranthene 3.33 2.34 70 65 - 106Bis(2-chloroethoxy)methane 3.33 2.48 74 64 - 105Bis(2-chloroethyl)ether 3.33 2.76 83 63 - 125Bis(2-ethylhexyl) phthalate 3.33 2.68 80 65 - 125Butyl benzyl phthalate 3.33 2.68 80 66 - 115Carbazole 3.33 2.44 73 70 - 111Chrysene 3.33 2.90 87 60 - 130Dibenz(a,h)anthracene 3.33 2.40 72 67 - 107Dibenzofuran 3.33 2.75 83 66 - 117Diethyl phthalate 3.33 2.57 77 68 - 112Dimethyl phthalate 3.33 2.93 88 67 - 119Di-n-butyl phthalate 3.33 2.90 87 57 - 138Di-n-octyl phthalate 3.33 2.75 83 64 - 114Fluoranthene 3.33 2.51 75 66 - 110Fluorene 3.33 2.47 74 57 - 128Hexachlorobenzene 3.33 2.31 69 60 - 108Hexachlorobutadiene 3.33 2.13 64 50 - 129Hexachlorocyclopentadiene TestAmerica Edison Page 141 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Solid 1.0 Lab Control Sample - Batch: 460-478451 Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Z483637.D 15.0000 g 1 mLUnits:mg/Kg Method: 8270D Preparation: 3546 CBNAMS11LCS 460-478451/2-A Analysis Date: 11/20/2017 0925 Analysis Batch: Prep Batch: Leach Batch: 460-478549 460-478451 N/A Prep Date:Injection Volume:1 uL Leach Date: 11/19/2017 0938 N/A Analyte QualLimit% Rec.ResultSpike Amount 3.33 2.46 74 63 - 99Hexachloroethane 3.33 2.77 83 53 - 137Indeno[1,2,3-cd]pyrene 3.33 2.59 78 68 - 111Isophorone 3.33 2.38 71 65 - 102Naphthalene 3.33 2.63 79 66 - 108Nitrobenzene 3.33 2.82 85 63 - 117N-Nitrosodi-n-propylamine 3.33 2.35 71 65 - 114N-Nitrosodiphenylamine 3.33 2.51 75 68 - 111Phenanthrene 3.33 2.35 70 64 - 121Pyrene Surrogate % Rec Acceptance Limits 2-Fluorobiphenyl 68 38 - 95 Nitrobenzene-d5 (Surr)73 37 - 94 Terphenyl-d14 (Surr)68 24 - 109 TestAmerica Edison Page 142 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Dilution: Dilution: 11/19/2017 2355 11/20/2017 0017 Solid Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 460-478451 1.0 1.0 Client Matrix: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Client Matrix:Solid 11/19/2017 0938 11/19/2017 0938 L205271.D 15.0415 g 1 mL 1 uL L205272.D 15.0316 g 1 mL 1 uL Method: 8270D Preparation: 3546 CBNAMS12 CBNAMS12 460-145381-C-5-D MS 460-145381-C-5-E MSD MS Lab Sample ID: MSD Lab Sample ID: Analysis Date: Prep Date: Leach Date:N/A Analysis Date: Prep Date: Leach Date:N/A Analysis Batch: Prep Batch: Leach Batch: 460-478510 460-478451 Analysis Batch: Prep Batch: Leach Batch: 460-478510 460-478451 N/A N/A Analyte RPD LimitRPDLimit % Rec. MS MSD MS Qual MSD Qual 70 69 62 - 104 2 301,2,4-Trichlorobenzene 63 60 64 - 98 4 30 * *1,2-Dichlorobenzene 62 61 62 - 96 3 30 *1,3-Dichlorobenzene 62 60 63 - 97 3 30 * *1,4-Dichlorobenzene 60 58 39 - 122 3 302,2'-oxybis[1-chloropropane] 79 80 66 - 122 1 302,4-Dinitrotoluene 80 82 70 - 114 3 302,6-Dinitrotoluene 65 65 63 - 107 1 302-Chloronaphthalene 50 53 65 - 104 4 30 * *2-Methylnaphthalene 59 58 57 - 114 1 302-Nitroaniline 49 50 18 - 88 2 303,3'-Dichlorobenzidine 63 64 30 - 94 1 303-Nitroaniline 77 74 59 - 122 3 304-Bromophenyl phenyl ether 38 32 18 - 94 17 304-Chloroaniline 69 66 66 - 110 4 304-Chlorophenyl phenyl ether 46 48 49 - 118 4 30 * *4-Nitroaniline 65 61 62 - 108 6 30 *Acenaphthene 64 65 67 - 107 1 30 * *Acenaphthylene 66 65 69 - 111 2 30 * *Anthracene 68 67 68 - 110 2 30 *Benzo[a]anthracene 72 71 72 - 115 2 30 *Benzo[a]pyrene 76 75 69 - 119 2 30Benzo[b]fluoranthene 65 64 54 - 128 0 30Benzo[g,h,i]perylene 69 67 70 - 115 2 30 * *Benzo[k]fluoranthene 64 63 65 - 106 2 30 * *Bis(2-chloroethoxy)methane 62 59 64 - 105 4 30 * *Bis(2-chloroethyl)ether 64 62 63 - 125 3 30 *Bis(2-ethylhexyl) phthalate 67 64 65 - 125 4 30 *Butyl benzyl phthalate 64 62 66 - 115 3 30 * *Carbazole 68 66 70 - 111 3 30 * *Chrysene 69 70 60 - 130 1 30Dibenz(a,h)anthracene 66 67 67 - 107 1 30 *Dibenzofuran TestAmerica Edison Page 143 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Dilution: Dilution: 11/19/2017 2355 11/20/2017 0017 Solid Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 460-478451 1.0 1.0 Client Matrix: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Client Matrix:Solid 11/19/2017 0938 11/19/2017 0938 L205271.D 15.0415 g 1 mL 1 uL L205272.D 15.0316 g 1 mL 1 uL Method: 8270D Preparation: 3546 CBNAMS12 CBNAMS12 460-145381-C-5-D MS 460-145381-C-5-E MSD MS Lab Sample ID: MSD Lab Sample ID: Analysis Date: Prep Date: Leach Date:N/A Analysis Date: Prep Date: Leach Date:N/A Analysis Batch: Prep Batch: Leach Batch: 460-478510 460-478451 Analysis Batch: Prep Batch: Leach Batch: 460-478510 460-478451 N/A N/A Analyte RPD LimitRPDLimit % Rec. MS MSD MS Qual MSD Qual 63 63 66 - 117 0 30 * *Diethyl phthalate 68 68 68 - 112 1 30Dimethyl phthalate 60 58 67 - 119 4 30 * *Di-n-butyl phthalate 66 63 57 - 138 3 30Di-n-octyl phthalate 62 59 64 - 114 4 30 * *Fluoranthene 58 59 66 - 110 2 30 * *Fluorene 79 76 57 - 128 4 30Hexachlorobenzene 72 69 60 - 108 4 30Hexachlorobutadiene 72 70 50 - 129 3 30Hexachlorocyclopentadiene 63 62 63 - 99 2 30 *Hexachloroethane 74 74 53 - 137 0 30Indeno[1,2,3-cd]pyrene 64 63 68 - 111 2 30 * *Isophorone 61 61 65 - 102 1 30 * *Naphthalene 57 57 66 - 108 0 30 * *Nitrobenzene 65 65 63 - 117 0 30N-Nitrosodi-n-propylamine 87 88 65 - 114 2 30N-Nitrosodiphenylamine 61 60 68 - 111 2 30 * *Phenanthrene 74 71 64 - 121 5 30Pyrene Surrogate Acceptance LimitsMS % Rec MSD % Rec 2-Fluorobiphenyl 65 65 38 - 95 Nitrobenzene-d5 (Surr)60 56 37 - 94 Terphenyl-d14 (Surr)76 72 24 - 109 TestAmerica Edison Page 144 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc SolidClient Matrix: 1.0Dilution: Lab Sample ID: 11/24/2017 1204 Method Blank - Batch: 460-479261 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: f38649.D 15.0000 g 1 mLUnits:mg/Kg Method: 8270D Preparation: 3546 CBNAMS15MB 460-479261/1-A Analysis Date: Analysis Batch: Prep Batch: Leach Batch: 460-479517 460-479261 N/A Prep Date:Injection Volume:11/22/2017 0851 1 uL Leach Date:N/A Analyte Result Qual MDL RL 0.033 U 0.0330.00731,2,4-Trichlorobenzene 0.33 U 0.330.0111,2-Dichlorobenzene 0.33 U 0.330.0261,3-Dichlorobenzene 0.33 U 0.330.0261,4-Dichlorobenzene 0.33 U 0.330.0142,2'-oxybis[1-chloropropane] 0.067 U 0.0670.0132,4-Dinitrotoluene 0.067 U 0.0670.0182,6-Dinitrotoluene 0.33 U 0.330.00752-Chloronaphthalene 0.33 U 0.330.00732-Methylnaphthalene 0.33 U 0.330.0112-Nitroaniline 0.13 U 0.130.0373,3'-Dichlorobenzidine 0.33 U 0.330.00983-Nitroaniline 0.33 U 0.330.0104-Bromophenyl phenyl ether 0.33 U 0.330.00854-Chloroaniline 0.33 U 0.330.00994-Chlorophenyl phenyl ether 0.33 U 0.330.0134-Nitroaniline 0.33 U 0.330.0080Acenaphthene 0.33 U 0.330.0085Acenaphthylene 0.33 U 0.330.031Anthracene 0.033 U 0.0330.028Benzo[a]anthracene 0.033 U 0.0330.010Benzo[a]pyrene 0.033 U 0.0330.013Benzo[b]fluoranthene 0.33 U 0.330.019Benzo[g,h,i]perylene 0.033 U 0.0330.014Benzo[k]fluoranthene 0.33 U 0.330.010Bis(2-chloroethoxy)methane 0.033 U 0.0330.0078Bis(2-chloroethyl)ether 0.33 U 0.330.013Bis(2-ethylhexyl) phthalate 0.33 U 0.330.010Butyl benzyl phthalate 0.33 U 0.330.0082Carbazole 0.33 U 0.330.0090Chrysene 0.033 U 0.0330.017Dibenz(a,h)anthracene 0.33 U 0.330.010Dibenzofuran 0.33 U 0.330.0094Diethyl phthalate 0.33 U 0.330.0096Dimethyl phthalate 0.33 U 0.330.0099Di-n-butyl phthalate 0.33 U 0.330.017Di-n-octyl phthalate 0.33 U 0.330.0098Fluoranthene 0.33 U 0.330.0072Fluorene 0.033 U 0.0330.013Hexachlorobenzene 0.067 U 0.0670.0093Hexachlorobutadiene 0.33 U 0.330.021Hexachlorocyclopentadiene 0.033 U 0.0330.012Hexachloroethane 0.033 U 0.0330.022Indeno[1,2,3-cd]pyrene 0.13 U 0.130.0071Isophorone 0.33 U 0.330.0084Naphthalene TestAmerica Edison Page 145 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc SolidClient Matrix: 1.0Dilution: Lab Sample ID: 11/24/2017 1204 Method Blank - Batch: 460-479261 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: f38649.D 15.0000 g 1 mLUnits:mg/Kg Method: 8270D Preparation: 3546 CBNAMS15MB 460-479261/1-A Analysis Date: Analysis Batch: Prep Batch: Leach Batch: 460-479517 460-479261 N/A Prep Date:Injection Volume:11/22/2017 0851 1 uL Leach Date:N/A Analyte Result Qual MDL RL 0.033 U 0.0330.010Nitrobenzene 0.033 U 0.0330.011N-Nitrosodi-n-propylamine 0.33 U 0.330.030N-Nitrosodiphenylamine 0.33 U 0.330.0088Phenanthrene 0.33 U 0.330.015Pyrene Surrogate % Rec Acceptance Limits 2-Fluorobiphenyl 102 38 - 95* Nitrobenzene-d5 (Surr)83 37 - 94 Terphenyl-d14 (Surr)71 24 - 109 TestAmerica Edison Page 146 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Solid 1.0 Lab Control Sample - Batch: 460-479261 Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: f38650.D 15.0000 g 1 mLUnits:mg/Kg Method: 8270D Preparation: 3546 CBNAMS15LCS 460-479261/2-A Analysis Date: 11/24/2017 1226 Analysis Batch: Prep Batch: Leach Batch: 460-479517 460-479261 N/A Prep Date:Injection Volume:1 uL Leach Date: 11/22/2017 0851 N/A Analyte QualLimit% Rec.ResultSpike Amount 3.33 3.15 95 62 - 1041,2,4-Trichlorobenzene 3.33 2.93 88 64 - 981,2-Dichlorobenzene 3.33 2.99 90 62 - 961,3-Dichlorobenzene 3.33 2.95 89 63 - 971,4-Dichlorobenzene 3.33 1.80 54 39 - 1222,2'-oxybis[1-chloropropane] 3.33 2.61 78 66 - 1222,4-Dinitrotoluene 3.33 2.99 90 70 - 1142,6-Dinitrotoluene 3.33 3.29 99 63 - 1072-Chloronaphthalene 3.33 2.85 85 65 - 1042-Methylnaphthalene 3.33 2.52 76 57 - 1142-Nitroaniline 3.33 2.47 74 18 - 883,3'-Dichlorobenzidine 3.33 2.94 88 30 - 943-Nitroaniline 3.33 3.45 104 59 - 1224-Bromophenyl phenyl ether 3.33 1.30 39 18 - 944-Chloroaniline 3.33 3.12 94 66 - 1104-Chlorophenyl phenyl ether 3.33 2.62 79 49 - 1184-Nitroaniline 3.33 2.87 86 62 - 108Acenaphthene 3.33 3.17 95 67 - 107Acenaphthylene 3.33 3.37 101 69 - 111Anthracene 3.33 3.27 98 68 - 110Benzo[a]anthracene 3.33 3.55 107 72 - 115Benzo[a]pyrene 3.33 3.67 110 69 - 119Benzo[b]fluoranthene 3.33 2.04 61 54 - 128Benzo[g,h,i]perylene 3.33 3.73 112 70 - 115Benzo[k]fluoranthene 3.33 3.10 93 65 - 106Bis(2-chloroethoxy)methane 3.33 2.79 84 64 - 105Bis(2-chloroethyl)ether 3.33 2.93 88 63 - 125Bis(2-ethylhexyl) phthalate 3.33 2.70 81 65 - 125Butyl benzyl phthalate 3.33 3.39 102 66 - 115Carbazole 3.33 3.36 101 70 - 111Chrysene 3.33 2.61 78 60 - 130Dibenz(a,h)anthracene 3.33 3.10 93 67 - 107Dibenzofuran 3.33 3.22 96 66 - 117Diethyl phthalate 3.33 3.44 103 68 - 112Dimethyl phthalate 3.33 3.44 103 67 - 119Di-n-butyl phthalate 3.33 3.40 102 57 - 138Di-n-octyl phthalate 3.33 3.70 111 64 - 114Fluoranthene 3.33 2.98 89 66 - 110Fluorene 3.33 3.55 106 57 - 128Hexachlorobenzene 3.33 3.45 104 60 - 108Hexachlorobutadiene 3.33 1.91 57 50 - 129Hexachlorocyclopentadiene TestAmerica Edison Page 147 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Solid 1.0 Lab Control Sample - Batch: 460-479261 Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: f38650.D 15.0000 g 1 mLUnits:mg/Kg Method: 8270D Preparation: 3546 CBNAMS15LCS 460-479261/2-A Analysis Date: 11/24/2017 1226 Analysis Batch: Prep Batch: Leach Batch: 460-479517 460-479261 N/A Prep Date:Injection Volume:1 uL Leach Date: 11/22/2017 0851 N/A Analyte QualLimit% Rec.ResultSpike Amount 3.33 2.82 85 63 - 99Hexachloroethane 3.33 2.48 74 53 - 137Indeno[1,2,3-cd]pyrene 3.33 2.92 87 68 - 111Isophorone 3.33 3.09 93 65 - 102Naphthalene 3.33 3.15 94 66 - 108Nitrobenzene 3.33 2.81 84 63 - 117N-Nitrosodi-n-propylamine 3.33 3.52 105 65 - 114N-Nitrosodiphenylamine 3.33 3.32 100 68 - 111Phenanthrene 3.33 2.51 75 64 - 121Pyrene Surrogate % Rec Acceptance Limits 2-Fluorobiphenyl 100 38 - 95* Nitrobenzene-d5 (Surr)88 37 - 94 Terphenyl-d14 (Surr)70 24 - 109 TestAmerica Edison Page 148 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Dilution: Dilution: 11/24/2017 1438 11/24/2017 1500 Solid Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 460-479261 1.0 1.0 Client Matrix: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Client Matrix:Solid 11/22/2017 0851 11/22/2017 0851 f38656.D 15.0158 g 1 mL 1 uL f38657.D 15.0129 g 1 mL 1 uL Method: 8270D Preparation: 3546 CBNAMS15 CBNAMS15 460-145556-A-1-B MS 460-145556-A-1-C MSD MS Lab Sample ID: MSD Lab Sample ID: Analysis Date: Prep Date: Leach Date:N/A Analysis Date: Prep Date: Leach Date:N/A Analysis Batch: Prep Batch: Leach Batch: 460-479517 460-479261 Analysis Batch: Prep Batch: Leach Batch: 460-479517 460-479261 N/A N/A Analyte RPD LimitRPDLimit % Rec. MS MSD MS Qual MSD Qual 72 76 62 - 104 6 301,2,4-Trichlorobenzene 66 70 64 - 98 6 301,2-Dichlorobenzene 67 70 62 - 96 4 301,3-Dichlorobenzene 67 71 63 - 97 5 301,4-Dichlorobenzene 41 44 39 - 122 7 302,2'-oxybis[1-chloropropane] 51 54 66 - 122 7 30 * *2,4-Dinitrotoluene 61 66 70 - 114 8 30 * *2,6-Dinitrotoluene 78 82 63 - 107 6 302-Chloronaphthalene 65 70 65 - 104 8 302-Methylnaphthalene 51 55 57 - 114 9 30 * *2-Nitroaniline 75 79 18 - 88 5 303,3'-Dichlorobenzidine 74 81 30 - 94 8 303-Nitroaniline 81 86 59 - 122 6 304-Bromophenyl phenyl ether 50 62 18 - 94 21 304-Chloroaniline 71 75 66 - 110 6 304-Chlorophenyl phenyl ether 55 60 49 - 118 8 304-Nitroaniline 67 71 62 - 108 6 30Acenaphthene 73 77 67 - 107 5 30Acenaphthylene 77 81 69 - 111 5 30Anthracene 75 78 68 - 110 3 30Benzo[a]anthracene 81 85 72 - 115 5 30Benzo[a]pyrene 82 86 69 - 119 5 30Benzo[b]fluoranthene 54 51 54 - 128 6 30 *Benzo[g,h,i]perylene 81 88 70 - 115 8 30Benzo[k]fluoranthene 71 75 65 - 106 5 30Bis(2-chloroethoxy)methane 63 66 64 - 105 6 30 *Bis(2-chloroethyl)ether 67 69 63 - 125 3 30Bis(2-ethylhexyl) phthalate 63 64 65 - 125 1 30 * *Butyl benzyl phthalate 74 79 66 - 115 6 30Carbazole 78 80 70 - 111 3 30Chrysene 66 64 60 - 130 3 30Dibenz(a,h)anthracene 71 75 67 - 107 5 30Dibenzofuran TestAmerica Edison Page 149 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Dilution: Dilution: 11/24/2017 1438 11/24/2017 1500 Solid Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 460-479261 1.0 1.0 Client Matrix: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Client Matrix:Solid 11/22/2017 0851 11/22/2017 0851 f38656.D 15.0158 g 1 mL 1 uL f38657.D 15.0129 g 1 mL 1 uL Method: 8270D Preparation: 3546 CBNAMS15 CBNAMS15 460-145556-A-1-B MS 460-145556-A-1-C MSD MS Lab Sample ID: MSD Lab Sample ID: Analysis Date: Prep Date: Leach Date:N/A Analysis Date: Prep Date: Leach Date:N/A Analysis Batch: Prep Batch: Leach Batch: 460-479517 460-479261 Analysis Batch: Prep Batch: Leach Batch: 460-479517 460-479261 N/A N/A Analyte RPD LimitRPDLimit % Rec. MS MSD MS Qual MSD Qual 72 78 66 - 117 8 30Diethyl phthalate 77 83 68 - 112 7 30Dimethyl phthalate 78 82 67 - 119 5 30Di-n-butyl phthalate 72 76 57 - 138 6 30Di-n-octyl phthalate 79 84 64 - 114 6 30Fluoranthene 67 71 66 - 110 6 30Fluorene 81 85 57 - 128 5 30Hexachlorobenzene 80 85 60 - 108 6 30Hexachlorobutadiene 41 37 50 - 129 10 30 * *Hexachlorocyclopentadiene 63 67 63 - 99 6 30Hexachloroethane 63 61 53 - 137 4 30Indeno[1,2,3-cd]pyrene 67 72 68 - 111 7 30 *Isophorone 71 75 65 - 102 6 30Naphthalene 70 75 66 - 108 6 30Nitrobenzene 63 68 63 - 117 7 30N-Nitrosodi-n-propylamine 83 87 65 - 114 5 30N-Nitrosodiphenylamine 76 79 68 - 111 5 30Phenanthrene 60 61 64 - 121 1 30 * *Pyrene Surrogate Acceptance LimitsMS % Rec MSD % Rec 2-Fluorobiphenyl 79 84 38 - 95 Nitrobenzene-d5 (Surr)65 70 37 - 94 Terphenyl-d14 (Surr)56 56 24 - 109 TestAmerica Edison Page 150 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc WaterClient Matrix: 1.0Dilution: Lab Sample ID: 11/24/2017 0912 Method Blank - Batch: 460-479363 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: A111380.D 250 mL 2 mLUnits:ug/L Method: 8270D Preparation: 3510C CBNAMS16MB 460-479363/1-A Analysis Date: Analysis Batch: Prep Batch: Leach Batch: 460-479531 460-479363 N/A Prep Date:Injection Volume:11/22/2017 1439 5 uL Leach Date:N/A Analyte Result Qual MDL RL 1.0 U 1.00.611,2,4-Trichlorobenzene 10 U 100.831,2-Dichlorobenzene 10 U 101.11,3-Dichlorobenzene 10 U 100.661,4-Dichlorobenzene 10 U 100.932,2'-oxybis[1-chloropropane] 2.0 U 2.01.02,4-Dinitrotoluene 2.0 U 2.00.882,6-Dinitrotoluene 10 U 100.612-Chloronaphthalene 10 U 100.882-Methylnaphthalene 10 U 100.652-Nitroaniline 10 U 101.03,3'-Dichlorobenzidine 10 U 100.823-Nitroaniline 10 U 101.04-Bromophenyl phenyl ether 10 U 100.734-Chloroaniline 10 U 100.964-Chlorophenyl phenyl ether 10 U 100.484-Nitroaniline 10 U 100.88Acenaphthene 10 U 100.65Acenaphthylene 10 U 100.57Anthracene 1.0 U 1.00.55Benzo[a]anthracene 1.0 U 1.00.16Benzo[a]pyrene 1.0 U 1.00.44Benzo[b]fluoranthene 10 U 100.75Benzo[g,h,i]perylene 1.0 U 1.00.18Benzo[k]fluoranthene 10 U 100.69Bis(2-chloroethoxy)methane 1.0 U 1.00.12Bis(2-chloroethyl)ether 2.0 U 2.00.72Bis(2-ethylhexyl) phthalate 10 U 100.60Butyl benzyl phthalate 10 U 100.85Carbazole 2.0 U 2.00.67Chrysene 1.0 U 1.00.090Dibenz(a,h)anthracene 10 U 100.85Dibenzofuran 10 U 101.0Diethyl phthalate 10 U 100.98Dimethyl phthalate 10 U 100.82Di-n-butyl phthalate 10 U 100.69Di-n-octyl phthalate 10 U 100.72Fluoranthene 10 U 100.80Fluorene 1.0 U 1.00.47Hexachlorobenzene 1.0 U 1.00.76Hexachlorobutadiene 10 U 100.61Hexachlorocyclopentadiene 1.0 U 1.00.090Hexachloroethane 1.0 U 1.00.21Indeno[1,2,3-cd]pyrene 10 U 100.67Isophorone 10 U 100.80Naphthalene TestAmerica Edison Page 151 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc WaterClient Matrix: 1.0Dilution: Lab Sample ID: 11/24/2017 0912 Method Blank - Batch: 460-479363 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: A111380.D 250 mL 2 mLUnits:ug/L Method: 8270D Preparation: 3510C CBNAMS16MB 460-479363/1-A Analysis Date: Analysis Batch: Prep Batch: Leach Batch: 460-479531 460-479363 N/A Prep Date:Injection Volume:11/22/2017 1439 5 uL Leach Date:N/A Analyte Result Qual MDL RL 1.0 U 1.00.49Nitrobenzene 1.0 U 1.00.83N-Nitrosodi-n-propylamine 10 U 100.74N-Nitrosodiphenylamine 10 U 100.65Phenanthrene 10 U 100.83Pyrene Surrogate % Rec Acceptance Limits 2-Fluorobiphenyl 75 45 - 107 Nitrobenzene-d5 (Surr)79 51 - 108 Terphenyl-d14 (Surr)76 40 - 148 TestAmerica Edison Page 152 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Dilution: Dilution: 11/24/2017 0952 Lab Control Sample/ Lab Control Sample Duplicate Recovery Report - Batch: 460-479363 1.0 1.0 Water LCS Lab Sample ID: LCSD Lab Sample ID: Client Matrix: Units: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Client Matrix:Water Units: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: ug/L A111381.D 250 mL 2 mL 5 uL A111382.D 250 mL 2 mL 5 uL ug/L 11/22/2017 1439 Method: 8270D Preparation: 3510C CBNAMS16 CBNAMS16 LCS 460-479363/2-A LCSD 460-479363/3-A Analysis Date: Prep Date: Leach Date: 11/24/2017 0932 11/22/2017 1439 Analysis Batch: Prep Batch: Leach Batch: 460-479531 460-479363 Analysis Date: Prep Date: Leach Date: Analysis Batch: Prep Batch: Leach Batch: 460-479531 460-479363 N/A N/A N/A N/A Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS % Rec. 7571 43 - 98 6 301,2,4-Trichlorobenzene 7165 42 - 95 8 301,2-Dichlorobenzene 7063 40 - 92 11 301,3-Dichlorobenzene 7265 42 - 94 9 301,4-Dichlorobenzene 7571 50 - 108 6 302,2'-oxybis[1-chloropropane] 117112 70 - 123 4 302,4-Dinitrotoluene 111103 68 - 121 7 302,6-Dinitrotoluene 8883 54 - 105 6 302-Chloronaphthalene 8381 47 - 104 2 302-Methylnaphthalene 8499 46 - 124 16 302-Nitroaniline 112105 68 - 123 6 303,3'-Dichlorobenzidine 8882 60 - 117 7 303-Nitroaniline 9392 57 - 126 0 304-Bromophenyl phenyl ether 8479 51 - 108 5 304-Chloroaniline 108106 60 - 114 2 304-Chlorophenyl phenyl ether 108102 48 - 135 6 304-Nitroaniline 9996 58 - 107 4 30Acenaphthene 9086 61 - 106 5 30Acenaphthylene 103103 70 - 118 0 30Anthracene 107105 73 - 119 1 30Benzo[a]anthracene 114116 76 - 125 2 30Benzo[a]pyrene 113115 78 - 123 1 30Benzo[b]fluoranthene 106107 63 - 133 1 30Benzo[g,h,i]perylene 107112 71 - 126 5 30Benzo[k]fluoranthene 9391 67 - 104 1 30Bis(2-chloroethoxy)methane 8584 63 - 106 2 30Bis(2-chloroethyl)ether 127125 63 - 135 2 30Bis(2-ethylhexyl) phthalate 111110 66 - 129 1 30Butyl benzyl phthalate 114114 68 - 121 1 30Carbazole 106107 73 - 121 2 30Chrysene 106109 59 - 136 3 30Dibenz(a,h)anthracene 9692 67 - 108 4 30Dibenzofuran 120114 61 - 129 6 30Diethyl phthalate 109105 65 - 121 3 30Dimethyl phthalate 128124 64 - 130 3 30Di-n-butyl phthalate TestAmerica Edison Page 153 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Dilution: Dilution: 11/24/2017 0952 Lab Control Sample/ Lab Control Sample Duplicate Recovery Report - Batch: 460-479363 1.0 1.0 Water LCS Lab Sample ID: LCSD Lab Sample ID: Client Matrix: Units: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Client Matrix:Water Units: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: ug/L A111381.D 250 mL 2 mL 5 uL A111382.D 250 mL 2 mL 5 uL ug/L 11/22/2017 1439 Method: 8270D Preparation: 3510C CBNAMS16 CBNAMS16 LCS 460-479363/2-A LCSD 460-479363/3-A Analysis Date: Prep Date: Leach Date: 11/24/2017 0932 11/22/2017 1439 Analysis Batch: Prep Batch: Leach Batch: 460-479531 460-479363 Analysis Date: Prep Date: Leach Date: Analysis Batch: Prep Batch: Leach Batch: 460-479531 460-479363 N/A N/A N/A N/A Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS % Rec. 127129 64 - 131 1 30Di-n-octyl phthalate 125122 66 - 123 2 30 *Fluoranthene 105103 67 - 112 2 30Fluorene 9697 63 - 125 1 30Hexachlorobenzene 7569 34 - 99 8 30Hexachlorobutadiene 7068 18 - 99 3 30Hexachlorocyclopentadiene 6964 39 - 92 6 30Hexachloroethane 101105 57 - 142 4 30Indeno[1,2,3-cd]pyrene 9187 55 - 105 4 30Isophorone 8279 51 - 98 4 30Naphthalene 9289 56 - 106 4 30Nitrobenzene 9892 48 - 118 7 30N-Nitrosodi-n-propylamine 9595 69 - 118 0 30N-Nitrosodiphenylamine 103101 70 - 117 2 30Phenanthrene 8687 63 - 129 1 30Pyrene Surrogate LCS % Rec LCSD % Rec Acceptance Limits 2-Fluorobiphenyl 79 85 45 - 107 Nitrobenzene-d5 (Surr)85 90 51 - 108 Terphenyl-d14 (Surr)80 83 40 - 148 TestAmerica Edison Page 154 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc SolidClient Matrix: 1.0Dilution: Lab Sample ID: 11/21/2017 2107 Method Blank - Batch: 460-478818 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: P4006833.D +15.0000 g 10 mLUnits:mg/Kg Method: 8081B Preparation: 3546 CPESTGC4MB 460-478818/1-A Analysis Date: Analysis Batch: Prep Batch: Leach Batch: 460-479079 460-478818 N/A Prep Date:Injection Volume:11/21/2017 0040 1 uL Column ID:PRIMARYLeach Date:N/A Analyte Result Qual MDL RL 0.0067 U 0.00670.00114,4'-DDD 0.0067 U 0.00670.000794,4'-DDE 0.0067 U 0.00670.00124,4'-DDT 0.0067 U 0.00670.0010Aldrin 0.0020 U 0.00200.00068alpha-BHC 0.0020 U 0.00200.00075beta-BHC 0.067 U 0.0670.016Chlordane (technical) 0.0020 U 0.00200.00041delta-BHC 0.0020 U 0.00200.00087Dieldrin 0.0067 U 0.00670.0010Endosulfan I 0.0067 U 0.00670.0017Endosulfan II 0.0067 U 0.00670.00084Endosulfan sulfate 0.0067 U 0.00670.00096Endrin 0.0067 U 0.00670.0016Endrin aldehyde 0.0067 U 0.00670.0013Endrin ketone 0.0020 U 0.00200.00062gamma-BHC (Lindane) 0.0067 U 0.00670.00079Heptachlor 0.0067 U 0.00670.0010Heptachlor epoxide 0.0067 U 0.00670.0015Methoxychlor 0.067 U 0.0670.024Toxaphene Surrogate % Rec Acceptance Limits DCB Decachlorobiphenyl 119 50 - 150 Tetrachloro-m-xylene 119 47 - 150 Surrogate % Rec Acceptance Limits DCB Decachlorobiphenyl 113 50 - 150 Tetrachloro-m-xylene 114 47 - 150 TestAmerica Edison Page 155 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Solid 1.0 Lab Control Sample - Batch: 460-478818 Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: P4006834.D +15.0000 g 10 mLUnits:mg/Kg Method: 8081B Preparation: 3546 CPESTGC4LCS 460-478818/2-A Analysis Date: 11/21/2017 2120 Analysis Batch: Prep Batch: Leach Batch: 460-479079 460-478818 N/A Prep Date:Injection Volume:1 uL Leach Date: 11/21/2017 0040 Column ID:PRIMARYN/A Analyte QualLimit% Rec.ResultSpike Amount 0.133 0.149 112 64 - 1294,4'-DDD 0.133 0.148 111 65 - 1294,4'-DDE 0.133 0.150 112 59 - 1244,4'-DDT 0.133 0.144 108 66 - 127Aldrin 0.133 0.153 115 69 - 131alpha-BHC 0.133 0.149 112 69 - 127beta-BHC 0.133 0.154 115 64 - 129delta-BHC 0.133 0.145 109 65 - 128Dieldrin 0.133 0.145 109 66 - 126Endosulfan I 0.133 0.150 113 64 - 124Endosulfan II 0.133 0.146 109 62 - 123Endosulfan sulfate 0.133 0.151 113 58 - 126Endrin 0.133 0.144 108 69 - 131Endrin aldehyde 0.133 0.148 111 62 - 125Endrin ketone 0.133 0.150 113 67 - 126gamma-BHC (Lindane) 0.133 0.147 110 63 - 125Heptachlor 0.133 0.143 107 64 - 125Heptachlor epoxide 0.133 0.149 112 56 - 123Methoxychlor Surrogate % Rec Acceptance Limits DCB Decachlorobiphenyl 112 50 - 150 Tetrachloro-m-xylene 113 47 - 150 Solid 1.0 Lab Control Sample - Batch: 460-478818 Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: P4006834.D +15.0000 g 10 mLUnits:mg/Kg Method: 8081B Preparation: 3546 CPESTGC4LCS 460-478818/2-A Analysis Date: 11/21/2017 2120 Analysis Batch: Prep Batch: Leach Batch: 460-479079 460-478818 N/A Prep Date:Injection Volume:1 uL Leach Date: 11/21/2017 0040 Column ID:SECONDARYN/A Analyte QualLimit% Rec.ResultSpike Amount 0.133 0.145 109 64 - 1294,4'-DDD 0.133 0.143 107 65 - 1294,4'-DDE 0.133 0.143 107 59 - 1244,4'-DDT 0.133 0.133 100 66 - 127Aldrin 0.133 0.139 104 69 - 131alpha-BHC 0.133 0.140 105 69 - 127beta-BHC TestAmerica Edison Page 156 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Solid 1.0 Lab Control Sample - Batch: 460-478818 Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: P4006834.D +15.0000 g 10 mLUnits:mg/Kg Method: 8081B Preparation: 3546 CPESTGC4LCS 460-478818/2-A Analysis Date: 11/21/2017 2120 Analysis Batch: Prep Batch: Leach Batch: 460-479079 460-478818 N/A Prep Date:Injection Volume:1 uL Leach Date: 11/21/2017 0040 Column ID:SECONDARYN/A Analyte QualLimit% Rec.ResultSpike Amount 0.133 0.137 103 64 - 129delta-BHC 0.133 0.139 104 65 - 128Dieldrin 0.133 0.139 104 66 - 126Endosulfan I 0.133 0.144 108 64 - 124Endosulfan II 0.133 0.145 109 62 - 123Endosulfan sulfate 0.133 0.143 107 58 - 126Endrin 0.133 0.138 103 69 - 131Endrin aldehyde 0.133 0.143 107 62 - 125Endrin ketone 0.133 0.136 102 67 - 126gamma-BHC (Lindane) 0.133 0.134 100 63 - 125Heptachlor 0.133 0.139 104 64 - 125Heptachlor epoxide 0.133 0.141 106 56 - 123Methoxychlor Surrogate % Rec Acceptance Limits DCB Decachlorobiphenyl 108 50 - 150 Tetrachloro-m-xylene 112 47 - 150 TestAmerica Edison Page 157 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Dilution: Dilution: 11/22/2017 1017 11/22/2017 1030 Solid Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 460-478818 1.0 1.0 Client Matrix: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Column ID: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Column ID: Client Matrix:Solid 11/21/2017 0040 11/21/2017 0040 P4006855.D +15.0066 g 10 mL 1 uL PRIMARY P4006856.D +15.0301 g 10 mL 1 uL PRIMARY Method: 8081B Preparation: 3546 CPESTGC4 CPESTGC4 460-145399-E-1-C MS 460-145399-E-1-D MSD MS Lab Sample ID: MSD Lab Sample ID: Analysis Date: Prep Date: Leach Date:N/A Analysis Date: Prep Date: Leach Date:N/A Analysis Batch: Prep Batch: Leach Batch: 460-479230 460-478818 Analysis Batch: Prep Batch: Leach Batch: 460-479230 460-478818 N/A N/A Analyte RPD LimitRPDLimit % Rec. MS MSD MS Qual MSD Qual 115 108 64 - 129 6 304,4'-DDD 112 106 65 - 129 6 304,4'-DDE 112 105 59 - 124 7 304,4'-DDT 110 104 66 - 127 6 30Aldrin 116 108 69 - 131 8 30alpha-BHC 113 106 69 - 127 7 30beta-BHC 117 110 64 - 129 6 30delta-BHC 111 105 65 - 128 6 30Dieldrin 109 103 66 - 126 6 30Endosulfan I 115 108 64 - 124 6 30Endosulfan II 109 104 62 - 123 5 30Endosulfan sulfate 114 107 58 - 126 6 30Endrin 111 105 69 - 131 6 30Endrin aldehyde 110 106 62 - 125 4 30Endrin ketone 115 107 67 - 126 7 30gamma-BHC (Lindane) 111 105 63 - 125 6 30Heptachlor 109 103 64 - 125 6 30Heptachlor epoxide 107 103 56 - 123 4 30Methoxychlor Surrogate Acceptance LimitsMS % Rec MSD % Rec DCB Decachlorobiphenyl 113 107 50 - 150 Tetrachloro-m-xylene 115 107 47 - 150 TestAmerica Edison Page 158 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Dilution: Dilution: 11/22/2017 1017 11/22/2017 1030 Solid Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 460-478818 1.0 1.0 Client Matrix: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Column ID: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Column ID: Client Matrix:Solid 11/21/2017 0040 11/21/2017 0040 P4006855.D +15.0066 g 10 mL 1 uL SECONDARY P4006856.D +15.0301 g 10 mL 1 uL SECONDARY Method: 8081B Preparation: 3546 CPESTGC4 CPESTGC4 460-145399-E-1-C MS 460-145399-E-1-D MSD MS Lab Sample ID: MSD Lab Sample ID: Analysis Date: Prep Date: Leach Date:N/A Analysis Date: Prep Date: Leach Date:N/A Analysis Batch: Prep Batch: Leach Batch: 460-479230 460-478818 Analysis Batch: Prep Batch: Leach Batch: 460-479230 460-478818 N/A N/A Analyte RPD LimitRPDLimit % Rec. MS MSD MS Qual MSD Qual 108 103 64 - 129 5 304,4'-DDD 108 103 65 - 129 5 304,4'-DDE 103 98 59 - 124 5 304,4'-DDT 101 96 66 - 127 5 30Aldrin 105 98 69 - 131 7 30alpha-BHC 104 99 69 - 127 5 30beta-BHC 103 98 64 - 129 6 30delta-BHC 105 101 65 - 128 4 30Dieldrin 105 100 66 - 126 5 30Endosulfan I 107 101 64 - 124 5 30Endosulfan II 107 102 62 - 123 5 30Endosulfan sulfate 106 101 58 - 126 5 30Endrin 102 97 69 - 131 5 30Endrin aldehyde 108 103 62 - 125 5 30Endrin ketone 103 97 67 - 126 6 30gamma-BHC (Lindane) 101 95 63 - 125 6 30Heptachlor 105 101 64 - 125 4 30Heptachlor epoxide 104 100 56 - 123 4 30Methoxychlor Surrogate Acceptance LimitsMS % Rec MSD % Rec DCB Decachlorobiphenyl 113 106 50 - 150 Tetrachloro-m-xylene 113 105 47 - 150 TestAmerica Edison Page 159 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc SolidClient Matrix: 1.0Dilution: Lab Sample ID: 11/22/2017 0931 Method Blank - Batch: 460-479140 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: 5F914746.D +15.0000 g 10 mLUnits:mg/Kg Method: 8081B Preparation: 3546 CPESTGC5MB 460-479140/1-A Analysis Date: Analysis Batch: Prep Batch: Leach Batch: 460-479228 460-479140 N/A Prep Date:Injection Volume:11/22/2017 0001 1 uL Column ID:PRIMARYLeach Date:N/A Analyte Result Qual MDL RL 0.0067 U 0.00670.00114,4'-DDD 0.0067 U 0.00670.000794,4'-DDE 0.0067 U 0.00670.00124,4'-DDT 0.0067 U 0.00670.0010Aldrin 0.0020 U 0.00200.00068alpha-BHC 0.0020 U 0.00200.00075beta-BHC 0.067 U 0.0670.016Chlordane (technical) 0.0020 U 0.00200.00041delta-BHC 0.0020 U 0.00200.00087Dieldrin 0.0067 U 0.00670.0010Endosulfan I 0.0067 U 0.00670.0017Endosulfan II 0.0067 U 0.00670.00084Endosulfan sulfate 0.0067 U 0.00670.00096Endrin 0.0067 U 0.00670.0016Endrin aldehyde 0.0067 U 0.00670.0013Endrin ketone 0.0020 U 0.00200.00062gamma-BHC (Lindane) 0.0067 U 0.00670.00079Heptachlor 0.0067 U 0.00670.0010Heptachlor epoxide 0.0067 U 0.00670.0015Methoxychlor 0.067 U 0.0670.024Toxaphene Surrogate % Rec Acceptance Limits DCB Decachlorobiphenyl 99 50 - 150 Tetrachloro-m-xylene 109 47 - 150 Surrogate % Rec Acceptance Limits DCB Decachlorobiphenyl 95 50 - 150 Tetrachloro-m-xylene 107 47 - 150 TestAmerica Edison Page 160 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Solid 1.0 Lab Control Sample - Batch: 460-479140 Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: 5F914747.D +15.0000 g 10 mLUnits:mg/Kg Method: 8081B Preparation: 3546 CPESTGC5LCS 460-479140/2-A Analysis Date: 11/22/2017 0944 Analysis Batch: Prep Batch: Leach Batch: 460-479228 460-479140 N/A Prep Date:Injection Volume:1 uL Leach Date: 11/22/2017 0001 Column ID:PRIMARYN/A Analyte QualLimit% Rec.ResultSpike Amount 0.133 0.123 93 64 - 1294,4'-DDD 0.133 0.137 103 65 - 1294,4'-DDE 0.133 0.126 94 59 - 1244,4'-DDT 0.133 0.142 106 66 - 127Aldrin 0.133 0.153 115 69 - 131alpha-BHC 0.133 0.139 104 69 - 127beta-BHC 0.133 0.144 108 64 - 129delta-BHC 0.133 0.138 104 65 - 128Dieldrin 0.133 0.142 107 66 - 126Endosulfan I 0.133 0.144 108 64 - 124Endosulfan II 0.133 0.130 98 62 - 123Endosulfan sulfate 0.133 0.131 98 58 - 126Endrin 0.133 0.138 103 69 - 131Endrin aldehyde 0.133 0.138 103 62 - 125Endrin ketone 0.133 0.143 107 67 - 126gamma-BHC (Lindane) 0.133 0.136 102 63 - 125Heptachlor 0.133 0.136 102 64 - 125Heptachlor epoxide 0.133 0.113 85 56 - 123Methoxychlor Surrogate % Rec Acceptance Limits DCB Decachlorobiphenyl 99 50 - 150 Tetrachloro-m-xylene 111 47 - 150 Solid 1.0 Lab Control Sample - Batch: 460-479140 Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: 5F914747.D +15.0000 g 10 mLUnits:mg/Kg Method: 8081B Preparation: 3546 CPESTGC5LCS 460-479140/2-A Analysis Date: 11/22/2017 0944 Analysis Batch: Prep Batch: Leach Batch: 460-479228 460-479140 N/A Prep Date:Injection Volume:1 uL Leach Date: 11/22/2017 0001 Column ID:SECONDARYN/A Analyte QualLimit% Rec.ResultSpike Amount 0.133 0.114 86 64 - 1294,4'-DDD 0.133 0.122 91 65 - 1294,4'-DDE 0.133 0.117 88 59 - 1244,4'-DDT 0.133 0.138 103 66 - 127Aldrin 0.133 0.145 109 69 - 131alpha-BHC 0.133 0.137 103 69 - 127beta-BHC TestAmerica Edison Page 161 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Solid 1.0 Lab Control Sample - Batch: 460-479140 Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: 5F914747.D +15.0000 g 10 mLUnits:mg/Kg Method: 8081B Preparation: 3546 CPESTGC5LCS 460-479140/2-A Analysis Date: 11/22/2017 0944 Analysis Batch: Prep Batch: Leach Batch: 460-479228 460-479140 N/A Prep Date:Injection Volume:1 uL Leach Date: 11/22/2017 0001 Column ID:SECONDARYN/A Analyte QualLimit% Rec.ResultSpike Amount 0.133 0.136 102 64 - 129delta-BHC 0.133 0.135 102 65 - 128Dieldrin 0.133 0.142 106 66 - 126Endosulfan I 0.133 0.132 99 64 - 124Endosulfan II 0.133 0.125 93 62 - 123Endosulfan sulfate 0.133 0.128 96 58 - 126Endrin 0.133 0.123 93 69 - 131Endrin aldehyde 0.133 0.133 100 62 - 125Endrin ketone 0.133 0.136 102 67 - 126gamma-BHC (Lindane) 0.133 0.135 101 63 - 125Heptachlor 0.133 0.133 100 64 - 125Heptachlor epoxide 0.133 0.102 76 56 - 123Methoxychlor Surrogate % Rec Acceptance Limits DCB Decachlorobiphenyl 98 50 - 150 Tetrachloro-m-xylene 102 47 - 150 TestAmerica Edison Page 162 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Dilution: Dilution: 11/22/2017 0956 11/22/2017 1009 Solid Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 460-479140 1.0 1.0 Client Matrix: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Column ID: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Column ID: Client Matrix:Solid 11/22/2017 0001 11/22/2017 0001 5F914748.D +15.0055 g 10 mL 1 uL PRIMARY 5F914749.D +15.0141 g 10 mL 1 uL PRIMARY Method: 8081B Preparation: 3546 CPESTGC5 CPESTGC5 460-145501-A-1-E MS 460-145501-A-1-F MSD MS Lab Sample ID: MSD Lab Sample ID: Analysis Date: Prep Date: Leach Date:N/A Analysis Date: Prep Date: Leach Date:N/A Analysis Batch: Prep Batch: Leach Batch: 460-479228 460-479140 Analysis Batch: Prep Batch: Leach Batch: 460-479228 460-479140 N/A N/A Analyte RPD LimitRPDLimit % Rec. MS MSD MS Qual MSD Qual 110 112 64 - 129 1 304,4'-DDD 113 112 65 - 129 2 304,4'-DDE 115 113 59 - 124 2 304,4'-DDT 113 109 66 - 127 4 30Aldrin 124 122 69 - 131 2 30alpha-BHC 110 105 69 - 127 5 30beta-BHC 119 117 64 - 129 2 30delta-BHC 116 115 65 - 128 2 30Dieldrin 114 112 66 - 126 2 30Endosulfan I 117 115 64 - 124 2 30Endosulfan II 111 111 62 - 123 0 30Endosulfan sulfate 110 110 58 - 126 1 30Endrin 112 111 69 - 131 1 30Endrin aldehyde 115 114 62 - 125 1 30Endrin ketone 118 115 67 - 126 3 30gamma-BHC (Lindane) 109 107 63 - 125 3 30Heptachlor 108 106 64 - 125 2 30Heptachlor epoxide 118 122 56 - 123 3 30Methoxychlor Surrogate Acceptance LimitsMS % Rec MSD % Rec DCB Decachlorobiphenyl 118 114 50 - 150 Tetrachloro-m-xylene 123 119 47 - 150 TestAmerica Edison Page 163 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Dilution: Dilution: 11/22/2017 0956 11/22/2017 1009 Solid Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 460-479140 1.0 1.0 Client Matrix: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Column ID: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Column ID: Client Matrix:Solid 11/22/2017 0001 11/22/2017 0001 5F914748.D +15.0055 g 10 mL 1 uL SECONDARY 5F914749.D +15.0141 g 10 mL 1 uL SECONDARY Method: 8081B Preparation: 3546 CPESTGC5 CPESTGC5 460-145501-A-1-E MS 460-145501-A-1-F MSD MS Lab Sample ID: MSD Lab Sample ID: Analysis Date: Prep Date: Leach Date:N/A Analysis Date: Prep Date: Leach Date:N/A Analysis Batch: Prep Batch: Leach Batch: 460-479228 460-479140 Analysis Batch: Prep Batch: Leach Batch: 460-479228 460-479140 N/A N/A Analyte RPD LimitRPDLimit % Rec. MS MSD MS Qual MSD Qual 105 102 64 - 129 3 304,4'-DDD 103 101 65 - 129 3 304,4'-DDE 104 105 59 - 124 0 304,4'-DDT 112 108 66 - 127 3 30Aldrin 118 115 69 - 131 2 30alpha-BHC 105 102 69 - 127 2 30beta-BHC 114 112 64 - 129 2 30delta-BHC 108 105 65 - 128 3 30Dieldrin 105 101 66 - 126 3 30Endosulfan I 108 111 64 - 124 2 30Endosulfan II 95 98 62 - 123 4 30Endosulfan sulfate 107 104 58 - 126 3 30Endrin 106 109 69 - 131 2 30Endrin aldehyde 106 104 62 - 125 2 30Endrin ketone 114 112 67 - 126 2 30gamma-BHC (Lindane) 109 107 63 - 125 2 30Heptachlor 108 105 64 - 125 2 30Heptachlor epoxide 102 101 56 - 123 1 30Methoxychlor Surrogate Acceptance LimitsMS % Rec MSD % Rec DCB Decachlorobiphenyl 102 99 50 - 150 Tetrachloro-m-xylene 109 109 47 - 150 TestAmerica Edison Page 164 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc SolidClient Matrix: 1.0Dilution: Lab Sample ID: 11/21/2017 1259 Method Blank - Batch: 460-478820 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: T136934.D +15.0000 g 10 mLUnits:mg/Kg Method: 8082A Preparation: 3546 CPESTGC11MB 460-478820/1-A Analysis Date: Analysis Batch: Prep Batch: Leach Batch: 460-478940 460-478820 N/A Prep Date:Injection Volume:11/21/2017 0049 1 uL Column ID:PRIMARYLeach Date:N/A Analyte Result Qual MDL RL 0.067 U 0.0670.0089Aroclor 1016 0.067 U 0.0670.0089Aroclor 1221 0.067 U 0.0670.0089Aroclor 1232 0.067 U 0.0670.0089Aroclor 1242 0.067 U 0.0670.0089Aroclor 1248 0.067 U 0.0670.0092Aroclor 1254 0.067 U 0.0670.0092Aroclor 1260 0.067 U 0.0670.0092Aroclor-1262 0.067 U 0.0670.0092Aroclor 1268 0.067 U 0.0670.0092Polychlorinated biphenyls, Total Surrogate % Rec Acceptance Limits DCB Decachlorobiphenyl 125 35 - 150 Surrogate % Rec Acceptance Limits DCB Decachlorobiphenyl 108 35 - 150 TestAmerica Edison Page 165 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Solid 1.0 Lab Control Sample - Batch: 460-478820 Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: T136935.D +15.0000 g 10 mLUnits:mg/Kg Method: 8082A Preparation: 3546 CPESTGC11LCS 460-478820/2-A Analysis Date: 11/21/2017 1314 Analysis Batch: Prep Batch: Leach Batch: 460-478940 460-478820 N/A Prep Date:Injection Volume:1 uL Leach Date: 11/21/2017 0049 Column ID:PRIMARYN/A Analyte QualLimit% Rec.ResultSpike Amount 0.333 0.325 97 77 - 150Aroclor 1016 0.333 0.332 100 79 - 150Aroclor 1260 Surrogate % Rec Acceptance Limits DCB Decachlorobiphenyl 126 35 - 150 Solid 1.0 Lab Control Sample - Batch: 460-478820 Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: T136935.D +15.0000 g 10 mLUnits:mg/Kg Method: 8082A Preparation: 3546 CPESTGC11LCS 460-478820/2-A Analysis Date: 11/21/2017 1314 Analysis Batch: Prep Batch: Leach Batch: 460-478940 460-478820 N/A Prep Date:Injection Volume:1 uL Leach Date: 11/21/2017 0049 Column ID:SECONDARYN/A Analyte QualLimit% Rec.ResultSpike Amount 0.333 0.317 95 77 - 150Aroclor 1016 0.333 0.295 88 79 - 150Aroclor 1260 Surrogate % Rec Acceptance Limits DCB Decachlorobiphenyl 106 35 - 150 TestAmerica Edison Page 166 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Dilution: Dilution: 11/21/2017 1358 11/21/2017 1412 Solid Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 460-478820 1.0 1.0 Client Matrix: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Column ID: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Column ID: Client Matrix:Solid 11/21/2017 0049 11/21/2017 0049 T136938.D +15.0001 g 10 mL 1 uL PRIMARY T136939.D +15.0016 g 10 mL 1 uL PRIMARY Method: 8082A Preparation: 3546 CPESTGC11 CPESTGC11 460-145455-A-6-D MS 460-145455-A-6-E MSD MS Lab Sample ID: MSD Lab Sample ID: Analysis Date: Prep Date: Leach Date:N/A Analysis Date: Prep Date: Leach Date:N/A Analysis Batch: Prep Batch: Leach Batch: 460-478940 460-478820 Analysis Batch: Prep Batch: Leach Batch: 460-478940 460-478820 N/A N/A Analyte RPD LimitRPDLimit % Rec. MS MSD MS Qual MSD Qual 127 126 77 - 150 1 30Aroclor 1016 88 92 79 - 150 3 30Aroclor 1260 Surrogate Acceptance LimitsMS % Rec MSD % Rec DCB Decachlorobiphenyl 123 119 35 - 150 Dilution: Dilution: 11/21/2017 1358 11/21/2017 1412 Solid Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 460-478820 1.0 1.0 Client Matrix: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Column ID: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Column ID: Client Matrix:Solid 11/21/2017 0049 11/21/2017 0049 T136938.D +15.0001 g 10 mL 1 uL SECONDARY T136939.D +15.0016 g 10 mL 1 uL SECONDARY Method: 8082A Preparation: 3546 CPESTGC11 CPESTGC11 460-145455-A-6-D MS 460-145455-A-6-E MSD MS Lab Sample ID: MSD Lab Sample ID: Analysis Date: Prep Date: Leach Date:N/A Analysis Date: Prep Date: Leach Date:N/A Analysis Batch: Prep Batch: Leach Batch: 460-478940 460-478820 Analysis Batch: Prep Batch: Leach Batch: 460-478940 460-478820 N/A N/A Analyte RPD LimitRPDLimit % Rec. MS MSD MS Qual MSD Qual 117 114 77 - 150 3 30Aroclor 1016 86 86 79 - 150 0 30Aroclor 1260 Surrogate Acceptance LimitsMS % Rec MSD % Rec DCB Decachlorobiphenyl 104 102 35 - 150 TestAmerica Edison Page 167 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc SolidClient Matrix: 1.0Dilution: Lab Sample ID: 11/22/2017 0859 Method Blank - Batch: 460-479142 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: T136990.D +15.0000 g 10 mLUnits:mg/Kg Method: 8082A Preparation: 3546 CPESTGC11MB 460-479142/1-A Analysis Date: Analysis Batch: Prep Batch: Leach Batch: 460-479233 460-479142 N/A Prep Date:Injection Volume:11/22/2017 0008 1 uL Column ID:PRIMARYLeach Date:N/A Analyte Result Qual MDL RL 0.067 U 0.0670.0089Aroclor 1016 0.067 U 0.0670.0089Aroclor 1221 0.067 U 0.0670.0089Aroclor 1232 0.067 U 0.0670.0089Aroclor 1242 0.067 U 0.0670.0089Aroclor 1248 0.067 U 0.0670.0092Aroclor 1254 0.067 U 0.0670.0092Aroclor 1260 0.067 U 0.0670.0092Aroclor-1262 0.067 U 0.0670.0092Aroclor 1268 0.067 U 0.0670.0092Polychlorinated biphenyls, Total Surrogate % Rec Acceptance Limits DCB Decachlorobiphenyl 93 35 - 150 Surrogate % Rec Acceptance Limits DCB Decachlorobiphenyl 92 35 - 150 TestAmerica Edison Page 168 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Solid 1.0 Lab Control Sample - Batch: 460-479142 Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: T136998.D +15.0000 g 10 mLUnits:mg/Kg Method: 8082A Preparation: 3546 CPESTGC11LCS 460-479142/2-A Analysis Date: 11/22/2017 1130 Analysis Batch: Prep Batch: Leach Batch: 460-479233 460-479142 N/A Prep Date:Injection Volume:1 uL Leach Date: 11/22/2017 0008 Column ID:PRIMARYN/A Analyte QualLimit% Rec.ResultSpike Amount 0.333 0.364 109 77 - 150Aroclor 1016 0.333 0.363 109 79 - 150Aroclor 1260 Surrogate % Rec Acceptance Limits DCB Decachlorobiphenyl 132 35 - 150 Solid 1.0 Lab Control Sample - Batch: 460-479142 Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: T136998.D +15.0000 g 10 mLUnits:mg/Kg Method: 8082A Preparation: 3546 CPESTGC11LCS 460-479142/2-A Analysis Date: 11/22/2017 1130 Analysis Batch: Prep Batch: Leach Batch: 460-479233 460-479142 N/A Prep Date:Injection Volume:1 uL Leach Date: 11/22/2017 0008 Column ID:SECONDARYN/A Analyte QualLimit% Rec.ResultSpike Amount 0.333 0.341 102 77 - 150Aroclor 1016 0.333 0.354 106 79 - 150Aroclor 1260 Surrogate % Rec Acceptance Limits DCB Decachlorobiphenyl 131 35 - 150 TestAmerica Edison Page 169 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Dilution: Dilution: 11/22/2017 0928 11/22/2017 0943 Solid Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 460-479142 1.0 1.0 Client Matrix: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Column ID: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Column ID: Client Matrix:Solid 11/22/2017 0008 11/22/2017 0008 T136992.D +15.0065 g 10 mL 1 uL PRIMARY T136993.D +15.0015 g 10 mL 1 uL PRIMARY Method: 8082A Preparation: 3546 CPESTGC11 CPESTGC11 460-145501-A-1-H MS 460-145501-A-1-I MSD MS Lab Sample ID: MSD Lab Sample ID: Analysis Date: Prep Date: Leach Date:N/A Analysis Date: Prep Date: Leach Date:N/A Analysis Batch: Prep Batch: Leach Batch: 460-479233 460-479142 Analysis Batch: Prep Batch: Leach Batch: 460-479233 460-479142 N/A N/A Analyte RPD LimitRPDLimit % Rec. MS MSD MS Qual MSD Qual 101 102 77 - 150 1 30Aroclor 1016 96 95 79 - 150 1 30Aroclor 1260 Surrogate Acceptance LimitsMS % Rec MSD % Rec DCB Decachlorobiphenyl 105 110 35 - 150 Dilution: Dilution: 11/22/2017 0928 11/22/2017 0943 Solid Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 460-479142 1.0 1.0 Client Matrix: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Column ID: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Injection Volume: Column ID: Client Matrix:Solid 11/22/2017 0008 11/22/2017 0008 T136992.D +15.0065 g 10 mL 1 uL SECONDARY T136993.D +15.0015 g 10 mL 1 uL SECONDARY Method: 8082A Preparation: 3546 CPESTGC11 CPESTGC11 460-145501-A-1-H MS 460-145501-A-1-I MSD MS Lab Sample ID: MSD Lab Sample ID: Analysis Date: Prep Date: Leach Date:N/A Analysis Date: Prep Date: Leach Date:N/A Analysis Batch: Prep Batch: Leach Batch: 460-479233 460-479142 Analysis Batch: Prep Batch: Leach Batch: 460-479233 460-479142 N/A N/A Analyte RPD LimitRPDLimit % Rec. MS MSD MS Qual MSD Qual 87 88 77 - 150 2 30Aroclor 1016 85 91 79 - 150 7 30Aroclor 1260 Surrogate Acceptance LimitsMS % Rec MSD % Rec DCB Decachlorobiphenyl 103 104 35 - 150 TestAmerica Edison Page 170 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc SolidClient Matrix: 2.0Dilution: Lab Sample ID: 11/22/2017 1233 Method Blank - Batch: 460-478536 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: 479166D1.asc 1.0 g 50 mLUnits:mg/Kg Method: 6010C Preparation: 3050B ICP5MB 460-478536/1-A ^2 Analysis Date: Analysis Batch: Prep Batch: Leach Batch: 460-479312 460-478536 N/A Prep Date: 11/20/2017 0237 Leach Date:N/A Analyte Result Qual MDL RL 20.0 U 20.04.1Aluminum 2.0 U 2.00.24Antimony 1.5 U 1.50.37Arsenic 20.0 U 20.01.6Barium 0.20 U 0.200.023Beryllium 0.40 U 0.400.060Cadmium 500 U 50051.0Calcium 1.0 U 1.00.28Chromium 5.0 U 5.00.57Cobalt 2.5 U 2.50.57Copper 15.0 U 15.02.7Iron 1.0 U 1.00.30Lead 500 U 50038.6Magnesium 1.5 U 1.50.16Manganese 4.0 U 4.00.38Nickel 500 U 50026.6Potassium 2.0 U 2.00.61Selenium 1.0 U 1.00.15Silver 500 U 50038.5Sodium 2.0 U 2.00.59Thallium 5.0 U 5.00.60Vanadium 3.0 U 3.00.26Zinc TestAmerica Edison Page 171 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Solid 4.0 LCS-Certified Reference Material - Batch: 460-478536 Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: 479166D1.asc 1.01 g 50 mLUnits:mg/Kg Method: 6010C Preparation: 3050B ICP5LCSSRM 460-478536/2-A ^4 Analysis Date: 11/22/2017 1218 Analysis Batch: Prep Batch: Leach Batch: 460-479312 460-478536 N/A Prep Date: Leach Date: 11/20/2017 0237 N/A Analyte QualLimit% Rec.ResultSpike Amount 8000 6735 84.2 47.4 - 152.5Aluminum 65.1 48.12 73.9 0.2 - 212.0Antimony 147 136.3 92.7 83.0 - 117.0Arsenic 314 304.0 96.8 82.2 - 117.8Barium 53.4 52.46 98.2 82.8 - 117.2Beryllium 193 184.3 95.5 82.4 - 117.6Cadmium 4580 4176 91.2 80.8 - 119.0Calcium 82.6 80.28 97.2 81.8 - 118.2Chromium 81.3 80.89 99.5 83.4 - 116.6Cobalt 171 158.2 92.5 83.6 - 116.4Copper 14100 13490 95.7 60.4 - 139.7Iron 92.3 92.81 100.6 82.8 - 117.0Lead 2240 2026 90.4 75.4 - 125.0Magnesium 222 221.0 99.5 82.0 - 118.0Manganese 137 138.1 100.8 82.5 - 118.2Nickel 2000 1793 89.6 69.5 - 130.5Potassium 187 173.3 92.7 79.1 - 121.4Selenium 40.7 36.93 90.7 79.6 - 120.4Silver 216 183.0 84.7 J72.2 - 127.8Sodium 153 162.3 106.1 81.0 - 119.0Thallium 86.6 81.70 94.3 77.6 - 122.4Vanadium 189 184.4 97.6 79.9 - 120.1Zinc TestAmerica Edison Page 172 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Solid 4.0 Matrix Spike - Batch: 460-478536 Lab Sample ID: Client Matrix: Dilution: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: 479166D1.asc 1.05 g 50 mLUnits:mg/Kg Method: 6010C Preparation: 3050B ICP5460-145281-A-1-C MS ^4 Analysis Date: 11/22/2017 1210 Analysis Batch: Prep Batch: Leach Batch: 460-479312 460-478536 N/A Prep Date: Leach Date: 11/20/2017 0237 N/A Analyte QualLimit% Rec.ResultSpike AmountSample Result/Qual 35200 224 35340 40 75 - 125 4Aluminum 7.5 224 211.0 91 75 - 125Arsenic 183 224 376.4 86 75 - 125Barium 2.2 5.60 7.62 97 75 - 125Beryllium 0.91 U 5.60 4.97 89 75 - 125Cadmium 858 J 2240 2961 94 75 - 125Calcium 50.0 22.4 76.56 119 75 - 125Chromium 15.0 56.0 70.21 99 75 - 125Cobalt 26.9 28.0 53.92 97 75 - 125Copper 41600 112 42460 731 75 - 125 4Iron 25.0 56.0 84.69 107 75 - 125Lead 6950 2240 8411 65 75 - 125 NMagnesium 442 56.0 492.6 91 75 - 125 4Manganese 24.8 56.0 79.97 99 75 - 125Nickel 5540 2240 6887 60 75 - 125 NPotassium 4.6 U 224 201.9 90 75 - 125Selenium 2.3 U 5.60 4.61 82 75 - 125Silver 1140 U 2240 2162 97 75 - 125Sodium 4.6 U 224 226.7 101 75 - 125Thallium 98.1 56.0 146.8 87 75 - 125Vanadium 72.4 56.0 128.5 100 75 - 125Zinc TestAmerica Edison Page 173 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc mg/KgUnits: Solid Dilution:4.0 Duplicate - Batch: 460-478536 Lab Sample ID: Client Matrix: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: 479166D1.asc 1.0 g 50 mL Method: 6010C Preparation: 3050B ICP5460-145281-A-1-B DU ^4 Analysis Date: Analysis Batch: 11/22/2017 1214 Prep Batch: Leach Batch:N/A 460-479312 460-478536 Prep Date: Leach Date: 11/20/2017 0237 N/A Analyte QualLimitRPDResultSample Result/Qual 3245035200 8 20Aluminum 7.407.5 0.9 20Arsenic 153.8183 17 20Barium 2.082.2 7 20Beryllium 0.940.91 U NC 20 UCadmium 962.3858 J 12 20 JCalcium 47.6150.0 5 20Chromium 13.7615.0 9 20Cobalt 23.7626.9 12 20Copper 3943041600 5 20Iron 28.8325.0 14 20Lead 59526950 15 20Magnesium 405.8442 9 20Manganese 23.5224.8 5 20Nickel 43645540 24 20 *Potassium 4.74.6 U NC 20 USelenium 2.32.3 U NC 20 USilver 11701140 U NC 20 USodium 4.74.6 U NC 20 UThallium 87.4498.1 11 20Vanadium 68.4572.4 6 20Zinc TestAmerica Edison Page 174 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc SolidClient Matrix: 2.0Dilution: Lab Sample ID: 11/22/2017 1143 Method Blank - Batch: 460-479166 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: 479166D1.asc 1.0 g 50 mLUnits:mg/Kg Method: 6010C Preparation: 3050B ICP5MB 460-479166/1-A ^2 Analysis Date: Analysis Batch: Prep Batch: Leach Batch: 460-479312 460-479166 N/A Prep Date: 11/22/2017 0239 Leach Date:N/A Analyte Result Qual MDL RL 20.0 U 20.04.1Aluminum 2.0 U 2.00.24Antimony 1.5 U 1.50.37Arsenic 20.0 U 20.01.6Barium 0.20 U 0.200.023Beryllium 0.40 U 0.400.060Cadmium 500 U 50051.0Calcium 1.0 U 1.00.28Chromium 5.0 U 5.00.57Cobalt 2.5 U 2.50.57Copper 15.0 U 15.02.7Iron 1.0 U 1.00.30Lead 500 U 50038.6Magnesium 1.5 U 1.50.16Manganese 4.0 U 4.00.38Nickel 500 U 50026.6Potassium 2.0 U 2.00.61Selenium 1.0 U 1.00.15Silver 500 U 50038.5Sodium 2.0 U 2.00.59Thallium 5.0 U 5.00.60Vanadium 3.0 U 3.00.26Zinc TestAmerica Edison Page 175 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Solid 4.0 LCS-Certified Reference Material - Batch: 460-479166 Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: 479166D1.asc 1.01 g 50 mLUnits:mg/Kg Method: 6010C Preparation: 3050B ICP5LCSSRM 460-479166/2-A ^4 Analysis Date: 11/22/2017 1125 Analysis Batch: Prep Batch: Leach Batch: 460-479312 460-479166 N/A Prep Date: Leach Date: 11/22/2017 0239 N/A Analyte QualLimit% Rec.ResultSpike Amount 8000 6721 84.0 47.4 - 152.5Aluminum 65.1 47.58 73.1 0.2 - 212.0Antimony 147 133.8 91.0 83.0 - 117.0Arsenic 314 311.3 99.1 82.2 - 117.8Barium 53.4 51.96 97.3 82.8 - 117.2Beryllium 193 184.0 95.3 82.4 - 117.6Cadmium 4580 4168 91.0 80.8 - 119.0Calcium 82.6 78.79 95.4 81.8 - 118.2Chromium 81.3 81.90 100.7 83.4 - 116.6Cobalt 171 156.4 91.5 83.6 - 116.4Copper 14100 12880 91.3 60.4 - 139.7Iron 92.3 91.43 99.1 82.8 - 117.0Lead 2240 2008 89.6 75.4 - 125.0Magnesium 222 212.1 95.5 82.0 - 118.0Manganese 137 139.4 101.8 82.5 - 118.2Nickel 2000 1785 89.2 69.5 - 130.5Potassium 187 172.4 92.2 79.1 - 121.4Selenium 40.7 35.92 88.3 79.6 - 120.4Silver 216 187.9 87.0 J72.2 - 127.8Sodium 153 157.9 103.2 81.0 - 119.0Thallium 86.6 81.41 94.0 77.6 - 122.4Vanadium 189 186.3 98.6 79.9 - 120.1Zinc TestAmerica Edison Page 176 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc Solid 4.0 Matrix Spike - Batch: 460-479166 Lab Sample ID: Client Matrix: Dilution: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: 479166D1.asc 1.05 g 50 mLUnits:mg/Kg Method: 6010C Preparation: 3050B ICP5460-145501-B-1-D MS ^4 Analysis Date: 11/22/2017 1109 Analysis Batch: Prep Batch: Leach Batch: 460-479312 460-479166 N/A Prep Date: Leach Date: 11/22/2017 0239 N/A Analyte QualLimit% Rec.ResultSpike AmountSample Result/Qual 6170 221 6867 314 75 - 125 4Aluminum 4.5 U 55.2 30.95 56 75 - 125 NAntimony 6.1 221 214.4 94 75 - 125Arsenic 75.3 221 295.3 100 75 - 125Barium 0.47 5.52 5.94 99 75 - 125Beryllium 0.13 J 5.52 5.64 100 75 - 125Cadmium 7700 2210 8665 44 75 - 125 NCalcium 16.8 22.1 37.18 92 75 - 125Chromium 7.1 J 55.2 63.24 102 75 - 125Cobalt 54.0 27.6 75.63 78 75 - 125Copper 16200 110 14450 -1616 75 - 125 4Iron 137 55.2 174.1 68 75 - 125 NLead 2650 2210 4539 86 75 - 125Magnesium 194 55.2 224.4 55 75 - 125 NManganese 16.6 55.2 70.91 98 75 - 125Nickel 954 J 2210 3103 97 75 - 125Potassium 4.5 U 221 207.3 94 75 - 125Selenium 2.3 U 5.52 4.95 90 75 - 125Silver 188 J 2210 2313 96 75 - 125Sodium 4.5 U 221 232.4 105 75 - 125Thallium 22.3 55.2 75.88 97 75 - 125Vanadium 125 55.2 165.5 74 75 - 125 NZinc TestAmerica Edison Page 177 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc mg/KgUnits: Solid Dilution:4.0 Duplicate - Batch: 460-479166 Lab Sample ID: Client Matrix: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: 479166D1.asc 1.05 g 50 mL Method: 6010C Preparation: 3050B ICP5460-145501-B-1-C DU ^4 Analysis Date: Analysis Batch: 11/22/2017 1113 Prep Batch: Leach Batch:N/A 460-479312 460-479166 Prep Date: Leach Date: 11/22/2017 0239 N/A Analyte QualLimitRPDResultSample Result/Qual 59906170 3 20Aluminum 4.44.5 U NC 20 UAntimony 5.056.1 19 20Arsenic 105.275.3 33 20Barium 0.4900.47 3 20Beryllium 0.880.13 J NC 20 UCadmium 92867700 19 20Calcium 15.2016.8 10 20Chromium 6.277.1 J 13 20 JCobalt 62.7154.0 15 20Copper 1442016200 12 20Iron 152.9137 11 20Lead 30532650 14 20Magnesium 182.7194 6 20Manganese 15.3116.6 8 20Nickel 960.2954 J 0.6 20 JPotassium 4.44.5 U NC 20 USelenium 2.22.3 U NC 20 USilver 192.9188 J 3 20 JSodium 4.44.5 U NC 20 UThallium 21.8122.3 2 20Vanadium 125.8125 0.9 20Zinc TestAmerica Edison Page 178 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc SolidClient Matrix: 1.0Dilution: Lab Sample ID: 11/20/2017 1031 Method Blank - Batch: 460-478547 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: 478540HG1.CSV 0.60 g 50 mLUnits:mg/Kg Method: 7471B Preparation: 7471B LEEMAN7MB 460-478547/1-A Analysis Date: Analysis Batch: Prep Batch: Leach Batch: 460-478647 460-478547 N/A Prep Date: 11/20/2017 0511 Leach Date:N/A Analyte Result Qual MDL RL 0.017 U 0.0170.011Mercury Solid 40 LCS-Certified Reference Material - Batch: 460-478547 Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: 478540HG1.CSV 0.60 g 50 mLUnits:mg/Kg Method: 7471B Preparation: 7471B LEEMAN7LCSSRM 460-478547/2-A ^40 Analysis Date: 11/20/2017 1033 Analysis Batch: Prep Batch: Leach Batch: 460-478647 460-478547 N/A Prep Date: Leach Date: 11/20/2017 0511 N/A Analyte QualLimit% Rec.ResultSpike Amount 17.8 17.07 95.9 66.9 - 133.1Mercury Solid 1.0 Matrix Spike - Batch: 460-478547 Lab Sample ID: Client Matrix: Dilution: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: 478540HG1.CSV 0.65 g 50 mLUnits:mg/Kg Method: 7471B Preparation: 7471B LEEMAN7460-145378-E-1-E MS Analysis Date: 11/20/2017 1038 Analysis Batch: Prep Batch: Leach Batch: 460-478647 460-478547 N/A Prep Date: Leach Date: 11/20/2017 0511 N/A Analyte QualLimit% Rec.ResultSpike AmountSample Result/Qual 0.055 0.0839 0.155 119 75 - 125Mercury TestAmerica Edison Page 179 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc mg/KgUnits: Solid Dilution:1.0 Duplicate - Batch: 460-478547 Lab Sample ID: Client Matrix: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: 478540HG1.CSV 0.65 g 50 mL Method: 7471B Preparation: 7471B LEEMAN7460-145378-E-1-D DU Analysis Date: Analysis Batch: 11/20/2017 1036 Prep Batch: Leach Batch:N/A 460-478647 460-478547 Prep Date: Leach Date: 11/20/2017 0511 N/A Analyte QualLimitRPDResultSample Result/Qual 0.05730.055 4 20Mercury TestAmerica Edison Page 180 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc SolidClient Matrix: 1.0Dilution: Lab Sample ID: 11/22/2017 1050 Method Blank - Batch: 460-479171 Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: 479171HG1.CSV 0.60 g 50 mLUnits:mg/Kg Method: 7471B Preparation: 7471B LEEMAN7MB 460-479171/10-A Analysis Date: Analysis Batch: Prep Batch: Leach Batch: 460-479302 460-479171 N/A Prep Date: 11/22/2017 0402 Leach Date:N/A Analyte Result Qual MDL RL 0.017 U 0.0170.011Mercury Solid 40 LCS-Certified Reference Material - Batch: 460-479171 Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: 479171HG1.CSV 0.60 g 50 mLUnits:mg/Kg Method: 7471B Preparation: 7471B LEEMAN7LCSSRM 460-479171/11-A ^40 Analysis Date: 11/22/2017 0853 Analysis Batch: Prep Batch: Leach Batch: 460-479302 460-479171 N/A Prep Date: Leach Date: 11/22/2017 0402 N/A Analyte QualLimit% Rec.ResultSpike Amount 17.8 18.82 105.8 66.9 - 133.1Mercury Solid 1.0 Matrix Spike - Batch: 460-479171 Lab Sample ID: Client Matrix: Dilution: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: 479171HG1.CSV 0.61 g 50 mLUnits:mg/Kg Method: 7471B Preparation: 7471B LEEMAN7460-144734-A-6-D MS Analysis Date: 11/22/2017 0859 Analysis Batch: Prep Batch: Leach Batch: 460-479302 460-479171 N/A Prep Date: Leach Date: 11/22/2017 0402 N/A Analyte QualLimit% Rec.ResultSpike AmountSample Result/Qual 0.019 U 0.0953 0.0966 101 75 - 125Mercury TestAmerica Edison Page 181 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc mg/KgUnits: Solid Dilution:1.0 Duplicate - Batch: 460-479171 Lab Sample ID: Client Matrix: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: 479171HG1.CSV 0.61 g 50 mL Method: 7471B Preparation: 7471B LEEMAN7460-144734-A-6-C DU Analysis Date: Analysis Batch: 11/22/2017 0857 Prep Batch: Leach Batch:N/A 460-479302 460-479171 Prep Date: Leach Date: 11/22/2017 0402 N/A Analyte QualLimitRPDResultSample Result/Qual 0.0190.019 U NC 20 UMercury TestAmerica Edison Page 182 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc %Units: Solid Dilution:1.0 Duplicate - Batch: 460-478966 Lab Sample ID: Client Matrix: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Method: Moisture Preparation: N/A No Equipment Assigned460-145401-3 Analysis Date: Analysis Batch: 11/21/2017 1112 Prep Batch: Leach Batch: N/AN/A N/A 460-478966 Prep Date: Leach Date: N/A N/A Analyte QualLimitRPDResultSample Result/Qual 8.58.1 6 20Percent Moisture 91.591.9 0.5 20Percent Solids TestAmerica Edison Page 183 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc %Units: Solid Dilution:1.0 Duplicate - Batch: 460-478972 Lab Sample ID: Client Matrix: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Method: Moisture Preparation: N/A No Equipment Assigned460-145407-B-8 DU Analysis Date: Analysis Batch: 11/21/2017 1130 Prep Batch: Leach Batch: N/AN/A N/A 460-478972 Prep Date: Leach Date: N/A N/A Analyte QualLimitRPDResultSample Result/Qual 17.617.8 1 20Percent Moisture 82.482.2 0.2 20Percent Solids TestAmerica Edison Page 184 of 194 Quality Control Results Job Number: 460-145401-1Client: AKRF Inc %Units: Solid Dilution:1.0 Duplicate - Batch: 460-479372 Lab Sample ID: Client Matrix: Instrument ID: Lab File ID: Initial Weight/Volume: Final Weight/Volume: Method: Moisture Preparation: N/A No Equipment Assigned460-145555-E-1 DU Analysis Date: Analysis Batch: 11/22/2017 1538 Prep Batch: Leach Batch: N/AN/A N/A 460-479372 Prep Date: Leach Date: N/A N/A Analyte QualLimitRPDResultSample Result/Qual 16.316.2 0.8 20Percent Moisture 83.783.8 0.2 20Percent Solids TestAmerica Edison Page 185 of 194 Page 186 of 194 Page 187 of 194 Page 188 of 194 Page 189 of 194 Page 190 of 194 Page 191 of 194 Login Sample Receipt Checklist Client: AKRF Inc Job Number: 460-145401-1 Login Number: 145401 Question Answer Comment Creator: Rivera, Kenneth List Source: TestAmerica Edison List Number: 1 N/ARadioactivity wasn't checked or is </= background as measured by a survey meter. TrueThe cooler's custody seal, if present, is intact. TrueSample custody seals, if present, are intact. TrueThe cooler or samples do not appear to have been compromised or tampered with. TrueSamples were received on ice. TrueCooler Temperature is acceptable. TrueCooler Temperature is recorded. TrueCOC is present. TrueCOC is filled out in ink and legible. TrueCOC is filled out with all pertinent information. TrueIs the Field Sampler's name present on COC? TrueThere are no discrepancies between the containers received and the COC. TrueSamples are received within Holding Time (excluding tests with immediate HTs) TrueSample containers have legible labels. TrueContainers are not broken or leaking. TrueSample collection date/times are provided. TrueAppropriate sample containers are used. TrueSample bottles are completely filled. TrueSample Preservation Verified. TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4"). TrueMultiphasic samples are not present. TrueSamples do not require splitting or compositing. N/AResidual Chlorine Checked. TestAmerica Edison Page 192 of 194 Login Sample Receipt Checklist Client: AKRF Inc Job Number: 460-145401-1 Login Number: 145515 Question Answer Comment Creator: Meyers, Gary List Source: TestAmerica Edison List Number: 1 N/ARadioactivity wasn't checked or is </= background as measured by a survey meter. N/AThe cooler's custody seal, if present, is intact.Not present TrueSample custody seals, if present, are intact. TrueThe cooler or samples do not appear to have been compromised or tampered with. TrueSamples were received on ice. TrueCooler Temperature is acceptable. TrueCooler Temperature is recorded. TrueCOC is present. TrueCOC is filled out in ink and legible. TrueCOC is filled out with all pertinent information. TrueIs the Field Sampler's name present on COC? TrueThere are no discrepancies between the containers received and the COC. TrueSamples are received within Holding Time (excluding tests with immediate HTs) TrueSample containers have legible labels. TrueContainers are not broken or leaking. TrueSample collection date/times are provided. TrueAppropriate sample containers are used. TrueSample bottles are completely filled. TrueSample Preservation Verified. TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4"). TrueMultiphasic samples are not present. TrueSamples do not require splitting or compositing. N/AResidual Chlorine Checked.No analysis requiring residual chlorine check assigned. TestAmerica Edison Page 193 of 194 Login Sample Receipt Checklist Client: AKRF Inc Job Number: 460-145401-1 Login Number: 145597 Question Answer Comment Creator: Villanueva, Angelica P List Source: TestAmerica Edison List Number: 1 N/ARadioactivity wasn't checked or is </= background as measured by a survey meter. TrueThe cooler's custody seal, if present, is intact. TrueSample custody seals, if present, are intact. TrueThe cooler or samples do not appear to have been compromised or tampered with. TrueSamples were received on ice. TrueCooler Temperature is acceptable. TrueCooler Temperature is recorded. TrueCOC is present. TrueCOC is filled out in ink and legible. TrueCOC is filled out with all pertinent information. TrueIs the Field Sampler's name present on COC? TrueThere are no discrepancies between the containers received and the COC. TrueSamples are received within Holding Time (excluding tests with immediate HTs) TrueSample containers have legible labels. TrueContainers are not broken or leaking. TrueSample collection date/times are provided. TrueAppropriate sample containers are used. TrueSample bottles are completely filled. TrueSample Preservation Verified. TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs FalseContainers requiring zero headspace have no headspace or bubble is <6mm (1/4"). Refer to Job Narrative for details. TrueMultiphasic samples are not present. TrueSamples do not require splitting or compositing. N/AResidual Chlorine Checked. TestAmerica Edison Page 194 of 194 ANALYTICAL REPORT Job Number: 200-41113-1 SDG Number: 200-41113-1 Job Description: 900 King Street For: AKRF Inc 440 Park Avenue South 7th Floor New York, NY 10016 Attention: Ms. Elizabeth Matamoros _____________________________________________ Approved for release. Kristine A Dusablon Project Manager II 11/30/2017 10:10 AM Kristine A Dusablon, Project Manager II 30 Community Drive, South Burlington, VT, 05403 (802)660-1990 kris.dusablon@testamericainc.com 11/30/2017 cc: Mr. Timothy McClintock The test results in this report relate only to sample(s) as received by the laboratory. These test results were derived under a quality system that adheres to the requirements of NELAC. Pursuant to NELAC, this report may not be produced in full without written approval from the laboratory TestAmerica Laboratories, Inc. TestAmerica Burlington 30 Community Drive, Suite 11, South Burlington, VT 05403 Tel (802) 660-1990 Fax (802) 660-1919 www.testamericainc.com Page 1 of 478 Table of Contents Cover Title Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Data Summaries . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5 Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9 Default Detection Limits . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .23 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .26 QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .33 Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .34 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .35 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .36 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .37 Detection Limit Exceptions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .38 Manual Integration Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .39 Reagent Traceability . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .42 COAs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .123 Organic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 135 Air - GC/MS VOA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .135 Method TO15 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .135 Method TO15 QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .136 Method TO15 Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .143 Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .298 Method TO15 ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .298 Method TO15 CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .352 Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .366 Page 2 of 478 Table of Contents Method TO15 Tune Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .366 Method TO15 Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .374 Method TO15 LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .385 Method TO15 Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .392 Method TO15 Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .394 Clean Canister Certification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .395 Pre-shipment Certification . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .395 LCS Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .397 Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .401 Tune Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .417 IS/RT Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .421 Clean Canister Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .425 ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .439 ICV/CCV Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .459 Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .471 Shipping and Receiving Documents . . . . . . . . . . . . . . . . . . . . . . . . . . . 475 Client Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .476 Sample Receipt Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .478 Page 3 of 478 Definitions/Glossary TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Qualifiers Air - GC/MS VOA Qualifier Description U Indicates the analyte was analyzed for but not detected. Qualifier Air - GC/MS VOA TICs Qualifier Description J Indicates an Estimated Value for TICs Qualifier N This flag indicates the presumptive evidence of a compound. Glossary These commonly used abbreviations may or may not be present in this report. ¤Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation %R Percent Recovery CFL Contains Free Liquid CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TestAmerica Burlington Page 4 of 478 CASE NARRATIVE Client: AKRF Inc Project: 900 King Street Report Number: 200-41113-1 With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required. Calculations are performed before rounding to avoid round-off errors in calculated results. All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below. RECEIPT The samples were received on 11/22/2017; the samples arrived in good condition. VOLATILE ORGANIC COMPOUNDS Samples SV-3, SV-2, SV-1 and AA-1 were analyzed for Volatile Organic Compounds in accordance with EPA Method TO-15. The samples were analyzed on 11/24/2017. Samples SV-2[2.98X] and SV-1[2.5X] required dilution prior to analysis. The reporting limits have been adjusted accordingly. No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. Page 5 of 478 Detection Summary TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Client Sample ID: SV-3 Lab Sample ID: 200-41113-1 n-Butane RL 0.50 ppb v/v RLAnalyteResult Qualifier Unit Dil Fac D Method Prep Type Total/NA111TO-15 1,3-Butadiene 0.20 ppb v/v Total/NA12.1 TO-15 Acetone 5.0 ppb v/v Total/NA112TO-15 Carbon disulfide 0.50 ppb v/v Total/NA13.6 TO-15 n-Hexane 0.20 ppb v/v Total/NA11.3 TO-15 Methyl Ethyl Ketone 0.50 ppb v/v Total/NA12.5 TO-15 Chloroform 0.20 ppb v/v Total/NA15.1 TO-15 Cyclohexane 0.20 ppb v/v Total/NA10.35 TO-15 Carbon tetrachloride 0.035 ppb v/v Total/NA10.052 TO-15 Benzene 0.20 ppb v/v Total/NA11.5 TO-15 n-Heptane 0.20 ppb v/v Total/NA10.65 TO-15 Bromodichloromethane 0.20 ppb v/v Total/NA10.38 TO-15 Toluene 0.20 ppb v/v Total/NA16.0 TO-15 Ethylbenzene 0.20 ppb v/v Total/NA10.97 TO-15 m,p-Xylene 0.50 ppb v/v Total/NA12.8 TO-15 Xylene, o-0.20 ppb v/v Total/NA10.99 TO-15 Xylene (total)0.70 ppb v/v Total/NA13.8 TO-15 n-Propylbenzene 0.20 ppb v/v Total/NA10.26 TO-15 4-Ethyltoluene 0.20 ppb v/v Total/NA10.36 TO-15 1,3,5-Trimethylbenzene 0.20 ppb v/v Total/NA10.32 TO-15 1,2,4-Trimethylbenzene 0.20 ppb v/v Total/NA11.1 TO-15 n-Butane RL 1.2 ug/m3 RLAnalyteResult Qualifier Unit Dil Fac D Method Prep Type Total/NA125TO-15 1,3-Butadiene 0.44 ug/m3 Total/NA14.7 TO-15 Acetone 12 ug/m3 Total/NA130TO-15 Carbon disulfide 1.6 ug/m3 Total/NA111TO-15 n-Hexane 0.70 ug/m3 Total/NA14.5 TO-15 Methyl Ethyl Ketone 1.5 ug/m3 Total/NA17.5 TO-15 Chloroform 0.98 ug/m3 Total/NA125TO-15 Cyclohexane 0.69 ug/m3 Total/NA11.2 TO-15 Carbon tetrachloride 0.22 ug/m3 Total/NA10.32 TO-15 Benzene 0.64 ug/m3 Total/NA14.9 TO-15 n-Heptane 0.82 ug/m3 Total/NA12.7 TO-15 Bromodichloromethane 1.3 ug/m3 Total/NA12.5 TO-15 Toluene 0.75 ug/m3 Total/NA123TO-15 Ethylbenzene 0.87 ug/m3 Total/NA14.2 TO-15 m,p-Xylene 2.2 ug/m3 Total/NA112TO-15 Xylene, o-0.87 ug/m3 Total/NA14.3 TO-15 Xylene (total)3.0 ug/m3 Total/NA116TO-15 n-Propylbenzene 0.98 ug/m3 Total/NA11.3 TO-15 4-Ethyltoluene 0.98 ug/m3 Total/NA11.8 TO-15 1,3,5-Trimethylbenzene 0.98 ug/m3 Total/NA11.6 TO-15 1,2,4-Trimethylbenzene 0.98 ug/m3 Total/NA15.5 TO-15 Client Sample ID: SV-2 Lab Sample ID: 200-41113-2 n-Butane RL 1.5 ppb v/v RLAnalyteResult Qualifier Unit Dil Fac D Method Prep Type Total/NA2.9817 TO-15 1,3-Butadiene 0.60 ppb v/v Total/NA2.982.2 TO-15 Acetone 15 ppb v/v Total/NA2.9838 TO-15 TestAmerica Burlington This Detection Summary does not include radiochemical test results. Page 6 of 478 Detection Summary TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Client Sample ID: SV-2 (Continued)Lab Sample ID: 200-41113-2 Carbon disulfide RL 1.5 ppb v/v RLAnalyteResult Qualifier Unit Dil Fac D Method Prep Type Total/NA2.985.1 TO-15 n-Hexane 0.60 ppb v/v Total/NA2.981.3 TO-15 Methyl Ethyl Ketone 1.5 ppb v/v Total/NA2.986.0 TO-15 Chloroform 0.60 ppb v/v Total/NA2.985.3 TO-15 2,2,4-Trimethylpentane 0.60 ppb v/v Total/NA2.9820 TO-15 Benzene 0.60 ppb v/v Total/NA2.981.4 TO-15 n-Heptane 0.60 ppb v/v Total/NA2.980.71 TO-15 Toluene 0.60 ppb v/v Total/NA2.985.0 TO-15 Ethylbenzene 0.60 ppb v/v Total/NA2.9837 TO-15 m,p-Xylene 1.5 ppb v/v Total/NA2.98140 TO-15 Xylene, o-0.60 ppb v/v Total/NA2.9846 TO-15 Xylene (total)2.1 ppb v/v Total/NA2.98190 TO-15 Cumene 0.60 ppb v/v Total/NA2.980.67 TO-15 1,2,4-Trimethylbenzene 0.60 ppb v/v Total/NA2.980.75 TO-15 n-Butane RL 3.5 ug/m3 RLAnalyteResult Qualifier Unit Dil Fac D Method Prep Type Total/NA2.9840 TO-15 1,3-Butadiene 1.3 ug/m3 Total/NA2.984.9 TO-15 Acetone 35 ug/m3 Total/NA2.9890 TO-15 Carbon disulfide 4.6 ug/m3 Total/NA2.9816 TO-15 n-Hexane 2.1 ug/m3 Total/NA2.984.5 TO-15 Methyl Ethyl Ketone 4.4 ug/m3 Total/NA2.9818 TO-15 Chloroform 2.9 ug/m3 Total/NA2.9826 TO-15 2,2,4-Trimethylpentane 2.8 ug/m3 Total/NA2.9893 TO-15 Benzene 1.9 ug/m3 Total/NA2.984.3 TO-15 n-Heptane 2.4 ug/m3 Total/NA2.982.9 TO-15 Toluene 2.2 ug/m3 Total/NA2.9819 TO-15 Ethylbenzene 2.6 ug/m3 Total/NA2.98160 TO-15 m,p-Xylene 6.5 ug/m3 Total/NA2.98620 TO-15 Xylene, o-2.6 ug/m3 Total/NA2.98200 TO-15 Xylene (total)9.1 ug/m3 Total/NA2.98810 TO-15 Cumene 2.9 ug/m3 Total/NA2.983.3 TO-15 1,2,4-Trimethylbenzene 2.9 ug/m3 Total/NA2.983.7 TO-15 Client Sample ID: SV-1 Lab Sample ID: 200-41113-3 n-Butane RL 1.3 ppb v/v RLAnalyteResult Qualifier Unit Dil Fac D Method Prep Type Total/NA2.544 TO-15 1,3-Butadiene 0.50 ppb v/v Total/NA2.53.3 TO-15 Carbon disulfide 1.3 ppb v/v Total/NA2.55.2 TO-15 n-Hexane 0.50 ppb v/v Total/NA2.51.5 TO-15 Methyl Ethyl Ketone 1.3 ppb v/v Total/NA2.51.4 TO-15 Chloroform 0.50 ppb v/v Total/NA2.52.3 TO-15 Cyclohexane 0.50 ppb v/v Total/NA2.50.73 TO-15 Benzene 0.50 ppb v/v Total/NA2.51.6 TO-15 n-Heptane 0.50 ppb v/v Total/NA2.50.74 TO-15 Toluene 0.50 ppb v/v Total/NA2.54.4 TO-15 Ethylbenzene 0.50 ppb v/v Total/NA2.59.1 TO-15 m,p-Xylene 1.3 ppb v/v Total/NA2.536 TO-15 Xylene, o-0.50 ppb v/v Total/NA2.512 TO-15 Xylene (total)1.8 ppb v/v Total/NA2.548 TO-15 TestAmerica Burlington This Detection Summary does not include radiochemical test results. Page 7 of 478 Detection Summary TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Client Sample ID: SV-1 (Continued)Lab Sample ID: 200-41113-3 1,2,4-Trimethylbenzene RL 0.50 ppb v/v RLAnalyteResult Qualifier Unit Dil Fac D Method Prep Type Total/NA2.50.93 TO-15 n-Butane RL 3.0 ug/m3 RLAnalyteResult Qualifier Unit Dil Fac D Method Prep Type Total/NA2.5110 TO-15 1,3-Butadiene 1.1 ug/m3 Total/NA2.57.3 TO-15 Carbon disulfide 3.9 ug/m3 Total/NA2.516 TO-15 n-Hexane 1.8 ug/m3 Total/NA2.55.4 TO-15 Methyl Ethyl Ketone 3.7 ug/m3 Total/NA2.54.2 TO-15 Chloroform 2.4 ug/m3 Total/NA2.511 TO-15 Cyclohexane 1.7 ug/m3 Total/NA2.52.5 TO-15 Benzene 1.6 ug/m3 Total/NA2.55.1 TO-15 n-Heptane 2.0 ug/m3 Total/NA2.53.1 TO-15 Toluene 1.9 ug/m3 Total/NA2.517 TO-15 Ethylbenzene 2.2 ug/m3 Total/NA2.540 TO-15 m,p-Xylene 5.4 ug/m3 Total/NA2.5150 TO-15 Xylene, o-2.2 ug/m3 Total/NA2.553 TO-15 Xylene (total)7.6 ug/m3 Total/NA2.5210 TO-15 1,2,4-Trimethylbenzene 2.5 ug/m3 Total/NA2.54.6 TO-15 Client Sample ID: AA-1 Lab Sample ID: 200-41113-4 Carbon tetrachloride RL 0.035 ppb v/v RLAnalyteResult Qualifier Unit Dil Fac D Method Prep Type Total/NA10.061 TO-15 Carbon tetrachloride RL 0.22 ug/m3 RLAnalyteResult Qualifier Unit Dil Fac D Method Prep Type Total/NA10.39 TO-15 TestAmerica Burlington This Detection Summary does not include radiochemical test results. Page 8 of 478 Client Sample Results TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Lab Sample ID: 200-41113-1Client Sample ID: SV-3 Matrix: AirDate Collected: 11/20/17 13:18 Date Received: 11/22/17 10:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air RL RL Dichlorodifluoromethane 0.50 U 0.50 ppb v/v 11/24/17 15:47 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier 0.50 ppb v/v 11/24/17 15:47 1Freon 22 0.50 U 0.20 ppb v/v 11/24/17 15:47 11,2-Dichlorotetrafluoroethane 0.20 U 0.50 ppb v/v 11/24/17 15:47 1Chloromethane0.50 U 0.50 ppb v/v 11/24/17 15:47 1n-Butane 11 0.035 ppb v/v 11/24/17 15:47 1Vinyl chloride 0.035 U 0.20 ppb v/v 11/24/17 15:47 11,3-Butadiene 2.1 0.20 ppb v/v 11/24/17 15:47 1Bromomethane0.20 U 0.50 ppb v/v 11/24/17 15:47 1Chloroethane0.50 U 0.20 ppb v/v 11/24/17 15:47 1Bromoethene(Vinyl Bromide)0.20 U 0.20 ppb v/v 11/24/17 15:47 1Trichlorofluoromethane0.20 U 0.20 ppb v/v 11/24/17 15:47 1Freon TF 0.20 U 0.035 ppb v/v 11/24/17 15:47 11,1-Dichloroethene 0.035 U 5.0 ppb v/v 11/24/17 15:47 1Acetone12 5.0 ppb v/v 11/24/17 15:47 1Isopropyl alcohol 5.0 U 0.50 ppb v/v 11/24/17 15:47 1Carbon disulfide 3.6 0.50 ppb v/v 11/24/17 15:47 13-Chloropropene 0.50 U 0.50 ppb v/v 11/24/17 15:47 1Methylene Chloride 0.50 U 5.0 ppb v/v 11/24/17 15:47 1tert-Butyl alcohol 5.0 U 0.20 ppb v/v 11/24/17 15:47 1Methyl tert-butyl ether 0.20 U 0.20 ppb v/v 11/24/17 15:47 1trans-1,2-Dichloroethene 0.20 U 0.20 ppb v/v 11/24/17 15:47 1n-Hexane 1.3 0.20 ppb v/v 11/24/17 15:47 11,1-Dichloroethane 0.20 U 0.50 ppb v/v 11/24/17 15:47 1Methyl Ethyl Ketone 2.5 0.035 ppb v/v 11/24/17 15:47 1cis-1,2-Dichloroethene 0.035 U 0.40 ppb v/v 11/24/17 15:47 11,2-Dichloroethene, Total 0.40 U 0.20 ppb v/v 11/24/17 15:47 1Chloroform5.1 5.0 ppb v/v 11/24/17 15:47 1Tetrahydrofuran5.0 U 0.20 ppb v/v 11/24/17 15:47 11,1,1-Trichloroethane 0.20 U 0.20 ppb v/v 11/24/17 15:47 1Cyclohexane0.35 0.035 ppb v/v 11/24/17 15:47 1Carbon tetrachloride 0.052 0.20 ppb v/v 11/24/17 15:47 12,2,4-Trimethylpentane 0.20 U 0.20 ppb v/v 11/24/17 15:47 1Benzene1.5 0.20 ppb v/v 11/24/17 15:47 11,2-Dichloroethane 0.20 U 0.20 ppb v/v 11/24/17 15:47 1n-Heptane 0.65 0.035 ppb v/v 11/24/17 15:47 1Trichloroethene0.035 U 0.50 ppb v/v 11/24/17 15:47 1Methyl methacrylate 0.50 U 0.20 ppb v/v 11/24/17 15:47 11,2-Dichloropropane 0.20 U 5.0 ppb v/v 11/24/17 15:47 11,4-Dioxane 5.0 U 0.20 ppb v/v 11/24/17 15:47 1Bromodichloromethane0.38 0.20 ppb v/v 11/24/17 15:47 1cis-1,3-Dichloropropene 0.20 U 0.50 ppb v/v 11/24/17 15:47 1methyl isobutyl ketone 0.50 U 0.20 ppb v/v 11/24/17 15:47 1Toluene6.0 0.20 ppb v/v 11/24/17 15:47 1trans-1,3-Dichloropropene 0.20 U 0.20 ppb v/v 11/24/17 15:47 11,1,2-Trichloroethane 0.20 U 0.20 ppb v/v 11/24/17 15:47 1Tetrachloroethene0.20 U 0.50 ppb v/v 11/24/17 15:47 1Methyl Butyl Ketone (2-Hexanone)0.50 U 0.20 ppb v/v 11/24/17 15:47 1Dibromochloromethane0.20 U TestAmerica Burlington Page 9 of 478 Client Sample Results TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Lab Sample ID: 200-41113-1Client Sample ID: SV-3 Matrix: AirDate Collected: 11/20/17 13:18 Date Received: 11/22/17 10:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) RL RL 1,2-Dibromoethane 0.20 U 0.20 ppb v/v 11/24/17 15:47 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier 0.20 ppb v/v 11/24/17 15:47 1Chlorobenzene0.20 U 0.20 ppb v/v 11/24/17 15:47 1Ethylbenzene0.97 0.50 ppb v/v 11/24/17 15:47 1m,p-Xylene 2.8 0.20 ppb v/v 11/24/17 15:47 1Xylene, o-0.99 0.70 ppb v/v 11/24/17 15:47 1Xylene (total)3.8 0.20 ppb v/v 11/24/17 15:47 1Styrene0.20 U 0.20 ppb v/v 11/24/17 15:47 1Bromoform0.20 U 0.20 ppb v/v 11/24/17 15:47 1Cumene0.20 U 0.20 ppb v/v 11/24/17 15:47 11,1,2,2-Tetrachloroethane 0.20 U 0.20 ppb v/v 11/24/17 15:47 1n-Propylbenzene 0.26 0.20 ppb v/v 11/24/17 15:47 14-Ethyltoluene 0.36 0.20 ppb v/v 11/24/17 15:47 11,3,5-Trimethylbenzene 0.32 0.20 ppb v/v 11/24/17 15:47 12-Chlorotoluene 0.20 U 0.20 ppb v/v 11/24/17 15:47 1tert-Butylbenzene 0.20 U 0.20 ppb v/v 11/24/17 15:47 11,2,4-Trimethylbenzene 1.1 0.20 ppb v/v 11/24/17 15:47 1sec-Butylbenzene 0.20 U 0.20 ppb v/v 11/24/17 15:47 14-Isopropyltoluene 0.20 U 0.20 ppb v/v 11/24/17 15:47 11,3-Dichlorobenzene 0.20 U 0.20 ppb v/v 11/24/17 15:47 11,4-Dichlorobenzene 0.20 U 0.20 ppb v/v 11/24/17 15:47 1Benzyl chloride 0.20 U 0.20 ppb v/v 11/24/17 15:47 1n-Butylbenzene 0.20 U 0.20 ppb v/v 11/24/17 15:47 11,2-Dichlorobenzene 0.20 U 0.50 ppb v/v 11/24/17 15:47 11,2,4-Trichlorobenzene 0.50 U 0.20 ppb v/v 11/24/17 15:47 1Hexachlorobutadiene0.20 U 0.50 ppb v/v 11/24/17 15:47 1Naphthalene0.50 U RL RL Dichlorodifluoromethane 2.5 U 2.5 ug/m3 11/24/17 15:47 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier 1.8 ug/m3 11/24/17 15:47 1Freon 22 1.8 U 1.4 ug/m3 11/24/17 15:47 11,2-Dichlorotetrafluoroethane 1.4 U 1.0 ug/m3 11/24/17 15:47 1Chloromethane1.0 U 1.2 ug/m3 11/24/17 15:47 1n-Butane 25 0.089 ug/m3 11/24/17 15:47 1Vinyl chloride 0.089 U 0.44 ug/m3 11/24/17 15:47 11,3-Butadiene 4.7 0.78 ug/m3 11/24/17 15:47 1Bromomethane0.78 U 1.3 ug/m3 11/24/17 15:47 1Chloroethane1.3 U 0.87 ug/m3 11/24/17 15:47 1Bromoethene(Vinyl Bromide)0.87 U 1.1 ug/m3 11/24/17 15:47 1Trichlorofluoromethane1.1 U 1.5 ug/m3 11/24/17 15:47 1Freon TF 1.5 U 0.14 ug/m3 11/24/17 15:47 11,1-Dichloroethene 0.14 U 12 ug/m3 11/24/17 15:47 1Acetone30 12 ug/m3 11/24/17 15:47 1Isopropyl alcohol 12 U 1.6 ug/m3 11/24/17 15:47 1Carbon disulfide 11 1.6 ug/m3 11/24/17 15:47 13-Chloropropene 1.6 U 1.7 ug/m3 11/24/17 15:47 1Methylene Chloride 1.7 U 15 ug/m3 11/24/17 15:47 1tert-Butyl alcohol 15 U 0.72 ug/m3 11/24/17 15:47 1Methyl tert-butyl ether 0.72 U 0.79 ug/m3 11/24/17 15:47 1trans-1,2-Dichloroethene 0.79 U TestAmerica Burlington Page 10 of 478 Client Sample Results TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Lab Sample ID: 200-41113-1Client Sample ID: SV-3 Matrix: AirDate Collected: 11/20/17 13:18 Date Received: 11/22/17 10:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) RL RL n-Hexane 4.5 0.70 ug/m3 11/24/17 15:47 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier 0.81 ug/m3 11/24/17 15:47 11,1-Dichloroethane 0.81 U 1.5 ug/m3 11/24/17 15:47 1Methyl Ethyl Ketone 7.5 0.14 ug/m3 11/24/17 15:47 1cis-1,2-Dichloroethene 0.14 U 1.6 ug/m3 11/24/17 15:47 11,2-Dichloroethene, Total 1.6 U 0.98 ug/m3 11/24/17 15:47 1Chloroform25 15 ug/m3 11/24/17 15:47 1Tetrahydrofuran15 U 1.1 ug/m3 11/24/17 15:47 11,1,1-Trichloroethane 1.1 U 0.69 ug/m3 11/24/17 15:47 1Cyclohexane1.2 0.22 ug/m3 11/24/17 15:47 1Carbon tetrachloride 0.32 0.93 ug/m3 11/24/17 15:47 12,2,4-Trimethylpentane 0.93 U 0.64 ug/m3 11/24/17 15:47 1Benzene4.9 0.81 ug/m3 11/24/17 15:47 11,2-Dichloroethane 0.81 U 0.82 ug/m3 11/24/17 15:47 1n-Heptane 2.7 0.19 ug/m3 11/24/17 15:47 1Trichloroethene0.19 U 2.0 ug/m3 11/24/17 15:47 1Methyl methacrylate 2.0 U 0.92 ug/m3 11/24/17 15:47 11,2-Dichloropropane 0.92 U 18 ug/m3 11/24/17 15:47 11,4-Dioxane 18 U 1.3 ug/m3 11/24/17 15:47 1Bromodichloromethane2.5 0.91 ug/m3 11/24/17 15:47 1cis-1,3-Dichloropropene 0.91 U 2.0 ug/m3 11/24/17 15:47 1methyl isobutyl ketone 2.0 U 0.75 ug/m3 11/24/17 15:47 1Toluene23 0.91 ug/m3 11/24/17 15:47 1trans-1,3-Dichloropropene 0.91 U 1.1 ug/m3 11/24/17 15:47 11,1,2-Trichloroethane 1.1 U 1.4 ug/m3 11/24/17 15:47 1Tetrachloroethene1.4 U 2.0 ug/m3 11/24/17 15:47 1Methyl Butyl Ketone (2-Hexanone)2.0 U 1.7 ug/m3 11/24/17 15:47 1Dibromochloromethane1.7 U 1.5 ug/m3 11/24/17 15:47 11,2-Dibromoethane 1.5 U 0.92 ug/m3 11/24/17 15:47 1Chlorobenzene0.92 U 0.87 ug/m3 11/24/17 15:47 1Ethylbenzene4.2 2.2 ug/m3 11/24/17 15:47 1m,p-Xylene 12 0.87 ug/m3 11/24/17 15:47 1Xylene, o-4.3 3.0 ug/m3 11/24/17 15:47 1Xylene (total)16 0.85 ug/m3 11/24/17 15:47 1Styrene0.85 U 2.1 ug/m3 11/24/17 15:47 1Bromoform2.1 U 0.98 ug/m3 11/24/17 15:47 1Cumene0.98 U 1.4 ug/m3 11/24/17 15:47 11,1,2,2-Tetrachloroethane 1.4 U 0.98 ug/m3 11/24/17 15:47 1n-Propylbenzene 1.3 0.98 ug/m3 11/24/17 15:47 14-Ethyltoluene 1.8 0.98 ug/m3 11/24/17 15:47 11,3,5-Trimethylbenzene 1.6 1.0 ug/m3 11/24/17 15:47 12-Chlorotoluene 1.0 U 1.1 ug/m3 11/24/17 15:47 1tert-Butylbenzene 1.1 U 0.98 ug/m3 11/24/17 15:47 11,2,4-Trimethylbenzene 5.5 1.1 ug/m3 11/24/17 15:47 1sec-Butylbenzene 1.1 U 1.1 ug/m3 11/24/17 15:47 14-Isopropyltoluene 1.1 U 1.2 ug/m3 11/24/17 15:47 11,3-Dichlorobenzene 1.2 U 1.2 ug/m3 11/24/17 15:47 11,4-Dichlorobenzene 1.2 U 1.0 ug/m3 11/24/17 15:47 1Benzyl chloride 1.0 U TestAmerica Burlington Page 11 of 478 Client Sample Results TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Lab Sample ID: 200-41113-1Client Sample ID: SV-3 Matrix: AirDate Collected: 11/20/17 13:18 Date Received: 11/22/17 10:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) RL RL n-Butylbenzene 1.1 U 1.1 ug/m3 11/24/17 15:47 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier 1.2 ug/m3 11/24/17 15:47 11,2-Dichlorobenzene 1.2 U 3.7 ug/m3 11/24/17 15:47 11,2,4-Trichlorobenzene 3.7 U 2.1 ug/m3 11/24/17 15:47 1Hexachlorobutadiene2.1 U 2.6 ug/m3 11/24/17 15:47 1Naphthalene2.6 U Propene 15 J N ppb v/v 3.14 115-07-1 11/24/17 15:47 1 Tentatively Identified Compound Dil FacAnalyzedPreparedUnit DQualifierEst. Result CAS No.RT 111/24/17 15:47JUnknown6.0 ppb v/v 14.67 111/24/17 15:47J NOctane, 3-methyl-2216-33-34.7 ppb v/v 14.84 111/24/17 15:47JUnknown3.4 ppb v/v 15.67 111/24/17 15:47J NOctane, 3,5-dimethyl-15869-93-95.2 ppb v/v 15.79 111/24/17 15:47JUnknown4.4 ppb v/v 15.85 111/24/17 15:47JUnknown4.7 ppb v/v 16.08 111/24/17 15:47J NNonane, 2-methyl-871-83-011ppb v/v 16.41 111/24/17 15:47J NNonane, 3-methyl-5911-04-611ppb v/v 16.54 111/24/17 15:47J NDecane 124-18-515ppb v/v 16.94 Lab Sample ID: 200-41113-2Client Sample ID: SV-2 Matrix: AirDate Collected: 11/20/17 13:34 Date Received: 11/22/17 10:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air RL RL Dichlorodifluoromethane 1.5 U 1.5 ppb v/v 11/24/17 16:40 2.98 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier 1.5 ppb v/v 11/24/17 16:40 2.98Freon 22 1.5 U 0.60 ppb v/v 11/24/17 16:40 2.981,2-Dichlorotetrafluoroethane 0.60 U 1.5 ppb v/v 11/24/17 16:40 2.98Chloromethane1.5 U 1.5 ppb v/v 11/24/17 16:40 2.98n-Butane 17 0.10 ppb v/v 11/24/17 16:40 2.98Vinyl chloride 0.10 U 0.60 ppb v/v 11/24/17 16:40 2.981,3-Butadiene 2.2 0.60 ppb v/v 11/24/17 16:40 2.98Bromomethane0.60 U 1.5 ppb v/v 11/24/17 16:40 2.98Chloroethane1.5 U 0.60 ppb v/v 11/24/17 16:40 2.98Bromoethene(Vinyl Bromide)0.60 U 0.60 ppb v/v 11/24/17 16:40 2.98Trichlorofluoromethane0.60 U 0.60 ppb v/v 11/24/17 16:40 2.98Freon TF 0.60 U 0.10 ppb v/v 11/24/17 16:40 2.981,1-Dichloroethene 0.10 U 15 ppb v/v 11/24/17 16:40 2.98Acetone38 15 ppb v/v 11/24/17 16:40 2.98Isopropyl alcohol 15 U 1.5 ppb v/v 11/24/17 16:40 2.98Carbon disulfide 5.1 1.5 ppb v/v 11/24/17 16:40 2.983-Chloropropene 1.5 U 1.5 ppb v/v 11/24/17 16:40 2.98Methylene Chloride 1.5 U 15 ppb v/v 11/24/17 16:40 2.98tert-Butyl alcohol 15 U 0.60 ppb v/v 11/24/17 16:40 2.98Methyl tert-butyl ether 0.60 U 0.60 ppb v/v 11/24/17 16:40 2.98trans-1,2-Dichloroethene 0.60 U 0.60 ppb v/v 11/24/17 16:40 2.98n-Hexane 1.3 0.60 ppb v/v 11/24/17 16:40 2.981,1-Dichloroethane 0.60 U 1.5 ppb v/v 11/24/17 16:40 2.98Methyl Ethyl Ketone 6.0 TestAmerica Burlington Page 12 of 478 Client Sample Results TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Lab Sample ID: 200-41113-2Client Sample ID: SV-2 Matrix: AirDate Collected: 11/20/17 13:34 Date Received: 11/22/17 10:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) RL RL cis-1,2-Dichloroethene 0.10 U 0.10 ppb v/v 11/24/17 16:40 2.98 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier 1.2 ppb v/v 11/24/17 16:40 2.981,2-Dichloroethene, Total 1.2 U 0.60 ppb v/v 11/24/17 16:40 2.98Chloroform5.3 15 ppb v/v 11/24/17 16:40 2.98Tetrahydrofuran15 U 0.60 ppb v/v 11/24/17 16:40 2.981,1,1-Trichloroethane 0.60 U 0.60 ppb v/v 11/24/17 16:40 2.98Cyclohexane0.60 U 0.10 ppb v/v 11/24/17 16:40 2.98Carbon tetrachloride 0.10 U 0.60 ppb v/v 11/24/17 16:40 2.982,2,4-Trimethylpentane 20 0.60 ppb v/v 11/24/17 16:40 2.98Benzene1.4 0.60 ppb v/v 11/24/17 16:40 2.981,2-Dichloroethane 0.60 U 0.60 ppb v/v 11/24/17 16:40 2.98n-Heptane 0.71 0.10 ppb v/v 11/24/17 16:40 2.98Trichloroethene0.10 U 1.5 ppb v/v 11/24/17 16:40 2.98Methyl methacrylate 1.5 U 0.60 ppb v/v 11/24/17 16:40 2.981,2-Dichloropropane 0.60 U 15 ppb v/v 11/24/17 16:40 2.981,4-Dioxane 15 U 0.60 ppb v/v 11/24/17 16:40 2.98Bromodichloromethane0.60 U 0.60 ppb v/v 11/24/17 16:40 2.98cis-1,3-Dichloropropene 0.60 U 1.5 ppb v/v 11/24/17 16:40 2.98methyl isobutyl ketone 1.5 U 0.60 ppb v/v 11/24/17 16:40 2.98Toluene5.0 0.60 ppb v/v 11/24/17 16:40 2.98trans-1,3-Dichloropropene 0.60 U 0.60 ppb v/v 11/24/17 16:40 2.981,1,2-Trichloroethane 0.60 U 0.60 ppb v/v 11/24/17 16:40 2.98Tetrachloroethene0.60 U 1.5 ppb v/v 11/24/17 16:40 2.98Methyl Butyl Ketone (2-Hexanone)1.5 U 0.60 ppb v/v 11/24/17 16:40 2.98Dibromochloromethane0.60 U 0.60 ppb v/v 11/24/17 16:40 2.981,2-Dibromoethane 0.60 U 0.60 ppb v/v 11/24/17 16:40 2.98Chlorobenzene0.60 U 0.60 ppb v/v 11/24/17 16:40 2.98Ethylbenzene37 1.5 ppb v/v 11/24/17 16:40 2.98m,p-Xylene 140 0.60 ppb v/v 11/24/17 16:40 2.98Xylene, o-46 2.1 ppb v/v 11/24/17 16:40 2.98Xylene (total)190 0.60 ppb v/v 11/24/17 16:40 2.98Styrene0.60 U 0.60 ppb v/v 11/24/17 16:40 2.98Bromoform0.60 U 0.60 ppb v/v 11/24/17 16:40 2.98Cumene0.67 0.60 ppb v/v 11/24/17 16:40 2.981,1,2,2-Tetrachloroethane 0.60 U 0.60 ppb v/v 11/24/17 16:40 2.98n-Propylbenzene 0.60 U 0.60 ppb v/v 11/24/17 16:40 2.984-Ethyltoluene 0.60 U 0.60 ppb v/v 11/24/17 16:40 2.981,3,5-Trimethylbenzene 0.60 U 0.60 ppb v/v 11/24/17 16:40 2.982-Chlorotoluene 0.60 U 0.60 ppb v/v 11/24/17 16:40 2.98tert-Butylbenzene 0.60 U 0.60 ppb v/v 11/24/17 16:40 2.981,2,4-Trimethylbenzene 0.75 0.60 ppb v/v 11/24/17 16:40 2.98sec-Butylbenzene 0.60 U 0.60 ppb v/v 11/24/17 16:40 2.984-Isopropyltoluene 0.60 U 0.60 ppb v/v 11/24/17 16:40 2.981,3-Dichlorobenzene 0.60 U 0.60 ppb v/v 11/24/17 16:40 2.981,4-Dichlorobenzene 0.60 U 0.60 ppb v/v 11/24/17 16:40 2.98Benzyl chloride 0.60 U 0.60 ppb v/v 11/24/17 16:40 2.98n-Butylbenzene 0.60 U 0.60 ppb v/v 11/24/17 16:40 2.981,2-Dichlorobenzene 0.60 U 1.5 ppb v/v 11/24/17 16:40 2.981,2,4-Trichlorobenzene 1.5 U TestAmerica Burlington Page 13 of 478 Client Sample Results TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Lab Sample ID: 200-41113-2Client Sample ID: SV-2 Matrix: AirDate Collected: 11/20/17 13:34 Date Received: 11/22/17 10:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) RL RL Hexachlorobutadiene 0.60 U 0.60 ppb v/v 11/24/17 16:40 2.98 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier 1.5 ppb v/v 11/24/17 16:40 2.98Naphthalene1.5 U RL RL Dichlorodifluoromethane 7.4 U 7.4 ug/m3 11/24/17 16:40 2.98 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier 5.3 ug/m3 11/24/17 16:40 2.98Freon 22 5.3 U 4.2 ug/m3 11/24/17 16:40 2.981,2-Dichlorotetrafluoroethane 4.2 U 3.1 ug/m3 11/24/17 16:40 2.98Chloromethane3.1 U 3.5 ug/m3 11/24/17 16:40 2.98n-Butane 40 0.27 ug/m3 11/24/17 16:40 2.98Vinyl chloride 0.27 U 1.3 ug/m3 11/24/17 16:40 2.981,3-Butadiene 4.9 2.3 ug/m3 11/24/17 16:40 2.98Bromomethane2.3 U 3.9 ug/m3 11/24/17 16:40 2.98Chloroethane3.9 U 2.6 ug/m3 11/24/17 16:40 2.98Bromoethene(Vinyl Bromide)2.6 U 3.3 ug/m3 11/24/17 16:40 2.98Trichlorofluoromethane3.3 U 4.6 ug/m3 11/24/17 16:40 2.98Freon TF 4.6 U 0.41 ug/m3 11/24/17 16:40 2.981,1-Dichloroethene 0.41 U 35 ug/m3 11/24/17 16:40 2.98Acetone90 37 ug/m3 11/24/17 16:40 2.98Isopropyl alcohol 37 U 4.6 ug/m3 11/24/17 16:40 2.98Carbon disulfide 16 4.7 ug/m3 11/24/17 16:40 2.983-Chloropropene 4.7 U 5.2 ug/m3 11/24/17 16:40 2.98Methylene Chloride 5.2 U 45 ug/m3 11/24/17 16:40 2.98tert-Butyl alcohol 45 U 2.1 ug/m3 11/24/17 16:40 2.98Methyl tert-butyl ether 2.1 U 2.4 ug/m3 11/24/17 16:40 2.98trans-1,2-Dichloroethene 2.4 U 2.1 ug/m3 11/24/17 16:40 2.98n-Hexane 4.5 2.4 ug/m3 11/24/17 16:40 2.981,1-Dichloroethane 2.4 U 4.4 ug/m3 11/24/17 16:40 2.98Methyl Ethyl Ketone 18 0.41 ug/m3 11/24/17 16:40 2.98cis-1,2-Dichloroethene 0.41 U 4.7 ug/m3 11/24/17 16:40 2.981,2-Dichloroethene, Total 4.7 U 2.9 ug/m3 11/24/17 16:40 2.98Chloroform26 44 ug/m3 11/24/17 16:40 2.98Tetrahydrofuran44 U 3.3 ug/m3 11/24/17 16:40 2.981,1,1-Trichloroethane 3.3 U 2.1 ug/m3 11/24/17 16:40 2.98Cyclohexane2.1 U 0.66 ug/m3 11/24/17 16:40 2.98Carbon tetrachloride 0.66 U 2.8 ug/m3 11/24/17 16:40 2.982,2,4-Trimethylpentane 93 1.9 ug/m3 11/24/17 16:40 2.98Benzene4.3 2.4 ug/m3 11/24/17 16:40 2.981,2-Dichloroethane 2.4 U 2.4 ug/m3 11/24/17 16:40 2.98n-Heptane 2.9 0.56 ug/m3 11/24/17 16:40 2.98Trichloroethene0.56 U 6.1 ug/m3 11/24/17 16:40 2.98Methyl methacrylate 6.1 U 2.8 ug/m3 11/24/17 16:40 2.981,2-Dichloropropane 2.8 U 54 ug/m3 11/24/17 16:40 2.981,4-Dioxane 54 U 4.0 ug/m3 11/24/17 16:40 2.98Bromodichloromethane4.0 U 2.7 ug/m3 11/24/17 16:40 2.98cis-1,3-Dichloropropene 2.7 U 6.1 ug/m3 11/24/17 16:40 2.98methyl isobutyl ketone 6.1 U 2.2 ug/m3 11/24/17 16:40 2.98Toluene19 2.7 ug/m3 11/24/17 16:40 2.98trans-1,3-Dichloropropene 2.7 U 3.3 ug/m3 11/24/17 16:40 2.981,1,2-Trichloroethane 3.3 U TestAmerica Burlington Page 14 of 478 Client Sample Results TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Lab Sample ID: 200-41113-2Client Sample ID: SV-2 Matrix: AirDate Collected: 11/20/17 13:34 Date Received: 11/22/17 10:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) RL RL Tetrachloroethene 4.0 U 4.0 ug/m3 11/24/17 16:40 2.98 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier 6.1 ug/m3 11/24/17 16:40 2.98Methyl Butyl Ketone (2-Hexanone)6.1 U 5.1 ug/m3 11/24/17 16:40 2.98Dibromochloromethane5.1 U 4.6 ug/m3 11/24/17 16:40 2.981,2-Dibromoethane 4.6 U 2.7 ug/m3 11/24/17 16:40 2.98Chlorobenzene2.7 U 2.6 ug/m3 11/24/17 16:40 2.98Ethylbenzene160 6.5 ug/m3 11/24/17 16:40 2.98m,p-Xylene 620 2.6 ug/m3 11/24/17 16:40 2.98Xylene, o-200 9.1 ug/m3 11/24/17 16:40 2.98Xylene (total)810 2.5 ug/m3 11/24/17 16:40 2.98Styrene2.5 U 6.2 ug/m3 11/24/17 16:40 2.98Bromoform6.2 U 2.9 ug/m3 11/24/17 16:40 2.98Cumene3.3 4.1 ug/m3 11/24/17 16:40 2.981,1,2,2-Tetrachloroethane 4.1 U 2.9 ug/m3 11/24/17 16:40 2.98n-Propylbenzene 2.9 U 2.9 ug/m3 11/24/17 16:40 2.984-Ethyltoluene 2.9 U 2.9 ug/m3 11/24/17 16:40 2.981,3,5-Trimethylbenzene 2.9 U 3.1 ug/m3 11/24/17 16:40 2.982-Chlorotoluene 3.1 U 3.3 ug/m3 11/24/17 16:40 2.98tert-Butylbenzene 3.3 U 2.9 ug/m3 11/24/17 16:40 2.981,2,4-Trimethylbenzene 3.7 3.3 ug/m3 11/24/17 16:40 2.98sec-Butylbenzene 3.3 U 3.3 ug/m3 11/24/17 16:40 2.984-Isopropyltoluene 3.3 U 3.6 ug/m3 11/24/17 16:40 2.981,3-Dichlorobenzene 3.6 U 3.6 ug/m3 11/24/17 16:40 2.981,4-Dichlorobenzene 3.6 U 3.1 ug/m3 11/24/17 16:40 2.98Benzyl chloride 3.1 U 3.3 ug/m3 11/24/17 16:40 2.98n-Butylbenzene 3.3 U 3.6 ug/m3 11/24/17 16:40 2.981,2-Dichlorobenzene 3.6 U 11 ug/m3 11/24/17 16:40 2.981,2,4-Trichlorobenzene 11 U 6.4 ug/m3 11/24/17 16:40 2.98Hexachlorobutadiene6.4 U 7.8 ug/m3 11/24/17 16:40 2.98Naphthalene7.8 U Cyclohexane, 1,3-dimethyl-, cis-48 J N ppb v/v 13.03 638-04-0 11/24/17 16:40 2.98 Tentatively Identified Compound Dil FacAnalyzedPreparedUnit DQualifierEst. Result CAS No.RT 2.9811/24/17 16:40J NCyclohexane, 1,4-dimethyl-, trans-2207-04-727ppb v/v 13.72 2.9811/24/17 16:40J NCyclohexane, 1,3,5-trimethyl-1839-63-025ppb v/v 14.26 2.9811/24/17 16:40J NCyclohexane, ethyl-1678-91-733ppb v/v 14.39 2.9811/24/17 16:40J NCyclohexane, 1,1,3-trimethyl-3073-66-351ppb v/v 14.44 2.9811/24/17 16:40JUnknown47ppb v/v 14.68 2.9811/24/17 16:40J NCyclohexane, 1,2,4-trimethyl-, (1.alpha.,2.beta.,4.beta.)- 7667-60-941ppb v/v 14.76 2.9811/24/17 16:40J NOctane, 3-methyl-2216-33-342ppb v/v 14.84 2.9811/24/17 16:40J NCyclohexane, 1,2,4-trimethyl-2234-75-526ppb v/v 15.28 2.9811/24/17 16:40JUnknown26ppb v/v 15.85 TestAmerica Burlington Page 15 of 478 Client Sample Results TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Lab Sample ID: 200-41113-3Client Sample ID: SV-1 Matrix: AirDate Collected: 11/20/17 00:00 Date Received: 11/22/17 10:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air RL RL Dichlorodifluoromethane 1.3 U 1.3 ppb v/v 11/24/17 17:32 2.5 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier 1.3 ppb v/v 11/24/17 17:32 2.5Freon 22 1.3 U 0.50 ppb v/v 11/24/17 17:32 2.51,2-Dichlorotetrafluoroethane 0.50 U 1.3 ppb v/v 11/24/17 17:32 2.5Chloromethane1.3 U 1.3 ppb v/v 11/24/17 17:32 2.5n-Butane 44 0.088 ppb v/v 11/24/17 17:32 2.5Vinyl chloride 0.088 U 0.50 ppb v/v 11/24/17 17:32 2.51,3-Butadiene 3.3 0.50 ppb v/v 11/24/17 17:32 2.5Bromomethane0.50 U 1.3 ppb v/v 11/24/17 17:32 2.5Chloroethane1.3 U 0.50 ppb v/v 11/24/17 17:32 2.5Bromoethene(Vinyl Bromide)0.50 U 0.50 ppb v/v 11/24/17 17:32 2.5Trichlorofluoromethane0.50 U 0.50 ppb v/v 11/24/17 17:32 2.5Freon TF 0.50 U 0.088 ppb v/v 11/24/17 17:32 2.51,1-Dichloroethene 0.088 U 13 ppb v/v 11/24/17 17:32 2.5Acetone13 U 13 ppb v/v 11/24/17 17:32 2.5Isopropyl alcohol 13 U 1.3 ppb v/v 11/24/17 17:32 2.5Carbon disulfide 5.2 1.3 ppb v/v 11/24/17 17:32 2.53-Chloropropene 1.3 U 1.3 ppb v/v 11/24/17 17:32 2.5Methylene Chloride 1.3 U 13 ppb v/v 11/24/17 17:32 2.5tert-Butyl alcohol 13 U 0.50 ppb v/v 11/24/17 17:32 2.5Methyl tert-butyl ether 0.50 U 0.50 ppb v/v 11/24/17 17:32 2.5trans-1,2-Dichloroethene 0.50 U 0.50 ppb v/v 11/24/17 17:32 2.5n-Hexane 1.5 0.50 ppb v/v 11/24/17 17:32 2.51,1-Dichloroethane 0.50 U 1.3 ppb v/v 11/24/17 17:32 2.5Methyl Ethyl Ketone 1.4 0.088 ppb v/v 11/24/17 17:32 2.5cis-1,2-Dichloroethene 0.088 U 1.0 ppb v/v 11/24/17 17:32 2.51,2-Dichloroethene, Total 1.0 U 0.50 ppb v/v 11/24/17 17:32 2.5Chloroform2.3 13 ppb v/v 11/24/17 17:32 2.5Tetrahydrofuran13 U 0.50 ppb v/v 11/24/17 17:32 2.51,1,1-Trichloroethane 0.50 U 0.50 ppb v/v 11/24/17 17:32 2.5Cyclohexane0.73 0.088 ppb v/v 11/24/17 17:32 2.5Carbon tetrachloride 0.088 U 0.50 ppb v/v 11/24/17 17:32 2.52,2,4-Trimethylpentane 0.50 U 0.50 ppb v/v 11/24/17 17:32 2.5Benzene1.6 0.50 ppb v/v 11/24/17 17:32 2.51,2-Dichloroethane 0.50 U 0.50 ppb v/v 11/24/17 17:32 2.5n-Heptane 0.74 0.088 ppb v/v 11/24/17 17:32 2.5Trichloroethene0.088 U 1.3 ppb v/v 11/24/17 17:32 2.5Methyl methacrylate 1.3 U 0.50 ppb v/v 11/24/17 17:32 2.51,2-Dichloropropane 0.50 U 13 ppb v/v 11/24/17 17:32 2.51,4-Dioxane 13 U 0.50 ppb v/v 11/24/17 17:32 2.5Bromodichloromethane0.50 U 0.50 ppb v/v 11/24/17 17:32 2.5cis-1,3-Dichloropropene 0.50 U 1.3 ppb v/v 11/24/17 17:32 2.5methyl isobutyl ketone 1.3 U 0.50 ppb v/v 11/24/17 17:32 2.5Toluene4.4 0.50 ppb v/v 11/24/17 17:32 2.5trans-1,3-Dichloropropene 0.50 U 0.50 ppb v/v 11/24/17 17:32 2.51,1,2-Trichloroethane 0.50 U 0.50 ppb v/v 11/24/17 17:32 2.5Tetrachloroethene0.50 U 1.3 ppb v/v 11/24/17 17:32 2.5Methyl Butyl Ketone (2-Hexanone)1.3 U 0.50 ppb v/v 11/24/17 17:32 2.5Dibromochloromethane0.50 U TestAmerica Burlington Page 16 of 478 Client Sample Results TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Lab Sample ID: 200-41113-3Client Sample ID: SV-1 Matrix: AirDate Collected: 11/20/17 00:00 Date Received: 11/22/17 10:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) RL RL 1,2-Dibromoethane 0.50 U 0.50 ppb v/v 11/24/17 17:32 2.5 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier 0.50 ppb v/v 11/24/17 17:32 2.5Chlorobenzene0.50 U 0.50 ppb v/v 11/24/17 17:32 2.5Ethylbenzene9.1 1.3 ppb v/v 11/24/17 17:32 2.5m,p-Xylene 36 0.50 ppb v/v 11/24/17 17:32 2.5Xylene, o-12 1.8 ppb v/v 11/24/17 17:32 2.5Xylene (total)48 0.50 ppb v/v 11/24/17 17:32 2.5Styrene0.50 U 0.50 ppb v/v 11/24/17 17:32 2.5Bromoform0.50 U 0.50 ppb v/v 11/24/17 17:32 2.5Cumene0.50 U 0.50 ppb v/v 11/24/17 17:32 2.51,1,2,2-Tetrachloroethane 0.50 U 0.50 ppb v/v 11/24/17 17:32 2.5n-Propylbenzene 0.50 U 0.50 ppb v/v 11/24/17 17:32 2.54-Ethyltoluene 0.50 U 0.50 ppb v/v 11/24/17 17:32 2.51,3,5-Trimethylbenzene 0.50 U 0.50 ppb v/v 11/24/17 17:32 2.52-Chlorotoluene 0.50 U 0.50 ppb v/v 11/24/17 17:32 2.5tert-Butylbenzene 0.50 U 0.50 ppb v/v 11/24/17 17:32 2.51,2,4-Trimethylbenzene 0.93 0.50 ppb v/v 11/24/17 17:32 2.5sec-Butylbenzene 0.50 U 0.50 ppb v/v 11/24/17 17:32 2.54-Isopropyltoluene 0.50 U 0.50 ppb v/v 11/24/17 17:32 2.51,3-Dichlorobenzene 0.50 U 0.50 ppb v/v 11/24/17 17:32 2.51,4-Dichlorobenzene 0.50 U 0.50 ppb v/v 11/24/17 17:32 2.5Benzyl chloride 0.50 U 0.50 ppb v/v 11/24/17 17:32 2.5n-Butylbenzene 0.50 U 0.50 ppb v/v 11/24/17 17:32 2.51,2-Dichlorobenzene 0.50 U 1.3 ppb v/v 11/24/17 17:32 2.51,2,4-Trichlorobenzene 1.3 U 0.50 ppb v/v 11/24/17 17:32 2.5Hexachlorobutadiene0.50 U 1.3 ppb v/v 11/24/17 17:32 2.5Naphthalene1.3 U RL RL Dichlorodifluoromethane 6.2 U 6.2 ug/m3 11/24/17 17:32 2.5 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier 4.4 ug/m3 11/24/17 17:32 2.5Freon 22 4.4 U 3.5 ug/m3 11/24/17 17:32 2.51,2-Dichlorotetrafluoroethane 3.5 U 2.6 ug/m3 11/24/17 17:32 2.5Chloromethane2.6 U 3.0 ug/m3 11/24/17 17:32 2.5n-Butane 110 0.22 ug/m3 11/24/17 17:32 2.5Vinyl chloride 0.22 U 1.1 ug/m3 11/24/17 17:32 2.51,3-Butadiene 7.3 1.9 ug/m3 11/24/17 17:32 2.5Bromomethane1.9 U 3.3 ug/m3 11/24/17 17:32 2.5Chloroethane3.3 U 2.2 ug/m3 11/24/17 17:32 2.5Bromoethene(Vinyl Bromide)2.2 U 2.8 ug/m3 11/24/17 17:32 2.5Trichlorofluoromethane2.8 U 3.8 ug/m3 11/24/17 17:32 2.5Freon TF 3.8 U 0.35 ug/m3 11/24/17 17:32 2.51,1-Dichloroethene 0.35 U 30 ug/m3 11/24/17 17:32 2.5Acetone30 U 31 ug/m3 11/24/17 17:32 2.5Isopropyl alcohol 31 U 3.9 ug/m3 11/24/17 17:32 2.5Carbon disulfide 16 3.9 ug/m3 11/24/17 17:32 2.53-Chloropropene 3.9 U 4.3 ug/m3 11/24/17 17:32 2.5Methylene Chloride 4.3 U 38 ug/m3 11/24/17 17:32 2.5tert-Butyl alcohol 38 U 1.8 ug/m3 11/24/17 17:32 2.5Methyl tert-butyl ether 1.8 U 2.0 ug/m3 11/24/17 17:32 2.5trans-1,2-Dichloroethene 2.0 U TestAmerica Burlington Page 17 of 478 Client Sample Results TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Lab Sample ID: 200-41113-3Client Sample ID: SV-1 Matrix: AirDate Collected: 11/20/17 00:00 Date Received: 11/22/17 10:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) RL RL n-Hexane 5.4 1.8 ug/m3 11/24/17 17:32 2.5 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier 2.0 ug/m3 11/24/17 17:32 2.51,1-Dichloroethane 2.0 U 3.7 ug/m3 11/24/17 17:32 2.5Methyl Ethyl Ketone 4.2 0.35 ug/m3 11/24/17 17:32 2.5cis-1,2-Dichloroethene 0.35 U 4.0 ug/m3 11/24/17 17:32 2.51,2-Dichloroethene, Total 4.0 U 2.4 ug/m3 11/24/17 17:32 2.5Chloroform11 37 ug/m3 11/24/17 17:32 2.5Tetrahydrofuran37 U 2.7 ug/m3 11/24/17 17:32 2.51,1,1-Trichloroethane 2.7 U 1.7 ug/m3 11/24/17 17:32 2.5Cyclohexane2.5 0.55 ug/m3 11/24/17 17:32 2.5Carbon tetrachloride 0.55 U 2.3 ug/m3 11/24/17 17:32 2.52,2,4-Trimethylpentane 2.3 U 1.6 ug/m3 11/24/17 17:32 2.5Benzene5.1 2.0 ug/m3 11/24/17 17:32 2.51,2-Dichloroethane 2.0 U 2.0 ug/m3 11/24/17 17:32 2.5n-Heptane 3.1 0.47 ug/m3 11/24/17 17:32 2.5Trichloroethene0.47 U 5.1 ug/m3 11/24/17 17:32 2.5Methyl methacrylate 5.1 U 2.3 ug/m3 11/24/17 17:32 2.51,2-Dichloropropane 2.3 U 45 ug/m3 11/24/17 17:32 2.51,4-Dioxane 45 U 3.4 ug/m3 11/24/17 17:32 2.5Bromodichloromethane3.4 U 2.3 ug/m3 11/24/17 17:32 2.5cis-1,3-Dichloropropene 2.3 U 5.1 ug/m3 11/24/17 17:32 2.5methyl isobutyl ketone 5.1 U 1.9 ug/m3 11/24/17 17:32 2.5Toluene17 2.3 ug/m3 11/24/17 17:32 2.5trans-1,3-Dichloropropene 2.3 U 2.7 ug/m3 11/24/17 17:32 2.51,1,2-Trichloroethane 2.7 U 3.4 ug/m3 11/24/17 17:32 2.5Tetrachloroethene3.4 U 5.1 ug/m3 11/24/17 17:32 2.5Methyl Butyl Ketone (2-Hexanone)5.1 U 4.3 ug/m3 11/24/17 17:32 2.5Dibromochloromethane4.3 U 3.8 ug/m3 11/24/17 17:32 2.51,2-Dibromoethane 3.8 U 2.3 ug/m3 11/24/17 17:32 2.5Chlorobenzene2.3 U 2.2 ug/m3 11/24/17 17:32 2.5Ethylbenzene40 5.4 ug/m3 11/24/17 17:32 2.5m,p-Xylene 150 2.2 ug/m3 11/24/17 17:32 2.5Xylene, o-53 7.6 ug/m3 11/24/17 17:32 2.5Xylene (total)210 2.1 ug/m3 11/24/17 17:32 2.5Styrene2.1 U 5.2 ug/m3 11/24/17 17:32 2.5Bromoform5.2 U 2.5 ug/m3 11/24/17 17:32 2.5Cumene2.5 U 3.4 ug/m3 11/24/17 17:32 2.51,1,2,2-Tetrachloroethane 3.4 U 2.5 ug/m3 11/24/17 17:32 2.5n-Propylbenzene 2.5 U 2.5 ug/m3 11/24/17 17:32 2.54-Ethyltoluene 2.5 U 2.5 ug/m3 11/24/17 17:32 2.51,3,5-Trimethylbenzene 2.5 U 2.6 ug/m3 11/24/17 17:32 2.52-Chlorotoluene 2.6 U 2.7 ug/m3 11/24/17 17:32 2.5tert-Butylbenzene 2.7 U 2.5 ug/m3 11/24/17 17:32 2.51,2,4-Trimethylbenzene 4.6 2.7 ug/m3 11/24/17 17:32 2.5sec-Butylbenzene 2.7 U 2.7 ug/m3 11/24/17 17:32 2.54-Isopropyltoluene 2.7 U 3.0 ug/m3 11/24/17 17:32 2.51,3-Dichlorobenzene 3.0 U 3.0 ug/m3 11/24/17 17:32 2.51,4-Dichlorobenzene 3.0 U 2.6 ug/m3 11/24/17 17:32 2.5Benzyl chloride 2.6 U TestAmerica Burlington Page 18 of 478 Client Sample Results TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Lab Sample ID: 200-41113-3Client Sample ID: SV-1 Matrix: AirDate Collected: 11/20/17 00:00 Date Received: 11/22/17 10:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) RL RL n-Butylbenzene 2.7 U 2.7 ug/m3 11/24/17 17:32 2.5 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier 3.0 ug/m3 11/24/17 17:32 2.51,2-Dichlorobenzene 3.0 U 9.3 ug/m3 11/24/17 17:32 2.51,2,4-Trichlorobenzene 9.3 U 5.3 ug/m3 11/24/17 17:32 2.5Hexachlorobutadiene5.3 U 6.6 ug/m3 11/24/17 17:32 2.5Naphthalene6.6 U Isobutane 9.4 J N ppb v/v 3.44 75-28-5 11/24/17 17:32 2.5 Tentatively Identified Compound Dil FacAnalyzedPreparedUnit DQualifierEst. Result CAS No.RT 2.511/24/17 17:32J NCyclohexane, 1,4-dimethyl-, cis-624-29-313ppb v/v 13.04 2.511/24/17 17:32J NCyclohexane, 1,4-dimethyl-, trans-2207-04-76.6 ppb v/v 13.72 2.511/24/17 17:32J NCyclohexane, ethyl-1678-91-78.2 ppb v/v 14.39 2.511/24/17 17:32J NCyclohexane, 1,1,3-trimethyl-3073-66-312ppb v/v 14.44 2.511/24/17 17:32JUnknown12ppb v/v 14.67 2.511/24/17 17:32J NCyclohexane, 1,2,4-trimethyl-, (1.alpha.,2.beta.,4.beta.)- 7667-60-98.9 ppb v/v 14.75 2.511/24/17 17:32J NOctane, 3-methyl-2216-33-310ppb v/v 14.84 2.511/24/17 17:32J NCyclohexane, 1,2,3-trimethyl-, (1.alpha.,2.beta.,3.alpha.)- 1678-81-56.6 ppb v/v 15.27 2.511/24/17 17:32JUnknown7.9 ppb v/v 15.85 Lab Sample ID: 200-41113-4Client Sample ID: AA-1 Matrix: AirDate Collected: 11/20/17 00:00 Date Received: 11/22/17 10:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air RL RL Dichlorodifluoromethane 0.50 U 0.50 ppb v/v 11/24/17 18:24 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier 0.50 ppb v/v 11/24/17 18:24 1Freon 22 0.50 U 0.20 ppb v/v 11/24/17 18:24 11,2-Dichlorotetrafluoroethane 0.20 U 0.50 ppb v/v 11/24/17 18:24 1Chloromethane0.50 U 0.50 ppb v/v 11/24/17 18:24 1n-Butane 0.50 U 0.035 ppb v/v 11/24/17 18:24 1Vinyl chloride 0.035 U 0.20 ppb v/v 11/24/17 18:24 11,3-Butadiene 0.20 U 0.20 ppb v/v 11/24/17 18:24 1Bromomethane0.20 U 0.50 ppb v/v 11/24/17 18:24 1Chloroethane0.50 U 0.20 ppb v/v 11/24/17 18:24 1Bromoethene(Vinyl Bromide)0.20 U 0.20 ppb v/v 11/24/17 18:24 1Trichlorofluoromethane0.20 U 0.20 ppb v/v 11/24/17 18:24 1Freon TF 0.20 U 0.035 ppb v/v 11/24/17 18:24 11,1-Dichloroethene 0.035 U 5.0 ppb v/v 11/24/17 18:24 1Acetone5.0 U 5.0 ppb v/v 11/24/17 18:24 1Isopropyl alcohol 5.0 U 0.50 ppb v/v 11/24/17 18:24 1Carbon disulfide 0.50 U 0.50 ppb v/v 11/24/17 18:24 13-Chloropropene 0.50 U 0.50 ppb v/v 11/24/17 18:24 1Methylene Chloride 0.50 U 5.0 ppb v/v 11/24/17 18:24 1tert-Butyl alcohol 5.0 U 0.20 ppb v/v 11/24/17 18:24 1Methyl tert-butyl ether 0.20 U 0.20 ppb v/v 11/24/17 18:24 1trans-1,2-Dichloroethene 0.20 U 0.20 ppb v/v 11/24/17 18:24 1n-Hexane 0.20 U TestAmerica Burlington Page 19 of 478 Client Sample Results TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Lab Sample ID: 200-41113-4Client Sample ID: AA-1 Matrix: AirDate Collected: 11/20/17 00:00 Date Received: 11/22/17 10:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) RL RL 1,1-Dichloroethane 0.20 U 0.20 ppb v/v 11/24/17 18:24 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier 0.50 ppb v/v 11/24/17 18:24 1Methyl Ethyl Ketone 0.50 U 0.035 ppb v/v 11/24/17 18:24 1cis-1,2-Dichloroethene 0.035 U 0.40 ppb v/v 11/24/17 18:24 11,2-Dichloroethene, Total 0.40 U 0.20 ppb v/v 11/24/17 18:24 1Chloroform0.20 U 5.0 ppb v/v 11/24/17 18:24 1Tetrahydrofuran5.0 U 0.20 ppb v/v 11/24/17 18:24 11,1,1-Trichloroethane 0.20 U 0.20 ppb v/v 11/24/17 18:24 1Cyclohexane0.20 U 0.035 ppb v/v 11/24/17 18:24 1Carbon tetrachloride 0.061 0.20 ppb v/v 11/24/17 18:24 12,2,4-Trimethylpentane 0.20 U 0.20 ppb v/v 11/24/17 18:24 1Benzene0.20 U 0.20 ppb v/v 11/24/17 18:24 11,2-Dichloroethane 0.20 U 0.20 ppb v/v 11/24/17 18:24 1n-Heptane 0.20 U 0.035 ppb v/v 11/24/17 18:24 1Trichloroethene0.035 U 0.50 ppb v/v 11/24/17 18:24 1Methyl methacrylate 0.50 U 0.20 ppb v/v 11/24/17 18:24 11,2-Dichloropropane 0.20 U 5.0 ppb v/v 11/24/17 18:24 11,4-Dioxane 5.0 U 0.20 ppb v/v 11/24/17 18:24 1Bromodichloromethane0.20 U 0.20 ppb v/v 11/24/17 18:24 1cis-1,3-Dichloropropene 0.20 U 0.50 ppb v/v 11/24/17 18:24 1methyl isobutyl ketone 0.50 U 0.20 ppb v/v 11/24/17 18:24 1Toluene0.20 U 0.20 ppb v/v 11/24/17 18:24 1trans-1,3-Dichloropropene 0.20 U 0.20 ppb v/v 11/24/17 18:24 11,1,2-Trichloroethane 0.20 U 0.20 ppb v/v 11/24/17 18:24 1Tetrachloroethene0.20 U 0.50 ppb v/v 11/24/17 18:24 1Methyl Butyl Ketone (2-Hexanone)0.50 U 0.20 ppb v/v 11/24/17 18:24 1Dibromochloromethane0.20 U 0.20 ppb v/v 11/24/17 18:24 11,2-Dibromoethane 0.20 U 0.20 ppb v/v 11/24/17 18:24 1Chlorobenzene0.20 U 0.20 ppb v/v 11/24/17 18:24 1Ethylbenzene0.20 U 0.50 ppb v/v 11/24/17 18:24 1m,p-Xylene 0.50 U 0.20 ppb v/v 11/24/17 18:24 1Xylene, o-0.20 U 0.70 ppb v/v 11/24/17 18:24 1Xylene (total)0.70 U 0.20 ppb v/v 11/24/17 18:24 1Styrene0.20 U 0.20 ppb v/v 11/24/17 18:24 1Bromoform0.20 U 0.20 ppb v/v 11/24/17 18:24 1Cumene0.20 U 0.20 ppb v/v 11/24/17 18:24 11,1,2,2-Tetrachloroethane 0.20 U 0.20 ppb v/v 11/24/17 18:24 1n-Propylbenzene 0.20 U 0.20 ppb v/v 11/24/17 18:24 14-Ethyltoluene 0.20 U 0.20 ppb v/v 11/24/17 18:24 11,3,5-Trimethylbenzene 0.20 U 0.20 ppb v/v 11/24/17 18:24 12-Chlorotoluene 0.20 U 0.20 ppb v/v 11/24/17 18:24 1tert-Butylbenzene 0.20 U 0.20 ppb v/v 11/24/17 18:24 11,2,4-Trimethylbenzene 0.20 U 0.20 ppb v/v 11/24/17 18:24 1sec-Butylbenzene 0.20 U 0.20 ppb v/v 11/24/17 18:24 14-Isopropyltoluene 0.20 U 0.20 ppb v/v 11/24/17 18:24 11,3-Dichlorobenzene 0.20 U 0.20 ppb v/v 11/24/17 18:24 11,4-Dichlorobenzene 0.20 U 0.20 ppb v/v 11/24/17 18:24 1Benzyl chloride 0.20 U 0.20 ppb v/v 11/24/17 18:24 1n-Butylbenzene 0.20 U TestAmerica Burlington Page 20 of 478 Client Sample Results TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Lab Sample ID: 200-41113-4Client Sample ID: AA-1 Matrix: AirDate Collected: 11/20/17 00:00 Date Received: 11/22/17 10:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) RL RL 1,2-Dichlorobenzene 0.20 U 0.20 ppb v/v 11/24/17 18:24 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier 0.50 ppb v/v 11/24/17 18:24 11,2,4-Trichlorobenzene 0.50 U 0.20 ppb v/v 11/24/17 18:24 1Hexachlorobutadiene0.20 U 0.50 ppb v/v 11/24/17 18:24 1Naphthalene0.50 U RL RL Dichlorodifluoromethane 2.5 U 2.5 ug/m3 11/24/17 18:24 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier 1.8 ug/m3 11/24/17 18:24 1Freon 22 1.8 U 1.4 ug/m3 11/24/17 18:24 11,2-Dichlorotetrafluoroethane 1.4 U 1.0 ug/m3 11/24/17 18:24 1Chloromethane1.0 U 1.2 ug/m3 11/24/17 18:24 1n-Butane 1.2 U 0.089 ug/m3 11/24/17 18:24 1Vinyl chloride 0.089 U 0.44 ug/m3 11/24/17 18:24 11,3-Butadiene 0.44 U 0.78 ug/m3 11/24/17 18:24 1Bromomethane0.78 U 1.3 ug/m3 11/24/17 18:24 1Chloroethane1.3 U 0.87 ug/m3 11/24/17 18:24 1Bromoethene(Vinyl Bromide)0.87 U 1.1 ug/m3 11/24/17 18:24 1Trichlorofluoromethane1.1 U 1.5 ug/m3 11/24/17 18:24 1Freon TF 1.5 U 0.14 ug/m3 11/24/17 18:24 11,1-Dichloroethene 0.14 U 12 ug/m3 11/24/17 18:24 1Acetone12 U 12 ug/m3 11/24/17 18:24 1Isopropyl alcohol 12 U 1.6 ug/m3 11/24/17 18:24 1Carbon disulfide 1.6 U 1.6 ug/m3 11/24/17 18:24 13-Chloropropene 1.6 U 1.7 ug/m3 11/24/17 18:24 1Methylene Chloride 1.7 U 15 ug/m3 11/24/17 18:24 1tert-Butyl alcohol 15 U 0.72 ug/m3 11/24/17 18:24 1Methyl tert-butyl ether 0.72 U 0.79 ug/m3 11/24/17 18:24 1trans-1,2-Dichloroethene 0.79 U 0.70 ug/m3 11/24/17 18:24 1n-Hexane 0.70 U 0.81 ug/m3 11/24/17 18:24 11,1-Dichloroethane 0.81 U 1.5 ug/m3 11/24/17 18:24 1Methyl Ethyl Ketone 1.5 U 0.14 ug/m3 11/24/17 18:24 1cis-1,2-Dichloroethene 0.14 U 1.6 ug/m3 11/24/17 18:24 11,2-Dichloroethene, Total 1.6 U 0.98 ug/m3 11/24/17 18:24 1Chloroform0.98 U 15 ug/m3 11/24/17 18:24 1Tetrahydrofuran15 U 1.1 ug/m3 11/24/17 18:24 11,1,1-Trichloroethane 1.1 U 0.69 ug/m3 11/24/17 18:24 1Cyclohexane0.69 U 0.22 ug/m3 11/24/17 18:24 1Carbon tetrachloride 0.39 0.93 ug/m3 11/24/17 18:24 12,2,4-Trimethylpentane 0.93 U 0.64 ug/m3 11/24/17 18:24 1Benzene0.64 U 0.81 ug/m3 11/24/17 18:24 11,2-Dichloroethane 0.81 U 0.82 ug/m3 11/24/17 18:24 1n-Heptane 0.82 U 0.19 ug/m3 11/24/17 18:24 1Trichloroethene0.19 U 2.0 ug/m3 11/24/17 18:24 1Methyl methacrylate 2.0 U 0.92 ug/m3 11/24/17 18:24 11,2-Dichloropropane 0.92 U 18 ug/m3 11/24/17 18:24 11,4-Dioxane 18 U 1.3 ug/m3 11/24/17 18:24 1Bromodichloromethane1.3 U 0.91 ug/m3 11/24/17 18:24 1cis-1,3-Dichloropropene 0.91 U 2.0 ug/m3 11/24/17 18:24 1methyl isobutyl ketone 2.0 U 0.75 ug/m3 11/24/17 18:24 1Toluene0.75 U TestAmerica Burlington Page 21 of 478 Client Sample Results TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Lab Sample ID: 200-41113-4Client Sample ID: AA-1 Matrix: AirDate Collected: 11/20/17 00:00 Date Received: 11/22/17 10:20 Sample Container: Summa Canister 6L Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) RL RL trans-1,3-Dichloropropene 0.91 U 0.91 ug/m3 11/24/17 18:24 1 Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier 1.1 ug/m3 11/24/17 18:24 11,1,2-Trichloroethane 1.1 U 1.4 ug/m3 11/24/17 18:24 1Tetrachloroethene1.4 U 2.0 ug/m3 11/24/17 18:24 1Methyl Butyl Ketone (2-Hexanone)2.0 U 1.7 ug/m3 11/24/17 18:24 1Dibromochloromethane1.7 U 1.5 ug/m3 11/24/17 18:24 11,2-Dibromoethane 1.5 U 0.92 ug/m3 11/24/17 18:24 1Chlorobenzene0.92 U 0.87 ug/m3 11/24/17 18:24 1Ethylbenzene0.87 U 2.2 ug/m3 11/24/17 18:24 1m,p-Xylene 2.2 U 0.87 ug/m3 11/24/17 18:24 1Xylene, o-0.87 U 3.0 ug/m3 11/24/17 18:24 1Xylene (total)3.0 U 0.85 ug/m3 11/24/17 18:24 1Styrene0.85 U 2.1 ug/m3 11/24/17 18:24 1Bromoform2.1 U 0.98 ug/m3 11/24/17 18:24 1Cumene0.98 U 1.4 ug/m3 11/24/17 18:24 11,1,2,2-Tetrachloroethane 1.4 U 0.98 ug/m3 11/24/17 18:24 1n-Propylbenzene 0.98 U 0.98 ug/m3 11/24/17 18:24 14-Ethyltoluene 0.98 U 0.98 ug/m3 11/24/17 18:24 11,3,5-Trimethylbenzene 0.98 U 1.0 ug/m3 11/24/17 18:24 12-Chlorotoluene 1.0 U 1.1 ug/m3 11/24/17 18:24 1tert-Butylbenzene 1.1 U 0.98 ug/m3 11/24/17 18:24 11,2,4-Trimethylbenzene 0.98 U 1.1 ug/m3 11/24/17 18:24 1sec-Butylbenzene 1.1 U 1.1 ug/m3 11/24/17 18:24 14-Isopropyltoluene 1.1 U 1.2 ug/m3 11/24/17 18:24 11,3-Dichlorobenzene 1.2 U 1.2 ug/m3 11/24/17 18:24 11,4-Dichlorobenzene 1.2 U 1.0 ug/m3 11/24/17 18:24 1Benzyl chloride 1.0 U 1.1 ug/m3 11/24/17 18:24 1n-Butylbenzene 1.1 U 1.2 ug/m3 11/24/17 18:24 11,2-Dichlorobenzene 1.2 U 3.7 ug/m3 11/24/17 18:24 11,2,4-Trichlorobenzene 3.7 U 2.1 ug/m3 11/24/17 18:24 1Hexachlorobutadiene2.1 U 2.6 ug/m3 11/24/17 18:24 1Naphthalene2.6 U Tentatively Identified Compound None ppb v/v 11/24/17 18:24 1 Tentatively Identified Compound Dil FacAnalyzedPreparedUnit DQualifierEst. Result CAS No.RT TestAmerica Burlington Page 22 of 478 Default Detection Limits Client: AKRF Inc TestAmerica Job ID: 200-41113-1 Project/Site: 900 King Street SDG: 200-41113-1 Method: TO-15 - Volatile Organic Compounds in Ambient Air 0.201,1,1-Trichloroethane ppb v/v Analyte Units MethodRLRL 0.20 TO-15 1.11,1,1-Trichloroethane ug/m31.1 TO-15 0.201,1,2,2-Tetrachloroethane ppb v/v0.20 TO-15 1.41,1,2,2-Tetrachloroethane ug/m31.4 TO-15 0.201,1,2-Trichloroethane ppb v/v0.20 TO-15 1.11,1,2-Trichloroethane ug/m31.1 TO-15 0.201,1-Dichloroethane ppb v/v0.20 TO-15 0.811,1-Dichloroethane ug/m30.81 TO-15 0.0351,1-Dichloroethene ppb v/v0.035 TO-15 0.141,1-Dichloroethene ug/m30.14 TO-15 0.501,2,4-Trichlorobenzene ppb v/v0.50 TO-15 3.71,2,4-Trichlorobenzene ug/m33.7 TO-15 0.201,2,4-Trimethylbenzene ppb v/v0.20 TO-15 0.981,2,4-Trimethylbenzene ug/m30.98 TO-15 0.201,2-Dibromoethane ppb v/v0.20 TO-15 1.51,2-Dibromoethane ug/m31.5 TO-15 0.201,2-Dichlorobenzene ppb v/v0.20 TO-15 1.21,2-Dichlorobenzene ug/m31.2 TO-15 0.201,2-Dichloroethane ppb v/v0.20 TO-15 0.811,2-Dichloroethane ug/m30.81 TO-15 0.401,2-Dichloroethene, Total ppb v/v0.40 TO-15 1.61,2-Dichloroethene, Total ug/m31.6 TO-15 0.201,2-Dichloropropane ppb v/v0.20 TO-15 0.921,2-Dichloropropane ug/m30.92 TO-15 0.201,2-Dichlorotetrafluoroethane ppb v/v0.20 TO-15 1.41,2-Dichlorotetrafluoroethane ug/m31.4 TO-15 0.201,3,5-Trimethylbenzene ppb v/v0.20 TO-15 0.981,3,5-Trimethylbenzene ug/m30.98 TO-15 0.201,3-Butadiene ppb v/v0.20 TO-15 0.441,3-Butadiene ug/m30.44 TO-15 0.201,3-Dichlorobenzene ppb v/v0.20 TO-15 1.21,3-Dichlorobenzene ug/m31.2 TO-15 0.201,4-Dichlorobenzene ppb v/v0.20 TO-15 1.21,4-Dichlorobenzene ug/m31.2 TO-15 5.01,4-Dioxane ppb v/v5.0 TO-15 181,4-Dioxane ug/m318 TO-15 0.202,2,4-Trimethylpentane ppb v/v0.20 TO-15 0.932,2,4-Trimethylpentane ug/m30.93 TO-15 0.202-Chlorotoluene ppb v/v0.20 TO-15 1.02-Chlorotoluene ug/m31.0 TO-15 0.503-Chloropropene ppb v/v0.50 TO-15 1.63-Chloropropene ug/m31.6 TO-15 0.204-Ethyltoluene ppb v/v0.20 TO-15 0.984-Ethyltoluene ug/m30.98 TO-15 0.204-Isopropyltoluene ppb v/v0.20 TO-15 1.14-Isopropyltoluene ug/m31.1 TO-15 5.0Acetone ppb v/v5.0 TO-15 12Acetone ug/m312 TO-15 0.20Benzene ppb v/v0.20 TO-15 0.64Benzene ug/m30.64 TO-15 0.20Benzyl chloride ppb v/v0.20 TO-15 1.0Benzyl chloride ug/m31.0 TO-15 TestAmerica Burlington Page 23 of 478 Default Detection Limits Client: AKRF Inc TestAmerica Job ID: 200-41113-1 Project/Site: 900 King Street SDG: 200-41113-1 Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) 0.20Bromodichloromethane ppb v/v Analyte Units MethodRLRL 0.20 TO-15 1.3Bromodichloromethane ug/m31.3 TO-15 0.20Bromoethene(Vinyl Bromide)ppb v/v0.20 TO-15 0.87Bromoethene(Vinyl Bromide)ug/m30.87 TO-15 0.20Bromoform ppb v/v0.20 TO-15 2.1Bromoform ug/m32.1 TO-15 0.20Bromomethane ppb v/v0.20 TO-15 0.78Bromomethane ug/m30.78 TO-15 0.50Carbon disulfide ppb v/v0.50 TO-15 1.6Carbon disulfide ug/m31.6 TO-15 0.035Carbon tetrachloride ppb v/v0.035 TO-15 0.22Carbon tetrachloride ug/m30.22 TO-15 0.20Chlorobenzene ppb v/v0.20 TO-15 0.92Chlorobenzene ug/m30.92 TO-15 0.50Chloroethane ppb v/v0.50 TO-15 1.3Chloroethane ug/m31.3 TO-15 0.20Chloroform ppb v/v0.20 TO-15 0.98Chloroform ug/m30.98 TO-15 0.50Chloromethane ppb v/v0.50 TO-15 1.0Chloromethane ug/m31.0 TO-15 0.035cis-1,2-Dichloroethene ppb v/v0.035 TO-15 0.14cis-1,2-Dichloroethene ug/m30.14 TO-15 0.20cis-1,3-Dichloropropene ppb v/v0.20 TO-15 0.91cis-1,3-Dichloropropene ug/m30.91 TO-15 0.20Cumene ppb v/v0.20 TO-15 0.98Cumene ug/m30.98 TO-15 0.20Cyclohexane ppb v/v0.20 TO-15 0.69Cyclohexane ug/m30.69 TO-15 0.20Dibromochloromethane ppb v/v0.20 TO-15 1.7Dibromochloromethane ug/m31.7 TO-15 0.50Dichlorodifluoromethane ppb v/v0.50 TO-15 2.5Dichlorodifluoromethane ug/m32.5 TO-15 0.20Ethylbenzene ppb v/v0.20 TO-15 0.87Ethylbenzene ug/m30.87 TO-15 0.50Freon 22 ppb v/v0.50 TO-15 1.8Freon 22 ug/m31.8 TO-15 0.20Freon TF ppb v/v0.20 TO-15 1.5Freon TF ug/m31.5 TO-15 0.20Hexachlorobutadiene ppb v/v0.20 TO-15 2.1Hexachlorobutadiene ug/m32.1 TO-15 5.0Isopropyl alcohol ppb v/v5.0 TO-15 12Isopropyl alcohol ug/m312 TO-15 0.50m,p-Xylene ppb v/v0.50 TO-15 2.2m,p-Xylene ug/m32.2 TO-15 0.50Methyl Butyl Ketone (2-Hexanone)ppb v/v0.50 TO-15 2.0Methyl Butyl Ketone (2-Hexanone)ug/m32.0 TO-15 0.50Methyl Ethyl Ketone ppb v/v0.50 TO-15 1.5Methyl Ethyl Ketone ug/m31.5 TO-15 0.50methyl isobutyl ketone ppb v/v0.50 TO-15 2.0methyl isobutyl ketone ug/m32.0 TO-15 0.50Methyl methacrylate ppb v/v0.50 TO-15 2.0Methyl methacrylate ug/m32.0 TO-15 TestAmerica Burlington Page 24 of 478 Default Detection Limits Client: AKRF Inc TestAmerica Job ID: 200-41113-1 Project/Site: 900 King Street SDG: 200-41113-1 Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) 0.20Methyl tert-butyl ether ppb v/v Analyte Units MethodRLRL 0.20 TO-15 0.72Methyl tert-butyl ether ug/m30.72 TO-15 0.50Methylene Chloride ppb v/v0.50 TO-15 1.7Methylene Chloride ug/m31.7 TO-15 0.50Naphthalene ppb v/v0.50 TO-15 2.6Naphthalene ug/m32.6 TO-15 0.50n-Butane ppb v/v0.50 TO-15 1.2n-Butane ug/m31.2 TO-15 0.20n-Butylbenzene ppb v/v0.20 TO-15 1.1n-Butylbenzene ug/m31.1 TO-15 0.20n-Heptane ppb v/v0.20 TO-15 0.82n-Heptane ug/m30.82 TO-15 0.20n-Hexane ppb v/v0.20 TO-15 0.70n-Hexane ug/m30.70 TO-15 0.20n-Propylbenzene ppb v/v0.20 TO-15 0.98n-Propylbenzene ug/m30.98 TO-15 0.20sec-Butylbenzene ppb v/v0.20 TO-15 1.1sec-Butylbenzene ug/m31.1 TO-15 0.20Styrene ppb v/v0.20 TO-15 0.85Styrene ug/m30.85 TO-15 5.0tert-Butyl alcohol ppb v/v5.0 TO-15 15tert-Butyl alcohol ug/m315 TO-15 0.20tert-Butylbenzene ppb v/v0.20 TO-15 1.1tert-Butylbenzene ug/m31.1 TO-15 0.20Tetrachloroethene ppb v/v0.20 TO-15 1.4Tetrachloroethene ug/m31.4 TO-15 5.0Tetrahydrofuran ppb v/v5.0 TO-15 15Tetrahydrofuran ug/m315 TO-15 0.20Toluene ppb v/v0.20 TO-15 0.75Toluene ug/m30.75 TO-15 0.20trans-1,2-Dichloroethene ppb v/v0.20 TO-15 0.79trans-1,2-Dichloroethene ug/m30.79 TO-15 0.20trans-1,3-Dichloropropene ppb v/v0.20 TO-15 0.91trans-1,3-Dichloropropene ug/m30.91 TO-15 0.035Trichloroethene ppb v/v0.035 TO-15 0.19Trichloroethene ug/m30.19 TO-15 0.20Trichlorofluoromethane ppb v/v0.20 TO-15 1.1Trichlorofluoromethane ug/m31.1 TO-15 0.035Vinyl chloride ppb v/v0.035 TO-15 0.089Vinyl chloride ug/m30.089 TO-15 0.70Xylene (total)ppb v/v0.70 TO-15 3.0Xylene (total)ug/m33.0 TO-15 0.20Xylene, o-ppb v/v0.20 TO-15 0.87Xylene, o-ug/m30.87 TO-15 TestAmerica Burlington Page 25 of 478 QC Sample Results TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Method: TO-15 - Volatile Organic Compounds in Ambient Air Client Sample ID: Method BlankLab Sample ID: MB 200-123710/4 Matrix: Air Prep Type: Total/NA Analysis Batch: 123710 RL RL Dichlorodifluoromethane 0.50 U 0.50 ppb v/v 11/24/17 12:18 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier 0.50 U 0.50 ppb v/v 11/24/17 12:18 1Freon 22 0.20 U 0.20 ppb v/v 11/24/17 12:18 11,2-Dichlorotetrafluoroethane 0.50 U 0.50 ppb v/v 11/24/17 12:18 1Chloromethane 0.50 U 0.50 ppb v/v 11/24/17 12:18 1n-Butane 0.035 U 0.035 ppb v/v 11/24/17 12:18 1Vinyl chloride 0.20 U 0.20 ppb v/v 11/24/17 12:18 11,3-Butadiene 0.20 U 0.20 ppb v/v 11/24/17 12:18 1Bromomethane 0.50 U 0.50 ppb v/v 11/24/17 12:18 1Chloroethane 0.20 U 0.20 ppb v/v 11/24/17 12:18 1Bromoethene(Vinyl Bromide) 0.20 U 0.20 ppb v/v 11/24/17 12:18 1Trichlorofluoromethane 0.20 U 0.20 ppb v/v 11/24/17 12:18 1Freon TF 0.035 U 0.035 ppb v/v 11/24/17 12:18 11,1-Dichloroethene 5.0 U 5.0 ppb v/v 11/24/17 12:18 1Acetone 5.0 U 5.0 ppb v/v 11/24/17 12:18 1Isopropyl alcohol 0.50 U 0.50 ppb v/v 11/24/17 12:18 1Carbon disulfide 0.50 U 0.50 ppb v/v 11/24/17 12:18 13-Chloropropene 0.50 U 0.50 ppb v/v 11/24/17 12:18 1Methylene Chloride 5.0 U 5.0 ppb v/v 11/24/17 12:18 1tert-Butyl alcohol 0.20 U 0.20 ppb v/v 11/24/17 12:18 1Methyl tert-butyl ether 0.20 U 0.20 ppb v/v 11/24/17 12:18 1trans-1,2-Dichloroethene 0.20 U 0.20 ppb v/v 11/24/17 12:18 1n-Hexane 0.20 U 0.20 ppb v/v 11/24/17 12:18 11,1-Dichloroethane 0.50 U 0.50 ppb v/v 11/24/17 12:18 1Methyl Ethyl Ketone 0.035 U 0.035 ppb v/v 11/24/17 12:18 1cis-1,2-Dichloroethene 0.40 U 0.40 ppb v/v 11/24/17 12:18 11,2-Dichloroethene, Total 0.20 U 0.20 ppb v/v 11/24/17 12:18 1Chloroform 5.0 U 5.0 ppb v/v 11/24/17 12:18 1Tetrahydrofuran 0.20 U 0.20 ppb v/v 11/24/17 12:18 11,1,1-Trichloroethane 0.20 U 0.20 ppb v/v 11/24/17 12:18 1Cyclohexane 0.035 U 0.035 ppb v/v 11/24/17 12:18 1Carbon tetrachloride 0.20 U 0.20 ppb v/v 11/24/17 12:18 12,2,4-Trimethylpentane 0.20 U 0.20 ppb v/v 11/24/17 12:18 1Benzene 0.20 U 0.20 ppb v/v 11/24/17 12:18 11,2-Dichloroethane 0.20 U 0.20 ppb v/v 11/24/17 12:18 1n-Heptane 0.035 U 0.035 ppb v/v 11/24/17 12:18 1Trichloroethene 0.50 U 0.50 ppb v/v 11/24/17 12:18 1Methyl methacrylate 0.20 U 0.20 ppb v/v 11/24/17 12:18 11,2-Dichloropropane 5.0 U 5.0 ppb v/v 11/24/17 12:18 11,4-Dioxane 0.20 U 0.20 ppb v/v 11/24/17 12:18 1Bromodichloromethane 0.20 U 0.20 ppb v/v 11/24/17 12:18 1cis-1,3-Dichloropropene 0.50 U 0.50 ppb v/v 11/24/17 12:18 1methyl isobutyl ketone 0.20 U 0.20 ppb v/v 11/24/17 12:18 1Toluene 0.20 U 0.20 ppb v/v 11/24/17 12:18 1trans-1,3-Dichloropropene 0.20 U 0.20 ppb v/v 11/24/17 12:18 11,1,2-Trichloroethane 0.20 U 0.20 ppb v/v 11/24/17 12:18 1Tetrachloroethene 0.50 U 0.50 ppb v/v 11/24/17 12:18 1Methyl Butyl Ketone (2-Hexanone) 0.20 U 0.20 ppb v/v 11/24/17 12:18 1Dibromochloromethane TestAmerica Burlington Page 26 of 478 QC Sample Results TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) Client Sample ID: Method BlankLab Sample ID: MB 200-123710/4 Matrix: Air Prep Type: Total/NA Analysis Batch: 123710 RL RL 1,2-Dibromoethane 0.20 U 0.20 ppb v/v 11/24/17 12:18 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier 0.20 U 0.20 ppb v/v 11/24/17 12:18 1Chlorobenzene 0.20 U 0.20 ppb v/v 11/24/17 12:18 1Ethylbenzene 0.50 U 0.50 ppb v/v 11/24/17 12:18 1m,p-Xylene 0.20 U 0.20 ppb v/v 11/24/17 12:18 1Xylene, o- 0.70 U 0.70 ppb v/v 11/24/17 12:18 1Xylene (total) 0.20 U 0.20 ppb v/v 11/24/17 12:18 1Styrene 0.20 U 0.20 ppb v/v 11/24/17 12:18 1Bromoform 0.20 U 0.20 ppb v/v 11/24/17 12:18 1Cumene 0.20 U 0.20 ppb v/v 11/24/17 12:18 11,1,2,2-Tetrachloroethane 0.20 U 0.20 ppb v/v 11/24/17 12:18 1n-Propylbenzene 0.20 U 0.20 ppb v/v 11/24/17 12:18 14-Ethyltoluene 0.20 U 0.20 ppb v/v 11/24/17 12:18 11,3,5-Trimethylbenzene 0.20 U 0.20 ppb v/v 11/24/17 12:18 12-Chlorotoluene 0.20 U 0.20 ppb v/v 11/24/17 12:18 1tert-Butylbenzene 0.20 U 0.20 ppb v/v 11/24/17 12:18 11,2,4-Trimethylbenzene 0.20 U 0.20 ppb v/v 11/24/17 12:18 1sec-Butylbenzene 0.20 U 0.20 ppb v/v 11/24/17 12:18 14-Isopropyltoluene 0.20 U 0.20 ppb v/v 11/24/17 12:18 11,3-Dichlorobenzene 0.20 U 0.20 ppb v/v 11/24/17 12:18 11,4-Dichlorobenzene 0.20 U 0.20 ppb v/v 11/24/17 12:18 1Benzyl chloride 0.20 U 0.20 ppb v/v 11/24/17 12:18 1n-Butylbenzene 0.20 U 0.20 ppb v/v 11/24/17 12:18 11,2-Dichlorobenzene 0.50 U 0.50 ppb v/v 11/24/17 12:18 11,2,4-Trichlorobenzene 0.20 U 0.20 ppb v/v 11/24/17 12:18 1Hexachlorobutadiene 0.50 U 0.50 ppb v/v 11/24/17 12:18 1Naphthalene RL RL Dichlorodifluoromethane 2.5 U 2.5 ug/m3 11/24/17 12:18 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier 1.8 U 1.8 ug/m3 11/24/17 12:18 1Freon 22 1.4 U 1.4 ug/m3 11/24/17 12:18 11,2-Dichlorotetrafluoroethane 1.0 U 1.0 ug/m3 11/24/17 12:18 1Chloromethane 1.2 U 1.2 ug/m3 11/24/17 12:18 1n-Butane 0.089 U 0.089 ug/m3 11/24/17 12:18 1Vinyl chloride 0.44 U 0.44 ug/m3 11/24/17 12:18 11,3-Butadiene 0.78 U 0.78 ug/m3 11/24/17 12:18 1Bromomethane 1.3 U 1.3 ug/m3 11/24/17 12:18 1Chloroethane 0.87 U 0.87 ug/m3 11/24/17 12:18 1Bromoethene(Vinyl Bromide) 1.1 U 1.1 ug/m3 11/24/17 12:18 1Trichlorofluoromethane 1.5 U 1.5 ug/m3 11/24/17 12:18 1Freon TF 0.14 U 0.14 ug/m3 11/24/17 12:18 11,1-Dichloroethene 12 U 12 ug/m3 11/24/17 12:18 1Acetone 12 U 12 ug/m3 11/24/17 12:18 1Isopropyl alcohol 1.6 U 1.6 ug/m3 11/24/17 12:18 1Carbon disulfide 1.6 U 1.6 ug/m3 11/24/17 12:18 13-Chloropropene 1.7 U 1.7 ug/m3 11/24/17 12:18 1Methylene Chloride 15 U 15 ug/m3 11/24/17 12:18 1tert-Butyl alcohol 0.72 U 0.72 ug/m3 11/24/17 12:18 1Methyl tert-butyl ether TestAmerica Burlington Page 27 of 478 QC Sample Results TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) Client Sample ID: Method BlankLab Sample ID: MB 200-123710/4 Matrix: Air Prep Type: Total/NA Analysis Batch: 123710 RL RL trans-1,2-Dichloroethene 0.79 U 0.79 ug/m3 11/24/17 12:18 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier 0.70 U 0.70 ug/m3 11/24/17 12:18 1n-Hexane 0.81 U 0.81 ug/m3 11/24/17 12:18 11,1-Dichloroethane 1.5 U 1.5 ug/m3 11/24/17 12:18 1Methyl Ethyl Ketone 0.14 U 0.14 ug/m3 11/24/17 12:18 1cis-1,2-Dichloroethene 1.6 U 1.6 ug/m3 11/24/17 12:18 11,2-Dichloroethene, Total 0.98 U 0.98 ug/m3 11/24/17 12:18 1Chloroform 15 U 15 ug/m3 11/24/17 12:18 1Tetrahydrofuran 1.1 U 1.1 ug/m3 11/24/17 12:18 11,1,1-Trichloroethane 0.69 U 0.69 ug/m3 11/24/17 12:18 1Cyclohexane 0.22 U 0.22 ug/m3 11/24/17 12:18 1Carbon tetrachloride 0.93 U 0.93 ug/m3 11/24/17 12:18 12,2,4-Trimethylpentane 0.64 U 0.64 ug/m3 11/24/17 12:18 1Benzene 0.81 U 0.81 ug/m3 11/24/17 12:18 11,2-Dichloroethane 0.82 U 0.82 ug/m3 11/24/17 12:18 1n-Heptane 0.19 U 0.19 ug/m3 11/24/17 12:18 1Trichloroethene 2.0 U 2.0 ug/m3 11/24/17 12:18 1Methyl methacrylate 0.92 U 0.92 ug/m3 11/24/17 12:18 11,2-Dichloropropane 18 U 18 ug/m3 11/24/17 12:18 11,4-Dioxane 1.3 U 1.3 ug/m3 11/24/17 12:18 1Bromodichloromethane 0.91 U 0.91 ug/m3 11/24/17 12:18 1cis-1,3-Dichloropropene 2.0 U 2.0 ug/m3 11/24/17 12:18 1methyl isobutyl ketone 0.75 U 0.75 ug/m3 11/24/17 12:18 1Toluene 0.91 U 0.91 ug/m3 11/24/17 12:18 1trans-1,3-Dichloropropene 1.1 U 1.1 ug/m3 11/24/17 12:18 11,1,2-Trichloroethane 1.4 U 1.4 ug/m3 11/24/17 12:18 1Tetrachloroethene 2.0 U 2.0 ug/m3 11/24/17 12:18 1Methyl Butyl Ketone (2-Hexanone) 1.7 U 1.7 ug/m3 11/24/17 12:18 1Dibromochloromethane 1.5 U 1.5 ug/m3 11/24/17 12:18 11,2-Dibromoethane 0.92 U 0.92 ug/m3 11/24/17 12:18 1Chlorobenzene 0.87 U 0.87 ug/m3 11/24/17 12:18 1Ethylbenzene 2.2 U 2.2 ug/m3 11/24/17 12:18 1m,p-Xylene 0.87 U 0.87 ug/m3 11/24/17 12:18 1Xylene, o- 3.0 U 3.0 ug/m3 11/24/17 12:18 1Xylene (total) 0.85 U 0.85 ug/m3 11/24/17 12:18 1Styrene 2.1 U 2.1 ug/m3 11/24/17 12:18 1Bromoform 0.98 U 0.98 ug/m3 11/24/17 12:18 1Cumene 1.4 U 1.4 ug/m3 11/24/17 12:18 11,1,2,2-Tetrachloroethane 0.98 U 0.98 ug/m3 11/24/17 12:18 1n-Propylbenzene 0.98 U 0.98 ug/m3 11/24/17 12:18 14-Ethyltoluene 0.98 U 0.98 ug/m3 11/24/17 12:18 11,3,5-Trimethylbenzene 1.0 U 1.0 ug/m3 11/24/17 12:18 12-Chlorotoluene 1.1 U 1.1 ug/m3 11/24/17 12:18 1tert-Butylbenzene 0.98 U 0.98 ug/m3 11/24/17 12:18 11,2,4-Trimethylbenzene 1.1 U 1.1 ug/m3 11/24/17 12:18 1sec-Butylbenzene 1.1 U 1.1 ug/m3 11/24/17 12:18 14-Isopropyltoluene 1.2 U 1.2 ug/m3 11/24/17 12:18 11,3-Dichlorobenzene 1.2 U 1.2 ug/m3 11/24/17 12:18 11,4-Dichlorobenzene TestAmerica Burlington Page 28 of 478 QC Sample Results TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) Client Sample ID: Method BlankLab Sample ID: MB 200-123710/4 Matrix: Air Prep Type: Total/NA Analysis Batch: 123710 RL RL Benzyl chloride 1.0 U 1.0 ug/m3 11/24/17 12:18 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier 1.1 U 1.1 ug/m3 11/24/17 12:18 1n-Butylbenzene 1.2 U 1.2 ug/m3 11/24/17 12:18 11,2-Dichlorobenzene 3.7 U 3.7 ug/m3 11/24/17 12:18 11,2,4-Trichlorobenzene 2.1 U 2.1 ug/m3 11/24/17 12:18 1Hexachlorobutadiene 2.6 U 2.6 ug/m3 11/24/17 12:18 1Naphthalene Tentatively Identified Compound None ppb v/v 11/24/17 12:18 1 MB MB Tentatively Identified Compound Dil FacPrepared AnalyzedDUnitQualifierEst. Result RT CAS No. Client Sample ID: Lab Control SampleLab Sample ID: LCS 200-123710/3 Matrix: Air Prep Type: Total/NA Analysis Batch: 123710 Dichlorodifluoromethane 10.0 8.04 ppb v/v 80 68 -128 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Freon 22 10.0 7.83 ppb v/v 78 64 -128 1,2-Dichlorotetrafluoroethane 10.0 9.49 ppb v/v 95 78 -138 Chloromethane 10.0 8.02 ppb v/v 80 57 -126 n-Butane 10.0 7.93 ppb v/v 79 56 -130 Vinyl chloride 10.0 8.80 ppb v/v 88 62 -125 1,3-Butadiene 10.0 8.67 ppb v/v 87 59 -125 Bromomethane 10.0 9.53 ppb v/v 95 68 -128 Chloroethane 10.0 9.16 ppb v/v 92 65 -125 Bromoethene(Vinyl Bromide)10.0 9.77 ppb v/v 98 67 -127 Trichlorofluoromethane 10.0 8.64 ppb v/v 86 67 -127 Freon TF 10.0 9.45 ppb v/v 95 68 -128 1,1-Dichloroethene 10.0 9.39 ppb v/v 94 67 -127 Acetone 10.0 8.71 ppb v/v 87 64 -136 Isopropyl alcohol 10.0 8.35 ppb v/v 84 55 -124 Carbon disulfide 10.0 10.8 ppb v/v 108 81 -141 3-Chloropropene 10.0 8.26 ppb v/v 83 53 -133 Methylene Chloride 10.0 8.61 ppb v/v 86 62 -122 tert-Butyl alcohol 10.0 8.73 ppb v/v 87 64 -124 Methyl tert-butyl ether 10.0 9.08 ppb v/v 91 67 -127 trans-1,2-Dichloroethene 10.0 9.56 ppb v/v 96 72 -132 n-Hexane 10.0 9.28 ppb v/v 93 71 -131 1,1-Dichloroethane 10.0 8.97 ppb v/v 90 66 -126 Methyl Ethyl Ketone 10.0 9.30 ppb v/v 93 62 -122 cis-1,2-Dichloroethene 10.0 9.44 ppb v/v 94 67 -127 Chloroform 10.0 8.93 ppb v/v 89 69 -129 Tetrahydrofuran 10.0 8.89 ppb v/v 89 61 -136 1,1,1-Trichloroethane 10.0 8.87 ppb v/v 89 70 -130 Cyclohexane 10.0 9.76 ppb v/v 98 69 -129 Carbon tetrachloride 10.0 9.50 ppb v/v 95 62 -143 2,2,4-Trimethylpentane 10.0 9.17 ppb v/v 92 67 -127 Benzene 10.0 9.25 ppb v/v 93 67 -127 1,2-Dichloroethane 10.0 8.47 ppb v/v 85 67 -132 TestAmerica Burlington Page 29 of 478 QC Sample Results TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 200-123710/3 Matrix: Air Prep Type: Total/NA Analysis Batch: 123710 n-Heptane 10.0 8.47 ppb v/v 85 62 -130 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Trichloroethene 10.0 9.67 ppb v/v 97 68 -128 Methyl methacrylate 10.0 9.66 ppb v/v 97 70 -130 1,2-Dichloropropane 10.0 9.16 ppb v/v 92 67 -127 1,4-Dioxane 10.0 9.85 ppb v/v 99 66 -132 Bromodichloromethane 10.0 8.79 ppb v/v 88 69 -129 cis-1,3-Dichloropropene 10.0 9.47 ppb v/v 95 70 -130 methyl isobutyl ketone 10.0 8.46 ppb v/v 85 62 -130 Toluene 10.0 9.45 ppb v/v 95 67 -127 trans-1,3-Dichloropropene 10.0 9.47 ppb v/v 95 69 -129 1,1,2-Trichloroethane 10.0 9.61 ppb v/v 96 69 -129 Tetrachloroethene 10.0 9.78 ppb v/v 98 70 -130 Methyl Butyl Ketone (2-Hexanone) 10.0 8.87 ppb v/v 89 61 -127 Dibromochloromethane 10.0 9.35 ppb v/v 93 66 -130 1,2-Dibromoethane 10.0 9.67 ppb v/v 97 70 -130 Chlorobenzene 10.0 9.65 ppb v/v 96 68 -128 Ethylbenzene 10.0 9.31 ppb v/v 93 68 -128 m,p-Xylene 20.0 19.0 ppb v/v 95 68 -128 Xylene, o-10.0 9.22 ppb v/v 92 67 -127 Styrene 10.0 9.70 ppb v/v 97 68 -128 Bromoform 10.0 9.86 ppb v/v 99 34 -170 Cumene 10.0 9.20 ppb v/v 92 67 -127 1,1,2,2-Tetrachloroethane 10.0 9.53 ppb v/v 95 69 -129 n-Propylbenzene 10.0 9.17 ppb v/v 92 67 -127 4-Ethyltoluene 10.0 9.47 ppb v/v 95 69 -129 1,3,5-Trimethylbenzene 10.0 8.93 ppb v/v 89 65 -125 2-Chlorotoluene 10.0 9.04 ppb v/v 90 67 -127 tert-Butylbenzene 10.0 8.68 ppb v/v 87 63 -125 1,2,4-Trimethylbenzene 10.0 8.63 ppb v/v 86 65 -125 sec-Butylbenzene 10.0 8.52 ppb v/v 85 66 -126 4-Isopropyltoluene 10.0 8.58 ppb v/v 86 67 -129 1,3-Dichlorobenzene 10.0 9.01 ppb v/v 90 67 -127 1,4-Dichlorobenzene 10.0 8.95 ppb v/v 90 66 -126 Benzyl chloride 10.0 9.03 ppb v/v 90 54 -135 n-Butylbenzene 10.0 8.73 ppb v/v 87 67 -127 1,2-Dichlorobenzene 10.0 8.65 ppb v/v 87 67 -127 1,2,4-Trichlorobenzene 10.0 8.86 ppb v/v 89 59 -126 Hexachlorobutadiene 10.0 8.73 ppb v/v 87 62 -130 Naphthalene 10.0 8.33 ppb v/v 83 50 -121 Dichlorodifluoromethane 49 39.7 ug/m3 80 68 -128 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Freon 22 35 27.7 ug/m3 78 64 -128 1,2-Dichlorotetrafluoroethane 70 66.3 ug/m3 95 78 -138 Chloromethane 21 16.6 ug/m3 80 57 -126 n-Butane 24 18.9 ug/m3 79 56 -130 Vinyl chloride 26 22.5 ug/m3 88 62 -125 TestAmerica Burlington Page 30 of 478 QC Sample Results TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 200-123710/3 Matrix: Air Prep Type: Total/NA Analysis Batch: 123710 1,3-Butadiene 22 19.2 ug/m3 87 59 -125 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Bromomethane 39 37.0 ug/m3 95 68 -128 Chloroethane 26 24.2 ug/m3 92 65 -125 Bromoethene(Vinyl Bromide)44 42.7 ug/m3 98 67 -127 Trichlorofluoromethane 56 48.5 ug/m3 86 67 -127 Freon TF 77 72.4 ug/m3 95 68 -128 1,1-Dichloroethene 40 37.2 ug/m3 94 67 -127 Acetone 24 20.7 ug/m3 87 64 -136 Isopropyl alcohol 25 20.5 ug/m3 84 55 -124 Carbon disulfide 31 33.6 ug/m3 108 81 -141 3-Chloropropene 31 25.9 ug/m3 83 53 -133 Methylene Chloride 35 29.9 ug/m3 86 62 -122 tert-Butyl alcohol 30 26.5 ug/m3 87 64 -124 Methyl tert-butyl ether 36 32.7 ug/m3 91 67 -127 trans-1,2-Dichloroethene 40 37.9 ug/m3 96 72 -132 n-Hexane 35 32.7 ug/m3 93 71 -131 1,1-Dichloroethane 40 36.3 ug/m3 90 66 -126 Methyl Ethyl Ketone 29 27.4 ug/m3 93 62 -122 cis-1,2-Dichloroethene 40 37.4 ug/m3 94 67 -127 Chloroform 49 43.6 ug/m3 89 69 -129 Tetrahydrofuran 29 26.2 ug/m3 89 61 -136 1,1,1-Trichloroethane 55 48.4 ug/m3 89 70 -130 Cyclohexane 34 33.6 ug/m3 98 69 -129 Carbon tetrachloride 63 59.7 ug/m3 95 62 -143 2,2,4-Trimethylpentane 47 42.8 ug/m3 92 67 -127 Benzene 32 29.6 ug/m3 93 67 -127 1,2-Dichloroethane 40 34.3 ug/m3 85 67 -132 n-Heptane 41 34.7 ug/m3 85 62 -130 Trichloroethene 54 51.9 ug/m3 97 68 -128 Methyl methacrylate 41 39.6 ug/m3 97 70 -130 1,2-Dichloropropane 46 42.3 ug/m3 92 67 -127 1,4-Dioxane 36 35.5 ug/m3 99 66 -132 Bromodichloromethane 67 58.9 ug/m3 88 69 -129 cis-1,3-Dichloropropene 45 43.0 ug/m3 95 70 -130 methyl isobutyl ketone 41 34.7 ug/m3 85 62 -130 Toluene 38 35.6 ug/m3 95 67 -127 trans-1,3-Dichloropropene 45 43.0 ug/m3 95 69 -129 1,1,2-Trichloroethane 55 52.5 ug/m3 96 69 -129 Tetrachloroethene 68 66.3 ug/m3 98 70 -130 Methyl Butyl Ketone (2-Hexanone) 41 36.4 ug/m3 89 61 -127 Dibromochloromethane 85 79.6 ug/m3 93 66 -130 1,2-Dibromoethane 77 74.3 ug/m3 97 70 -130 Chlorobenzene 46 44.4 ug/m3 96 68 -128 Ethylbenzene 43 40.4 ug/m3 93 68 -128 m,p-Xylene 87 82.5 ug/m3 95 68 -128 Xylene, o-43 40.0 ug/m3 92 67 -127 Styrene 43 41.3 ug/m3 97 68 -128 TestAmerica Burlington Page 31 of 478 QC Sample Results TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Method: TO-15 - Volatile Organic Compounds in Ambient Air (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 200-123710/3 Matrix: Air Prep Type: Total/NA Analysis Batch: 123710 Bromoform 100 102 ug/m3 99 34 -170 Analyte LCS LCS DUnitResult Qualifier %Rec Spike Added %Rec. Limits Cumene 49 45.2 ug/m3 92 67 -127 1,1,2,2-Tetrachloroethane 69 65.4 ug/m3 95 69 -129 n-Propylbenzene 49 45.1 ug/m3 92 67 -127 4-Ethyltoluene 49 46.6 ug/m3 95 69 -129 1,3,5-Trimethylbenzene 49 43.9 ug/m3 89 65 -125 2-Chlorotoluene 52 46.8 ug/m3 90 67 -127 tert-Butylbenzene 55 47.7 ug/m3 87 63 -125 1,2,4-Trimethylbenzene 49 42.4 ug/m3 86 65 -125 sec-Butylbenzene 55 46.8 ug/m3 85 66 -126 4-Isopropyltoluene 55 47.1 ug/m3 86 67 -129 1,3-Dichlorobenzene 60 54.2 ug/m3 90 67 -127 1,4-Dichlorobenzene 60 53.8 ug/m3 90 66 -126 Benzyl chloride 52 46.8 ug/m3 90 54 -135 n-Butylbenzene 55 47.9 ug/m3 87 67 -127 1,2-Dichlorobenzene 60 52.0 ug/m3 87 67 -127 1,2,4-Trichlorobenzene 74 65.7 ug/m3 89 59 -126 Hexachlorobutadiene 110 93.2 ug/m3 87 62 -130 Naphthalene 52 43.7 ug/m3 83 50 -121 TestAmerica Burlington Page 32 of 478 QC Association Summary TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Air - GC/MS VOA Analysis Batch: 123710 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Air TO-15200-41113-1 SV-3 Total/NA Air TO-15200-41113-2 SV-2 Total/NA Air TO-15200-41113-3 SV-1 Total/NA Air TO-15200-41113-4 AA-1 Total/NA Air TO-15MB 200-123710/4 Method Blank Total/NA Air TO-15LCS 200-123710/3 Lab Control Sample Total/NA TestAmerica Burlington Page 33 of 478 Lab Chronicle Client: AKRF Inc TestAmerica Job ID: 200-41113-1 Project/Site: 900 King Street SDG: 200-41113-1 Client Sample ID: SV-3 Lab Sample ID: 200-41113-1 Matrix: AirDate Collected: 11/20/17 13:18 Date Received: 11/22/17 10:20 Analysis TO-15 11/24/17 15:47 K1P1 123710 TAL BUR Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA Client Sample ID: SV-2 Lab Sample ID: 200-41113-2 Matrix: AirDate Collected: 11/20/17 13:34 Date Received: 11/22/17 10:20 Analysis TO-15 11/24/17 16:40 K1P2.98 123710 TAL BUR Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA Client Sample ID: SV-1 Lab Sample ID: 200-41113-3 Matrix: AirDate Collected: 11/20/17 00:00 Date Received: 11/22/17 10:20 Analysis TO-15 11/24/17 17:32 K1P2.5 123710 TAL BUR Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA Client Sample ID: AA-1 Lab Sample ID: 200-41113-4 Matrix: AirDate Collected: 11/20/17 00:00 Date Received: 11/22/17 10:20 Analysis TO-15 11/24/17 18:24 K1P1 123710 TAL BUR Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA Laboratory References: TAL BUR = TestAmerica Burlington, 30 Community Drive, Suite 11, South Burlington, VT 05403, TEL (802)660-1990 TestAmerica Burlington Page 34 of 478 Accreditation/Certification Summary Client: AKRF Inc TestAmerica Job ID: 200-41113-1 Project/Site: 900 King Street SDG: 200-41113-1 Laboratory: TestAmerica Burlington Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below. Authority Program EPA Region Identification Number Expiration Date New Jersey VT9722NELAP 06-30-18 Analysis Method Prep Method Matrix Analyte The following analytes are included in this report, but are not accredited/certified under this accreditation/certification: TO-15 Air 1,2-Dichloroethene, Total TO-15 Air 4-Isopropyltoluene TO-15 Air Cumene TO-15 Air Freon 22 TO-15 Air n-Butane TO-15 Air n-Butylbenzene TO-15 Air n-Propylbenzene TO-15 Air sec-Butylbenzene TO-15 Air tert-Butylbenzene TestAmerica Burlington Page 35 of 478 Method Summary TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Method Method Description LaboratoryProtocol EPATO-15 Volatile Organic Compounds in Ambient Air TAL BUR Protocol References: EPA = US Environmental Protection Agency Laboratory References: TAL BUR = TestAmerica Burlington, 30 Community Drive, Suite 11, South Burlington, VT 05403, TEL (802)660-1990 TestAmerica Burlington Page 36 of 478 Sample Summary TestAmerica Job ID: 200-41113-1Client: AKRF Inc SDG: 200-41113-1Project/Site: 900 King Street Lab Sample ID Client Sample ID ReceivedCollectedMatrix 200-41113-1 SV-3 Air 11/20/17 13:18 11/22/17 10:20 200-41113-2 SV-2 Air 11/20/17 13:34 11/22/17 10:20 200-41113-3 SV-1 Air 11/20/17 00:00 11/22/17 10:20 200-41113-4 AA-1 Air 11/20/17 00:00 11/22/17 10:20 TestAmerica Burlington Page 37 of 478 Quantitation Limit Exceptions Summary Client: AKRF Inc TestAmerica Job ID: 200-41113-1 Project/Site: 900 King Street SDG: 200-41113-1 Method Lab PQLClient RLUnitsAnalyteMatrix The requested project specific reporting limits listed below were less than laboratory standard quantitation limits (PQL) but greater than or equal to the laboratory method detection limits (MDL). It must be noted that results reported below lab standard quantitation limits may result in false positive/false negative values and less accurate quantitation. Routine laboratory procedures do not indicate corrective action for detections below the laboratory's PQL. TO-15 0.200.035ppb v/v1,1-DichloroetheneAir TO-15 0.200.035ppb v/vCarbon tetrachlorideAir TO-15 0.200.035ppb v/vcis-1,2-DichloroetheneAir TO-15 0.200.035ppb v/vTrichloroetheneAir TO-15 0.200.035ppb v/vVinyl chlorideAir TestAmerica Burlington Page 38 of 478 Lab Name:Job No.: SDG No.: AIR - GC/MS VOA MANUAL INTEGRATION SUMMARY TestAmerica Burlington 200-41113-1 200-41113-1 Instrument ID:Analysis Batch Number:CHB.i 122990 Lab Sample ID:Client Sample ID: Date Analyzed:Lab File ID: COMPOUND NAME RETENTION TIME MANUAL INTEGRATION DATEANALYSTREASON IC 200-122990/4 27754-04.D11/06/17 17:59 GC Column:RTX-624 ID:0.32(mm) 1,1-Dichloroethene Missed Peak daiglep 11/07/17 08:536.33 cis-1,2-Dichloroethene Incomplete Integration daiglep 11/07/17 08:559.33 Trichloroethene Incomplete Integration daiglep 11/07/17 08:5611.48 Tetrachloroethene Incomplete Integration daiglep 11/07/17 08:5614.04 Lab Sample ID:Client Sample ID: Date Analyzed:Lab File ID: COMPOUND NAME RETENTION TIME MANUAL INTEGRATION DATEANALYSTREASON IC 200-122990/5 27754-05.D11/06/17 18:52 GC Column:RTX-624 ID:0.32(mm) 1,1,2-Trichloroethane Incomplete Integration daiglep 11/07/17 09:0413.90 TO-15 Page 39 of 478 Lab Name:Job No.: SDG No.: AIR - GC/MS VOA MANUAL INTEGRATION SUMMARY TestAmerica Burlington 200-41113-1 200-41113-1 Instrument ID:Analysis Batch Number:CHB.i 123710 Lab Sample ID:Client Sample ID: Date Analyzed:Lab File ID: COMPOUND NAME RETENTION TIME MANUAL INTEGRATION DATEANALYSTREASON 200-41113-1 SV-3 28034-08.D11/24/17 15:47 GC Column:RTX-624 ID:0.32(mm) 1,2-Dichlorotetrafluoroethane Assign Peak puangmale ek 11/28/17 09:183.41 Lab Sample ID:Client Sample ID: Date Analyzed:Lab File ID: COMPOUND NAME RETENTION TIME MANUAL INTEGRATION DATEANALYSTREASON 200-41113-2 SV-2 28034-09.D11/24/17 16:40 GC Column:RTX-624 ID:0.32(mm) n-Heptane Assign Peak puangmale ek 11/28/17 09:2610.77 Cumene Assign Peak puangmale ek 11/28/17 09:2716.39 n-Propylbenzene Assign Peak puangmale ek 11/28/17 09:2816.87 4-Ethyltoluene Assign Peak puangmale ek 11/28/17 09:2816.99 1,3,5-Trimethylbenzene Assign Peak puangmale ek 11/28/17 09:2817.06 Lab Sample ID:Client Sample ID: Date Analyzed:Lab File ID: COMPOUND NAME RETENTION TIME MANUAL INTEGRATION DATEANALYSTREASON 200-41113-3 SV-1 28034-10.D11/24/17 17:32 GC Column:RTX-624 ID:0.32(mm) Trichlorofluoromethane Assign Peak puangmale ek 11/28/17 09:315.23 n-Propylbenzene Assign Peak puangmale ek 11/28/17 09:3416.87 1,3,5-Trimethylbenzene Assign Peak puangmale ek 11/28/17 09:3417.06 TO-15 Page 40 of 478 Lab Name:Job No.: SDG No.: AIR - GC/MS VOA MANUAL INTEGRATION SUMMARY TestAmerica Burlington 200-41113-1 200-41113-1 Instrument ID:Analysis Batch Number:CHB.i 123710 Lab Sample ID:Client Sample ID: Date Analyzed:Lab File ID: COMPOUND NAME RETENTION TIME MANUAL INTEGRATION DATEANALYSTREASON 200-41113-4 AA-1 28034-11.D11/24/17 18:24 GC Column:RTX-624 ID:0.32(mm) Ethylbenzene Assign Peak puangmale ek 11/28/17 09:4015.32 TO-15 Page 41 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 1,2-Dichloroethene, TotalATTO15BISs_00006 1,4-Difluorobenzene 100 ppb v/v BFB 100 ppb v/v Chlorobenzene-d5 100 ppb v/v Chlorobromomethane 100 ppb v/v Cyclohexane, 1,1,3-trimethyl- Total Alkanes Xylene (total) ATTO15CAL6w_00144 1,1,1-Trichloroethane 0.20044 ppb v/v 15.463 L 155 mL12/17/17 09/19/17ATTO15CAL1w_00179 Zero Air, Lot 12 1,1,2,2-Tetrachloroethane 0.20044 ppb v/v 1,1,2-Trichloroethane 0.20044 ppb v/v 1,1-Dichloroethane 0.20044 ppb v/v 1,1-Dichloroethene 0.20044 ppb v/v 1,2,3-Trichlorobenzene 0.20044 ppb v/v 1,2,3-Trichloropropane 0.20044 ppb v/v 1,2,4-Trichlorobenzene 0.20044 ppb v/v 1,2,4-Trimethylbenzene 0.20044 ppb v/v 1,2-Dibromoethane 0.20044 ppb v/v 1,2-Dichlorobenzene 0.20044 ppb v/v 1,2-Dichloroethane 0.20044 ppb v/v 1,2-Dichloropropane 0.20044 ppb v/v 1,2-Dichlorotetrafluoroethane 0.20044 ppb v/v 1,3,5-Trimethylbenzene 0.20044 ppb v/v 1,3-Butadiene 0.20044 ppb v/v 1,3-Dichlorobenzene 0.20044 ppb v/v 1,4-Dichlorobenzene 0.20044 ppb v/v 1,4-Dioxane 0.20044 ppb v/v 2,2,4-Trimethylpentane 0.20044 ppb v/v Page 42 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 2-Chlorotoluene 0.20044 ppb v/v 2-Methylbutane 0.20044 ppb v/v 3-Chloropropene 0.20044 ppb v/v 4-Ethyltoluene 0.20044 ppb v/v 4-Isopropyltoluene 0.20044 ppb v/v Acetone 0.20044 ppb v/v Acetonitrile 0.20044 ppb v/v Acrolein 0.20044 ppb v/v Acrylonitrile 0.20044 ppb v/v Alpha Methyl Styrene 0.20044 ppb v/v Benzene 0.20044 ppb v/v Benzyl chloride 0.20044 ppb v/v Bromodichloromethane 0.20044 ppb v/v Bromoethene(Vinyl Bromide)0.20044 ppb v/v Bromoform 0.20044 ppb v/v Bromomethane 0.20044 ppb v/v Carbon disulfide 0.20044 ppb v/v Carbon tetrachloride 0.20044 ppb v/v Chlorobenzene 0.20044 ppb v/v Chloroethane 0.20044 ppb v/v Chloroform 0.20044 ppb v/v Chloromethane 0.20044 ppb v/v cis-1,2-Dichloroethene 0.20044 ppb v/v cis-1,3-Dichloropropene 0.20044 ppb v/v Cumene 0.20044 ppb v/v Page 43 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Cyclohexane 0.20044 ppb v/v Dibromochloromethane 0.20044 ppb v/v Dibromomethane 0.20044 ppb v/v Dichlorodifluoromethane 0.20044 ppb v/v Dodecane 0.20044 ppb v/v Ethyl acetate 0.20044 ppb v/v Ethyl ether 0.20044 ppb v/v Ethylbenzene 0.20044 ppb v/v Freon 22 0.20044 ppb v/v Freon TF 0.20044 ppb v/v Hexachlorobutadiene 0.20044 ppb v/v Isopropyl alcohol 0.20044 ppb v/v m,p-Xylene 0.400879 ppb v/v Methyl Butyl Ketone (2-Hexanone) 0.20044 ppb v/v Methyl Ethyl Ketone 0.20044 ppb v/v methyl isobutyl ketone 0.20044 ppb v/v Methyl methacrylate 0.20044 ppb v/v Methyl tert-butyl ether 0.20044 ppb v/v Methylene Chloride 0.20044 ppb v/v n-Butane 0.20044 ppb v/v n-Butanol 0.20044 ppb v/v n-Butylbenzene 0.20044 ppb v/v n-Decane 0.20044 ppb v/v n-Heptane 0.20044 ppb v/v n-Hexane 0.20044 ppb v/v Page 44 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte n-Nonane 0.20044 ppb v/v n-Octane 0.20044 ppb v/v n-Propylbenzene 0.20044 ppb v/v Naphthalene 0.20044 ppb v/v Pentane 0.20044 ppb v/v Propene 0.20044 ppb v/v sec-Butylbenzene 0.20044 ppb v/v Styrene 0.20044 ppb v/v tert-Butyl alcohol 0.20044 ppb v/v tert-Butylbenzene 0.20044 ppb v/v Tetrachloroethene 0.20044 ppb v/v Tetrahydrofuran 0.20044 ppb v/v Toluene 0.20044 ppb v/v trans-1,2-Dichloroethene 0.20044 ppb v/v trans-1,3-Dichloropropene 0.20044 ppb v/v Trichloroethene 0.20044 ppb v/v Trichlorofluoromethane 0.20044 ppb v/v Undecane 0.20044 ppb v/v Vinyl acetate 0.20044 ppb v/v Vinyl chloride 0.20044 ppb v/v Xylene, o-0.20044 ppb v/v Ethanol 0.400944 ppb v/v ATTO15CALSTKi_00094 1,1,1-Trichloroethane 19.9961 ppb v/v 15.463 L 1546 mL12/17/17 09/19/17.ATTO15CAL6w_00144 Zero Air, Lot 1 1,1,2,2-Tetrachloroethane 19.9961 ppb v/v 1,1,2-Trichloroethane 19.9961 ppb v/v Page 45 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 1,1-Dichloroethane 19.9961 ppb v/v 1,1-Dichloroethene 19.9961 ppb v/v 1,2,3-Trichlorobenzene 19.9961 ppb v/v 1,2,3-Trichloropropane 19.9961 ppb v/v 1,2,4-Trichlorobenzene 19.9961 ppb v/v 1,2,4-Trimethylbenzene 19.9961 ppb v/v 1,2-Dibromoethane 19.9961 ppb v/v 1,2-Dichlorobenzene 19.9961 ppb v/v 1,2-Dichloroethane 19.9961 ppb v/v 1,2-Dichloropropane 19.9961 ppb v/v 1,2-Dichlorotetrafluoroethane 19.9961 ppb v/v 1,3,5-Trimethylbenzene 19.9961 ppb v/v 1,3-Butadiene 19.9961 ppb v/v 1,3-Dichlorobenzene 19.9961 ppb v/v 1,4-Dichlorobenzene 19.9961 ppb v/v 1,4-Dioxane 19.9961 ppb v/v 2,2,4-Trimethylpentane 19.9961 ppb v/v 2-Chlorotoluene 19.9961 ppb v/v 2-Methylbutane 19.9961 ppb v/v 3-Chloropropene 19.9961 ppb v/v 4-Ethyltoluene 19.9961 ppb v/v 4-Isopropyltoluene 19.9961 ppb v/v Acetone 19.9961 ppb v/v Acetonitrile 19.9961 ppb v/v Acrolein 19.9961 ppb v/v Page 46 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Acrylonitrile 19.9961 ppb v/v Alpha Methyl Styrene 19.9961 ppb v/v Benzene 19.9961 ppb v/v Benzyl chloride 19.9961 ppb v/v Bromodichloromethane 19.9961 ppb v/v Bromoethene(Vinyl Bromide)19.9961 ppb v/v Bromoform 19.9961 ppb v/v Bromomethane 19.9961 ppb v/v Carbon disulfide 19.9961 ppb v/v Carbon tetrachloride 19.9961 ppb v/v Chlorobenzene 19.9961 ppb v/v Chloroethane 19.9961 ppb v/v Chloroform 19.9961 ppb v/v Chloromethane 19.9961 ppb v/v cis-1,2-Dichloroethene 19.9961 ppb v/v cis-1,3-Dichloropropene 19.9961 ppb v/v Cumene 19.9961 ppb v/v Cyclohexane 19.9961 ppb v/v Dibromochloromethane 19.9961 ppb v/v Dibromomethane 19.9961 ppb v/v Dichlorodifluoromethane 19.9961 ppb v/v Dodecane 19.9961 ppb v/v Ethyl acetate 19.9961 ppb v/v Ethyl ether 19.9961 ppb v/v Ethylbenzene 19.9961 ppb v/v Page 47 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Freon 22 19.9961 ppb v/v Freon TF 19.9961 ppb v/v Hexachlorobutadiene 19.9961 ppb v/v Isopropyl alcohol 19.9961 ppb v/v m,p-Xylene 39.9922 ppb v/v Methyl Butyl Ketone (2-Hexanone) 19.9961 ppb v/v Methyl Ethyl Ketone 19.9961 ppb v/v methyl isobutyl ketone 19.9961 ppb v/v Methyl methacrylate 19.9961 ppb v/v Methyl tert-butyl ether 19.9961 ppb v/v Methylene Chloride 19.9961 ppb v/v n-Butane 19.9961 ppb v/v n-Butanol 19.9961 ppb v/v n-Butylbenzene 19.9961 ppb v/v n-Decane 19.9961 ppb v/v n-Heptane 19.9961 ppb v/v n-Hexane 19.9961 ppb v/v n-Nonane 19.9961 ppb v/v n-Octane 19.9961 ppb v/v n-Propylbenzene 19.9961 ppb v/v Naphthalene 19.9961 ppb v/v Pentane 19.9961 ppb v/v Propene 19.9961 ppb v/v sec-Butylbenzene 19.9961 ppb v/v Styrene 19.9961 ppb v/v Page 48 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte tert-Butyl alcohol 19.9961 ppb v/v tert-Butylbenzene 19.9961 ppb v/v Tetrachloroethene 19.9961 ppb v/v Tetrahydrofuran 19.9961 ppb v/v Toluene 19.9961 ppb v/v trans-1,2-Dichloroethene 19.9961 ppb v/v trans-1,3-Dichloropropene 19.9961 ppb v/v Trichloroethene 19.9961 ppb v/v Trichlorofluoromethane 19.9961 ppb v/v Undecane 19.9961 ppb v/v Vinyl acetate 19.9961 ppb v/v Vinyl chloride 19.9961 ppb v/v Xylene, o-19.9961 ppb v/v ATTO15EthCALw_00088 1237 mL Ethanol 39.9987 ppb v/v ATTO15CALs_00026 1,1,1-Trichloroethane 200 ppb v/v37.5 L 7500 mL12/17/17 09/18/17..ATTO15CALSTKi_00094 Zero Air, Lot 13 1,1,2,2-Tetrachloroethane 200 ppb v/v 1,1,2-Trichloroethane 200 ppb v/v 1,1-Dichloroethane 200 ppb v/v 1,1-Dichloroethene 200 ppb v/v 1,2,3-Trichlorobenzene 200 ppb v/v 1,2,3-Trichloropropane 200 ppb v/v 1,2,4-Trichlorobenzene 200 ppb v/v 1,2,4-Trimethylbenzene 200 ppb v/v 1,2-Dibromoethane 200 ppb v/v 1,2-Dichlorobenzene 200 ppb v/v 1,2-Dichloroethane 200 ppb v/v 1,2-Dichloropropane 200 ppb v/v 1,2-Dichlorotetrafluoroethane 200 ppb v/v 1,3,5-Trimethylbenzene 200 ppb v/v 1,3-Butadiene 200 ppb v/v 1,3-Dichlorobenzene 200 ppb v/v 1,4-Dichlorobenzene 200 ppb v/v 1,4-Dioxane 200 ppb v/v 2,2,4-Trimethylpentane 200 ppb v/v 2-Chlorotoluene 200 ppb v/v Page 49 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 2-Methylbutane 200 ppb v/v 3-Chloropropene 200 ppb v/v 4-Ethyltoluene 200 ppb v/v 4-Isopropyltoluene 200 ppb v/v Acetone 200 ppb v/v Acetonitrile 200 ppb v/v Acrolein 200 ppb v/v Acrylonitrile 200 ppb v/v Alpha Methyl Styrene 200 ppb v/v Benzene 200 ppb v/v Benzyl chloride 200 ppb v/v Bromodichloromethane 200 ppb v/v Bromoethene(Vinyl Bromide) 200 ppb v/v Bromoform 200 ppb v/v Bromomethane 200 ppb v/v Carbon disulfide 200 ppb v/v Carbon tetrachloride 200 ppb v/v Chlorobenzene 200 ppb v/v Chloroethane 200 ppb v/v Chloroform 200 ppb v/v Chloromethane 200 ppb v/v cis-1,2-Dichloroethene 200 ppb v/v cis-1,3-Dichloropropene 200 ppb v/v Cumene 200 ppb v/v Cyclohexane 200 ppb v/v Dibromochloromethane 200 ppb v/v Dibromomethane 200 ppb v/v Dichlorodifluoromethane 200 ppb v/v Dodecane 200 ppb v/v Ethyl acetate 200 ppb v/v Ethyl ether 200 ppb v/v Ethylbenzene 200 ppb v/v Freon 22 200 ppb v/v Freon TF 200 ppb v/v Hexachlorobutadiene 200 ppb v/v Isopropyl alcohol 200 ppb v/v m,p-Xylene 400 ppb v/v Methyl Butyl Ketone (2-Hexanone) 200 ppb v/v Methyl Ethyl Ketone 200 ppb v/v methyl isobutyl ketone 200 ppb v/v Methyl methacrylate 200 ppb v/v Methyl tert-butyl ether 200 ppb v/v Methylene Chloride 200 ppb v/v n-Butane 200 ppb v/v n-Butanol 200 ppb v/v n-Butylbenzene 200 ppb v/v n-Decane 200 ppb v/v Page 50 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte n-Heptane 200 ppb v/v n-Hexane 200 ppb v/v n-Nonane 200 ppb v/v n-Octane 200 ppb v/v n-Propylbenzene 200 ppb v/v Naphthalene 200 ppb v/v Pentane 200 ppb v/v Propene 200 ppb v/v sec-Butylbenzene 200 ppb v/v Styrene 200 ppb v/v tert-Butyl alcohol 200 ppb v/v tert-Butylbenzene 200 ppb v/v Tetrachloroethene 200 ppb v/v Tetrahydrofuran 200 ppb v/v Toluene 200 ppb v/v trans-1,2-Dichloroethene 200 ppb v/v trans-1,3-Dichloropropene 200 ppb v/v Trichloroethene 200 ppb v/v Trichlorofluoromethane 200 ppb v/v Undecane 200 ppb v/v Vinyl acetate 200 ppb v/v Vinyl chloride 200 ppb v/v Xylene, o-200 ppb v/v 12/19/17 (Purchased Reagent)1,1,1-Trichloroethane 1 ppm v/vSpectra Gases, Lot cc-90855...ATTO15CALs_00026 1,1,2,2-Tetrachloroethane 1 ppm v/v 1,1,2-Trichloroethane 1 ppm v/v 1,1-Dichloroethane 1 ppm v/v 1,1-Dichloroethene 1 ppm v/v 1,2,3-Trichlorobenzene 1 ppm v/v 1,2,3-Trichloropropane 1 ppm v/v 1,2,4-Trichlorobenzene 1 ppm v/v 1,2,4-Trimethylbenzene 1 ppm v/v 1,2-Dibromoethane 1 ppm v/v 1,2-Dichlorobenzene 1 ppm v/v 1,2-Dichloroethane 1 ppm v/v 1,2-Dichloropropane 1 ppm v/v 1,2-Dichlorotetrafluoroethane 1 ppm v/v 1,3,5-Trimethylbenzene 1 ppm v/v 1,3-Butadiene 1 ppm v/v 1,3-Dichlorobenzene 1 ppm v/v 1,4-Dichlorobenzene 1 ppm v/v 1,4-Dioxane 1 ppm v/v 2,2,4-Trimethylpentane 1 ppm v/v 2-Chlorotoluene 1 ppm v/v 2-Methylbutane 1 ppm v/v 3-Chloropropene 1 ppm v/v 4-Ethyltoluene 1 ppm v/v 4-Isopropyltoluene 1 ppm v/v Page 51 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Acetone 1 ppm v/v Acetonitrile 1 ppm v/v Acrolein 1 ppm v/v Acrylonitrile 1 ppm v/v Alpha Methyl Styrene 1 ppm v/v Benzene 1 ppm v/v Benzyl chloride 1 ppm v/v Bromodichloromethane 1 ppm v/v Bromoethene(Vinyl Bromide)1 ppm v/v Bromoform 1 ppm v/v Bromomethane 1 ppm v/v Carbon disulfide 1 ppm v/v Carbon tetrachloride 1 ppm v/v Chlorobenzene 1 ppm v/v Chloroethane 1 ppm v/v Chloroform 1 ppm v/v Chloromethane 1 ppm v/v cis-1,2-Dichloroethene 1 ppm v/v cis-1,3-Dichloropropene 1 ppm v/v Cumene 1 ppm v/v Cyclohexane 1 ppm v/v Dibromochloromethane 1 ppm v/v Dibromomethane 1 ppm v/v Dichlorodifluoromethane 1 ppm v/v Dodecane 1 ppm v/v Ethyl acetate 1 ppm v/v Ethyl ether 1 ppm v/v Ethylbenzene 1 ppm v/v Freon 22 1 ppm v/v Freon TF 1 ppm v/v Hexachlorobutadiene 1 ppm v/v Isopropyl alcohol 1 ppm v/v m,p-Xylene 2 ppm v/v Methyl Butyl Ketone (2-Hexanone) 1 ppm v/v Methyl Ethyl Ketone 1 ppm v/v methyl isobutyl ketone 1 ppm v/v Methyl methacrylate 1 ppm v/v Methyl tert-butyl ether 1 ppm v/v Methylene Chloride 1 ppm v/v n-Butane 1 ppm v/v n-Butanol 1 ppm v/v n-Butylbenzene 1 ppm v/v n-Decane 1 ppm v/v n-Heptane 1 ppm v/v n-Hexane 1 ppm v/v n-Nonane 1 ppm v/v n-Octane 1 ppm v/v Page 52 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte n-Propylbenzene 1 ppm v/v Naphthalene 1 ppm v/v Pentane 1 ppm v/v Propene 1 ppm v/v sec-Butylbenzene 1 ppm v/v Styrene 1 ppm v/v tert-Butyl alcohol 1 ppm v/v tert-Butylbenzene 1 ppm v/v Tetrachloroethene 1 ppm v/v Tetrahydrofuran 1 ppm v/v Toluene 1 ppm v/v trans-1,2-Dichloroethene 1 ppm v/v trans-1,3-Dichloropropene 1 ppm v/v Trichloroethene 1 ppm v/v Trichlorofluoromethane 1 ppm v/v Undecane 1 ppm v/v Vinyl acetate 1 ppm v/v Vinyl chloride 1 ppm v/v Xylene, o-1 ppm v/v 12/19/17 09/19/17 37.5 ppb ATTO15EthCALs_00010 18.75 uL Ethanol 500 ppb v/v..ATTO15EthCALw_00088 Zero Air, Lot 12 08/14/18 (Purchased Reagent)Ethanol 1 mL/mLChem Service, Lot 5301900...ATTO15EthCALs_00010 ATTO15CAL6w_00144 1,1,1-Trichloroethane 0.500453 ppb v/v 15.463 L 387 mL12/17/17 09/19/17ATTO15CAL2w_00245 Zero Air, Lot 12 1,1,2,2-Tetrachloroethane 0.500453 ppb v/v 1,1,2-Trichloroethane 0.500453 ppb v/v 1,1-Dichloroethane 0.500453 ppb v/v 1,1-Dichloroethene 0.500453 ppb v/v 1,2,3-Trichlorobenzene 0.500453 ppb v/v 1,2,3-Trichloropropane 0.500453 ppb v/v 1,2,4-Trichlorobenzene 0.500453 ppb v/v 1,2,4-Trimethylbenzene 0.500453 ppb v/v 1,2-Dibromoethane 0.500453 ppb v/v 1,2-Dichlorobenzene 0.500453 ppb v/v 1,2-Dichloroethane 0.500453 ppb v/v 1,2-Dichloropropane 0.500453 ppb v/v 1,2-Dichlorotetrafluoroethane 0.500453 ppb v/v Page 53 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 1,3,5-Trimethylbenzene 0.500453 ppb v/v 1,3-Butadiene 0.500453 ppb v/v 1,3-Dichlorobenzene 0.500453 ppb v/v 1,4-Dichlorobenzene 0.500453 ppb v/v 1,4-Dioxane 0.500453 ppb v/v 2,2,4-Trimethylpentane 0.500453 ppb v/v 2-Chlorotoluene 0.500453 ppb v/v 2-Methylbutane 0.500453 ppb v/v 3-Chloropropene 0.500453 ppb v/v 4-Ethyltoluene 0.500453 ppb v/v 4-Isopropyltoluene 0.500453 ppb v/v Acetone 0.500453 ppb v/v Acetonitrile 0.500453 ppb v/v Acrolein 0.500453 ppb v/v Acrylonitrile 0.500453 ppb v/v Alpha Methyl Styrene 0.500453 ppb v/v Benzene 0.500453 ppb v/v Benzyl chloride 0.500453 ppb v/v Bromodichloromethane 0.500453 ppb v/v Bromoethene(Vinyl Bromide)0.500453 ppb v/v Bromoform 0.500453 ppb v/v Bromomethane 0.500453 ppb v/v Carbon disulfide 0.500453 ppb v/v Carbon tetrachloride 0.500453 ppb v/v Chlorobenzene 0.500453 ppb v/v Page 54 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Chloroethane 0.500453 ppb v/v Chloroform 0.500453 ppb v/v Chloromethane 0.500453 ppb v/v cis-1,2-Dichloroethene 0.500453 ppb v/v cis-1,3-Dichloropropene 0.500453 ppb v/v Cumene 0.500453 ppb v/v Cyclohexane 0.500453 ppb v/v Dibromochloromethane 0.500453 ppb v/v Dibromomethane 0.500453 ppb v/v Dichlorodifluoromethane 0.500453 ppb v/v Dodecane 0.500453 ppb v/v Ethyl acetate 0.500453 ppb v/v Ethyl ether 0.500453 ppb v/v Ethylbenzene 0.500453 ppb v/v Freon 22 0.500453 ppb v/v Freon TF 0.500453 ppb v/v Hexachlorobutadiene 0.500453 ppb v/v Isopropyl alcohol 0.500453 ppb v/v m,p-Xylene 1.00091 ppb v/v Methyl Butyl Ketone (2-Hexanone) 0.500453 ppb v/v Methyl Ethyl Ketone 0.500453 ppb v/v methyl isobutyl ketone 0.500453 ppb v/v Methyl methacrylate 0.500453 ppb v/v Methyl tert-butyl ether 0.500453 ppb v/v Methylene Chloride 0.500453 ppb v/v Page 55 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte n-Butane 0.500453 ppb v/v n-Butanol 0.500453 ppb v/v n-Butylbenzene 0.500453 ppb v/v n-Decane 0.500453 ppb v/v n-Heptane 0.500453 ppb v/v n-Hexane 0.500453 ppb v/v n-Nonane 0.500453 ppb v/v n-Octane 0.500453 ppb v/v n-Propylbenzene 0.500453 ppb v/v Naphthalene 0.500453 ppb v/v Pentane 0.500453 ppb v/v Propene 0.500453 ppb v/v sec-Butylbenzene 0.500453 ppb v/v Styrene 0.500453 ppb v/v tert-Butyl alcohol 0.500453 ppb v/v tert-Butylbenzene 0.500453 ppb v/v Tetrachloroethene 0.500453 ppb v/v Tetrahydrofuran 0.500453 ppb v/v Toluene 0.500453 ppb v/v trans-1,2-Dichloroethene 0.500453 ppb v/v trans-1,3-Dichloropropene 0.500453 ppb v/v Trichloroethene 0.500453 ppb v/v Trichlorofluoromethane 0.500453 ppb v/v Undecane 0.500453 ppb v/v Vinyl acetate 0.500453 ppb v/v Page 56 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Vinyl chloride 0.500453 ppb v/v Xylene, o-0.500453 ppb v/v Ethanol 5.01064 ppb v/v ATTO15EthCALw_00088 124 mL Ethanol 5.01064 ppb v/v ATTO15CALSTKi_00094 1,1,1-Trichloroethane 19.9961 ppb v/v 15.463 L 1546 mL12/17/17 09/19/17.ATTO15CAL6w_00144 Zero Air, Lot 1 1,1,2,2-Tetrachloroethane 19.9961 ppb v/v 1,1,2-Trichloroethane 19.9961 ppb v/v 1,1-Dichloroethane 19.9961 ppb v/v 1,1-Dichloroethene 19.9961 ppb v/v 1,2,3-Trichlorobenzene 19.9961 ppb v/v 1,2,3-Trichloropropane 19.9961 ppb v/v 1,2,4-Trichlorobenzene 19.9961 ppb v/v 1,2,4-Trimethylbenzene 19.9961 ppb v/v 1,2-Dibromoethane 19.9961 ppb v/v 1,2-Dichlorobenzene 19.9961 ppb v/v 1,2-Dichloroethane 19.9961 ppb v/v 1,2-Dichloropropane 19.9961 ppb v/v 1,2-Dichlorotetrafluoroethane 19.9961 ppb v/v 1,3,5-Trimethylbenzene 19.9961 ppb v/v 1,3-Butadiene 19.9961 ppb v/v 1,3-Dichlorobenzene 19.9961 ppb v/v 1,4-Dichlorobenzene 19.9961 ppb v/v 1,4-Dioxane 19.9961 ppb v/v 2,2,4-Trimethylpentane 19.9961 ppb v/v 2-Chlorotoluene 19.9961 ppb v/v Page 57 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 2-Methylbutane 19.9961 ppb v/v 3-Chloropropene 19.9961 ppb v/v 4-Ethyltoluene 19.9961 ppb v/v 4-Isopropyltoluene 19.9961 ppb v/v Acetone 19.9961 ppb v/v Acetonitrile 19.9961 ppb v/v Acrolein 19.9961 ppb v/v Acrylonitrile 19.9961 ppb v/v Alpha Methyl Styrene 19.9961 ppb v/v Benzene 19.9961 ppb v/v Benzyl chloride 19.9961 ppb v/v Bromodichloromethane 19.9961 ppb v/v Bromoethene(Vinyl Bromide)19.9961 ppb v/v Bromoform 19.9961 ppb v/v Bromomethane 19.9961 ppb v/v Carbon disulfide 19.9961 ppb v/v Carbon tetrachloride 19.9961 ppb v/v Chlorobenzene 19.9961 ppb v/v Chloroethane 19.9961 ppb v/v Chloroform 19.9961 ppb v/v Chloromethane 19.9961 ppb v/v cis-1,2-Dichloroethene 19.9961 ppb v/v cis-1,3-Dichloropropene 19.9961 ppb v/v Cumene 19.9961 ppb v/v Cyclohexane 19.9961 ppb v/v Page 58 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Dibromochloromethane 19.9961 ppb v/v Dibromomethane 19.9961 ppb v/v Dichlorodifluoromethane 19.9961 ppb v/v Dodecane 19.9961 ppb v/v Ethyl acetate 19.9961 ppb v/v Ethyl ether 19.9961 ppb v/v Ethylbenzene 19.9961 ppb v/v Freon 22 19.9961 ppb v/v Freon TF 19.9961 ppb v/v Hexachlorobutadiene 19.9961 ppb v/v Isopropyl alcohol 19.9961 ppb v/v m,p-Xylene 39.9922 ppb v/v Methyl Butyl Ketone (2-Hexanone) 19.9961 ppb v/v Methyl Ethyl Ketone 19.9961 ppb v/v methyl isobutyl ketone 19.9961 ppb v/v Methyl methacrylate 19.9961 ppb v/v Methyl tert-butyl ether 19.9961 ppb v/v Methylene Chloride 19.9961 ppb v/v n-Butane 19.9961 ppb v/v n-Butanol 19.9961 ppb v/v n-Butylbenzene 19.9961 ppb v/v n-Decane 19.9961 ppb v/v n-Heptane 19.9961 ppb v/v n-Hexane 19.9961 ppb v/v n-Nonane 19.9961 ppb v/v Page 59 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte n-Octane 19.9961 ppb v/v n-Propylbenzene 19.9961 ppb v/v Naphthalene 19.9961 ppb v/v Pentane 19.9961 ppb v/v Propene 19.9961 ppb v/v sec-Butylbenzene 19.9961 ppb v/v Styrene 19.9961 ppb v/v tert-Butyl alcohol 19.9961 ppb v/v tert-Butylbenzene 19.9961 ppb v/v Tetrachloroethene 19.9961 ppb v/v Tetrahydrofuran 19.9961 ppb v/v Toluene 19.9961 ppb v/v trans-1,2-Dichloroethene 19.9961 ppb v/v trans-1,3-Dichloropropene 19.9961 ppb v/v Trichloroethene 19.9961 ppb v/v Trichlorofluoromethane 19.9961 ppb v/v Undecane 19.9961 ppb v/v Vinyl acetate 19.9961 ppb v/v Vinyl chloride 19.9961 ppb v/v Xylene, o-19.9961 ppb v/v ATTO15EthCALw_00088 1237 mL Ethanol 39.9987 ppb v/v ATTO15CALs_00026 1,1,1-Trichloroethane 200 ppb v/v37.5 L 7500 mL12/17/17 09/18/17..ATTO15CALSTKi_00094 Zero Air, Lot 13 1,1,2,2-Tetrachloroethane 200 ppb v/v 1,1,2-Trichloroethane 200 ppb v/v 1,1-Dichloroethane 200 ppb v/v 1,1-Dichloroethene 200 ppb v/v 1,2,3-Trichlorobenzene 200 ppb v/v 1,2,3-Trichloropropane 200 ppb v/v 1,2,4-Trichlorobenzene 200 ppb v/v Page 60 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 1,2,4-Trimethylbenzene 200 ppb v/v 1,2-Dibromoethane 200 ppb v/v 1,2-Dichlorobenzene 200 ppb v/v 1,2-Dichloroethane 200 ppb v/v 1,2-Dichloropropane 200 ppb v/v 1,2-Dichlorotetrafluoroethane 200 ppb v/v 1,3,5-Trimethylbenzene 200 ppb v/v 1,3-Butadiene 200 ppb v/v 1,3-Dichlorobenzene 200 ppb v/v 1,4-Dichlorobenzene 200 ppb v/v 1,4-Dioxane 200 ppb v/v 2,2,4-Trimethylpentane 200 ppb v/v 2-Chlorotoluene 200 ppb v/v 2-Methylbutane 200 ppb v/v 3-Chloropropene 200 ppb v/v 4-Ethyltoluene 200 ppb v/v 4-Isopropyltoluene 200 ppb v/v Acetone 200 ppb v/v Acetonitrile 200 ppb v/v Acrolein 200 ppb v/v Acrylonitrile 200 ppb v/v Alpha Methyl Styrene 200 ppb v/v Benzene 200 ppb v/v Benzyl chloride 200 ppb v/v Bromodichloromethane 200 ppb v/v Bromoethene(Vinyl Bromide) 200 ppb v/v Bromoform 200 ppb v/v Bromomethane 200 ppb v/v Carbon disulfide 200 ppb v/v Carbon tetrachloride 200 ppb v/v Chlorobenzene 200 ppb v/v Chloroethane 200 ppb v/v Chloroform 200 ppb v/v Chloromethane 200 ppb v/v cis-1,2-Dichloroethene 200 ppb v/v cis-1,3-Dichloropropene 200 ppb v/v Cumene 200 ppb v/v Cyclohexane 200 ppb v/v Dibromochloromethane 200 ppb v/v Dibromomethane 200 ppb v/v Dichlorodifluoromethane 200 ppb v/v Dodecane 200 ppb v/v Ethyl acetate 200 ppb v/v Ethyl ether 200 ppb v/v Ethylbenzene 200 ppb v/v Freon 22 200 ppb v/v Freon TF 200 ppb v/v Hexachlorobutadiene 200 ppb v/v Page 61 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Isopropyl alcohol 200 ppb v/v m,p-Xylene 400 ppb v/v Methyl Butyl Ketone (2-Hexanone) 200 ppb v/v Methyl Ethyl Ketone 200 ppb v/v methyl isobutyl ketone 200 ppb v/v Methyl methacrylate 200 ppb v/v Methyl tert-butyl ether 200 ppb v/v Methylene Chloride 200 ppb v/v n-Butane 200 ppb v/v n-Butanol 200 ppb v/v n-Butylbenzene 200 ppb v/v n-Decane 200 ppb v/v n-Heptane 200 ppb v/v n-Hexane 200 ppb v/v n-Nonane 200 ppb v/v n-Octane 200 ppb v/v n-Propylbenzene 200 ppb v/v Naphthalene 200 ppb v/v Pentane 200 ppb v/v Propene 200 ppb v/v sec-Butylbenzene 200 ppb v/v Styrene 200 ppb v/v tert-Butyl alcohol 200 ppb v/v tert-Butylbenzene 200 ppb v/v Tetrachloroethene 200 ppb v/v Tetrahydrofuran 200 ppb v/v Toluene 200 ppb v/v trans-1,2-Dichloroethene 200 ppb v/v trans-1,3-Dichloropropene 200 ppb v/v Trichloroethene 200 ppb v/v Trichlorofluoromethane 200 ppb v/v Undecane 200 ppb v/v Vinyl acetate 200 ppb v/v Vinyl chloride 200 ppb v/v Xylene, o-200 ppb v/v 12/19/17 (Purchased Reagent)1,1,1-Trichloroethane 1 ppm v/vSpectra Gases, Lot cc-90855...ATTO15CALs_00026 1,1,2,2-Tetrachloroethane 1 ppm v/v 1,1,2-Trichloroethane 1 ppm v/v 1,1-Dichloroethane 1 ppm v/v 1,1-Dichloroethene 1 ppm v/v 1,2,3-Trichlorobenzene 1 ppm v/v 1,2,3-Trichloropropane 1 ppm v/v 1,2,4-Trichlorobenzene 1 ppm v/v 1,2,4-Trimethylbenzene 1 ppm v/v 1,2-Dibromoethane 1 ppm v/v 1,2-Dichlorobenzene 1 ppm v/v 1,2-Dichloroethane 1 ppm v/v Page 62 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 1,2-Dichloropropane 1 ppm v/v 1,2-Dichlorotetrafluoroethane 1 ppm v/v 1,3,5-Trimethylbenzene 1 ppm v/v 1,3-Butadiene 1 ppm v/v 1,3-Dichlorobenzene 1 ppm v/v 1,4-Dichlorobenzene 1 ppm v/v 1,4-Dioxane 1 ppm v/v 2,2,4-Trimethylpentane 1 ppm v/v 2-Chlorotoluene 1 ppm v/v 2-Methylbutane 1 ppm v/v 3-Chloropropene 1 ppm v/v 4-Ethyltoluene 1 ppm v/v 4-Isopropyltoluene 1 ppm v/v Acetone 1 ppm v/v Acetonitrile 1 ppm v/v Acrolein 1 ppm v/v Acrylonitrile 1 ppm v/v Alpha Methyl Styrene 1 ppm v/v Benzene 1 ppm v/v Benzyl chloride 1 ppm v/v Bromodichloromethane 1 ppm v/v Bromoethene(Vinyl Bromide)1 ppm v/v Bromoform 1 ppm v/v Bromomethane 1 ppm v/v Carbon disulfide 1 ppm v/v Carbon tetrachloride 1 ppm v/v Chlorobenzene 1 ppm v/v Chloroethane 1 ppm v/v Chloroform 1 ppm v/v Chloromethane 1 ppm v/v cis-1,2-Dichloroethene 1 ppm v/v cis-1,3-Dichloropropene 1 ppm v/v Cumene 1 ppm v/v Cyclohexane 1 ppm v/v Dibromochloromethane 1 ppm v/v Dibromomethane 1 ppm v/v Dichlorodifluoromethane 1 ppm v/v Dodecane 1 ppm v/v Ethyl acetate 1 ppm v/v Ethyl ether 1 ppm v/v Ethylbenzene 1 ppm v/v Freon 22 1 ppm v/v Freon TF 1 ppm v/v Hexachlorobutadiene 1 ppm v/v Isopropyl alcohol 1 ppm v/v m,p-Xylene 2 ppm v/v Methyl Butyl Ketone (2-Hexanone) 1 ppm v/v Page 63 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Methyl Ethyl Ketone 1 ppm v/v methyl isobutyl ketone 1 ppm v/v Methyl methacrylate 1 ppm v/v Methyl tert-butyl ether 1 ppm v/v Methylene Chloride 1 ppm v/v n-Butane 1 ppm v/v n-Butanol 1 ppm v/v n-Butylbenzene 1 ppm v/v n-Decane 1 ppm v/v n-Heptane 1 ppm v/v n-Hexane 1 ppm v/v n-Nonane 1 ppm v/v n-Octane 1 ppm v/v n-Propylbenzene 1 ppm v/v Naphthalene 1 ppm v/v Pentane 1 ppm v/v Propene 1 ppm v/v sec-Butylbenzene 1 ppm v/v Styrene 1 ppm v/v tert-Butyl alcohol 1 ppm v/v tert-Butylbenzene 1 ppm v/v Tetrachloroethene 1 ppm v/v Tetrahydrofuran 1 ppm v/v Toluene 1 ppm v/v trans-1,2-Dichloroethene 1 ppm v/v trans-1,3-Dichloropropene 1 ppm v/v Trichloroethene 1 ppm v/v Trichlorofluoromethane 1 ppm v/v Undecane 1 ppm v/v Vinyl acetate 1 ppm v/v Vinyl chloride 1 ppm v/v Xylene, o-1 ppm v/v ATTO15EthCALs_00010 Ethanol 500 ppb v/v37.5 ppb 18.75 uL12/19/17 09/19/17..ATTO15EthCALw_00088 Zero Air, Lot 12 08/14/18 (Purchased Reagent)Ethanol 1 mL/mLChem Service, Lot 5301900...ATTO15EthCALs_00010 12/19/17 09/19/17 37.5 ppb ATTO15EthCALs_00010 18.75 uL Ethanol 500 ppb v/v.ATTO15EthCALw_00088 Zero Air, Lot 12 08/14/18 (Purchased Reagent)Ethanol 1 mL/mLChem Service, Lot 5301900..ATTO15EthCALs_00010 ATTO15CALSTKi_00094 1,1,1-Trichloroethane 4.99256 ppb v/v 15.463 L 386 mL12/17/17 09/19/17ATTO15CAL3w_00188 Zero Air, Lot 12 1,1,2,2-Tetrachloroethane 4.99256 ppb v/v 1,1,2-Trichloroethane 4.99256 ppb v/v 1,1-Dichloroethane 4.99256 ppb v/v 1,1-Dichloroethene 4.99256 ppb v/v 1,2,3-Trichlorobenzene 4.99256 ppb v/v Page 64 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 1,2,3-Trichloropropane 4.99256 ppb v/v 1,2,4-Trichlorobenzene 4.99256 ppb v/v 1,2,4-Trimethylbenzene 4.99256 ppb v/v 1,2-Dibromoethane 4.99256 ppb v/v 1,2-Dichlorobenzene 4.99256 ppb v/v 1,2-Dichloroethane 4.99256 ppb v/v 1,2-Dichloropropane 4.99256 ppb v/v 1,2-Dichlorotetrafluoroethane 4.99256 ppb v/v 1,3,5-Trimethylbenzene 4.99256 ppb v/v 1,3-Butadiene 4.99256 ppb v/v 1,3-Dichlorobenzene 4.99256 ppb v/v 1,4-Dichlorobenzene 4.99256 ppb v/v 1,4-Dioxane 4.99256 ppb v/v 2,2,4-Trimethylpentane 4.99256 ppb v/v 2-Chlorotoluene 4.99256 ppb v/v 2-Methylbutane 4.99256 ppb v/v 3-Chloropropene 4.99256 ppb v/v 4-Ethyltoluene 4.99256 ppb v/v 4-Isopropyltoluene 4.99256 ppb v/v Acetone 4.99256 ppb v/v Acetonitrile 4.99256 ppb v/v Acrolein 4.99256 ppb v/v Acrylonitrile 4.99256 ppb v/v Alpha Methyl Styrene 4.99256 ppb v/v Benzene 4.99256 ppb v/v Page 65 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Benzyl chloride 4.99256 ppb v/v Bromodichloromethane 4.99256 ppb v/v Bromoethene(Vinyl Bromide)4.99256 ppb v/v Bromoform 4.99256 ppb v/v Bromomethane 4.99256 ppb v/v Carbon disulfide 4.99256 ppb v/v Carbon tetrachloride 4.99256 ppb v/v Chlorobenzene 4.99256 ppb v/v Chloroethane 4.99256 ppb v/v Chloroform 4.99256 ppb v/v Chloromethane 4.99256 ppb v/v cis-1,2-Dichloroethene 4.99256 ppb v/v cis-1,3-Dichloropropene 4.99256 ppb v/v Cumene 4.99256 ppb v/v Cyclohexane 4.99256 ppb v/v Dibromochloromethane 4.99256 ppb v/v Dibromomethane 4.99256 ppb v/v Dichlorodifluoromethane 4.99256 ppb v/v Dodecane 4.99256 ppb v/v Ethyl acetate 4.99256 ppb v/v Ethyl ether 4.99256 ppb v/v Ethylbenzene 4.99256 ppb v/v Freon 22 4.99256 ppb v/v Freon TF 4.99256 ppb v/v Hexachlorobutadiene 4.99256 ppb v/v Page 66 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Isopropyl alcohol 4.99256 ppb v/v m,p-Xylene 9.98513 ppb v/v Methyl Butyl Ketone (2-Hexanone) 4.99256 ppb v/v Methyl Ethyl Ketone 4.99256 ppb v/v methyl isobutyl ketone 4.99256 ppb v/v Methyl methacrylate 4.99256 ppb v/v Methyl tert-butyl ether 4.99256 ppb v/v Methylene Chloride 4.99256 ppb v/v n-Butane 4.99256 ppb v/v n-Butanol 4.99256 ppb v/v n-Butylbenzene 4.99256 ppb v/v n-Decane 4.99256 ppb v/v n-Heptane 4.99256 ppb v/v n-Hexane 4.99256 ppb v/v n-Nonane 4.99256 ppb v/v n-Octane 4.99256 ppb v/v n-Propylbenzene 4.99256 ppb v/v Naphthalene 4.99256 ppb v/v Pentane 4.99256 ppb v/v Propene 4.99256 ppb v/v sec-Butylbenzene 4.99256 ppb v/v Styrene 4.99256 ppb v/v tert-Butyl alcohol 4.99256 ppb v/v tert-Butylbenzene 4.99256 ppb v/v Tetrachloroethene 4.99256 ppb v/v Page 67 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Tetrahydrofuran 4.99256 ppb v/v Toluene 4.99256 ppb v/v trans-1,2-Dichloroethene 4.99256 ppb v/v trans-1,3-Dichloropropene 4.99256 ppb v/v Trichloroethene 4.99256 ppb v/v Trichlorofluoromethane 4.99256 ppb v/v Undecane 4.99256 ppb v/v Vinyl acetate 4.99256 ppb v/v Vinyl chloride 4.99256 ppb v/v Xylene, o-4.99256 ppb v/v ATTO15EthCALw_00088 309 mL Ethanol 9.99159 ppb v/v ATTO15CALs_00026 1,1,1-Trichloroethane 200 ppb v/v37.5 L 7500 mL12/17/17 09/18/17.ATTO15CALSTKi_00094 Zero Air, Lot 13 1,1,2,2-Tetrachloroethane 200 ppb v/v 1,1,2-Trichloroethane 200 ppb v/v 1,1-Dichloroethane 200 ppb v/v 1,1-Dichloroethene 200 ppb v/v 1,2,3-Trichlorobenzene 200 ppb v/v 1,2,3-Trichloropropane 200 ppb v/v 1,2,4-Trichlorobenzene 200 ppb v/v 1,2,4-Trimethylbenzene 200 ppb v/v 1,2-Dibromoethane 200 ppb v/v 1,2-Dichlorobenzene 200 ppb v/v 1,2-Dichloroethane 200 ppb v/v 1,2-Dichloropropane 200 ppb v/v 1,2-Dichlorotetrafluoroethane 200 ppb v/v 1,3,5-Trimethylbenzene 200 ppb v/v 1,3-Butadiene 200 ppb v/v 1,3-Dichlorobenzene 200 ppb v/v 1,4-Dichlorobenzene 200 ppb v/v 1,4-Dioxane 200 ppb v/v 2,2,4-Trimethylpentane 200 ppb v/v 2-Chlorotoluene 200 ppb v/v 2-Methylbutane 200 ppb v/v 3-Chloropropene 200 ppb v/v 4-Ethyltoluene 200 ppb v/v 4-Isopropyltoluene 200 ppb v/v Acetone 200 ppb v/v Acetonitrile 200 ppb v/v Page 68 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Acrolein 200 ppb v/v Acrylonitrile 200 ppb v/v Alpha Methyl Styrene 200 ppb v/v Benzene 200 ppb v/v Benzyl chloride 200 ppb v/v Bromodichloromethane 200 ppb v/v Bromoethene(Vinyl Bromide) 200 ppb v/v Bromoform 200 ppb v/v Bromomethane 200 ppb v/v Carbon disulfide 200 ppb v/v Carbon tetrachloride 200 ppb v/v Chlorobenzene 200 ppb v/v Chloroethane 200 ppb v/v Chloroform 200 ppb v/v Chloromethane 200 ppb v/v cis-1,2-Dichloroethene 200 ppb v/v cis-1,3-Dichloropropene 200 ppb v/v Cumene 200 ppb v/v Cyclohexane 200 ppb v/v Dibromochloromethane 200 ppb v/v Dibromomethane 200 ppb v/v Dichlorodifluoromethane 200 ppb v/v Dodecane 200 ppb v/v Ethyl acetate 200 ppb v/v Ethyl ether 200 ppb v/v Ethylbenzene 200 ppb v/v Freon 22 200 ppb v/v Freon TF 200 ppb v/v Hexachlorobutadiene 200 ppb v/v Isopropyl alcohol 200 ppb v/v m,p-Xylene 400 ppb v/v Methyl Butyl Ketone (2-Hexanone) 200 ppb v/v Methyl Ethyl Ketone 200 ppb v/v methyl isobutyl ketone 200 ppb v/v Methyl methacrylate 200 ppb v/v Methyl tert-butyl ether 200 ppb v/v Methylene Chloride 200 ppb v/v n-Butane 200 ppb v/v n-Butanol 200 ppb v/v n-Butylbenzene 200 ppb v/v n-Decane 200 ppb v/v n-Heptane 200 ppb v/v n-Hexane 200 ppb v/v n-Nonane 200 ppb v/v n-Octane 200 ppb v/v n-Propylbenzene 200 ppb v/v Naphthalene 200 ppb v/v Page 69 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Pentane 200 ppb v/v Propene 200 ppb v/v sec-Butylbenzene 200 ppb v/v Styrene 200 ppb v/v tert-Butyl alcohol 200 ppb v/v tert-Butylbenzene 200 ppb v/v Tetrachloroethene 200 ppb v/v Tetrahydrofuran 200 ppb v/v Toluene 200 ppb v/v trans-1,2-Dichloroethene 200 ppb v/v trans-1,3-Dichloropropene 200 ppb v/v Trichloroethene 200 ppb v/v Trichlorofluoromethane 200 ppb v/v Undecane 200 ppb v/v Vinyl acetate 200 ppb v/v Vinyl chloride 200 ppb v/v Xylene, o-200 ppb v/v 12/19/17 (Purchased Reagent)1,1,1-Trichloroethane 1 ppm v/vSpectra Gases, Lot cc-90855..ATTO15CALs_00026 1,1,2,2-Tetrachloroethane 1 ppm v/v 1,1,2-Trichloroethane 1 ppm v/v 1,1-Dichloroethane 1 ppm v/v 1,1-Dichloroethene 1 ppm v/v 1,2,3-Trichlorobenzene 1 ppm v/v 1,2,3-Trichloropropane 1 ppm v/v 1,2,4-Trichlorobenzene 1 ppm v/v 1,2,4-Trimethylbenzene 1 ppm v/v 1,2-Dibromoethane 1 ppm v/v 1,2-Dichlorobenzene 1 ppm v/v 1,2-Dichloroethane 1 ppm v/v 1,2-Dichloropropane 1 ppm v/v 1,2-Dichlorotetrafluoroethane 1 ppm v/v 1,3,5-Trimethylbenzene 1 ppm v/v 1,3-Butadiene 1 ppm v/v 1,3-Dichlorobenzene 1 ppm v/v 1,4-Dichlorobenzene 1 ppm v/v 1,4-Dioxane 1 ppm v/v 2,2,4-Trimethylpentane 1 ppm v/v 2-Chlorotoluene 1 ppm v/v 2-Methylbutane 1 ppm v/v 3-Chloropropene 1 ppm v/v 4-Ethyltoluene 1 ppm v/v 4-Isopropyltoluene 1 ppm v/v Acetone 1 ppm v/v Acetonitrile 1 ppm v/v Acrolein 1 ppm v/v Acrylonitrile 1 ppm v/v Alpha Methyl Styrene 1 ppm v/v Benzene 1 ppm v/v Page 70 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Benzyl chloride 1 ppm v/v Bromodichloromethane 1 ppm v/v Bromoethene(Vinyl Bromide)1 ppm v/v Bromoform 1 ppm v/v Bromomethane 1 ppm v/v Carbon disulfide 1 ppm v/v Carbon tetrachloride 1 ppm v/v Chlorobenzene 1 ppm v/v Chloroethane 1 ppm v/v Chloroform 1 ppm v/v Chloromethane 1 ppm v/v cis-1,2-Dichloroethene 1 ppm v/v cis-1,3-Dichloropropene 1 ppm v/v Cumene 1 ppm v/v Cyclohexane 1 ppm v/v Dibromochloromethane 1 ppm v/v Dibromomethane 1 ppm v/v Dichlorodifluoromethane 1 ppm v/v Dodecane 1 ppm v/v Ethyl acetate 1 ppm v/v Ethyl ether 1 ppm v/v Ethylbenzene 1 ppm v/v Freon 22 1 ppm v/v Freon TF 1 ppm v/v Hexachlorobutadiene 1 ppm v/v Isopropyl alcohol 1 ppm v/v m,p-Xylene 2 ppm v/v Methyl Butyl Ketone (2-Hexanone) 1 ppm v/v Methyl Ethyl Ketone 1 ppm v/v methyl isobutyl ketone 1 ppm v/v Methyl methacrylate 1 ppm v/v Methyl tert-butyl ether 1 ppm v/v Methylene Chloride 1 ppm v/v n-Butane 1 ppm v/v n-Butanol 1 ppm v/v n-Butylbenzene 1 ppm v/v n-Decane 1 ppm v/v n-Heptane 1 ppm v/v n-Hexane 1 ppm v/v n-Nonane 1 ppm v/v n-Octane 1 ppm v/v n-Propylbenzene 1 ppm v/v Naphthalene 1 ppm v/v Pentane 1 ppm v/v Propene 1 ppm v/v sec-Butylbenzene 1 ppm v/v Styrene 1 ppm v/v Page 71 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte tert-Butyl alcohol 1 ppm v/v tert-Butylbenzene 1 ppm v/v Tetrachloroethene 1 ppm v/v Tetrahydrofuran 1 ppm v/v Toluene 1 ppm v/v trans-1,2-Dichloroethene 1 ppm v/v trans-1,3-Dichloropropene 1 ppm v/v Trichloroethene 1 ppm v/v Trichlorofluoromethane 1 ppm v/v Undecane 1 ppm v/v Vinyl acetate 1 ppm v/v Vinyl chloride 1 ppm v/v Xylene, o-1 ppm v/v 12/19/17 09/19/17 37.5 ppb ATTO15EthCALs_00010 18.75 uL Ethanol 500 ppb v/v.ATTO15EthCALw_00088 Zero Air, Lot 12 08/14/18 (Purchased Reagent)Ethanol 1 mL/mLChem Service, Lot 5301900..ATTO15EthCALs_00010 ATTO15CALSTKi_00094 1,1,1-Trichloroethane 9.99806 ppb v/v 15.463 L 773 mL12/17/17 09/19/17ATTO15CAL4w_00645 Zero Air, Lot 12 1,1,2,2-Tetrachloroethane 9.99806 ppb v/v 1,1,2-Trichloroethane 9.99806 ppb v/v 1,1-Dichloroethane 9.99806 ppb v/v 1,1-Dichloroethene 9.99806 ppb v/v 1,2,3-Trichlorobenzene 9.99806 ppb v/v 1,2,3-Trichloropropane 9.99806 ppb v/v 1,2,4-Trichlorobenzene 9.99806 ppb v/v 1,2,4-Trimethylbenzene 9.99806 ppb v/v 1,2-Dibromoethane 9.99806 ppb v/v 1,2-Dichlorobenzene 9.99806 ppb v/v 1,2-Dichloroethane 9.99806 ppb v/v 1,2-Dichloropropane 9.99806 ppb v/v 1,2-Dichlorotetrafluoroethane 9.99806 ppb v/v 1,3,5-Trimethylbenzene 9.99806 ppb v/v 1,3-Butadiene 9.99806 ppb v/v 1,3-Dichlorobenzene 9.99806 ppb v/v Page 72 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 1,4-Dichlorobenzene 9.99806 ppb v/v 1,4-Dioxane 9.99806 ppb v/v 2,2,4-Trimethylpentane 9.99806 ppb v/v 2-Chlorotoluene 9.99806 ppb v/v 2-Methylbutane 9.99806 ppb v/v 3-Chloropropene 9.99806 ppb v/v 4-Ethyltoluene 9.99806 ppb v/v 4-Isopropyltoluene 9.99806 ppb v/v Acetone 9.99806 ppb v/v Acetonitrile 9.99806 ppb v/v Acrolein 9.99806 ppb v/v Acrylonitrile 9.99806 ppb v/v Alpha Methyl Styrene 9.99806 ppb v/v Benzene 9.99806 ppb v/v Benzyl chloride 9.99806 ppb v/v Bromodichloromethane 9.99806 ppb v/v Bromoethene(Vinyl Bromide)9.99806 ppb v/v Bromoform 9.99806 ppb v/v Bromomethane 9.99806 ppb v/v Carbon disulfide 9.99806 ppb v/v Carbon tetrachloride 9.99806 ppb v/v Chlorobenzene 9.99806 ppb v/v Chloroethane 9.99806 ppb v/v Chloroform 9.99806 ppb v/v Chloromethane 9.99806 ppb v/v Page 73 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte cis-1,2-Dichloroethene 9.99806 ppb v/v cis-1,3-Dichloropropene 9.99806 ppb v/v Cumene 9.99806 ppb v/v Cyclohexane 9.99806 ppb v/v Dibromochloromethane 9.99806 ppb v/v Dibromomethane 9.99806 ppb v/v Dichlorodifluoromethane 9.99806 ppb v/v Dodecane 9.99806 ppb v/v Ethyl acetate 9.99806 ppb v/v Ethyl ether 9.99806 ppb v/v Ethylbenzene 9.99806 ppb v/v Freon 22 9.99806 ppb v/v Freon TF 9.99806 ppb v/v Hexachlorobutadiene 9.99806 ppb v/v Isopropyl alcohol 9.99806 ppb v/v m,p-Xylene 19.9961 ppb v/v Methyl Butyl Ketone (2-Hexanone) 9.99806 ppb v/v Methyl Ethyl Ketone 9.99806 ppb v/v methyl isobutyl ketone 9.99806 ppb v/v Methyl methacrylate 9.99806 ppb v/v Methyl tert-butyl ether 9.99806 ppb v/v Methylene Chloride 9.99806 ppb v/v n-Butane 9.99806 ppb v/v n-Butanol 9.99806 ppb v/v n-Butylbenzene 9.99806 ppb v/v Page 74 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte n-Decane 9.99806 ppb v/v n-Heptane 9.99806 ppb v/v n-Hexane 9.99806 ppb v/v n-Nonane 9.99806 ppb v/v n-Octane 9.99806 ppb v/v n-Propylbenzene 9.99806 ppb v/v Naphthalene 9.99806 ppb v/v Pentane 9.99806 ppb v/v Propene 9.99806 ppb v/v sec-Butylbenzene 9.99806 ppb v/v Styrene 9.99806 ppb v/v tert-Butyl alcohol 9.99806 ppb v/v tert-Butylbenzene 9.99806 ppb v/v Tetrachloroethene 9.99806 ppb v/v Tetrahydrofuran 9.99806 ppb v/v Toluene 9.99806 ppb v/v trans-1,2-Dichloroethene 9.99806 ppb v/v trans-1,3-Dichloropropene 9.99806 ppb v/v Trichloroethene 9.99806 ppb v/v Trichlorofluoromethane 9.99806 ppb v/v Undecane 9.99806 ppb v/v Vinyl acetate 9.99806 ppb v/v Vinyl chloride 9.99806 ppb v/v Xylene, o-9.99806 ppb v/v ATTO15EthCALw_00088 464 mL Ethanol 15.0036 ppb v/v ATTO15CALs_00026 1,1,1-Trichloroethane 200 ppb v/v37.5 L 7500 mL12/17/17 09/18/17.ATTO15CALSTKi_00094 Zero Air, Lot 13 Page 75 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 1,1,2,2-Tetrachloroethane 200 ppb v/v 1,1,2-Trichloroethane 200 ppb v/v 1,1-Dichloroethane 200 ppb v/v 1,1-Dichloroethene 200 ppb v/v 1,2,3-Trichlorobenzene 200 ppb v/v 1,2,3-Trichloropropane 200 ppb v/v 1,2,4-Trichlorobenzene 200 ppb v/v 1,2,4-Trimethylbenzene 200 ppb v/v 1,2-Dibromoethane 200 ppb v/v 1,2-Dichlorobenzene 200 ppb v/v 1,2-Dichloroethane 200 ppb v/v 1,2-Dichloropropane 200 ppb v/v 1,2-Dichlorotetrafluoroethane 200 ppb v/v 1,3,5-Trimethylbenzene 200 ppb v/v 1,3-Butadiene 200 ppb v/v 1,3-Dichlorobenzene 200 ppb v/v 1,4-Dichlorobenzene 200 ppb v/v 1,4-Dioxane 200 ppb v/v 2,2,4-Trimethylpentane 200 ppb v/v 2-Chlorotoluene 200 ppb v/v 2-Methylbutane 200 ppb v/v 3-Chloropropene 200 ppb v/v 4-Ethyltoluene 200 ppb v/v 4-Isopropyltoluene 200 ppb v/v Acetone 200 ppb v/v Acetonitrile 200 ppb v/v Acrolein 200 ppb v/v Acrylonitrile 200 ppb v/v Alpha Methyl Styrene 200 ppb v/v Benzene 200 ppb v/v Benzyl chloride 200 ppb v/v Bromodichloromethane 200 ppb v/v Bromoethene(Vinyl Bromide) 200 ppb v/v Bromoform 200 ppb v/v Bromomethane 200 ppb v/v Carbon disulfide 200 ppb v/v Carbon tetrachloride 200 ppb v/v Chlorobenzene 200 ppb v/v Chloroethane 200 ppb v/v Chloroform 200 ppb v/v Chloromethane 200 ppb v/v cis-1,2-Dichloroethene 200 ppb v/v cis-1,3-Dichloropropene 200 ppb v/v Cumene 200 ppb v/v Cyclohexane 200 ppb v/v Dibromochloromethane 200 ppb v/v Dibromomethane 200 ppb v/v Dichlorodifluoromethane 200 ppb v/v Page 76 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Dodecane 200 ppb v/v Ethyl acetate 200 ppb v/v Ethyl ether 200 ppb v/v Ethylbenzene 200 ppb v/v Freon 22 200 ppb v/v Freon TF 200 ppb v/v Hexachlorobutadiene 200 ppb v/v Isopropyl alcohol 200 ppb v/v m,p-Xylene 400 ppb v/v Methyl Butyl Ketone (2-Hexanone) 200 ppb v/v Methyl Ethyl Ketone 200 ppb v/v methyl isobutyl ketone 200 ppb v/v Methyl methacrylate 200 ppb v/v Methyl tert-butyl ether 200 ppb v/v Methylene Chloride 200 ppb v/v n-Butane 200 ppb v/v n-Butanol 200 ppb v/v n-Butylbenzene 200 ppb v/v n-Decane 200 ppb v/v n-Heptane 200 ppb v/v n-Hexane 200 ppb v/v n-Nonane 200 ppb v/v n-Octane 200 ppb v/v n-Propylbenzene 200 ppb v/v Naphthalene 200 ppb v/v Pentane 200 ppb v/v Propene 200 ppb v/v sec-Butylbenzene 200 ppb v/v Styrene 200 ppb v/v tert-Butyl alcohol 200 ppb v/v tert-Butylbenzene 200 ppb v/v Tetrachloroethene 200 ppb v/v Tetrahydrofuran 200 ppb v/v Toluene 200 ppb v/v trans-1,2-Dichloroethene 200 ppb v/v trans-1,3-Dichloropropene 200 ppb v/v Trichloroethene 200 ppb v/v Trichlorofluoromethane 200 ppb v/v Undecane 200 ppb v/v Vinyl acetate 200 ppb v/v Vinyl chloride 200 ppb v/v Xylene, o-200 ppb v/v 12/19/17 (Purchased Reagent)1,1,1-Trichloroethane 1 ppm v/vSpectra Gases, Lot cc-90855..ATTO15CALs_00026 1,1,2,2-Tetrachloroethane 1 ppm v/v 1,1,2-Trichloroethane 1 ppm v/v 1,1-Dichloroethane 1 ppm v/v 1,1-Dichloroethene 1 ppm v/v Page 77 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 1,2,3-Trichlorobenzene 1 ppm v/v 1,2,3-Trichloropropane 1 ppm v/v 1,2,4-Trichlorobenzene 1 ppm v/v 1,2,4-Trimethylbenzene 1 ppm v/v 1,2-Dibromoethane 1 ppm v/v 1,2-Dichlorobenzene 1 ppm v/v 1,2-Dichloroethane 1 ppm v/v 1,2-Dichloropropane 1 ppm v/v 1,2-Dichlorotetrafluoroethane 1 ppm v/v 1,3,5-Trimethylbenzene 1 ppm v/v 1,3-Butadiene 1 ppm v/v 1,3-Dichlorobenzene 1 ppm v/v 1,4-Dichlorobenzene 1 ppm v/v 1,4-Dioxane 1 ppm v/v 2,2,4-Trimethylpentane 1 ppm v/v 2-Chlorotoluene 1 ppm v/v 2-Methylbutane 1 ppm v/v 3-Chloropropene 1 ppm v/v 4-Ethyltoluene 1 ppm v/v 4-Isopropyltoluene 1 ppm v/v Acetone 1 ppm v/v Acetonitrile 1 ppm v/v Acrolein 1 ppm v/v Acrylonitrile 1 ppm v/v Alpha Methyl Styrene 1 ppm v/v Benzene 1 ppm v/v Benzyl chloride 1 ppm v/v Bromodichloromethane 1 ppm v/v Bromoethene(Vinyl Bromide)1 ppm v/v Bromoform 1 ppm v/v Bromomethane 1 ppm v/v Carbon disulfide 1 ppm v/v Carbon tetrachloride 1 ppm v/v Chlorobenzene 1 ppm v/v Chloroethane 1 ppm v/v Chloroform 1 ppm v/v Chloromethane 1 ppm v/v cis-1,2-Dichloroethene 1 ppm v/v cis-1,3-Dichloropropene 1 ppm v/v Cumene 1 ppm v/v Cyclohexane 1 ppm v/v Dibromochloromethane 1 ppm v/v Dibromomethane 1 ppm v/v Dichlorodifluoromethane 1 ppm v/v Dodecane 1 ppm v/v Ethyl acetate 1 ppm v/v Ethyl ether 1 ppm v/v Ethylbenzene 1 ppm v/v Page 78 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Freon 22 1 ppm v/v Freon TF 1 ppm v/v Hexachlorobutadiene 1 ppm v/v Isopropyl alcohol 1 ppm v/v m,p-Xylene 2 ppm v/v Methyl Butyl Ketone (2-Hexanone) 1 ppm v/v Methyl Ethyl Ketone 1 ppm v/v methyl isobutyl ketone 1 ppm v/v Methyl methacrylate 1 ppm v/v Methyl tert-butyl ether 1 ppm v/v Methylene Chloride 1 ppm v/v n-Butane 1 ppm v/v n-Butanol 1 ppm v/v n-Butylbenzene 1 ppm v/v n-Decane 1 ppm v/v n-Heptane 1 ppm v/v n-Hexane 1 ppm v/v n-Nonane 1 ppm v/v n-Octane 1 ppm v/v n-Propylbenzene 1 ppm v/v Naphthalene 1 ppm v/v Pentane 1 ppm v/v Propene 1 ppm v/v sec-Butylbenzene 1 ppm v/v Styrene 1 ppm v/v tert-Butyl alcohol 1 ppm v/v tert-Butylbenzene 1 ppm v/v Tetrachloroethene 1 ppm v/v Tetrahydrofuran 1 ppm v/v Toluene 1 ppm v/v trans-1,2-Dichloroethene 1 ppm v/v trans-1,3-Dichloropropene 1 ppm v/v Trichloroethene 1 ppm v/v Trichlorofluoromethane 1 ppm v/v Undecane 1 ppm v/v Vinyl acetate 1 ppm v/v Vinyl chloride 1 ppm v/v Xylene, o-1 ppm v/v 12/19/17 09/19/17 37.5 ppb ATTO15EthCALs_00010 18.75 uL Ethanol 500 ppb v/v.ATTO15EthCALw_00088 Zero Air, Lot 12 08/14/18 (Purchased Reagent)Ethanol 1 mL/mLChem Service, Lot 5301900..ATTO15EthCALs_00010 ATTO15CALSTKi_00095 1,1,1-Trichloroethane 9.99806 ppb v/v 15.463 L 773 mL12/19/17 10/19/17ATTO15CAL4w_00655 Zero Air, Lot 12 1,1,2,2-Tetrachloroethane 9.99806 ppb v/v 1,1,2-Trichloroethane 9.99806 ppb v/v Page 79 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 1,1-Dichloroethane 9.99806 ppb v/v 1,1-Dichloroethene 9.99806 ppb v/v 1,2,4-Trichlorobenzene 9.99806 ppb v/v 1,2,4-Trimethylbenzene 9.99806 ppb v/v 1,2-Dibromoethane 9.99806 ppb v/v 1,2-Dichlorobenzene 9.99806 ppb v/v 1,2-Dichloroethane 9.99806 ppb v/v 1,2-Dichloroethene, Total 19.9961 ppb v/v 1,2-Dichloropropane 9.99806 ppb v/v 1,2-Dichlorotetrafluoroethane 9.99806 ppb v/v 1,3,5-Trimethylbenzene 9.99806 ppb v/v 1,3-Butadiene 9.99806 ppb v/v 1,3-Dichlorobenzene 9.99806 ppb v/v 1,4-Dichlorobenzene 9.99806 ppb v/v 1,4-Dioxane 9.99806 ppb v/v 2,2,4-Trimethylpentane 9.99806 ppb v/v 2-Chlorotoluene 9.99806 ppb v/v 3-Chloropropene 9.99806 ppb v/v 4-Ethyltoluene 9.99806 ppb v/v 4-Isopropyltoluene 9.99806 ppb v/v Acetone 9.99806 ppb v/v Acrolein 9.99806 ppb v/v Acrylonitrile 9.99806 ppb v/v Alpha Methyl Styrene 9.99806 ppb v/v Benzene 9.99806 ppb v/v Page 80 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Benzyl chloride 9.99806 ppb v/v Bromodichloromethane 9.99806 ppb v/v Bromoethene(Vinyl Bromide)9.99806 ppb v/v Bromoform 9.99806 ppb v/v Bromomethane 9.99806 ppb v/v Carbon disulfide 9.99806 ppb v/v Carbon tetrachloride 9.99806 ppb v/v Chlorobenzene 9.99806 ppb v/v Chloroethane 9.99806 ppb v/v Chloroform 9.99806 ppb v/v Chloromethane 9.99806 ppb v/v cis-1,2-Dichloroethene 9.99806 ppb v/v cis-1,3-Dichloropropene 9.99806 ppb v/v Cumene 9.99806 ppb v/v Cyclohexane 9.99806 ppb v/v Dibromochloromethane 9.99806 ppb v/v Dibromomethane 9.99806 ppb v/v Dichlorodifluoromethane 9.99806 ppb v/v Dodecane 9.99806 ppb v/v Ethyl acetate 9.99806 ppb v/v Ethyl ether 9.99806 ppb v/v Ethylbenzene 9.99806 ppb v/v Freon 22 9.99806 ppb v/v Freon TF 9.99806 ppb v/v Hexachlorobutadiene 9.99806 ppb v/v Page 81 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Isopropyl alcohol 9.99806 ppb v/v m,p-Xylene 19.9961 ppb v/v Methyl Butyl Ketone (2-Hexanone) 9.99806 ppb v/v Methyl Ethyl Ketone 9.99806 ppb v/v methyl isobutyl ketone 9.99806 ppb v/v Methyl methacrylate 9.99806 ppb v/v Methyl tert-butyl ether 9.99806 ppb v/v Methylene Chloride 9.99806 ppb v/v n-Butane 9.99806 ppb v/v n-Butylbenzene 9.99806 ppb v/v n-Decane 9.99806 ppb v/v n-Heptane 9.99806 ppb v/v n-Hexane 9.99806 ppb v/v n-Nonane 9.99806 ppb v/v n-Propylbenzene 9.99806 ppb v/v Naphthalene 9.99806 ppb v/v sec-Butylbenzene 9.99806 ppb v/v Styrene 9.99806 ppb v/v tert-Butyl alcohol 9.99806 ppb v/v tert-Butylbenzene 9.99806 ppb v/v Tetrachloroethene 9.99806 ppb v/v Tetrahydrofuran 9.99806 ppb v/v Toluene 9.99806 ppb v/v trans-1,2-Dichloroethene 9.99806 ppb v/v trans-1,3-Dichloropropene 9.99806 ppb v/v Page 82 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Trichloroethene 9.99806 ppb v/v Trichlorofluoromethane 9.99806 ppb v/v Vinyl chloride 9.99806 ppb v/v Xylene (total)29.9942 ppb v/v Xylene, o-9.99806 ppb v/v ATTO15EthCALw_00089 464 mL Ethanol 15.0036 ppb v/v ATTO15CALs_00026 1,1,1-Trichloroethane 200 ppb v/v37.5 L 7500 mL12/19/17 10/17/17.ATTO15CALSTKi_00095 Zero Air, Lot 13 1,1,2,2-Tetrachloroethane 200 ppb v/v 1,1,2-Trichloroethane 200 ppb v/v 1,1-Dichloroethane 200 ppb v/v 1,1-Dichloroethene 200 ppb v/v 1,2,4-Trichlorobenzene 200 ppb v/v 1,2,4-Trimethylbenzene 200 ppb v/v 1,2-Dibromoethane 200 ppb v/v 1,2-Dichlorobenzene 200 ppb v/v 1,2-Dichloroethane 200 ppb v/v 1,2-Dichloroethene, Total 400 ppb v/v 1,2-Dichloropropane 200 ppb v/v 1,2-Dichlorotetrafluoroethane 200 ppb v/v 1,3,5-Trimethylbenzene 200 ppb v/v 1,3-Butadiene 200 ppb v/v 1,3-Dichlorobenzene 200 ppb v/v 1,4-Dichlorobenzene 200 ppb v/v 1,4-Dioxane 200 ppb v/v 2,2,4-Trimethylpentane 200 ppb v/v 2-Chlorotoluene 200 ppb v/v 3-Chloropropene 200 ppb v/v 4-Ethyltoluene 200 ppb v/v 4-Isopropyltoluene 200 ppb v/v Acetone 200 ppb v/v Acrolein 200 ppb v/v Acrylonitrile 200 ppb v/v Alpha Methyl Styrene 200 ppb v/v Benzene 200 ppb v/v Benzyl chloride 200 ppb v/v Bromodichloromethane 200 ppb v/v Bromoethene(Vinyl Bromide) 200 ppb v/v Bromoform 200 ppb v/v Bromomethane 200 ppb v/v Carbon disulfide 200 ppb v/v Carbon tetrachloride 200 ppb v/v Chlorobenzene 200 ppb v/v Chloroethane 200 ppb v/v Page 83 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Chloroform 200 ppb v/v Chloromethane 200 ppb v/v cis-1,2-Dichloroethene 200 ppb v/v cis-1,3-Dichloropropene 200 ppb v/v Cumene 200 ppb v/v Cyclohexane 200 ppb v/v Dibromochloromethane 200 ppb v/v Dibromomethane 200 ppb v/v Dichlorodifluoromethane 200 ppb v/v Dodecane 200 ppb v/v Ethyl acetate 200 ppb v/v Ethyl ether 200 ppb v/v Ethylbenzene 200 ppb v/v Freon 22 200 ppb v/v Freon TF 200 ppb v/v Hexachlorobutadiene 200 ppb v/v Isopropyl alcohol 200 ppb v/v m,p-Xylene 400 ppb v/v Methyl Butyl Ketone (2-Hexanone) 200 ppb v/v Methyl Ethyl Ketone 200 ppb v/v methyl isobutyl ketone 200 ppb v/v Methyl methacrylate 200 ppb v/v Methyl tert-butyl ether 200 ppb v/v Methylene Chloride 200 ppb v/v n-Butane 200 ppb v/v n-Butylbenzene 200 ppb v/v n-Decane 200 ppb v/v n-Heptane 200 ppb v/v n-Hexane 200 ppb v/v n-Nonane 200 ppb v/v n-Propylbenzene 200 ppb v/v Naphthalene 200 ppb v/v sec-Butylbenzene 200 ppb v/v Styrene 200 ppb v/v tert-Butyl alcohol 200 ppb v/v tert-Butylbenzene 200 ppb v/v Tetrachloroethene 200 ppb v/v Tetrahydrofuran 200 ppb v/v Toluene 200 ppb v/v trans-1,2-Dichloroethene 200 ppb v/v trans-1,3-Dichloropropene 200 ppb v/v Trichloroethene 200 ppb v/v Trichlorofluoromethane 200 ppb v/v Vinyl chloride 200 ppb v/v Xylene (total)600 ppb v/v Xylene, o-200 ppb v/v 12/19/17 (Purchased Reagent)1,1,1-Trichloroethane 1 ppm v/vSpectra Gases, Lot cc-90855..ATTO15CALs_00026 Page 84 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 1,1,2,2-Tetrachloroethane 1 ppm v/v 1,1,2-Trichloroethane 1 ppm v/v 1,1-Dichloroethane 1 ppm v/v 1,1-Dichloroethene 1 ppm v/v 1,2,4-Trichlorobenzene 1 ppm v/v 1,2,4-Trimethylbenzene 1 ppm v/v 1,2-Dibromoethane 1 ppm v/v 1,2-Dichlorobenzene 1 ppm v/v 1,2-Dichloroethane 1 ppm v/v 1,2-Dichloroethene, Total 2 ppm v/v 1,2-Dichloropropane 1 ppm v/v 1,2-Dichlorotetrafluoroethane 1 ppm v/v 1,3,5-Trimethylbenzene 1 ppm v/v 1,3-Butadiene 1 ppm v/v 1,3-Dichlorobenzene 1 ppm v/v 1,4-Dichlorobenzene 1 ppm v/v 1,4-Dioxane 1 ppm v/v 2,2,4-Trimethylpentane 1 ppm v/v 2-Chlorotoluene 1 ppm v/v 3-Chloropropene 1 ppm v/v 4-Ethyltoluene 1 ppm v/v 4-Isopropyltoluene 1 ppm v/v Acetone 1 ppm v/v Acrolein 1 ppm v/v Acrylonitrile 1 ppm v/v Alpha Methyl Styrene 1 ppm v/v Benzene 1 ppm v/v Benzyl chloride 1 ppm v/v Bromodichloromethane 1 ppm v/v Bromoethene(Vinyl Bromide)1 ppm v/v Bromoform 1 ppm v/v Bromomethane 1 ppm v/v Carbon disulfide 1 ppm v/v Carbon tetrachloride 1 ppm v/v Chlorobenzene 1 ppm v/v Chloroethane 1 ppm v/v Chloroform 1 ppm v/v Chloromethane 1 ppm v/v cis-1,2-Dichloroethene 1 ppm v/v cis-1,3-Dichloropropene 1 ppm v/v Cumene 1 ppm v/v Cyclohexane 1 ppm v/v Dibromochloromethane 1 ppm v/v Dibromomethane 1 ppm v/v Dichlorodifluoromethane 1 ppm v/v Dodecane 1 ppm v/v Ethyl acetate 1 ppm v/v Ethyl ether 1 ppm v/v Page 85 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Ethylbenzene 1 ppm v/v Freon 22 1 ppm v/v Freon TF 1 ppm v/v Hexachlorobutadiene 1 ppm v/v Isopropyl alcohol 1 ppm v/v m,p-Xylene 2 ppm v/v Methyl Butyl Ketone (2-Hexanone) 1 ppm v/v Methyl Ethyl Ketone 1 ppm v/v methyl isobutyl ketone 1 ppm v/v Methyl methacrylate 1 ppm v/v Methyl tert-butyl ether 1 ppm v/v Methylene Chloride 1 ppm v/v n-Butane 1 ppm v/v n-Butylbenzene 1 ppm v/v n-Decane 1 ppm v/v n-Heptane 1 ppm v/v n-Hexane 1 ppm v/v n-Nonane 1 ppm v/v n-Propylbenzene 1 ppm v/v Naphthalene 1 ppm v/v sec-Butylbenzene 1 ppm v/v Styrene 1 ppm v/v tert-Butyl alcohol 1 ppm v/v tert-Butylbenzene 1 ppm v/v Tetrachloroethene 1 ppm v/v Tetrahydrofuran 1 ppm v/v Toluene 1 ppm v/v trans-1,2-Dichloroethene 1 ppm v/v trans-1,3-Dichloropropene 1 ppm v/v Trichloroethene 1 ppm v/v Trichlorofluoromethane 1 ppm v/v Vinyl chloride 1 ppm v/v Xylene (total)3 ppm v/v Xylene, o-1 ppm v/v 01/18/18 10/18/17 37.5 ppb ATTO15EthCALs_00010 18.75 uL Ethanol 500 ppb v/v.ATTO15EthCALw_00089 Zero Air, Lot 12 08/14/18 (Purchased Reagent)Ethanol 1 mL/mLChem Service, Lot 5301900..ATTO15EthCALs_00010 ATTO15CALSTKi_00094 1,1,1-Trichloroethane 15.0036 ppb v/v 15.463 L 1160 mL12/17/17 09/19/17ATTO15CAL5w_00069 Zero Air, Lot 12 1,1,2,2-Tetrachloroethane 15.0036 ppb v/v 1,1,2-Trichloroethane 15.0036 ppb v/v 1,1-Dichloroethane 15.0036 ppb v/v 1,1-Dichloroethene 15.0036 ppb v/v Page 86 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 1,2,3-Trichlorobenzene 15.0036 ppb v/v 1,2,3-Trichloropropane 15.0036 ppb v/v 1,2,4-Trichlorobenzene 15.0036 ppb v/v 1,2,4-Trimethylbenzene 15.0036 ppb v/v 1,2-Dibromoethane 15.0036 ppb v/v 1,2-Dichlorobenzene 15.0036 ppb v/v 1,2-Dichloroethane 15.0036 ppb v/v 1,2-Dichloropropane 15.0036 ppb v/v 1,2-Dichlorotetrafluoroethane 15.0036 ppb v/v 1,3,5-Trimethylbenzene 15.0036 ppb v/v 1,3-Butadiene 15.0036 ppb v/v 1,3-Dichlorobenzene 15.0036 ppb v/v 1,4-Dichlorobenzene 15.0036 ppb v/v 1,4-Dioxane 15.0036 ppb v/v 2,2,4-Trimethylpentane 15.0036 ppb v/v 2-Chlorotoluene 15.0036 ppb v/v 2-Methylbutane 15.0036 ppb v/v 3-Chloropropene 15.0036 ppb v/v 4-Ethyltoluene 15.0036 ppb v/v 4-Isopropyltoluene 15.0036 ppb v/v Acetone 15.0036 ppb v/v Acetonitrile 15.0036 ppb v/v Acrolein 15.0036 ppb v/v Acrylonitrile 15.0036 ppb v/v Alpha Methyl Styrene 15.0036 ppb v/v Page 87 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Benzene 15.0036 ppb v/v Benzyl chloride 15.0036 ppb v/v Bromodichloromethane 15.0036 ppb v/v Bromoethene(Vinyl Bromide)15.0036 ppb v/v Bromoform 15.0036 ppb v/v Bromomethane 15.0036 ppb v/v Carbon disulfide 15.0036 ppb v/v Carbon tetrachloride 15.0036 ppb v/v Chlorobenzene 15.0036 ppb v/v Chloroethane 15.0036 ppb v/v Chloroform 15.0036 ppb v/v Chloromethane 15.0036 ppb v/v cis-1,2-Dichloroethene 15.0036 ppb v/v cis-1,3-Dichloropropene 15.0036 ppb v/v Cumene 15.0036 ppb v/v Cyclohexane 15.0036 ppb v/v Dibromochloromethane 15.0036 ppb v/v Dibromomethane 15.0036 ppb v/v Dichlorodifluoromethane 15.0036 ppb v/v Dodecane 15.0036 ppb v/v Ethyl acetate 15.0036 ppb v/v Ethyl ether 15.0036 ppb v/v Ethylbenzene 15.0036 ppb v/v Freon 22 15.0036 ppb v/v Freon TF 15.0036 ppb v/v Page 88 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Hexachlorobutadiene 15.0036 ppb v/v Isopropyl alcohol 15.0036 ppb v/v m,p-Xylene 30.0071 ppb v/v Methyl Butyl Ketone (2-Hexanone) 15.0036 ppb v/v Methyl Ethyl Ketone 15.0036 ppb v/v methyl isobutyl ketone 15.0036 ppb v/v Methyl methacrylate 15.0036 ppb v/v Methyl tert-butyl ether 15.0036 ppb v/v Methylene Chloride 15.0036 ppb v/v n-Butane 15.0036 ppb v/v n-Butanol 15.0036 ppb v/v n-Butylbenzene 15.0036 ppb v/v n-Decane 15.0036 ppb v/v n-Heptane 15.0036 ppb v/v n-Hexane 15.0036 ppb v/v n-Nonane 15.0036 ppb v/v n-Octane 15.0036 ppb v/v n-Propylbenzene 15.0036 ppb v/v Naphthalene 15.0036 ppb v/v Pentane 15.0036 ppb v/v Propene 15.0036 ppb v/v sec-Butylbenzene 15.0036 ppb v/v Styrene 15.0036 ppb v/v tert-Butyl alcohol 15.0036 ppb v/v tert-Butylbenzene 15.0036 ppb v/v Page 89 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Tetrachloroethene 15.0036 ppb v/v Tetrahydrofuran 15.0036 ppb v/v Toluene 15.0036 ppb v/v trans-1,2-Dichloroethene 15.0036 ppb v/v trans-1,3-Dichloropropene 15.0036 ppb v/v Trichloroethene 15.0036 ppb v/v Trichlorofluoromethane 15.0036 ppb v/v Undecane 15.0036 ppb v/v Vinyl acetate 15.0036 ppb v/v Vinyl chloride 15.0036 ppb v/v Xylene, o-15.0036 ppb v/v ATTO15EthCALw_00088 620 mL Ethanol 20.0479 ppb v/v ATTO15CALs_00026 1,1,1-Trichloroethane 200 ppb v/v37.5 L 7500 mL12/17/17 09/18/17.ATTO15CALSTKi_00094 Zero Air, Lot 13 1,1,2,2-Tetrachloroethane 200 ppb v/v 1,1,2-Trichloroethane 200 ppb v/v 1,1-Dichloroethane 200 ppb v/v 1,1-Dichloroethene 200 ppb v/v 1,2,3-Trichlorobenzene 200 ppb v/v 1,2,3-Trichloropropane 200 ppb v/v 1,2,4-Trichlorobenzene 200 ppb v/v 1,2,4-Trimethylbenzene 200 ppb v/v 1,2-Dibromoethane 200 ppb v/v 1,2-Dichlorobenzene 200 ppb v/v 1,2-Dichloroethane 200 ppb v/v 1,2-Dichloropropane 200 ppb v/v 1,2-Dichlorotetrafluoroethane 200 ppb v/v 1,3,5-Trimethylbenzene 200 ppb v/v 1,3-Butadiene 200 ppb v/v 1,3-Dichlorobenzene 200 ppb v/v 1,4-Dichlorobenzene 200 ppb v/v 1,4-Dioxane 200 ppb v/v 2,2,4-Trimethylpentane 200 ppb v/v 2-Chlorotoluene 200 ppb v/v 2-Methylbutane 200 ppb v/v 3-Chloropropene 200 ppb v/v 4-Ethyltoluene 200 ppb v/v 4-Isopropyltoluene 200 ppb v/v Page 90 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Acetone 200 ppb v/v Acetonitrile 200 ppb v/v Acrolein 200 ppb v/v Acrylonitrile 200 ppb v/v Alpha Methyl Styrene 200 ppb v/v Benzene 200 ppb v/v Benzyl chloride 200 ppb v/v Bromodichloromethane 200 ppb v/v Bromoethene(Vinyl Bromide) 200 ppb v/v Bromoform 200 ppb v/v Bromomethane 200 ppb v/v Carbon disulfide 200 ppb v/v Carbon tetrachloride 200 ppb v/v Chlorobenzene 200 ppb v/v Chloroethane 200 ppb v/v Chloroform 200 ppb v/v Chloromethane 200 ppb v/v cis-1,2-Dichloroethene 200 ppb v/v cis-1,3-Dichloropropene 200 ppb v/v Cumene 200 ppb v/v Cyclohexane 200 ppb v/v Dibromochloromethane 200 ppb v/v Dibromomethane 200 ppb v/v Dichlorodifluoromethane 200 ppb v/v Dodecane 200 ppb v/v Ethyl acetate 200 ppb v/v Ethyl ether 200 ppb v/v Ethylbenzene 200 ppb v/v Freon 22 200 ppb v/v Freon TF 200 ppb v/v Hexachlorobutadiene 200 ppb v/v Isopropyl alcohol 200 ppb v/v m,p-Xylene 400 ppb v/v Methyl Butyl Ketone (2-Hexanone) 200 ppb v/v Methyl Ethyl Ketone 200 ppb v/v methyl isobutyl ketone 200 ppb v/v Methyl methacrylate 200 ppb v/v Methyl tert-butyl ether 200 ppb v/v Methylene Chloride 200 ppb v/v n-Butane 200 ppb v/v n-Butanol 200 ppb v/v n-Butylbenzene 200 ppb v/v n-Decane 200 ppb v/v n-Heptane 200 ppb v/v n-Hexane 200 ppb v/v n-Nonane 200 ppb v/v n-Octane 200 ppb v/v Page 91 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte n-Propylbenzene 200 ppb v/v Naphthalene 200 ppb v/v Pentane 200 ppb v/v Propene 200 ppb v/v sec-Butylbenzene 200 ppb v/v Styrene 200 ppb v/v tert-Butyl alcohol 200 ppb v/v tert-Butylbenzene 200 ppb v/v Tetrachloroethene 200 ppb v/v Tetrahydrofuran 200 ppb v/v Toluene 200 ppb v/v trans-1,2-Dichloroethene 200 ppb v/v trans-1,3-Dichloropropene 200 ppb v/v Trichloroethene 200 ppb v/v Trichlorofluoromethane 200 ppb v/v Undecane 200 ppb v/v Vinyl acetate 200 ppb v/v Vinyl chloride 200 ppb v/v Xylene, o-200 ppb v/v 12/19/17 (Purchased Reagent)1,1,1-Trichloroethane 1 ppm v/vSpectra Gases, Lot cc-90855..ATTO15CALs_00026 1,1,2,2-Tetrachloroethane 1 ppm v/v 1,1,2-Trichloroethane 1 ppm v/v 1,1-Dichloroethane 1 ppm v/v 1,1-Dichloroethene 1 ppm v/v 1,2,3-Trichlorobenzene 1 ppm v/v 1,2,3-Trichloropropane 1 ppm v/v 1,2,4-Trichlorobenzene 1 ppm v/v 1,2,4-Trimethylbenzene 1 ppm v/v 1,2-Dibromoethane 1 ppm v/v 1,2-Dichlorobenzene 1 ppm v/v 1,2-Dichloroethane 1 ppm v/v 1,2-Dichloropropane 1 ppm v/v 1,2-Dichlorotetrafluoroethane 1 ppm v/v 1,3,5-Trimethylbenzene 1 ppm v/v 1,3-Butadiene 1 ppm v/v 1,3-Dichlorobenzene 1 ppm v/v 1,4-Dichlorobenzene 1 ppm v/v 1,4-Dioxane 1 ppm v/v 2,2,4-Trimethylpentane 1 ppm v/v 2-Chlorotoluene 1 ppm v/v 2-Methylbutane 1 ppm v/v 3-Chloropropene 1 ppm v/v 4-Ethyltoluene 1 ppm v/v 4-Isopropyltoluene 1 ppm v/v Acetone 1 ppm v/v Acetonitrile 1 ppm v/v Acrolein 1 ppm v/v Acrylonitrile 1 ppm v/v Page 92 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Alpha Methyl Styrene 1 ppm v/v Benzene 1 ppm v/v Benzyl chloride 1 ppm v/v Bromodichloromethane 1 ppm v/v Bromoethene(Vinyl Bromide)1 ppm v/v Bromoform 1 ppm v/v Bromomethane 1 ppm v/v Carbon disulfide 1 ppm v/v Carbon tetrachloride 1 ppm v/v Chlorobenzene 1 ppm v/v Chloroethane 1 ppm v/v Chloroform 1 ppm v/v Chloromethane 1 ppm v/v cis-1,2-Dichloroethene 1 ppm v/v cis-1,3-Dichloropropene 1 ppm v/v Cumene 1 ppm v/v Cyclohexane 1 ppm v/v Dibromochloromethane 1 ppm v/v Dibromomethane 1 ppm v/v Dichlorodifluoromethane 1 ppm v/v Dodecane 1 ppm v/v Ethyl acetate 1 ppm v/v Ethyl ether 1 ppm v/v Ethylbenzene 1 ppm v/v Freon 22 1 ppm v/v Freon TF 1 ppm v/v Hexachlorobutadiene 1 ppm v/v Isopropyl alcohol 1 ppm v/v m,p-Xylene 2 ppm v/v Methyl Butyl Ketone (2-Hexanone) 1 ppm v/v Methyl Ethyl Ketone 1 ppm v/v methyl isobutyl ketone 1 ppm v/v Methyl methacrylate 1 ppm v/v Methyl tert-butyl ether 1 ppm v/v Methylene Chloride 1 ppm v/v n-Butane 1 ppm v/v n-Butanol 1 ppm v/v n-Butylbenzene 1 ppm v/v n-Decane 1 ppm v/v n-Heptane 1 ppm v/v n-Hexane 1 ppm v/v n-Nonane 1 ppm v/v n-Octane 1 ppm v/v n-Propylbenzene 1 ppm v/v Naphthalene 1 ppm v/v Pentane 1 ppm v/v Propene 1 ppm v/v Page 93 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte sec-Butylbenzene 1 ppm v/v Styrene 1 ppm v/v tert-Butyl alcohol 1 ppm v/v tert-Butylbenzene 1 ppm v/v Tetrachloroethene 1 ppm v/v Tetrahydrofuran 1 ppm v/v Toluene 1 ppm v/v trans-1,2-Dichloroethene 1 ppm v/v trans-1,3-Dichloropropene 1 ppm v/v Trichloroethene 1 ppm v/v Trichlorofluoromethane 1 ppm v/v Undecane 1 ppm v/v Vinyl acetate 1 ppm v/v Vinyl chloride 1 ppm v/v Xylene, o-1 ppm v/v 12/19/17 09/19/17 37.5 ppb ATTO15EthCALs_00010 18.75 uL Ethanol 500 ppb v/v.ATTO15EthCALw_00088 Zero Air, Lot 12 08/14/18 (Purchased Reagent)Ethanol 1 mL/mLChem Service, Lot 5301900..ATTO15EthCALs_00010 ATTO15CALSTKi_00094 1,1,1-Trichloroethane 19.9961 ppb v/v 15.463 L 1546 mL12/17/17 09/19/17ATTO15CAL6w_00144 Zero Air, Lot 1 1,1,2,2-Tetrachloroethane 19.9961 ppb v/v 1,1,2-Trichloroethane 19.9961 ppb v/v 1,1-Dichloroethane 19.9961 ppb v/v 1,1-Dichloroethene 19.9961 ppb v/v 1,2,3-Trichlorobenzene 19.9961 ppb v/v 1,2,3-Trichloropropane 19.9961 ppb v/v 1,2,4-Trichlorobenzene 19.9961 ppb v/v 1,2,4-Trimethylbenzene 19.9961 ppb v/v 1,2-Dibromoethane 19.9961 ppb v/v 1,2-Dichlorobenzene 19.9961 ppb v/v 1,2-Dichloroethane 19.9961 ppb v/v 1,2-Dichloropropane 19.9961 ppb v/v 1,2-Dichlorotetrafluoroethane 19.9961 ppb v/v 1,3,5-Trimethylbenzene 19.9961 ppb v/v 1,3-Butadiene 19.9961 ppb v/v Page 94 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 1,3-Dichlorobenzene 19.9961 ppb v/v 1,4-Dichlorobenzene 19.9961 ppb v/v 1,4-Dioxane 19.9961 ppb v/v 2,2,4-Trimethylpentane 19.9961 ppb v/v 2-Chlorotoluene 19.9961 ppb v/v 2-Methylbutane 19.9961 ppb v/v 3-Chloropropene 19.9961 ppb v/v 4-Ethyltoluene 19.9961 ppb v/v 4-Isopropyltoluene 19.9961 ppb v/v Acetone 19.9961 ppb v/v Acetonitrile 19.9961 ppb v/v Acrolein 19.9961 ppb v/v Acrylonitrile 19.9961 ppb v/v Alpha Methyl Styrene 19.9961 ppb v/v Benzene 19.9961 ppb v/v Benzyl chloride 19.9961 ppb v/v Bromodichloromethane 19.9961 ppb v/v Bromoethene(Vinyl Bromide)19.9961 ppb v/v Bromoform 19.9961 ppb v/v Bromomethane 19.9961 ppb v/v Carbon disulfide 19.9961 ppb v/v Carbon tetrachloride 19.9961 ppb v/v Chlorobenzene 19.9961 ppb v/v Chloroethane 19.9961 ppb v/v Chloroform 19.9961 ppb v/v Page 95 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Chloromethane 19.9961 ppb v/v cis-1,2-Dichloroethene 19.9961 ppb v/v cis-1,3-Dichloropropene 19.9961 ppb v/v Cumene 19.9961 ppb v/v Cyclohexane 19.9961 ppb v/v Dibromochloromethane 19.9961 ppb v/v Dibromomethane 19.9961 ppb v/v Dichlorodifluoromethane 19.9961 ppb v/v Dodecane 19.9961 ppb v/v Ethyl acetate 19.9961 ppb v/v Ethyl ether 19.9961 ppb v/v Ethylbenzene 19.9961 ppb v/v Freon 22 19.9961 ppb v/v Freon TF 19.9961 ppb v/v Hexachlorobutadiene 19.9961 ppb v/v Isopropyl alcohol 19.9961 ppb v/v m,p-Xylene 39.9922 ppb v/v Methyl Butyl Ketone (2-Hexanone) 19.9961 ppb v/v Methyl Ethyl Ketone 19.9961 ppb v/v methyl isobutyl ketone 19.9961 ppb v/v Methyl methacrylate 19.9961 ppb v/v Methyl tert-butyl ether 19.9961 ppb v/v Methylene Chloride 19.9961 ppb v/v n-Butane 19.9961 ppb v/v n-Butanol 19.9961 ppb v/v Page 96 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte n-Butylbenzene 19.9961 ppb v/v n-Decane 19.9961 ppb v/v n-Heptane 19.9961 ppb v/v n-Hexane 19.9961 ppb v/v n-Nonane 19.9961 ppb v/v n-Octane 19.9961 ppb v/v n-Propylbenzene 19.9961 ppb v/v Naphthalene 19.9961 ppb v/v Pentane 19.9961 ppb v/v Propene 19.9961 ppb v/v sec-Butylbenzene 19.9961 ppb v/v Styrene 19.9961 ppb v/v tert-Butyl alcohol 19.9961 ppb v/v tert-Butylbenzene 19.9961 ppb v/v Tetrachloroethene 19.9961 ppb v/v Tetrahydrofuran 19.9961 ppb v/v Toluene 19.9961 ppb v/v trans-1,2-Dichloroethene 19.9961 ppb v/v trans-1,3-Dichloropropene 19.9961 ppb v/v Trichloroethene 19.9961 ppb v/v Trichlorofluoromethane 19.9961 ppb v/v Undecane 19.9961 ppb v/v Vinyl acetate 19.9961 ppb v/v Vinyl chloride 19.9961 ppb v/v Xylene, o-19.9961 ppb v/v Page 97 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte ATTO15EthCALw_00088 1237 mL Ethanol 39.9987 ppb v/v ATTO15CALs_00026 1,1,1-Trichloroethane 200 ppb v/v37.5 L 7500 mL12/17/17 09/18/17.ATTO15CALSTKi_00094 Zero Air, Lot 13 1,1,2,2-Tetrachloroethane 200 ppb v/v 1,1,2-Trichloroethane 200 ppb v/v 1,1-Dichloroethane 200 ppb v/v 1,1-Dichloroethene 200 ppb v/v 1,2,3-Trichlorobenzene 200 ppb v/v 1,2,3-Trichloropropane 200 ppb v/v 1,2,4-Trichlorobenzene 200 ppb v/v 1,2,4-Trimethylbenzene 200 ppb v/v 1,2-Dibromoethane 200 ppb v/v 1,2-Dichlorobenzene 200 ppb v/v 1,2-Dichloroethane 200 ppb v/v 1,2-Dichloropropane 200 ppb v/v 1,2-Dichlorotetrafluoroethane 200 ppb v/v 1,3,5-Trimethylbenzene 200 ppb v/v 1,3-Butadiene 200 ppb v/v 1,3-Dichlorobenzene 200 ppb v/v 1,4-Dichlorobenzene 200 ppb v/v 1,4-Dioxane 200 ppb v/v 2,2,4-Trimethylpentane 200 ppb v/v 2-Chlorotoluene 200 ppb v/v 2-Methylbutane 200 ppb v/v 3-Chloropropene 200 ppb v/v 4-Ethyltoluene 200 ppb v/v 4-Isopropyltoluene 200 ppb v/v Acetone 200 ppb v/v Acetonitrile 200 ppb v/v Acrolein 200 ppb v/v Acrylonitrile 200 ppb v/v Alpha Methyl Styrene 200 ppb v/v Benzene 200 ppb v/v Benzyl chloride 200 ppb v/v Bromodichloromethane 200 ppb v/v Bromoethene(Vinyl Bromide) 200 ppb v/v Bromoform 200 ppb v/v Bromomethane 200 ppb v/v Carbon disulfide 200 ppb v/v Carbon tetrachloride 200 ppb v/v Chlorobenzene 200 ppb v/v Chloroethane 200 ppb v/v Chloroform 200 ppb v/v Chloromethane 200 ppb v/v cis-1,2-Dichloroethene 200 ppb v/v cis-1,3-Dichloropropene 200 ppb v/v Cumene 200 ppb v/v Cyclohexane 200 ppb v/v Page 98 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Dibromochloromethane 200 ppb v/v Dibromomethane 200 ppb v/v Dichlorodifluoromethane 200 ppb v/v Dodecane 200 ppb v/v Ethyl acetate 200 ppb v/v Ethyl ether 200 ppb v/v Ethylbenzene 200 ppb v/v Freon 22 200 ppb v/v Freon TF 200 ppb v/v Hexachlorobutadiene 200 ppb v/v Isopropyl alcohol 200 ppb v/v m,p-Xylene 400 ppb v/v Methyl Butyl Ketone (2-Hexanone) 200 ppb v/v Methyl Ethyl Ketone 200 ppb v/v methyl isobutyl ketone 200 ppb v/v Methyl methacrylate 200 ppb v/v Methyl tert-butyl ether 200 ppb v/v Methylene Chloride 200 ppb v/v n-Butane 200 ppb v/v n-Butanol 200 ppb v/v n-Butylbenzene 200 ppb v/v n-Decane 200 ppb v/v n-Heptane 200 ppb v/v n-Hexane 200 ppb v/v n-Nonane 200 ppb v/v n-Octane 200 ppb v/v n-Propylbenzene 200 ppb v/v Naphthalene 200 ppb v/v Pentane 200 ppb v/v Propene 200 ppb v/v sec-Butylbenzene 200 ppb v/v Styrene 200 ppb v/v tert-Butyl alcohol 200 ppb v/v tert-Butylbenzene 200 ppb v/v Tetrachloroethene 200 ppb v/v Tetrahydrofuran 200 ppb v/v Toluene 200 ppb v/v trans-1,2-Dichloroethene 200 ppb v/v trans-1,3-Dichloropropene 200 ppb v/v Trichloroethene 200 ppb v/v Trichlorofluoromethane 200 ppb v/v Undecane 200 ppb v/v Vinyl acetate 200 ppb v/v Vinyl chloride 200 ppb v/v Xylene, o-200 ppb v/v 12/19/17 (Purchased Reagent)1,1,1-Trichloroethane 1 ppm v/vSpectra Gases, Lot cc-90855..ATTO15CALs_00026 1,1,2,2-Tetrachloroethane 1 ppm v/v Page 99 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 1,1,2-Trichloroethane 1 ppm v/v 1,1-Dichloroethane 1 ppm v/v 1,1-Dichloroethene 1 ppm v/v 1,2,3-Trichlorobenzene 1 ppm v/v 1,2,3-Trichloropropane 1 ppm v/v 1,2,4-Trichlorobenzene 1 ppm v/v 1,2,4-Trimethylbenzene 1 ppm v/v 1,2-Dibromoethane 1 ppm v/v 1,2-Dichlorobenzene 1 ppm v/v 1,2-Dichloroethane 1 ppm v/v 1,2-Dichloropropane 1 ppm v/v 1,2-Dichlorotetrafluoroethane 1 ppm v/v 1,3,5-Trimethylbenzene 1 ppm v/v 1,3-Butadiene 1 ppm v/v 1,3-Dichlorobenzene 1 ppm v/v 1,4-Dichlorobenzene 1 ppm v/v 1,4-Dioxane 1 ppm v/v 2,2,4-Trimethylpentane 1 ppm v/v 2-Chlorotoluene 1 ppm v/v 2-Methylbutane 1 ppm v/v 3-Chloropropene 1 ppm v/v 4-Ethyltoluene 1 ppm v/v 4-Isopropyltoluene 1 ppm v/v Acetone 1 ppm v/v Acetonitrile 1 ppm v/v Acrolein 1 ppm v/v Acrylonitrile 1 ppm v/v Alpha Methyl Styrene 1 ppm v/v Benzene 1 ppm v/v Benzyl chloride 1 ppm v/v Bromodichloromethane 1 ppm v/v Bromoethene(Vinyl Bromide)1 ppm v/v Bromoform 1 ppm v/v Bromomethane 1 ppm v/v Carbon disulfide 1 ppm v/v Carbon tetrachloride 1 ppm v/v Chlorobenzene 1 ppm v/v Chloroethane 1 ppm v/v Chloroform 1 ppm v/v Chloromethane 1 ppm v/v cis-1,2-Dichloroethene 1 ppm v/v cis-1,3-Dichloropropene 1 ppm v/v Cumene 1 ppm v/v Cyclohexane 1 ppm v/v Dibromochloromethane 1 ppm v/v Dibromomethane 1 ppm v/v Dichlorodifluoromethane 1 ppm v/v Dodecane 1 ppm v/v Page 100 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Ethyl acetate 1 ppm v/v Ethyl ether 1 ppm v/v Ethylbenzene 1 ppm v/v Freon 22 1 ppm v/v Freon TF 1 ppm v/v Hexachlorobutadiene 1 ppm v/v Isopropyl alcohol 1 ppm v/v m,p-Xylene 2 ppm v/v Methyl Butyl Ketone (2-Hexanone) 1 ppm v/v Methyl Ethyl Ketone 1 ppm v/v methyl isobutyl ketone 1 ppm v/v Methyl methacrylate 1 ppm v/v Methyl tert-butyl ether 1 ppm v/v Methylene Chloride 1 ppm v/v n-Butane 1 ppm v/v n-Butanol 1 ppm v/v n-Butylbenzene 1 ppm v/v n-Decane 1 ppm v/v n-Heptane 1 ppm v/v n-Hexane 1 ppm v/v n-Nonane 1 ppm v/v n-Octane 1 ppm v/v n-Propylbenzene 1 ppm v/v Naphthalene 1 ppm v/v Pentane 1 ppm v/v Propene 1 ppm v/v sec-Butylbenzene 1 ppm v/v Styrene 1 ppm v/v tert-Butyl alcohol 1 ppm v/v tert-Butylbenzene 1 ppm v/v Tetrachloroethene 1 ppm v/v Tetrahydrofuran 1 ppm v/v Toluene 1 ppm v/v trans-1,2-Dichloroethene 1 ppm v/v trans-1,3-Dichloropropene 1 ppm v/v Trichloroethene 1 ppm v/v Trichlorofluoromethane 1 ppm v/v Undecane 1 ppm v/v Vinyl acetate 1 ppm v/v Vinyl chloride 1 ppm v/v Xylene, o-1 ppm v/v 12/19/17 09/19/17 37.5 ppb ATTO15EthCALs_00010 18.75 uL Ethanol 500 ppb v/v.ATTO15EthCALw_00088 Zero Air, Lot 12 08/14/18 (Purchased Reagent)Ethanol 1 mL/mLChem Service, Lot 5301900..ATTO15EthCALs_00010 ATTO15CALSTKi_00094 1,1,1-Trichloroethane 39.9922 ppb v/v 15.463 L 3092 mL12/17/17 09/19/17ATTO15CAL7w_00071 Zero Air, Lot 12 1,1,2,2-Tetrachloroethane 39.9922 ppb v/v Page 101 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 1,1,2-Trichloroethane 39.9922 ppb v/v 1,1-Dichloroethane 39.9922 ppb v/v 1,1-Dichloroethene 39.9922 ppb v/v 1,2,3-Trichlorobenzene 39.9922 ppb v/v 1,2,3-Trichloropropane 39.9922 ppb v/v 1,2,4-Trichlorobenzene 39.9922 ppb v/v 1,2,4-Trimethylbenzene 39.9922 ppb v/v 1,2-Dibromoethane 39.9922 ppb v/v 1,2-Dichlorobenzene 39.9922 ppb v/v 1,2-Dichloroethane 39.9922 ppb v/v 1,2-Dichloropropane 39.9922 ppb v/v 1,2-Dichlorotetrafluoroethane 39.9922 ppb v/v 1,3,5-Trimethylbenzene 39.9922 ppb v/v 1,3-Butadiene 39.9922 ppb v/v 1,3-Dichlorobenzene 39.9922 ppb v/v 1,4-Dichlorobenzene 39.9922 ppb v/v 1,4-Dioxane 39.9922 ppb v/v 2,2,4-Trimethylpentane 39.9922 ppb v/v 2-Chlorotoluene 39.9922 ppb v/v 2-Methylbutane 39.9922 ppb v/v 3-Chloropropene 39.9922 ppb v/v 4-Ethyltoluene 39.9922 ppb v/v 4-Isopropyltoluene 39.9922 ppb v/v Acetone 39.9922 ppb v/v Acetonitrile 39.9922 ppb v/v Page 102 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Acrolein 39.9922 ppb v/v Acrylonitrile 39.9922 ppb v/v Alpha Methyl Styrene 39.9922 ppb v/v Benzene 39.9922 ppb v/v Benzyl chloride 39.9922 ppb v/v Bromodichloromethane 39.9922 ppb v/v Bromoethene(Vinyl Bromide)39.9922 ppb v/v Bromoform 39.9922 ppb v/v Bromomethane 39.9922 ppb v/v Carbon disulfide 39.9922 ppb v/v Carbon tetrachloride 39.9922 ppb v/v Chlorobenzene 39.9922 ppb v/v Chloroethane 39.9922 ppb v/v Chloroform 39.9922 ppb v/v Chloromethane 39.9922 ppb v/v cis-1,2-Dichloroethene 39.9922 ppb v/v cis-1,3-Dichloropropene 39.9922 ppb v/v Cumene 39.9922 ppb v/v Cyclohexane 39.9922 ppb v/v Dibromochloromethane 39.9922 ppb v/v Dibromomethane 39.9922 ppb v/v Dichlorodifluoromethane 39.9922 ppb v/v Dodecane 39.9922 ppb v/v Ethyl acetate 39.9922 ppb v/v Ethyl ether 39.9922 ppb v/v Page 103 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Ethylbenzene 39.9922 ppb v/v Freon 22 39.9922 ppb v/v Freon TF 39.9922 ppb v/v Hexachlorobutadiene 39.9922 ppb v/v Isopropyl alcohol 39.9922 ppb v/v m,p-Xylene 79.9845 ppb v/v Methyl Butyl Ketone (2-Hexanone) 39.9922 ppb v/v Methyl Ethyl Ketone 39.9922 ppb v/v methyl isobutyl ketone 39.9922 ppb v/v Methyl methacrylate 39.9922 ppb v/v Methyl tert-butyl ether 39.9922 ppb v/v Methylene Chloride 39.9922 ppb v/v n-Butane 39.9922 ppb v/v n-Butanol 39.9922 ppb v/v n-Butylbenzene 39.9922 ppb v/v n-Decane 39.9922 ppb v/v n-Heptane 39.9922 ppb v/v n-Hexane 39.9922 ppb v/v n-Nonane 39.9922 ppb v/v n-Octane 39.9922 ppb v/v n-Propylbenzene 39.9922 ppb v/v Naphthalene 39.9922 ppb v/v Pentane 39.9922 ppb v/v Propene 39.9922 ppb v/v sec-Butylbenzene 39.9922 ppb v/v Page 104 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Styrene 39.9922 ppb v/v tert-Butyl alcohol 39.9922 ppb v/v tert-Butylbenzene 39.9922 ppb v/v Tetrachloroethene 39.9922 ppb v/v Tetrahydrofuran 39.9922 ppb v/v Toluene 39.9922 ppb v/v trans-1,2-Dichloroethene 39.9922 ppb v/v trans-1,3-Dichloropropene 39.9922 ppb v/v Trichloroethene 39.9922 ppb v/v Trichlorofluoromethane 39.9922 ppb v/v Undecane 39.9922 ppb v/v Vinyl acetate 39.9922 ppb v/v Vinyl chloride 39.9922 ppb v/v Xylene, o-39.9922 ppb v/v ATTO15EthCALw_00088 3092 mL Ethanol 99.9806 ppb v/v ATTO15CALs_00026 1,1,1-Trichloroethane 200 ppb v/v37.5 L 7500 mL12/17/17 09/18/17.ATTO15CALSTKi_00094 Zero Air, Lot 13 1,1,2,2-Tetrachloroethane 200 ppb v/v 1,1,2-Trichloroethane 200 ppb v/v 1,1-Dichloroethane 200 ppb v/v 1,1-Dichloroethene 200 ppb v/v 1,2,3-Trichlorobenzene 200 ppb v/v 1,2,3-Trichloropropane 200 ppb v/v 1,2,4-Trichlorobenzene 200 ppb v/v 1,2,4-Trimethylbenzene 200 ppb v/v 1,2-Dibromoethane 200 ppb v/v 1,2-Dichlorobenzene 200 ppb v/v 1,2-Dichloroethane 200 ppb v/v 1,2-Dichloropropane 200 ppb v/v 1,2-Dichlorotetrafluoroethane 200 ppb v/v 1,3,5-Trimethylbenzene 200 ppb v/v 1,3-Butadiene 200 ppb v/v 1,3-Dichlorobenzene 200 ppb v/v 1,4-Dichlorobenzene 200 ppb v/v 1,4-Dioxane 200 ppb v/v 2,2,4-Trimethylpentane 200 ppb v/v Page 105 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 2-Chlorotoluene 200 ppb v/v 2-Methylbutane 200 ppb v/v 3-Chloropropene 200 ppb v/v 4-Ethyltoluene 200 ppb v/v 4-Isopropyltoluene 200 ppb v/v Acetone 200 ppb v/v Acetonitrile 200 ppb v/v Acrolein 200 ppb v/v Acrylonitrile 200 ppb v/v Alpha Methyl Styrene 200 ppb v/v Benzene 200 ppb v/v Benzyl chloride 200 ppb v/v Bromodichloromethane 200 ppb v/v Bromoethene(Vinyl Bromide) 200 ppb v/v Bromoform 200 ppb v/v Bromomethane 200 ppb v/v Carbon disulfide 200 ppb v/v Carbon tetrachloride 200 ppb v/v Chlorobenzene 200 ppb v/v Chloroethane 200 ppb v/v Chloroform 200 ppb v/v Chloromethane 200 ppb v/v cis-1,2-Dichloroethene 200 ppb v/v cis-1,3-Dichloropropene 200 ppb v/v Cumene 200 ppb v/v Cyclohexane 200 ppb v/v Dibromochloromethane 200 ppb v/v Dibromomethane 200 ppb v/v Dichlorodifluoromethane 200 ppb v/v Dodecane 200 ppb v/v Ethyl acetate 200 ppb v/v Ethyl ether 200 ppb v/v Ethylbenzene 200 ppb v/v Freon 22 200 ppb v/v Freon TF 200 ppb v/v Hexachlorobutadiene 200 ppb v/v Isopropyl alcohol 200 ppb v/v m,p-Xylene 400 ppb v/v Methyl Butyl Ketone (2-Hexanone) 200 ppb v/v Methyl Ethyl Ketone 200 ppb v/v methyl isobutyl ketone 200 ppb v/v Methyl methacrylate 200 ppb v/v Methyl tert-butyl ether 200 ppb v/v Methylene Chloride 200 ppb v/v n-Butane 200 ppb v/v n-Butanol 200 ppb v/v n-Butylbenzene 200 ppb v/v Page 106 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte n-Decane 200 ppb v/v n-Heptane 200 ppb v/v n-Hexane 200 ppb v/v n-Nonane 200 ppb v/v n-Octane 200 ppb v/v n-Propylbenzene 200 ppb v/v Naphthalene 200 ppb v/v Pentane 200 ppb v/v Propene 200 ppb v/v sec-Butylbenzene 200 ppb v/v Styrene 200 ppb v/v tert-Butyl alcohol 200 ppb v/v tert-Butylbenzene 200 ppb v/v Tetrachloroethene 200 ppb v/v Tetrahydrofuran 200 ppb v/v Toluene 200 ppb v/v trans-1,2-Dichloroethene 200 ppb v/v trans-1,3-Dichloropropene 200 ppb v/v Trichloroethene 200 ppb v/v Trichlorofluoromethane 200 ppb v/v Undecane 200 ppb v/v Vinyl acetate 200 ppb v/v Vinyl chloride 200 ppb v/v Xylene, o-200 ppb v/v 12/19/17 (Purchased Reagent)1,1,1-Trichloroethane 1 ppm v/vSpectra Gases, Lot cc-90855..ATTO15CALs_00026 1,1,2,2-Tetrachloroethane 1 ppm v/v 1,1,2-Trichloroethane 1 ppm v/v 1,1-Dichloroethane 1 ppm v/v 1,1-Dichloroethene 1 ppm v/v 1,2,3-Trichlorobenzene 1 ppm v/v 1,2,3-Trichloropropane 1 ppm v/v 1,2,4-Trichlorobenzene 1 ppm v/v 1,2,4-Trimethylbenzene 1 ppm v/v 1,2-Dibromoethane 1 ppm v/v 1,2-Dichlorobenzene 1 ppm v/v 1,2-Dichloroethane 1 ppm v/v 1,2-Dichloropropane 1 ppm v/v 1,2-Dichlorotetrafluoroethane 1 ppm v/v 1,3,5-Trimethylbenzene 1 ppm v/v 1,3-Butadiene 1 ppm v/v 1,3-Dichlorobenzene 1 ppm v/v 1,4-Dichlorobenzene 1 ppm v/v 1,4-Dioxane 1 ppm v/v 2,2,4-Trimethylpentane 1 ppm v/v 2-Chlorotoluene 1 ppm v/v 2-Methylbutane 1 ppm v/v 3-Chloropropene 1 ppm v/v 4-Ethyltoluene 1 ppm v/v Page 107 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 4-Isopropyltoluene 1 ppm v/v Acetone 1 ppm v/v Acetonitrile 1 ppm v/v Acrolein 1 ppm v/v Acrylonitrile 1 ppm v/v Alpha Methyl Styrene 1 ppm v/v Benzene 1 ppm v/v Benzyl chloride 1 ppm v/v Bromodichloromethane 1 ppm v/v Bromoethene(Vinyl Bromide)1 ppm v/v Bromoform 1 ppm v/v Bromomethane 1 ppm v/v Carbon disulfide 1 ppm v/v Carbon tetrachloride 1 ppm v/v Chlorobenzene 1 ppm v/v Chloroethane 1 ppm v/v Chloroform 1 ppm v/v Chloromethane 1 ppm v/v cis-1,2-Dichloroethene 1 ppm v/v cis-1,3-Dichloropropene 1 ppm v/v Cumene 1 ppm v/v Cyclohexane 1 ppm v/v Dibromochloromethane 1 ppm v/v Dibromomethane 1 ppm v/v Dichlorodifluoromethane 1 ppm v/v Dodecane 1 ppm v/v Ethyl acetate 1 ppm v/v Ethyl ether 1 ppm v/v Ethylbenzene 1 ppm v/v Freon 22 1 ppm v/v Freon TF 1 ppm v/v Hexachlorobutadiene 1 ppm v/v Isopropyl alcohol 1 ppm v/v m,p-Xylene 2 ppm v/v Methyl Butyl Ketone (2-Hexanone) 1 ppm v/v Methyl Ethyl Ketone 1 ppm v/v methyl isobutyl ketone 1 ppm v/v Methyl methacrylate 1 ppm v/v Methyl tert-butyl ether 1 ppm v/v Methylene Chloride 1 ppm v/v n-Butane 1 ppm v/v n-Butanol 1 ppm v/v n-Butylbenzene 1 ppm v/v n-Decane 1 ppm v/v n-Heptane 1 ppm v/v n-Hexane 1 ppm v/v n-Nonane 1 ppm v/v Page 108 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte n-Octane 1 ppm v/v n-Propylbenzene 1 ppm v/v Naphthalene 1 ppm v/v Pentane 1 ppm v/v Propene 1 ppm v/v sec-Butylbenzene 1 ppm v/v Styrene 1 ppm v/v tert-Butyl alcohol 1 ppm v/v tert-Butylbenzene 1 ppm v/v Tetrachloroethene 1 ppm v/v Tetrahydrofuran 1 ppm v/v Toluene 1 ppm v/v trans-1,2-Dichloroethene 1 ppm v/v trans-1,3-Dichloropropene 1 ppm v/v Trichloroethene 1 ppm v/v Trichlorofluoromethane 1 ppm v/v Undecane 1 ppm v/v Vinyl acetate 1 ppm v/v Vinyl chloride 1 ppm v/v Xylene, o-1 ppm v/v 12/19/17 09/19/17 37.5 ppb ATTO15EthCALs_00010 18.75 uL Ethanol 500 ppb v/v.ATTO15EthCALw_00088 Zero Air, Lot 12 08/14/18 (Purchased Reagent)Ethanol 1 mL/mLChem Service, Lot 5301900..ATTO15EthCALs_00010 ATTO15EthCALw_00086 Ethanol 15.0036 ppb v/v 15.463 L 464 mL11/11/17 08/23/17ATTO15LCSW_00712 Zero Air, Lot 13 1,1,1-Trichloroethane 9.99806 ppb v/v ATTO15LCSSTKi_00086 773 mL 1,1,2,2-Tetrachloroethane 9.99806 ppb v/v 1,1,2-Trichloroethane 9.99806 ppb v/v 1,1-Dichloroethane 9.99806 ppb v/v 1,1-Dichloroethene 9.99806 ppb v/v 1,2,3-Trichloropropane 9.99806 ppb v/v 1,2,4-Trichlorobenzene 9.99806 ppb v/v 1,2,4-Trimethylbenzene 9.99806 ppb v/v 1,2-Dibromoethane 9.99806 ppb v/v 1,2-Dichlorobenzene 9.99806 ppb v/v 1,2-Dichloroethane 9.99806 ppb v/v 1,2-Dichloroethene, Total 19.9961 ppb v/v Page 109 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 1,2-Dichloropropane 9.99806 ppb v/v 1,2-Dichlorotetrafluoroethane 9.99806 ppb v/v 1,3,5-Trimethylbenzene 9.99806 ppb v/v 1,3-Butadiene 9.99806 ppb v/v 1,3-Dichlorobenzene 9.99806 ppb v/v 1,4-Dichlorobenzene 9.99806 ppb v/v 1,4-Dioxane 9.99806 ppb v/v 2,2,4-Trimethylpentane 9.99806 ppb v/v 2-Chlorotoluene 9.99806 ppb v/v 3-Chloropropene 9.99806 ppb v/v 4-Ethyltoluene 9.99806 ppb v/v 4-Isopropyltoluene 9.99806 ppb v/v Acetone 9.99806 ppb v/v Acrylonitrile 9.99806 ppb v/v Alpha Methyl Styrene 9.99806 ppb v/v Benzene 9.99806 ppb v/v Benzyl chloride 9.99806 ppb v/v Bromodichloromethane 9.99806 ppb v/v Bromoethene(Vinyl Bromide)9.99806 ppb v/v Bromoform 9.99806 ppb v/v Bromomethane 9.99806 ppb v/v Carbon disulfide 9.99806 ppb v/v Carbon tetrachloride 9.99806 ppb v/v Chlorobenzene 9.99806 ppb v/v Chloroethane 9.99806 ppb v/v Page 110 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Chloroform 9.99806 ppb v/v Chloromethane 9.99806 ppb v/v cis-1,2-Dichloroethene 9.99806 ppb v/v cis-1,3-Dichloropropene 9.99806 ppb v/v Cumene 9.99806 ppb v/v Cyclohexane 9.99806 ppb v/v Dibromochloromethane 9.99806 ppb v/v Dichlorodifluoromethane 9.99806 ppb v/v Dodecane 9.99806 ppb v/v Ethyl ether 9.99806 ppb v/v Ethylbenzene 9.99806 ppb v/v Freon 22 9.99806 ppb v/v Freon TF 9.99806 ppb v/v Hexachlorobutadiene 9.99806 ppb v/v Isopropyl alcohol 9.99806 ppb v/v m,p-Xylene 19.9961 ppb v/v Methyl Butyl Ketone (2-Hexanone) 9.99806 ppb v/v Methyl Ethyl Ketone 9.99806 ppb v/v methyl isobutyl ketone 9.99806 ppb v/v Methyl methacrylate 9.99806 ppb v/v Methyl tert-butyl ether 9.99806 ppb v/v Methylene Chloride 9.99806 ppb v/v n-Butane 9.99806 ppb v/v n-Butanol 9.99806 ppb v/v n-Butylbenzene 9.99806 ppb v/v Page 111 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte n-Decane 9.99806 ppb v/v n-Heptane 9.99806 ppb v/v n-Hexane 9.99806 ppb v/v n-Nonane 9.99806 ppb v/v n-Propylbenzene 9.99806 ppb v/v Naphthalene 9.99806 ppb v/v sec-Butylbenzene 9.99806 ppb v/v Styrene 9.99806 ppb v/v tert-Butyl alcohol 9.99806 ppb v/v tert-Butylbenzene 9.99806 ppb v/v Tetrachloroethene 9.99806 ppb v/v Tetrahydrofuran 9.99806 ppb v/v Toluene 9.99806 ppb v/v trans-1,2-Dichloroethene 9.99806 ppb v/v trans-1,3-Dichloropropene 9.99806 ppb v/v Trichloroethene 9.99806 ppb v/v Trichlorofluoromethane 9.99806 ppb v/v Undecane 9.99806 ppb v/v Vinyl chloride 9.99806 ppb v/v Xylene (total)29.9942 ppb v/v Xylene, o-9.99806 ppb v/v 11/14/17 08/14/17 37.5 ppb ATTO15EthCALs_00008 18.75 uL Ethanol 500 ppb v/v.ATTO15EthCALw_00086 Zero Air, Lot 12 09/05/18 (Purchased Reagent)Ethanol 1 mL/mLChem Service, Lot 5301900..ATTO15EthCALs_00008 ATTO15LCSs_00020 1,1,1-Trichloroethane 200 ppb v/v37.5 L 7500 mL11/11/17 08/11/17.ATTO15LCSSTKi_00086 Zero Air, Lot 12 1,1,2,2-Tetrachloroethane 200 ppb v/v 1,1,2-Trichloroethane 200 ppb v/v 1,1-Dichloroethane 200 ppb v/v 1,1-Dichloroethene 200 ppb v/v 1,2,3-Trichloropropane 200 ppb v/v Page 112 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 1,2,4-Trichlorobenzene 200 ppb v/v 1,2,4-Trimethylbenzene 200 ppb v/v 1,2-Dibromoethane 200 ppb v/v 1,2-Dichlorobenzene 200 ppb v/v 1,2-Dichloroethane 200 ppb v/v 1,2-Dichloroethene, Total 400 ppb v/v 1,2-Dichloropropane 200 ppb v/v 1,2-Dichlorotetrafluoroethane 200 ppb v/v 1,3,5-Trimethylbenzene 200 ppb v/v 1,3-Butadiene 200 ppb v/v 1,3-Dichlorobenzene 200 ppb v/v 1,4-Dichlorobenzene 200 ppb v/v 1,4-Dioxane 200 ppb v/v 2,2,4-Trimethylpentane 200 ppb v/v 2-Chlorotoluene 200 ppb v/v 3-Chloropropene 200 ppb v/v 4-Ethyltoluene 200 ppb v/v 4-Isopropyltoluene 200 ppb v/v Acetone 200 ppb v/v Acrylonitrile 200 ppb v/v Alpha Methyl Styrene 200 ppb v/v Benzene 200 ppb v/v Benzyl chloride 200 ppb v/v Bromodichloromethane 200 ppb v/v Bromoethene(Vinyl Bromide) 200 ppb v/v Bromoform 200 ppb v/v Bromomethane 200 ppb v/v Carbon disulfide 200 ppb v/v Carbon tetrachloride 200 ppb v/v Chlorobenzene 200 ppb v/v Chloroethane 200 ppb v/v Chloroform 200 ppb v/v Chloromethane 200 ppb v/v cis-1,2-Dichloroethene 200 ppb v/v cis-1,3-Dichloropropene 200 ppb v/v Cumene 200 ppb v/v Cyclohexane 200 ppb v/v Dibromochloromethane 200 ppb v/v Dichlorodifluoromethane 200 ppb v/v Dodecane 200 ppb v/v Ethyl ether 200 ppb v/v Ethylbenzene 200 ppb v/v Freon 22 200 ppb v/v Freon TF 200 ppb v/v Hexachlorobutadiene 200 ppb v/v Isopropyl alcohol 200 ppb v/v m,p-Xylene 400 ppb v/v Page 113 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Methyl Butyl Ketone (2-Hexanone) 200 ppb v/v Methyl Ethyl Ketone 200 ppb v/v methyl isobutyl ketone 200 ppb v/v Methyl methacrylate 200 ppb v/v Methyl tert-butyl ether 200 ppb v/v Methylene Chloride 200 ppb v/v n-Butane 200 ppb v/v n-Butanol 200 ppb v/v n-Butylbenzene 200 ppb v/v n-Decane 200 ppb v/v n-Heptane 200 ppb v/v n-Hexane 200 ppb v/v n-Nonane 200 ppb v/v n-Propylbenzene 200 ppb v/v Naphthalene 200 ppb v/v sec-Butylbenzene 200 ppb v/v Styrene 200 ppb v/v tert-Butyl alcohol 200 ppb v/v tert-Butylbenzene 200 ppb v/v Tetrachloroethene 200 ppb v/v Tetrahydrofuran 200 ppb v/v Toluene 200 ppb v/v trans-1,2-Dichloroethene 200 ppb v/v trans-1,3-Dichloropropene 200 ppb v/v Trichloroethene 200 ppb v/v Trichlorofluoromethane 200 ppb v/v Undecane 200 ppb v/v Vinyl chloride 200 ppb v/v Xylene (total)600 ppb v/v Xylene, o-200 ppb v/v 12/19/17 (Purchased Reagent)1,1,1-Trichloroethane 1 ppm v/vSpectra Gases, Lot CC-250179..ATTO15LCSs_00020 1,1,2,2-Tetrachloroethane 1 ppm v/v 1,1,2-Trichloroethane 1 ppm v/v 1,1-Dichloroethane 1 ppm v/v 1,1-Dichloroethene 1 ppm v/v 1,2,3-Trichloropropane 1 ppm v/v 1,2,4-Trichlorobenzene 1 ppm v/v 1,2,4-Trimethylbenzene 1 ppm v/v 1,2-Dibromoethane 1 ppm v/v 1,2-Dichlorobenzene 1 ppm v/v 1,2-Dichloroethane 1 ppm v/v 1,2-Dichloroethene, Total 2 ppm v/v 1,2-Dichloropropane 1 ppm v/v 1,2-Dichlorotetrafluoroethane 1 ppm v/v 1,3,5-Trimethylbenzene 1 ppm v/v 1,3-Butadiene 1 ppm v/v 1,3-Dichlorobenzene 1 ppm v/v Page 114 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 1,4-Dichlorobenzene 1 ppm v/v 1,4-Dioxane 1 ppm v/v 2,2,4-Trimethylpentane 1 ppm v/v 2-Chlorotoluene 1 ppm v/v 3-Chloropropene 1 ppm v/v 4-Ethyltoluene 1 ppm v/v 4-Isopropyltoluene 1 ppm v/v Acetone 1 ppm v/v Acrylonitrile 1 ppm v/v Alpha Methyl Styrene 1 ppm v/v Benzene 1 ppm v/v Benzyl chloride 1 ppm v/v Bromodichloromethane 1 ppm v/v Bromoethene(Vinyl Bromide)1 ppm v/v Bromoform 1 ppm v/v Bromomethane 1 ppm v/v Carbon disulfide 1 ppm v/v Carbon tetrachloride 1 ppm v/v Chlorobenzene 1 ppm v/v Chloroethane 1 ppm v/v Chloroform 1 ppm v/v Chloromethane 1 ppm v/v cis-1,2-Dichloroethene 1 ppm v/v cis-1,3-Dichloropropene 1 ppm v/v Cumene 1 ppm v/v Cyclohexane 1 ppm v/v Dibromochloromethane 1 ppm v/v Dichlorodifluoromethane 1 ppm v/v Dodecane 1 ppm v/v Ethyl ether 1 ppm v/v Ethylbenzene 1 ppm v/v Freon 22 1 ppm v/v Freon TF 1 ppm v/v Hexachlorobutadiene 1 ppm v/v Isopropyl alcohol 1 ppm v/v m,p-Xylene 2 ppm v/v Methyl Butyl Ketone (2-Hexanone) 1 ppm v/v Methyl Ethyl Ketone 1 ppm v/v methyl isobutyl ketone 1 ppm v/v Methyl methacrylate 1 ppm v/v Methyl tert-butyl ether 1 ppm v/v Methylene Chloride 1 ppm v/v n-Butane 1 ppm v/v n-Butanol 1 ppm v/v n-Butylbenzene 1 ppm v/v n-Decane 1 ppm v/v n-Heptane 1 ppm v/v Page 115 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte n-Hexane 1 ppm v/v n-Nonane 1 ppm v/v n-Propylbenzene 1 ppm v/v Naphthalene 1 ppm v/v sec-Butylbenzene 1 ppm v/v Styrene 1 ppm v/v tert-Butyl alcohol 1 ppm v/v tert-Butylbenzene 1 ppm v/v Tetrachloroethene 1 ppm v/v Tetrahydrofuran 1 ppm v/v Toluene 1 ppm v/v trans-1,2-Dichloroethene 1 ppm v/v trans-1,3-Dichloropropene 1 ppm v/v Trichloroethene 1 ppm v/v Trichlorofluoromethane 1 ppm v/v Undecane 1 ppm v/v Vinyl chloride 1 ppm v/v Xylene (total)3 ppm v/v Xylene, o-1 ppm v/v ATTO15LCSSTKi_00087 1,1,1-Trichloroethane 9.99806 ppb v/v 15.463 L 773 mL12/19/17 11/10/17ATTO15LCSW_00723 Zero Air, Lot 13 1,1,2,2-Tetrachloroethane 9.99806 ppb v/v 1,1,2-Trichloroethane 9.99806 ppb v/v 1,1-Dichloroethane 9.99806 ppb v/v 1,1-Dichloroethene 9.99806 ppb v/v 1,2,4-Trichlorobenzene 9.99806 ppb v/v 1,2,4-Trimethylbenzene 9.99806 ppb v/v 1,2-Dibromoethane 9.99806 ppb v/v 1,2-Dichlorobenzene 9.99806 ppb v/v 1,2-Dichloroethane 9.99806 ppb v/v 1,2-Dichloroethene, Total 19.9961 ppb v/v 1,2-Dichloropropane 9.99806 ppb v/v 1,2-Dichlorotetrafluoroethane 9.99806 ppb v/v 1,3,5-Trimethylbenzene 9.99806 ppb v/v 1,3-Butadiene 9.99806 ppb v/v Page 116 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 1,3-Dichlorobenzene 9.99806 ppb v/v 1,4-Dichlorobenzene 9.99806 ppb v/v 1,4-Dioxane 9.99806 ppb v/v 2,2,4-Trimethylpentane 9.99806 ppb v/v 2-Chlorotoluene 9.99806 ppb v/v 3-Chloropropene 9.99806 ppb v/v 4-Ethyltoluene 9.99806 ppb v/v 4-Isopropyltoluene 9.99806 ppb v/v Acetone 9.99806 ppb v/v Benzene 9.99806 ppb v/v Benzyl chloride 9.99806 ppb v/v Bromodichloromethane 9.99806 ppb v/v Bromoethene(Vinyl Bromide)9.99806 ppb v/v Bromoform 9.99806 ppb v/v Bromomethane 9.99806 ppb v/v Carbon disulfide 9.99806 ppb v/v Carbon tetrachloride 9.99806 ppb v/v Chlorobenzene 9.99806 ppb v/v Chloroethane 9.99806 ppb v/v Chloroform 9.99806 ppb v/v Chloromethane 9.99806 ppb v/v cis-1,2-Dichloroethene 9.99806 ppb v/v cis-1,3-Dichloropropene 9.99806 ppb v/v Cumene 9.99806 ppb v/v Cyclohexane 9.99806 ppb v/v Page 117 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Dibromochloromethane 9.99806 ppb v/v Dichlorodifluoromethane 9.99806 ppb v/v Ethylbenzene 9.99806 ppb v/v Freon 22 9.99806 ppb v/v Freon TF 9.99806 ppb v/v Hexachlorobutadiene 9.99806 ppb v/v Isopropyl alcohol 9.99806 ppb v/v m,p-Xylene 19.9961 ppb v/v Methyl Butyl Ketone (2-Hexanone) 9.99806 ppb v/v Methyl Ethyl Ketone 9.99806 ppb v/v methyl isobutyl ketone 9.99806 ppb v/v Methyl methacrylate 9.99806 ppb v/v Methyl tert-butyl ether 9.99806 ppb v/v Methylene Chloride 9.99806 ppb v/v n-Butane 9.99806 ppb v/v n-Butylbenzene 9.99806 ppb v/v n-Heptane 9.99806 ppb v/v n-Hexane 9.99806 ppb v/v n-Propylbenzene 9.99806 ppb v/v Naphthalene 9.99806 ppb v/v sec-Butylbenzene 9.99806 ppb v/v Styrene 9.99806 ppb v/v tert-Butyl alcohol 9.99806 ppb v/v tert-Butylbenzene 9.99806 ppb v/v Tetrachloroethene 9.99806 ppb v/v Page 118 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Tetrahydrofuran 9.99806 ppb v/v Toluene 9.99806 ppb v/v trans-1,2-Dichloroethene 9.99806 ppb v/v trans-1,3-Dichloropropene 9.99806 ppb v/v Trichloroethene 9.99806 ppb v/v Trichlorofluoromethane 9.99806 ppb v/v Vinyl chloride 9.99806 ppb v/v Xylene (total)29.9942 ppb v/v Xylene, o-9.99806 ppb v/v ATTO15LCSs_00020 1,1,1-Trichloroethane 200 ppb v/v37.5 L 7500 mL12/19/17 11/10/17.ATTO15LCSSTKi_00087 Zero Air, Lot 12 1,1,2,2-Tetrachloroethane 200 ppb v/v 1,1,2-Trichloroethane 200 ppb v/v 1,1-Dichloroethane 200 ppb v/v 1,1-Dichloroethene 200 ppb v/v 1,2,4-Trichlorobenzene 200 ppb v/v 1,2,4-Trimethylbenzene 200 ppb v/v 1,2-Dibromoethane 200 ppb v/v 1,2-Dichlorobenzene 200 ppb v/v 1,2-Dichloroethane 200 ppb v/v 1,2-Dichloroethene, Total 400 ppb v/v 1,2-Dichloropropane 200 ppb v/v 1,2-Dichlorotetrafluoroethane 200 ppb v/v 1,3,5-Trimethylbenzene 200 ppb v/v 1,3-Butadiene 200 ppb v/v 1,3-Dichlorobenzene 200 ppb v/v 1,4-Dichlorobenzene 200 ppb v/v 1,4-Dioxane 200 ppb v/v 2,2,4-Trimethylpentane 200 ppb v/v 2-Chlorotoluene 200 ppb v/v 3-Chloropropene 200 ppb v/v 4-Ethyltoluene 200 ppb v/v 4-Isopropyltoluene 200 ppb v/v Acetone 200 ppb v/v Benzene 200 ppb v/v Benzyl chloride 200 ppb v/v Bromodichloromethane 200 ppb v/v Bromoethene(Vinyl Bromide) 200 ppb v/v Bromoform 200 ppb v/v Bromomethane 200 ppb v/v Carbon disulfide 200 ppb v/v Page 119 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Carbon tetrachloride 200 ppb v/v Chlorobenzene 200 ppb v/v Chloroethane 200 ppb v/v Chloroform 200 ppb v/v Chloromethane 200 ppb v/v cis-1,2-Dichloroethene 200 ppb v/v cis-1,3-Dichloropropene 200 ppb v/v Cumene 200 ppb v/v Cyclohexane 200 ppb v/v Dibromochloromethane 200 ppb v/v Dichlorodifluoromethane 200 ppb v/v Ethylbenzene 200 ppb v/v Freon 22 200 ppb v/v Freon TF 200 ppb v/v Hexachlorobutadiene 200 ppb v/v Isopropyl alcohol 200 ppb v/v m,p-Xylene 400 ppb v/v Methyl Butyl Ketone (2-Hexanone) 200 ppb v/v Methyl Ethyl Ketone 200 ppb v/v methyl isobutyl ketone 200 ppb v/v Methyl methacrylate 200 ppb v/v Methyl tert-butyl ether 200 ppb v/v Methylene Chloride 200 ppb v/v n-Butane 200 ppb v/v n-Butylbenzene 200 ppb v/v n-Heptane 200 ppb v/v n-Hexane 200 ppb v/v n-Propylbenzene 200 ppb v/v Naphthalene 200 ppb v/v sec-Butylbenzene 200 ppb v/v Styrene 200 ppb v/v tert-Butyl alcohol 200 ppb v/v tert-Butylbenzene 200 ppb v/v Tetrachloroethene 200 ppb v/v Tetrahydrofuran 200 ppb v/v Toluene 200 ppb v/v trans-1,2-Dichloroethene 200 ppb v/v trans-1,3-Dichloropropene 200 ppb v/v Trichloroethene 200 ppb v/v Trichlorofluoromethane 200 ppb v/v Vinyl chloride 200 ppb v/v Xylene (total)600 ppb v/v Xylene, o-200 ppb v/v 12/19/17 (Purchased Reagent)1,1,1-Trichloroethane 1 ppm v/vSpectra Gases, Lot CC-250179..ATTO15LCSs_00020 1,1,2,2-Tetrachloroethane 1 ppm v/v 1,1,2-Trichloroethane 1 ppm v/v 1,1-Dichloroethane 1 ppm v/v Page 120 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte 1,1-Dichloroethene 1 ppm v/v 1,2,4-Trichlorobenzene 1 ppm v/v 1,2,4-Trimethylbenzene 1 ppm v/v 1,2-Dibromoethane 1 ppm v/v 1,2-Dichlorobenzene 1 ppm v/v 1,2-Dichloroethane 1 ppm v/v 1,2-Dichloroethene, Total 2 ppm v/v 1,2-Dichloropropane 1 ppm v/v 1,2-Dichlorotetrafluoroethane 1 ppm v/v 1,3,5-Trimethylbenzene 1 ppm v/v 1,3-Butadiene 1 ppm v/v 1,3-Dichlorobenzene 1 ppm v/v 1,4-Dichlorobenzene 1 ppm v/v 1,4-Dioxane 1 ppm v/v 2,2,4-Trimethylpentane 1 ppm v/v 2-Chlorotoluene 1 ppm v/v 3-Chloropropene 1 ppm v/v 4-Ethyltoluene 1 ppm v/v 4-Isopropyltoluene 1 ppm v/v Acetone 1 ppm v/v Benzene 1 ppm v/v Benzyl chloride 1 ppm v/v Bromodichloromethane 1 ppm v/v Bromoethene(Vinyl Bromide)1 ppm v/v Bromoform 1 ppm v/v Bromomethane 1 ppm v/v Carbon disulfide 1 ppm v/v Carbon tetrachloride 1 ppm v/v Chlorobenzene 1 ppm v/v Chloroethane 1 ppm v/v Chloroform 1 ppm v/v Chloromethane 1 ppm v/v cis-1,2-Dichloroethene 1 ppm v/v cis-1,3-Dichloropropene 1 ppm v/v Cumene 1 ppm v/v Cyclohexane 1 ppm v/v Dibromochloromethane 1 ppm v/v Dichlorodifluoromethane 1 ppm v/v Ethylbenzene 1 ppm v/v Freon 22 1 ppm v/v Freon TF 1 ppm v/v Hexachlorobutadiene 1 ppm v/v Isopropyl alcohol 1 ppm v/v m,p-Xylene 2 ppm v/v Methyl Butyl Ketone (2-Hexanone) 1 ppm v/v Methyl Ethyl Ketone 1 ppm v/v methyl isobutyl ketone 1 ppm v/v Page 121 of 478 REAGENT TRACEABILITY SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added ConcentrationAnalyte Methyl methacrylate 1 ppm v/v Methyl tert-butyl ether 1 ppm v/v Methylene Chloride 1 ppm v/v n-Butane 1 ppm v/v n-Butylbenzene 1 ppm v/v n-Heptane 1 ppm v/v n-Hexane 1 ppm v/v n-Propylbenzene 1 ppm v/v Naphthalene 1 ppm v/v sec-Butylbenzene 1 ppm v/v Styrene 1 ppm v/v tert-Butyl alcohol 1 ppm v/v tert-Butylbenzene 1 ppm v/v Tetrachloroethene 1 ppm v/v Tetrahydrofuran 1 ppm v/v Toluene 1 ppm v/v trans-1,2-Dichloroethene 1 ppm v/v trans-1,3-Dichloropropene 1 ppm v/v Trichloroethene 1 ppm v/v Trichlorofluoromethane 1 ppm v/v Vinyl chloride 1 ppm v/v Xylene (total)3 ppm v/v Xylene, o-1 ppm v/v Page 122 of 478 Reagent ATTO15BISs_00006 Page 123 of 478 Page 124 of 478 Reagent ATTO15CALs_00026 Page 125 of 478 Page 126 of 478 Reagent ATTO15EthCALs_00008 Page 127 of 478 Page 128 of 478 Page 129 of 478 Reagent ATTO15EthCALs_00010 Page 130 of 478 Page 131 of 478 Page 132 of 478 Reagent ATTO15LCSs_00020 Page 133 of 478 Page 134 of 478 Method TO15 Volatile Organic Compounds (GC/MS) by Method TO15 Page 135 of 478 AIR - GC/MS VOA LAB CONTROL SAMPLE RECOVERY FORM III Job No.:Lab Name: 200-41113-1SDG No.: Level:Matrix:Low 200-41113-1 Lab File ID:28034-03.DAir Lab ID:LCS 200-123710/3 Client ID: TestAmerica Burlington REC % REC QC LIMITSCONCENTRATION (ppb v/v) SPIKE ADDED (ppb v/v) # LCS LCS COMPOUND Dichlorodifluoromethane 10.0 8.04 68-12880 Freon 22 10.0 7.83 64-12878 1,2-Dichlorotetrafluoroethane 10.0 9.49 78-13895 Chloromethane 10.0 8.02 57-12680 n-Butane 10.0 7.93 56-13079 Vinyl chloride 10.0 8.80 62-12588 1,3-Butadiene 10.0 8.67 59-12587 Bromomethane 10.0 9.53 68-12895 Chloroethane 10.0 9.16 65-12592 Bromoethene(Vinyl Bromide)10.0 9.77 67-12798 Trichlorofluoromethane 10.0 8.64 67-12786 Freon TF 10.0 9.45 68-12895 1,1-Dichloroethene 10.0 9.39 67-12794 Acetone 10.0 8.71 64-13687 Isopropyl alcohol 10.0 8.35 55-12484 Carbon disulfide 10.0 10.8 81-141108 3-Chloropropene 10.0 8.26 53-13383 Methylene Chloride 10.0 8.61 62-12286 tert-Butyl alcohol 10.0 8.73 64-12487 Methyl tert-butyl ether 10.0 9.08 67-12791 trans-1,2-Dichloroethene 10.0 9.56 72-13296 n-Hexane 10.0 9.28 71-13193 1,1-Dichloroethane 10.0 8.97 66-12690 Methyl Ethyl Ketone 10.0 9.30 62-12293 cis-1,2-Dichloroethene 10.0 9.44 67-12794 Chloroform 10.0 8.93 69-12989 Tetrahydrofuran 10.0 8.89 61-13689 1,1,1-Trichloroethane 10.0 8.87 70-13089 Cyclohexane 10.0 9.76 69-12998 Carbon tetrachloride 10.0 9.50 62-14395 2,2,4-Trimethylpentane 10.0 9.17 67-12792 Benzene 10.0 9.25 67-12793 1,2-Dichloroethane 10.0 8.47 67-13285 n-Heptane 10.0 8.47 62-13085 Trichloroethene 10.0 9.67 68-12897 Methyl methacrylate 10.0 9.66 70-13097 1,2-Dichloropropane 10.0 9.16 67-12792 1,4-Dioxane 10.0 9.85 66-13299 Bromodichloromethane 10.0 8.79 69-12988 cis-1,3-Dichloropropene 10.0 9.47 70-13095 methyl isobutyl ketone 10.0 8.46 62-13085 Toluene 10.0 9.45 67-12795 FORM III TO-15 # Column to be used to flag recovery and RPD values Page 136 of 478 AIR - GC/MS VOA LAB CONTROL SAMPLE RECOVERY FORM III Job No.:Lab Name: 200-41113-1SDG No.: Level:Matrix:Low 200-41113-1 Lab File ID:28034-03.DAir Lab ID:LCS 200-123710/3 Client ID: TestAmerica Burlington REC % REC QC LIMITSCONCENTRATION (ppb v/v) SPIKE ADDED (ppb v/v) # LCS LCS COMPOUND trans-1,3-Dichloropropene 10.0 9.47 69-12995 1,1,2-Trichloroethane 10.0 9.61 69-12996 Tetrachloroethene 10.0 9.78 70-13098 Methyl Butyl Ketone (2-Hexanone) 10.0 8.87 61-12789 Dibromochloromethane 10.0 9.35 66-13093 1,2-Dibromoethane 10.0 9.67 70-13097 Chlorobenzene 10.0 9.65 68-12896 Ethylbenzene 10.0 9.31 68-12893 m,p-Xylene 20.0 19.0 68-12895 Xylene, o-10.0 9.22 67-12792 Styrene 10.0 9.70 68-12897 Bromoform 10.0 9.86 34-17099 Cumene 10.0 9.20 67-12792 1,1,2,2-Tetrachloroethane 10.0 9.53 69-12995 n-Propylbenzene 10.0 9.17 67-12792 4-Ethyltoluene 10.0 9.47 69-12995 1,3,5-Trimethylbenzene 10.0 8.93 65-12589 2-Chlorotoluene 10.0 9.04 67-12790 tert-Butylbenzene 10.0 8.68 63-12587 1,2,4-Trimethylbenzene 10.0 8.63 65-12586 sec-Butylbenzene 10.0 8.52 66-12685 4-Isopropyltoluene 10.0 8.58 67-12986 1,3-Dichlorobenzene 10.0 9.01 67-12790 1,4-Dichlorobenzene 10.0 8.95 66-12690 Benzyl chloride 10.0 9.03 54-13590 n-Butylbenzene 10.0 8.73 67-12787 1,2-Dichlorobenzene 10.0 8.65 67-12787 1,2,4-Trichlorobenzene 10.0 8.86 59-12689 Hexachlorobutadiene 10.0 8.73 62-13087 Naphthalene 10.0 8.33 50-12183 FORM III TO-15 # Column to be used to flag recovery and RPD values Page 137 of 478 FORM IV AIR - GC/MS VOA METHOD BLANK SUMMARY Lab Name: SDG No.: Job No.: 200-41113-1 200-41113-1TestAmerica Burlington Date Analyzed: GC Column:ID: Instrument ID:11/24/2017 12:18 RTX-624 NHeated Purge:(Y/N) CHB.i 28034-04.DLab File ID:Lab Sample ID:MB 200-123710/4 AirMatrix: 0.32(mm) THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES: LAB SAMPLE ID LAB FILE ID DATE ANALYZEDCLIENT SAMPLE ID 11/24/2017 11:2528034-03.DLCS 200-123710/3 11/24/2017 15:4728034-08.D200-41113-1SV-3 11/24/2017 16:4028034-09.D200-41113-2SV-2 11/24/2017 17:3228034-10.D200-41113-3SV-1 11/24/2017 18:2428034-11.D200-41113-4AA-1 FORM IV TO-15 Page 138 of 478 FORM V Lab Name: SDG No.:200-41113-1 Job No.:200-41113-1 Lab File ID: Instrument ID: 27754-01.D CHB.i 11/06/2017 15:25 BFB Injection Date: BFB Injection Time: M/E ION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE Analysis Batch No.:122990 50 8.0 - 40.0% of mass 95 16.6 75 30.0 - 66.0% of mass 95 44.8 95 Base peak, 100% relative abundance 100.0 96 5.0 - 9.0% of mass 95 6.6 173 Less than 2.0% of mass 174 0.0 (0.0) 1 174 50.0 - 120.0% of mass 95 88.8 175 4.0 - 9.0 % of mass 174 6.4 (7.2) 1 176 93.0 - 101.0% of mass 174 87.0 (98.0) 1 177 5.0 - 9.0% of mass 176 5.6 (6.4) 2 1-Value is % mass 174 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS: 2-Value is % mass 176 AIR - GC/MS VOA INSTRUMENT PERFORMANCE CHECK TestAmerica Burlington CLIENT SAMPLE ID LAB FILE IDLAB SAMPLE ID DATE ANALYZED TIME ANALYZED 27754-04.D 11/06/2017 17:59IC 200-122990/4 27754-05.D 11/06/2017 18:52IC 200-122990/5 27754-07.D 11/06/2017 20:36IC 200-122990/7 27754-09.D 11/06/2017 22:20IC 200-122990/9 27754-10.D 11/06/2017 23:12ICIS 200-122990/10 27754-11.D 11/07/2017 00:05IC 200-122990/11 27754-12.D 11/07/2017 00:57IC 200-122990/12 27754-13.D 11/07/2017 01:49IC 200-122990/13 27754-24.D 11/07/2017 12:25ICV 200-122990/24 FORM V TO-15 Page 139 of 478 FORM V Lab Name: SDG No.:200-41113-1 Job No.:200-41113-1 Lab File ID: Instrument ID: 28034-01.D CHB.i 11/24/2017 09:42 BFB Injection Date: BFB Injection Time: M/E ION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE Analysis Batch No.:123710 50 8.0 - 40.0% of mass 95 14.1 75 30.0 - 66.0% of mass 95 40.8 95 Base peak, 100% relative abundance 100.0 96 5.0 - 9.0% of mass 95 6.6 173 Less than 2.0% of mass 174 0.0 (0.0) 1 174 50.0 - 120.0% of mass 95 91.6 175 4.0 - 9.0 % of mass 174 6.7 (7.3) 1 176 93.0 - 101.0% of mass 174 89.5 (97.7) 1 177 5.0 - 9.0% of mass 176 5.8 (6.5) 2 1-Value is % mass 174 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS: 2-Value is % mass 176 AIR - GC/MS VOA INSTRUMENT PERFORMANCE CHECK TestAmerica Burlington CLIENT SAMPLE ID LAB FILE IDLAB SAMPLE ID DATE ANALYZED TIME ANALYZED 28034-02.D 11/24/2017 10:33CCVIS 200-123710/2 28034-03.D 11/24/2017 11:25LCS 200-123710/3 28034-04.D 11/24/2017 12:18MB 200-123710/4 SV-3 28034-08.D 11/24/2017 15:47200-41113-1 SV-2 28034-09.D 11/24/2017 16:40200-41113-2 SV-1 28034-10.D 11/24/2017 17:32200-41113-3 AA-1 28034-11.D 11/24/2017 18:24200-41113-4 FORM V TO-15 Page 140 of 478 AIR - GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY Lab Name:Job No.: SDG No.:200-41113-1 FORM VIII TestAmerica Burlington 200-41113-1 Sample No.:ICIS 200-122990/10 Date Analyzed:11/06/2017 23:12 Lab File ID (Standard):27754-10.D Instrument ID:CHB.i GC Column:RTX-624 ID:0.32(mm) Heated Purge: (Y/N)N Calibration ID:38392 # RT #RT ## RT ## BCM DFBZ CBNZd5 AREA AREA AREA UPPER LIMIT LOWER LIMIT 379168 162500 818023 1908719 747848 1744978 9.70 11.11 15.21INITIAL CALIBRATION MID-POINT 10.03 9.37 11.44 10.78 15.54 14.88 270834 1363371 1246413 LAB SAMPLE ID CLIENT SAMPLE ID ICV 200-122990/24 311386 1538738 1393921 9.70 11.11 15.22 BCM = Bromochloromethane DFBZ = 1,4-Difluorobenzene CBNZd5 = Chlorobenzene-d5 Area Limit = 60%-140% of internal standard area RT Limit = ± 0.33 minutes of internal standard RT # Column used to flag values outside QC limits FORM VIII TO-15 Page 141 of 478 AIR - GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY Lab Name:Job No.: SDG No.:200-41113-1 FORM VIII TestAmerica Burlington 200-41113-1 Sample No.:CCVIS 200-123710/2 Date Analyzed:11/24/2017 10:33 Lab File ID (Standard):28034-02.D Instrument ID:CHB.i GC Column:RTX-624 ID:0.32(mm) Heated Purge: (Y/N)N Calibration ID:38392 # RT #RT ## RT ## BCM DFBZ CBNZd5 AREA AREA AREA UPPER LIMIT LOWER LIMIT 584163 250355 1238295 2889355 1093635 2551815 9.70 11.10 15.2112/24 HOUR STD 10.03 9.37 11.43 10.77 15.54 14.88 417259 2063825 1822725 LAB SAMPLE ID CLIENT SAMPLE ID LCS 200-123710/3 418664 2041262 1788667 9.72 11.12 15.22 MB 200-123710/4 421652 2106008 1754551 9.69 11.10 15.21 200-41113-1 SV-3 355479 1809784 1577709 9.69 11.10 15.21 200-41113-2 SV-2 360978 1819209 1541512 9.70 11.10 15.21 200-41113-3 SV-1 378133 1889521 1601689 9.69 11.10 15.21 200-41113-4 AA-1 393822 1967074 1688199 9.69 11.10 15.21 BCM = Bromochloromethane DFBZ = 1,4-Difluorobenzene CBNZd5 = Chlorobenzene-d5 Area Limit = 60%-140% of internal standard area RT Limit = ± 0.33 minutes of internal standard RT # Column used to flag values outside QC limits FORM VIII TO-15 Page 142 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: SV-3 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-1 TestAmerica Burlington Matrix:28034-08.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 13:18 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/24/2017 15:47 ID:RTX-624 Analysis Batch No.:123710 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 120.9175-71-8 Dichlorodifluoromethane 0.50 U 0.50 86.4775-45-6 Freon 22 0.50 U 0.50 170.9276-14-2 1,2-Dichlorotetrafluoroe thane 0.20 U 0.20 50.4974-87-3 Chloromethane 0.50 U 0.50 58.12106-97-8 n-Butane 11 0.50 62.5075-01-4 Vinyl chloride 0.035 U 0.035 54.09106-99-0 1,3-Butadiene 2.1 0.20 94.9474-83-9 Bromomethane 0.20 U 0.20 64.5275-00-3 Chloroethane 0.50 U 0.50 106.96593-60-2 Bromoethene(Vinyl Bromide) 0.20 U 0.20 137.3775-69-4 Trichlorofluoromethane 0.20 U 0.20 187.3876-13-1 Freon TF 0.20 U 0.20 96.9475-35-4 1,1-Dichloroethene 0.035 U 0.035 58.0867-64-1 Acetone 12 5.0 60.1067-63-0 Isopropyl alcohol 5.0 U 5.0 76.1475-15-0 Carbon disulfide 3.6 0.50 76.53107-05-1 3-Chloropropene 0.50 U 0.50 84.9375-09-2 Methylene Chloride 0.50 U 0.50 74.1275-65-0 tert-Butyl alcohol 5.0 U 5.0 88.151634-04-4 Methyl tert-butyl ether 0.20 U 0.20 96.94156-60-5 trans-1,2-Dichloroethene 0.20 U 0.20 86.17110-54-3 n-Hexane 1.3 0.20 98.9675-34-3 1,1-Dichloroethane 0.20 U 0.20 72.1178-93-3 Methyl Ethyl Ketone 2.5 0.50 96.94156-59-2 cis-1,2-Dichloroethene 0.035 U 0.035 96.94540-59-0 1,2-Dichloroethene, Total 0.40 U 0.40 119.3867-66-3 Chloroform 5.1 0.20 72.11109-99-9 Tetrahydrofuran 5.0 U 5.0 133.4171-55-6 1,1,1-Trichloroethane 0.20 U 0.20 84.16110-82-7 Cyclohexane 0.35 0.20 153.8156-23-5 Carbon tetrachloride 0.052 0.035 114.23540-84-1 2,2,4-Trimethylpentane 0.20 U 0.20 78.1171-43-2 Benzene 1.5 0.20 98.96107-06-2 1,2-Dichloroethane 0.20 U 0.20 FORM I TO-15 Page 143 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: SV-3 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-1 TestAmerica Burlington Matrix:28034-08.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 13:18 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/24/2017 15:47 ID:RTX-624 Analysis Batch No.:123710 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 100.21142-82-5 n-Heptane 0.65 0.20 131.3979-01-6 Trichloroethene 0.035 U 0.035 100.1280-62-6 Methyl methacrylate 0.50 U 0.50 112.9978-87-5 1,2-Dichloropropane 0.20 U 0.20 88.11123-91-1 1,4-Dioxane 5.0 U 5.0 163.8375-27-4 Bromodichloromethane 0.38 0.20 110.9710061-01-5 cis-1,3-Dichloropropene 0.20 U 0.20 100.16108-10-1 methyl isobutyl ketone 0.50 U 0.50 92.14108-88-3 Toluene 6.0 0.20 110.9710061-02-6 trans-1,3-Dichloropropen e 0.20 U 0.20 133.4179-00-5 1,1,2-Trichloroethane 0.20 U 0.20 165.83127-18-4 Tetrachloroethene 0.20 U 0.20 100.20591-78-6 Methyl Butyl Ketone (2-Hexanone) 0.50 U 0.50 208.29124-48-1 Dibromochloromethane 0.20 U 0.20 187.87106-93-4 1,2-Dibromoethane 0.20 U 0.20 112.56108-90-7 Chlorobenzene 0.20 U 0.20 106.17100-41-4 Ethylbenzene 0.97 0.20 106.17179601-23-1 m,p-Xylene 2.8 0.50 106.1795-47-6 Xylene, o-0.99 0.20 106.171330-20-7 Xylene (total)3.8 0.70 104.15100-42-5 Styrene 0.20 U 0.20 252.7575-25-2 Bromoform 0.20 U 0.20 120.1998-82-8 Cumene 0.20 U 0.20 167.8579-34-5 1,1,2,2-Tetrachloroethan e 0.20 U 0.20 120.19103-65-1 n-Propylbenzene 0.26 0.20 120.20622-96-8 4-Ethyltoluene 0.36 0.20 120.20108-67-8 1,3,5-Trimethylbenzene 0.32 0.20 126.5995-49-8 2-Chlorotoluene 0.20 U 0.20 134.2298-06-6 tert-Butylbenzene 0.20 U 0.20 120.2095-63-6 1,2,4-Trimethylbenzene 1.1 0.20 134.22135-98-8 sec-Butylbenzene 0.20 U 0.20 134.2299-87-6 4-Isopropyltoluene 0.20 U 0.20 147.00541-73-1 1,3-Dichlorobenzene 0.20 U 0.20 147.00106-46-7 1,4-Dichlorobenzene 0.20 U 0.20 FORM I TO-15 Page 144 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: SV-3 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-1 TestAmerica Burlington Matrix:28034-08.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 13:18 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/24/2017 15:47 ID:RTX-624 Analysis Batch No.:123710 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 126.58100-44-7 Benzyl chloride 0.20 U 0.20 134.22104-51-8 n-Butylbenzene 0.20 U 0.20 147.0095-50-1 1,2-Dichlorobenzene 0.20 U 0.20 181.45120-82-1 1,2,4-Trichlorobenzene 0.50 U 0.50 260.7687-68-3 Hexachlorobutadiene 0.20 U 0.20 128.1791-20-3 Naphthalene 0.50 U 0.50 FORM I TO-15 Page 145 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: SV-3 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-1 TestAmerica Burlington Matrix:28034-08.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 13:18 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/24/2017 15:47 ID:RTX-624 Analysis Batch No.:123710 ug/m3Units: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 120.9175-71-8 Dichlorodifluoromethane 2.5 U 2.5 86.4775-45-6 Freon 22 1.8 U 1.8 170.9276-14-2 1,2-Dichlorotetrafluoroe thane 1.4 U 1.4 50.4974-87-3 Chloromethane 1.0 U 1.0 58.12106-97-8 n-Butane 25 1.2 62.5075-01-4 Vinyl chloride 0.089 U 0.089 54.09106-99-0 1,3-Butadiene 4.7 0.44 94.9474-83-9 Bromomethane 0.78 U 0.78 64.5275-00-3 Chloroethane 1.3 U 1.3 106.96593-60-2 Bromoethene(Vinyl Bromide) 0.87 U 0.87 137.3775-69-4 Trichlorofluoromethane 1.1 U 1.1 187.3876-13-1 Freon TF 1.5 U 1.5 96.9475-35-4 1,1-Dichloroethene 0.14 U 0.14 58.0867-64-1 Acetone 30 12 60.1067-63-0 Isopropyl alcohol 12 U 12 76.1475-15-0 Carbon disulfide 11 1.6 76.53107-05-1 3-Chloropropene 1.6 U 1.6 84.9375-09-2 Methylene Chloride 1.7 U 1.7 74.1275-65-0 tert-Butyl alcohol 15 U 15 88.151634-04-4 Methyl tert-butyl ether 0.72 U 0.72 96.94156-60-5 trans-1,2-Dichloroethene 0.79 U 0.79 86.17110-54-3 n-Hexane 4.5 0.70 98.9675-34-3 1,1-Dichloroethane 0.81 U 0.81 72.1178-93-3 Methyl Ethyl Ketone 7.5 1.5 96.94156-59-2 cis-1,2-Dichloroethene 0.14 U 0.14 96.94540-59-0 1,2-Dichloroethene, Total 1.6 U 1.6 119.3867-66-3 Chloroform 25 0.98 72.11109-99-9 Tetrahydrofuran 15 U 15 133.4171-55-6 1,1,1-Trichloroethane 1.1 U 1.1 84.16110-82-7 Cyclohexane 1.2 0.69 153.8156-23-5 Carbon tetrachloride 0.32 0.22 114.23540-84-1 2,2,4-Trimethylpentane 0.93 U 0.93 78.1171-43-2 Benzene 4.9 0.64 98.96107-06-2 1,2-Dichloroethane 0.81 U 0.81 FORM I TO-15 Page 146 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: SV-3 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-1 TestAmerica Burlington Matrix:28034-08.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 13:18 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/24/2017 15:47 ID:RTX-624 Analysis Batch No.:123710 ug/m3Units: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 100.21142-82-5 n-Heptane 2.7 0.82 131.3979-01-6 Trichloroethene 0.19 U 0.19 100.1280-62-6 Methyl methacrylate 2.0 U 2.0 112.9978-87-5 1,2-Dichloropropane 0.92 U 0.92 88.11123-91-1 1,4-Dioxane 18 U 18 163.8375-27-4 Bromodichloromethane 2.5 1.3 110.9710061-01-5 cis-1,3-Dichloropropene 0.91 U 0.91 100.16108-10-1 methyl isobutyl ketone 2.0 U 2.0 92.14108-88-3 Toluene 23 0.75 110.9710061-02-6 trans-1,3-Dichloropropen e 0.91 U 0.91 133.4179-00-5 1,1,2-Trichloroethane 1.1 U 1.1 165.83127-18-4 Tetrachloroethene 1.4 U 1.4 100.20591-78-6 Methyl Butyl Ketone (2-Hexanone) 2.0 U 2.0 208.29124-48-1 Dibromochloromethane 1.7 U 1.7 187.87106-93-4 1,2-Dibromoethane 1.5 U 1.5 112.56108-90-7 Chlorobenzene 0.92 U 0.92 106.17100-41-4 Ethylbenzene 4.2 0.87 106.17179601-23-1 m,p-Xylene 12 2.2 106.1795-47-6 Xylene, o-4.3 0.87 106.171330-20-7 Xylene (total)16 3.0 104.15100-42-5 Styrene 0.85 U 0.85 252.7575-25-2 Bromoform 2.1 U 2.1 120.1998-82-8 Cumene 0.98 U 0.98 167.8579-34-5 1,1,2,2-Tetrachloroethan e 1.4 U 1.4 120.19103-65-1 n-Propylbenzene 1.3 0.98 120.20622-96-8 4-Ethyltoluene 1.8 0.98 120.20108-67-8 1,3,5-Trimethylbenzene 1.6 0.98 126.5995-49-8 2-Chlorotoluene 1.0 U 1.0 134.2298-06-6 tert-Butylbenzene 1.1 U 1.1 120.2095-63-6 1,2,4-Trimethylbenzene 5.5 0.98 134.22135-98-8 sec-Butylbenzene 1.1 U 1.1 134.2299-87-6 4-Isopropyltoluene 1.1 U 1.1 147.00541-73-1 1,3-Dichlorobenzene 1.2 U 1.2 147.00106-46-7 1,4-Dichlorobenzene 1.2 U 1.2 FORM I TO-15 Page 147 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: SV-3 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-1 TestAmerica Burlington Matrix:28034-08.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 13:18 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/24/2017 15:47 ID:RTX-624 Analysis Batch No.:123710 ug/m3Units: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 126.58100-44-7 Benzyl chloride 1.0 U 1.0 134.22104-51-8 n-Butylbenzene 1.1 U 1.1 147.0095-50-1 1,2-Dichlorobenzene 1.2 U 1.2 181.45120-82-1 1,2,4-Trichlorobenzene 3.7 U 3.7 260.7687-68-3 Hexachlorobutadiene 2.1 U 2.1 128.1791-20-3 Naphthalene 2.6 U 2.6 FORM I TO-15 Page 148 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS Client Sample ID: Lab Name:Job No.: SV-3 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-1 TestAmerica Burlington Matrix:28034-08.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 13:18 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/24/2017 15:47 ID:RTX-624 Analysis Batch No.:123710 ppb v/vUnits: Number TICs Found:TIC Result Total:80.410 QRTCOMPOUND NAME RESULTCAS NO.MATCH QUALITY 3.14 J N115-07-1 Propene 15 86% 14.67 JUnknown6.0 14.84 J N2216-33-3 Octane, 3-methyl-4.7 91% 15.67 JUnknown3.4 15.79 J N15869-93-9 Octane, 3,5-dimethyl-5.2 87% 15.85 JUnknown4.4 16.08 JUnknown4.7 16.41 J N871-83-0 Nonane, 2-methyl-11 91% 16.54 J N5911-04-6 Nonane, 3-methyl-11 94% 16.94 J N124-18-5 Decane 15 90% FORM I-TIC TO-15 Page 149 of 478 Report Date: 28-Nov-2017 09:23:16 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Target Compound Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Lims ID: 200-41113-A-1 Client ID: SV-3 Sample Type: Client Inject. Date: 24-Nov-2017 15:47:30 ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol:200.000 mL Dil. Factor: 1.0000 Sample Info: 200-0028034-008 Misc. Info.: 41113-01 Operator ID: VTP Instrument ID: CHB.i Method:\\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\TO15_LLNJ_TO3.m Limit Group: AI_TO15_ICAL Last Update: 28-Nov-2017 09:23:14 Calib Date: 07-Nov-2017 01:49:30 Integrator: RTE ID Type: Deconvolution ID Quant Method: Internal/External Standard Quant By: Initial Calibration Last ICal File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-13.D Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host:XAWRK022 First Level Reviewer: puangmaleek Date:28-Nov-2017 09:23:14 Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response OnCol Amt ppb v/v Flags 2 Dichlorodifluoromethane 85 3.193 3.193 0.000 99 30922 0.3927 3 Chlorodifluoromethane 51 3.225 3.225 0.000 97 9246 0.2065 4 1,2-Dichloro-1,1,2,2-tetra 85 3.412 3.417 0.000 81 1124 0.0136 7M 5 Chloromethane 50 3.535 3.535 0.000 81 10997 0.3916 7 6 Butane 43 3.711 3.711 0.000 95 512500 10.6 7 Vinyl chloride 62 3.748 ND 8 Butadiene 54 3.812 3.812 0.000 96 52387 2.11 10 Bromomethane 94 4.479 ND 11 Chloroethane 64 4.709 ND 13 Vinyl bromide 106 5.120 ND 14 Trichlorofluoromethane 101 5.216 5.216 0.000 96 14482 0.1724 19 1,1,2-Trichloro-1,2,2-trif 101 6.241 6.246 -0.005 47 4658 0.0660 20 1,1-Dichloroethene 96 6.315 ND 21 Acetone 43 6.465 6.465 0.000 96 655650 12.4 22 Isopropyl alcohol 45 6.683 ND 23 Carbon disulfide 76 6.748 6.748 0.000 98 354616 3.58 24 3-Chloro-1-propene 41 7.014 ND 27 Methylene Chloride 49 7.276 7.276 0.000 50 7936 0.1874 7 28 2-Methyl-2-propanol 59 7.383 ND 29 Methyl tert-butyl ether 73 7.623 ND 30 trans-1,2-Dichloroethene 61 7.687 ND 32 Hexane 57 8.013 8.012 0.001 87 82757 1.28 33 1,1-Dichloroethane 63 8.423 ND 36 2-Butanone (MEK) 72 9.320 9.315 0.005 100 52904 2.54 37 cis-1,2-Dichloroethene 96 9.331 ND * 39 Chlorobromomethane 128 9.694 9.699 -0.005 94 355479 10.0 38 Tetrahydrofuran 42 9.710 ND 40 Chloroform 83 9.768 9.774 -0.006 95 393942 5.14 S 41 1,2-Dichloroethene, Total 61 10.000 ND 42 1,1,1-Trichloroethane 97 10.030 ND 43 Cyclohexane 84 10.041 10.046 -0.005 94 20217 0.3547 Page 150 of 478 Report Date: 28-Nov-2017 09:23:16 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response OnCol Amt ppb v/v Flags 44 Carbon tetrachloride 117 10.233 10.238 -0.005 96 3700 0.0515 45 Isooctane 57 10.521 10.521 0.000 91 18666 0.0865 46 Benzene 78 10.558 10.563 -0.005 95 205276 1.54 47 1,2-Dichloroethane 62 10.659 ND 48 n-Heptane 43 10.772 10.772 0.000 95 53501 0.6485 * 50 1,4-Difluorobenzene 114 11.103 11.102 0.001 94 1809784 10.0 53 Trichloroethene 95 11.476 ND 54 1,2-Dichloropropane 63 11.839 ND 55 Methyl methacrylate 69 11.876 ND 56 1,4-Dioxane 88 11.967 ND 58 Dichlorobromomethane 83 12.197 12.202 -0.005 97 34043 0.3805 60 cis-1,3-Dichloropropene 75 12.826 ND 61 4-Methyl-2-pentanone (MIBK 43 12.976 ND 64 Toluene 92 13.259 13.259 0.000 93 565427 6.00 66 trans-1,3-Dichloropropene 75 13.621 ND 67 1,1,2-Trichloroethane 83 13.888 ND 68 Tetrachloroethene 166 14.038 14.032 0.006 91 1898 0.0254 69 2-Hexanone 43 14.150 ND 70 Chlorodibromomethane 129 14.438 14.449 -0.011 39 2826 0.0319 71 Ethylene Dibromide 107 14.646 ND * 72 Chlorobenzene-d5 117 15.212 15.212 0.000 85 1577709 10.0 73 Chlorobenzene 112 15.249 ND 74 Ethylbenzene 91 15.319 15.319 0.000 97 199455 0.9656 76 m-Xylene & p-Xylene 106 15.463 15.468 -0.005 0 225968 2.78 78 o-Xylene 106 15.975 15.975 0.000 99 79771 0.9854 S 77 Xylenes, Total 106 0 3.76 79 Styrene 104 16.002 16.002 0.000 88 14649 0.1201 80 Bromoform 173 16.295 ND 81 Isopropylbenzene 105 16.391 ND 83 1,1,2,2-Tetrachloroethane 83 16.797 ND 84 N-Propylbenzene 91 16.866 16.866 0.000 99 73722 0.2615 87 4-Ethyltoluene 105 16.989 16.994 -0.005 96 80199 0.3575 88 2-Chlorotoluene 91 17.037 ND 89 1,3,5-Trimethylbenzene 105 17.059 17.058 0.001 92 58642 0.3162 91 tert-Butylbenzene 119 17.437 ND 92 1,2,4-Trimethylbenzene 105 17.507 17.507 0.000 98 206477 1.13 93 sec-Butylbenzene 105 17.694 ND 94 4-Isopropyltoluene 119 17.848 17.848 0.005 45 15619 0.0682 7 95 1,3-Dichlorobenzene 146 17.923 ND 96 1,4-Dichlorobenzene 146 18.035 ND 97 Benzyl chloride 91 18.185 ND 99 n-Butylbenzene 91 18.350 18.350 0.000 91 19136 0.0910 100 1,2-Dichlorobenzene 146 18.521 ND 103 1,2,4-Trichlorobenzene 180 20.880 ND 104 Hexachlorobutadiene 225 21.045 ND 105 Naphthalene 128 21.360 21.360 0.000 68 8974 0.0597 7 Page 151 of 478 Report Date: 28-Nov-2017 09:23:16 Chrom Revision: 2.2 13-Nov-2017 17:19:06 QC Flag Legend Processing Flags 7 - Failed Limit of Detection Review Flags M - Manually Integrated Reagents: ATTO15BISs_00006 Amount Added: 20.00 Units: mL Run Reagent Page 152 of 478 Report Date: 28-Nov-2017 09:23:16 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Tentatively Identified Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Lims ID: 200-41113-A-1 Client ID: SV-3 Sample Type: Client Inject. Date: 24-Nov-2017 15:47:30 ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Sample Info: 200-0028034-008 Misc. Info.: 41113-01 Operator ID: VTP Instrument ID: CHB.i Method:\\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\TO15_LLNJ_TO3.m Limit Group: AI_TO15_ICAL Last Update: 28-Nov-2017 09:23:14 Calib Date: 07-Nov-2017 01:49:30 Tic RT Window: 0.000 -0.000 Response: area Quant By: Nearest ISTD Quant LOD: 10.00000 MS Library: \\ChromNA\Burlington\Database\NIST14.L Min. Match: 1 Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host:XAWRK022 First Level Reviewer: puangmaleek Date:28-Nov-2017 09:23:14 Tentative Identified Compound Results RT Area Amount ppb v/v Quant Cpnd Qual Lib Entry Molecular Formula Mol. Weight Flags 115-07-1 Propene 3.135 3395030 15.3 39 86 57 C3H6 42 Unknown 14.673 2706411 5.96 72 0 0 0 2216-33-3 Octane, 3-methyl- 14.838 2133910 4.70 72 91 12944 C9H20 128 Unknown 15.671 1553146 3.42 72 0 0 0 15869-93-9 Octane, 3,5-dimethyl- 15.794 2338437 5.15 72 87 19687 C10H22 142 Unknown 15.847 1986337 4.38 72 0 0 0 Unknown 16.077 2142347 4.72 72 0 0 0 871-83-0 Nonane, 2-methyl- 16.413 5134482 11.3 72 91 19660 C10H22 142 5911-04-6 Nonane, 3-methyl- 16.541 4928301 10.9 72 94 19659 C10H22 142 124-18-5 Decane 16.936 7023548 15.5 72 90 19650 C10H22 142 Page 153 of 478 Report Date: 28-Nov-2017 09:23:16 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Quantitation Compounds Compound RT Area Amount ppb v/v * 39 Chlorobromomethane 9.694 2216713 10.0 * 72 Chlorobenzene-d5 15.212 4537980 10.0 QC Flag Legend Processing Flags Reagents: ATTO15BISs_00006 Amount Added: 20.00 Units: mL Run Reagent Page 154 of 478 Report Date: 28-Nov-2017 09:23:16 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Operator ID: VTP Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Worklist Smp#: 8 Client ID: SV-3 Purge Vol: 200.000 mL Dil. Factor: 1.0000 ALS Bottle#: 8 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Y Scaling: Method Defined: Scale to the Nth Largest Target: 1 2.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 18.0 20.0 22.0 24.0 Min 0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 Y ( X 10 0 0 0 0 ) 28034-08[MS SCAN Chro]:Total * C h l o r o b r o m o m e t h a n e ( 9 . 6 9 4 ) * 1 ,4- D i f lu o r o b e n z en e ( 1 1 . 1 0 3 ) * C h l o r o b e n z en e - d 5 ( 1 5 . 2 1 2 ) Page 155 of 478 Report Date: 28-Nov-2017 09:23:16 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 6 Butane, CAS: 106-97-8 30 50 70 90 110 130 150 170 190 210 m/z 0 4 8 12 16 20 24 Y ( X 10 0 0 0 ) Raw Spec:Scan 137(3.71) 43 41 58 30 50 70 90 110 130 150 170 190 210m/z 0 4 8 12 16 20 24 Y ( X 10 0 0 0 ) Enhanced Spec:Scan 137(3.71), Qvalue=95 43 41 58 30 50 70 90 110 130 150 170 190 210 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 6 Butane (DATA) 43 41 58 30 50 70 90 110 130 150 170 190 210 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 137 @ 3.711 min.(Qvalue: 95) 41 42 58 3.2 3.5 3.8 4.1 Min 0 4 8 12 16 20 24 Y ( X 10 0 0 0 ) m/z 43.0 3 . 7 1 1 3.1 3.4 3.7 4.0Min 0 5 10 15 20 25 30 35 Y ( X 10 0 0 0 ) m/z 41.0 3 . 6 7 9 3.2 3.5 3.8 4.1 Min 0 5 10 15 20 25 30 35 Y ( X 10 0 0 ) m/z 58.0 3 . 7 1 1 3.1 3.4 3.7 4.0 4.3 Min 0 6 12 18 24 30 36 Y ( X 10 0 0 0 ) m/z 43.0 m/z 41.0 m/z 58.0 Page 156 of 478 Report Date: 28-Nov-2017 09:23:16 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 8 Butadiene, CAS: 106-99-0 36 40 44 48 52 56 m/z 0 4 8 12 16 20 24 28 Y ( X 10 0 0 ) Raw Spec:Scan 156(3.81) 5439 53 50 5751 4441 4938 55 36 40 44 48 52 56m/z 0 4 8 12 16 20 24 28 Y ( X 10 0 0 ) Enhanced Spec:Scan 156(3.81), Qvalue=96 5439 53 50 5751 4441 4938 55 36 40 44 48 52 56 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 8 Butadiene (DATA) 39 54 53 50 51 4938 36 40 44 48 52 56 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 156 @ 3.812 min.(Qvalue: 96) 574441545051 3.3 3.6 3.9 4.2 Min 0 4 8 12 16 20 24 28 Y ( X 10 0 0 ) m/z 54.0 3 . 8 1 2 Page 157 of 478 Report Date: 28-Nov-2017 09:23:16 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 21 Acetone, CAS: 67-64-1 30 50 70 90 110 130 150 170 190 210 m/z 0 3 6 9 12 15 18 21 24 Y ( X 10 0 0 0 ) Raw Spec:Scan 653(6.46) 43 44 58 42 30 50 70 90 110 130 150 170 190 210m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 653(6.46), Qvalue=96 43 58 42 30 50 70 90 110 130 150 170 190 210 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 21 Acetone (NIST) 43 58 42 30 50 70 90 110 130 150 170 190 210 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 6.470 min.(Qvalue: 96) 5844 5.9 6.2 6.5 6.8 Min 0 3 6 9 12 15 18 21 24 Y ( X 10 0 0 0 ) m/z 43.0 6 . 4 6 5 5.9 6.2 6.5 6.8Min 0 11 22 33 44 55 66 77 Y ( X 10 0 0 ) m/z 58.0 6 . 4 6 0 5.9 6.2 6.5 6.8 Min 0 4 8 12 16 20 24 Y ( X 10 0 0 0 ) m/z 43.0 m/z 58.0 Page 158 of 478 Report Date: 28-Nov-2017 09:23:16 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 23 Carbon disulfide, CAS: 75-15-0 38 42 46 50 54 58 62 66 70 74 78 m/z 0 2 4 6 8 10 12 14 Y ( X 10 0 0 0 ) Raw Spec:Scan 706(6.75) 76 44 38 42 46 50 54 58 62 66 70 74 78m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 706(6.75), Qvalue=98 76 44 38 42 46 50 54 58 62 66 70 74 78 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 23 Carbon disulfide (NIST) 76 44 38 42 46 50 54 58 62 66 70 74 78 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 6.750 min.(Qvalue: 98) 78 6.2 6.5 6.8 7.1 Min 0 2 4 6 8 10 12 14 Y ( X 10 0 0 0 ) m/z 76.0 6 . 7 4 8 Page 159 of 478 Report Date: 28-Nov-2017 09:23:16 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 32 Hexane, CAS: 110-54-3 37 41 45 49 53 57 61 65 69 73 77 81 85 m/z 0 5 10 15 20 25 30 35 Y ( X 10 0 0 ) Raw Spec:Scan 943(8.01) 43 57 56 72 86 55 7144 37 41 45 49 53 57 61 65 69 73 77 81 85m/z 0 2 4 6 8 10 12 Y ( X 10 0 ) Amdis Enhanced Spec: Scan 943(8.01), Qvalue=87 43 5741 56 72 86 55 71 37 41 45 49 53 57 61 65 69 73 77 81 85 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 32 Hexane (NIST) 57 43 56 86 55 37 41 45 49 53 57 61 65 69 73 77 81 85 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 8.020 min.(Qvalue: 87) 7243 7.5 7.8 8.1 8.4 Min 0 4 8 12 16 20 24 28 Y ( X 10 0 0 ) m/z 57.0 8 . 0 1 3 7.5 7.8 8.1 8.4Min 0 7 14 21 28 35 42 49 Y ( X 10 0 ) m/z 86.0 8 . 0 1 3 7.5 7.8 8.1 8.4 Min 0 5 10 15 20 25 30 Y ( X 10 0 0 ) m/z 57.0 m/z 86.0 Page 160 of 478 Report Date: 28-Nov-2017 09:23:16 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 36 2-Butanone (MEK), CAS: 78-93-3 30 50 70 90 110 130 150 m/z 0 10 20 30 40 50 60 70 80 Y ( X 10 0 0 ) Raw Spec:Scan 1188(9.32) 43 72 57 30 50 70 90 110 130 150m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 1188(9.32), Qvalue=100 43 72 57 30 50 70 90 110 130 150 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 36 2-Butanone (MEK) (DATA) 43 72 57 30 50 70 90 110 130 150 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 9.320 min.(Qvalue:100) 7242 8.8 9.1 9.4 9.7 Min 0 3 6 9 12 15 18 21 Y ( X 10 0 0 ) m/z 72.0 9 . 3 2 0 8.8 9.1 9.4 9.7Min 0 11 22 33 44 55 66 77 Y ( X 10 0 0 ) m/z 43.0 9 . 3 1 5 8.8 9.1 9.4 9.7 Min 0 12 24 36 48 60 72 Y ( X 10 0 0 ) m/z 72.0 m/z 43.0 Page 161 of 478 Report Date: 28-Nov-2017 09:23:17 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 40 Chloroform, CAS: 67-66-3 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 103107111115119123127 m/z 0 3 6 9 12 15 Y ( X 10 0 0 0 ) Raw Spec:Scan 1272(9.77) 83 85 47 8748 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 103107111115119123127m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 1272(9.77), Qvalue=95 83 85 47 8748 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 103107111115119123127 m/z 0 13 26 39 52 65 78 91 Y ( X 10 0 ) Ref Spec: 40 Chloroform (NIST) 83 85 47 48 87 82 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 103107111115119123127 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 9.770 min.(Qvalue: 95) 9.2 9.5 9.8 10.1 Min 0 3 6 9 12 15 Y ( X 10 0 0 0 ) m/z 83.0 9 . 7 6 8 9.2 9.5 9.8 10.1Min 0 2 4 6 8 10 Y ( X 10 0 0 0 ) m/z 85.0 9 . 7 6 8 9.2 9.5 9.8 10.1 Min 0 3 6 9 12 15 Y ( X 10 0 0 0 ) m/z 83.0 m/z 85.0 Page 162 of 478 Report Date: 28-Nov-2017 09:23:17 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 43 Cyclohexane, CAS: 110-82-7 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 m/z 0 2 4 6 8 10 12 Y ( X 10 0 0 ) Raw Spec:Scan 1323(10.04) 56 41 84 55 694357 67 7154 82 85 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97m/z 0 2 4 6 8 10 12 14 Y ( X 10 0 ) Amdis Enhanced Spec: Scan 1323(10.04), Qvalue=94 56 84 41 55 6943 67 8254 85 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 43 Cyclohexane (NIST) 56 84 41 55 69 42 54 8583 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 10.050 min.(Qvalue: 94) 43 8267 9.5 9.8 10.1 10.4 Min 0 9 18 27 36 45 54 63 Y ( X 10 0 ) m/z 84.0 1 0 . 0 4 1 9.5 9.8 10.1 10.4Min 0 2 4 6 8 10 12 Y ( X 10 0 0 ) m/z 56.0 1 0 . 0 4 1 9.5 9.8 10.1 10.4 Min 0 2 4 6 8 10 12 Y ( X 10 0 0 ) m/z 84.0 m/z 56.0 Page 163 of 478 Report Date: 28-Nov-2017 09:23:17 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 44 Carbon tetrachloride, CAS: 56-23-5 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 103107111115119123 m/z 0 2 4 6 8 10 12 14 16 Y ( X 10 0 ) Raw Spec:Scan 1359(10.23) 117 40 8244 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 103107111115119123m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 1359(10.23), Qvalue=96 117 82 47 84 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 103107111115119123 m/z 0 13 26 39 52 65 78 91 Y ( X 10 0 ) Ref Spec: 44 Carbon tetrachloride (NIST) 117 8247 84 49 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 103107111115119123 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 10.230 min.(Qvalue: 96) 119 9.7 10.0 10.3 10.6 Min 0 3 6 9 12 15 18 21 Y ( X 10 0 ) m/z 117.0 1 0 . 2 3 3 9.7 10.0 10.3 10.6Min 0 3 6 9 12 15 18 21 Y ( X 10 0 ) m/z 119.0 1 0 . 2 3 3 9.7 10.0 10.3 10.6 Min 0 3 6 9 12 15 18 21 Y ( X 10 0 ) m/z 117.0 m/z 119.0 Page 164 of 478 Report Date: 28-Nov-2017 09:23:17 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 46 Benzene, CAS: 71-43-2 36 40 44 48 52 56 60 64 68 72 76 80 m/z 0 11 22 33 44 55 66 77 Y ( X 10 0 0 ) Raw Spec:Scan 1420(10.56) 78 77 52 39 79 36 40 44 48 52 56 60 64 68 72 76 80m/z 0 11 22 33 44 55 66 77 Y ( X 10 0 0 ) Enhanced Spec:Scan 1420(10.56), Qvalue=95 78 77 52 39 79 36 40 44 48 52 56 60 64 68 72 76 80 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 46 Benzene (DATA) 78 775152 39 7974 36 40 44 48 52 56 60 64 68 72 76 80 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1420 @ 10.558 min.(Qvalue: 95) 10.0 10.3 10.6 10.9 Min 0 11 22 33 44 55 66 77 Y ( X 10 0 0 ) m/z 78.0 1 0 . 5 5 8 10.0 10.3 10.6 10.9Min 0 3 6 9 12 15 18 21 Y ( X 10 0 0 ) m/z 77.0 1 0 . 5 5 8 10.0 10.3 10.6 10.9 Min 0 12 24 36 48 60 72 84 Y ( X 10 0 0 ) m/z 78.0 m/z 77.0 Page 165 of 478 Report Date: 28-Nov-2017 09:23:17 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 48 n-Heptane, CAS: 142-82-5 38 42 46 50 54 58 62 66 70 74 78 82 86 90 94 98 m/z 0 3 6 9 12 15 18 21 Y ( X 10 0 0 ) Raw Spec:Scan 1460(10.77) 43 7157 56 70 44 1005558 38 42 46 50 54 58 62 66 70 74 78 82 86 90 94 98m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 1460(10.77), Qvalue=95 43 7157 56 70 100445558 38 42 46 50 54 58 62 66 70 74 78 82 86 90 94 98 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 48 n-Heptane (NIST) 43 57 71 56 70 10055 38 42 46 50 54 58 62 66 70 74 78 82 86 90 94 98 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 10.770 min.(Qvalue: 95) 44 71 10057 10.2 10.5 10.8 11.1 Min 0 3 6 9 12 15 18 21 Y ( X 10 0 0 ) m/z 43.0 1 0 . 7 7 2 10.2 10.5 10.8 11.1Min 0 2 4 6 8 10 12 Y ( X 10 0 0 ) m/z 71.0 1 0 . 7 6 6 10.2 10.5 10.8 11.1 Min 0 3 6 9 12 15 18 21 Y ( X 10 0 0 ) m/z 43.0 m/z 71.0 Page 166 of 478 Report Date: 28-Nov-2017 09:23:17 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 58 Dichlorobromomethane, CAS: 75-27-4 30 50 70 90 110 130 150 170 m/z 0 2 4 6 8 10 12 14 Y ( X 10 0 0 ) Raw Spec:Scan 1727(12.20) 83 85 7043 8155 87 12969 30 50 70 90 110 130 150 170m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 1727(12.20), Qvalue=97 83 85 704347 71 87 12969 30 50 70 90 110 130 150 170 m/z 0 13 26 39 52 65 78 91 Y ( X 10 0 ) Ref Spec: 58 Dichlorobromomethane (NIST) 83 85 47 48 1298779 30 50 70 90 110 130 150 170 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 12.200 min.(Qvalue: 97) 7043 7155 11.6 11.9 12.2 12.5 Min 0 2 4 6 8 10 12 14 Y ( X 10 0 0 ) m/z 83.0 1 2 . 1 9 7 11.7 12.0 12.3 12.6Min 0 12 24 36 48 60 72 84 Y ( X 10 0 ) m/z 85.0 1 2 . 2 0 2 11.6 11.9 12.2 12.5 12.8 Min 0 3 6 9 12 15 Y ( X 10 0 0 ) m/z 83.0 m/z 85.0 Page 167 of 478 Report Date: 28-Nov-2017 09:23:17 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 64 Toluene, CAS: 108-88-3 36 40 44 48 52 56 60 64 68 72 76 80 84 88 92 96 100 104 108 112 116 m/z 0 6 12 18 24 30 36 42 Y ( X 10 0 0 0 ) Raw Spec:Scan 1926(13.26) 91 92 43 65 8551 36 40 44 48 52 56 60 64 68 72 76 80 84 88 92 96 100 104 108 112 116m/z 0 5 10 15 20 25 30 35 Y ( X 10 0 ) Amdis Enhanced Spec: Scan 1926(13.26), Qvalue=93 91 92 43 856557417151 36 40 44 48 52 56 60 64 68 72 76 80 84 88 92 96 100 104 108 112 116 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 64 Toluene (NIST) 91 92 6551 93 36 40 44 48 52 56 60 64 68 72 76 80 84 88 92 96 100 104 108 112 116 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 13.250 min.(Qvalue: 93) 43 8557 12.7 13.0 13.3 13.6 Min 0 4 8 12 16 20 24 Y ( X 10 0 0 0 ) m/z 92.0 1 3 . 2 5 9 12.7 13.0 13.3 13.6Min 0 6 12 18 24 30 36 42 Y ( X 10 0 0 0 ) m/z 91.0 1 3 . 2 5 9 12.7 13.0 13.3 13.6 Min 0 6 12 18 24 30 36 42 Y ( X 10 0 0 0 ) m/z 92.0 m/z 91.0 Page 168 of 478 Report Date: 28-Nov-2017 09:23:17 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 74 Ethylbenzene, CAS: 100-41-4 30 50 70 90 110 130 150 170 190 210 m/z 0 3 6 9 12 15 18 Y ( X 10 0 0 0 ) Raw Spec:Scan 2312(15.32) 43 57 91 41 857156 1068469 30 50 70 90 110 130 150 170 190 210m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 2312(15.32), Qvalue=97 91 106 51 7765 78 105 30 50 70 90 110 130 150 170 190 210 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 74 Ethylbenzene (NIST) 91 106 51 65 77 78 105 30 50 70 90 110 130 150 170 190 210 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 15.320 min.(Qvalue: 97) 106 14.8 15.1 15.4 15.7 Min 0 3 6 9 12 15 18 21 Y ( X 10 0 0 0 ) m/z 91.0 1 5 . 3 1 9 14.8 15.1 15.4 15.7Min 0 2 4 6 8 10 12 Y ( X 10 0 0 0 ) m/z 106.0 1 5 . 3 1 3 14.8 15.1 15.4 15.7 Min 0 3 6 9 12 15 18 21 Y ( X 10 0 0 0 ) m/z 91.0 m/z 106.0 Page 169 of 478 Report Date: 28-Nov-2017 09:23:17 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 76 m-Xylene & p-Xylene, CAS: 179601-23-1 30 50 70 90 110 130 150 170 190 210 230 250 m/z 0 3 6 9 12 15 18 21 Y ( X 10 0 0 0 ) Raw Spec:Scan 2339(15.46) 91 106 55 77 30 50 70 90 110 130 150 170 190 210 230 250m/z 0 3 6 9 12 15 18 21 Y ( X 10 0 0 0 ) Enhanced Spec:Scan 2339(15.46), Qvalue=0 91 106 55 77 14.9 15.2 15.5 15.8 Min 0 2 4 6 8 10 12 Y ( X 10 0 0 0 ) m/z 106.0 1 5 . 4 6 3 14.9 15.2 15.5 15.8Min 0 3 6 9 12 15 18 21 Y ( X 10 0 0 0 ) m/z 91.0 1 5 . 4 6 3 14.9 15.2 15.5 15.8 Min 0 3 6 9 12 15 18 21 Y ( X 10 0 0 0 ) m/z 106.0 m/z 91.0 Page 170 of 478 Report Date: 28-Nov-2017 09:23:17 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 78 o-Xylene, CAS: 95-47-6 30 50 70 90 110 130 150 170 190 210 230 250 m/z 0 2 4 6 8 10 12 14 16 Y ( X 10 0 0 0 ) Raw Spec:Scan 2435(15.98) 57 71 91 43 106 113 30 50 70 90 110 130 150 170 190 210 230 250m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 2435(15.98), Qvalue=99 91 106 7751 30 50 70 90 110 130 150 170 190 210 230 250 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 78 o-Xylene (NIST) 91 106 7751 30 50 70 90 110 130 150 170 190 210 230 250 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 15.980 min.(Qvalue: 99) 97 15.4 15.7 16.0 16.3 Min 0 10 20 30 40 50 60 70 Y ( X 10 0 0 ) m/z 106.0 1 5 . 9 7 5 15.4 15.7 16.0 16.3Min 0 2 4 6 8 10 12 14 Y ( X 10 0 0 0 ) m/z 91.0 1 5 . 9 7 5 15.4 15.7 16.0 16.3 Min 0 3 6 9 12 15 Y ( X 10 0 0 0 ) m/z 106.0 m/z 91.0 Page 171 of 478 Report Date: 28-Nov-2017 09:23:17 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 84 N-Propylbenzene, CAS: 103-65-1 30 50 70 90 110 130 150 170 190 210 230 250 270 m/z 0 8 16 24 32 40 48 56 Y ( X 10 0 0 ) Raw Spec:Scan 2602(16.87) 55 91 97 69 120 140 30 50 70 90 110 130 150 170 190 210 230 250 270m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 2602(16.87), Qvalue=99 91 57 1207143 30 50 70 90 110 130 150 170 190 210 230 250 270 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 84 N-Propylbenzene (NIST) 91 120 9265 30 50 70 90 110 130 150 170 190 210 230 250 270 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 16.870 min.(Qvalue: 99) 57 71 111 16.3 16.6 16.9 17.2 Min 0 6 12 18 24 30 36 42 Y ( X 10 0 0 ) m/z 91.0 1 6 . 8 6 6 16.3 16.6 16.9 17.2Min 0 4 8 12 16 20 24 28 Y ( X 10 0 0 ) m/z 120.0 1 6 . 8 6 6 16.3 16.6 16.9 17.2 Min 0 2 4 6 8 10 12 14 Y ( X 10 0 0 ) m/z 92.0 1 6 . 8 7 2 16.3 16.6 16.9 17.2 Min 0 7 14 21 28 35 42 Y ( X 10 0 0 ) m/z 91.0 m/z 120.0 m/z 92.0 Page 172 of 478 Report Date: 28-Nov-2017 09:23:17 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 87 4-Ethyltoluene, CAS: 622-96-8 30 50 70 90 110 130 150 170 190 210 230 250 270 m/z 0 3 6 9 12 15 18 21 Y ( X 10 0 0 0 ) Raw Spec:Scan 2625(16.99) 9755 69 105 140 120 30 50 70 90 110 130 150 170 190 210 230 250 270m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 2625(16.99), Qvalue=96 10557 43 71 120 83 30 50 70 90 110 130 150 170 190 210 230 250 270 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 87 4-Ethyltoluene (NIST) 105 120 91 30 50 70 90 110 130 150 170 190 210 230 250 270 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 16.990 min.(Qvalue: 96) 57 43 71 98 16.4 16.7 17.0 17.3 Min 0 11 22 33 44 55 66 77 Y ( X 10 0 0 ) m/z 105.0 1 6 . 9 8 9 16.4 16.7 17.0 17.3Min 0 6 12 18 24 30 36 42 Y ( X 10 0 0 ) m/z 120.0 16.4 16.7 17.0 17.3 Min 0 12 24 36 48 60 72 84 Y ( X 10 0 0 ) m/z 105.0 m/z 120.0 Page 173 of 478 Report Date: 28-Nov-2017 09:23:17 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 89 1,3,5-Trimethylbenzene, CAS: 108-67-8 30 50 70 90 110 130 150 170 190 210 230 250 m/z 0 12 24 36 48 60 72 84 Y ( X 10 0 0 ) Raw Spec:Scan 2638(17.06) 55 97 105 120 140 30 50 70 90 110 130 150 170 190 210 230 250m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 2638(17.06), Qvalue=92 105 120 964377 121 30 50 70 90 110 130 150 170 190 210 230 250 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 89 1,3,5-Trimethylbenzene (NIST) 105 120 77 121 30 50 70 90 110 130 150 170 190 210 230 250 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 17.060 min.(Qvalue: 92) 1114391 16.5 16.8 17.1 17.4 Min 0 2 4 6 8 10 12 Y ( X 10 0 0 0 ) m/z 105.0 1 7 . 0 5 9 16.5 16.8 17.1 17.4Min 0 7 14 21 28 35 42 49 Y ( X 10 0 0 ) m/z 120.0 1 7 . 0 5 9 16.5 16.8 17.1 17.4 Min 0 2 4 6 8 10 12 Y ( X 10 0 0 0 ) m/z 105.0 m/z 120.0 Page 174 of 478 Report Date: 28-Nov-2017 09:23:17 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 92 1,2,4-Trimethylbenzene, CAS: 95-63-6 30 50 70 90 110 130 150 170 190 210 230 250 270 m/z 0 2 4 6 8 10 12 Y ( X 10 0 0 0 ) Raw Spec:Scan 2722(17.51) 105 120 57 71 121 30 50 70 90 110 130 150 170 190 210 230 250 270m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 2722(17.51), Qvalue=98 105 120 77 121 30 50 70 90 110 130 150 170 190 210 230 250 270 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 92 1,2,4-Trimethylbenzene (NIST) 105 120 77 30 50 70 90 110 130 150 170 190 210 230 250 270 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 17.510 min.(Qvalue: 98) 12091 17.0 17.3 17.6 17.9 Min 0 2 4 6 8 10 12 Y ( X 10 0 0 0 ) m/z 105.0 1 7 . 5 0 7 17.0 17.3 17.6 17.9Min 0 7 14 21 28 35 42 49 Y ( X 10 0 0 ) m/z 120.0 1 7 . 5 0 7 17.0 17.3 17.6 17.9 Min 0 2 4 6 8 10 12 Y ( X 10 0 0 0 ) m/z 105.0 m/z 120.0 Page 175 of 478 Report Date: 28-Nov-2017 09:23:16 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 4 1,2-Dichloro-1,1,2,2-tetrafluoroethane, CAS: 76-14-2 Signal: 1 Processing Integration Results RT: 3.19 Area: 30922 Amount: 0.373979 Amount Units: ppb v/v 2.9 3.1 3.3 3.5 3.7 Min 0 2 4 6 8 10 12 14 16 18 20 Y ( X 10 0 0 ) m/z 85.0 3 . 1 9 3 Manual Integration Results RT: 3.41 Area: 1124 Amount: 0.013594 Amount Units: ppb v/v 2.9 3.1 3.3 3.5 3.7 Min 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Y ( X 10 0 ) m/z 85.0 3 . 4 1 2 Reviewer: puangmaleek, 28-Nov-2017 09:18:37 Audit Action: Marked Compound Undetected Audit Reason: Invalid Compound ID Page 176 of 478 Report Date: 28-Nov-2017 09:23:16 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 4 1,2-Dichloro-1,1,2,2-tetrafluoroethane, CAS: 76-14-2 Signal: 1 Processing Integration Results RT: 3.19 Area: 30922 Amount: 0.373979 Amount Units: ppb v/v 2.9 3.1 3.3 3.5 3.7Min 0 2 4 6 8 10 12 14 16 18 20 Y ( X 10 0 0 ) m/z 85.0 3 . 1 9 3 Manual Integration Results RT: 3.41 Area: 1124 Amount: 0.013594 Amount Units: ppb v/v 2.9 3.1 3.3 3.5 3.7 Min 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 Y ( X 10 0 ) m/z 85.0 3 . 4 1 2 Reviewer: puangmaleek, 28-Nov-2017 09:18:47 Audit Action: Manually Integrated Audit Reason: Assign Peak Page 177 of 478 Report Date: 28-Nov-2017 09:23:16 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 4 1,2-Dichloro-1,1,2,2-tetrafluoroethane, CAS: 76-14-2 Signal: 2 Processing Integration Results RT: 3.41 Area: 0 Amount: 0.373979 Amount Units: ppb v/v 2.9 3.1 3.3 3.5 3.7Min 0 3 6 9 12 15 18 21 24 27 30 33 36 39 42 Y ( X 10 ) m/z 135.0 Manual Integration Results RT: 3.42 Area: 638 Amount: 0.013594 Amount Units: ppb v/v 2.9 3.1 3.3 3.5 3.7 Min 0 3 6 9 12 15 18 21 24 27 30 33 36 39 42 Y ( X 10 ) m/z 135.0 3 . 4 2 3 Reviewer: puangmaleek, 28-Nov-2017 09:18:57 Audit Action: Manually Integrated Audit Reason: Assign Peak Page 178 of 478 Report Date: 28-Nov-2017 09:23:16 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 4 1,2-Dichloro-1,1,2,2-tetrafluoroethane, CAS: 76-14-2 Signal: 3 Processing Integration Results RT: 3.19 Area: 9942 Amount: 0.373979 Amount Units: ppb v/v 2.9 3.1 3.3 3.5 3.7Min 0 5 10 15 20 25 30 35 40 45 50 55 60 Y ( X 10 0 ) m/z 87.0 3 . 1 9 3 Manual Integration Results RT: 3.42 Area: 167 Amount: 0.013594 Amount Units: ppb v/v 2.9 3.1 3.3 3.5 3.7 Min -1 3 7 11 15 19 23 27 31 35 39 43 47 51 55 59 Y ( X 10 ) m/z 87.0 3 . 4 1 7 Reviewer: puangmaleek, 28-Nov-2017 09:19:06 Audit Action: Manually Integrated Audit Reason: Assign Peak Page 179 of 478 Report Date: 28-Nov-2017 09:23:18 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Propene 115-07-1 NIST14.L 57 C3H6 42 86 Cyclopropane 75-19-4 NIST14.L 60 C3H6 42 10 Cyclopropene 2781-85-3 NIST14.L 50 C3H4 40 9 36 40 44 48 52 56 60 64 68 72 76 m/z 0 12 24 36 48 60 Y ( X 10 0 0 0 )Raw Spec: Scan 29(3.13) 4139 42 43 38 36 40 44 48 52 56 60 64 68 72 76m/z 0 12 24 36 48 60 Y ( X 10 0 0 0 )28034-08[MS SCAN Spec]:Scan 29(3.13) 4139 42 43 38 36 40 44 48 52 56 60 64 68 72 76 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #57, Propene (from NIST14.L) 41 39 42 38 36 40 44 48 52 56 60 64 68 72 76 m/z 2 20 38 56 74 92 Y ( X 10 0 ) Entry #60, Cyclopropane (from NIST14.L) 42 39 38 36 40 44 48 52 56 60 64 68 72 76 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #50, Cyclopropene (from NIST14.L) 39 40 38 41 Page 180 of 478 Report Date: 28-Nov-2017 09:23:18 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Unknown Octane,4-methyl-2216-34-4 NIST14.L 12942 C9H20 128 80 Octane,2-methyl-3221-61-2 NIST14.L 12947 C9H20 128 72 Heptane,2,4-dimethyl-2213-23-2 NIST14.L 12973 C9H20 128 64 36 40 44 48 52 56 60 64 68 72 76 80 84 88 92 96 100 104 108 112 116 120 124 128 m/z 0 6 12 18 24 30 Y ( X 10 0 0 0 )Raw Spec: Scan 2191(14.67) 43 57 71 8541 56 70 36 40 44 48 52 56 60 64 68 72 76 80 84 88 92 96 100 104 108 112 116 120 124 128 m/z 0 6 12 18 24 30 Y ( X 10 0 0 0 )28034-08[MS SCAN Spec]:Scan 2191(14.67) 43 57 71 8541 56 70 36 40 44 48 52 56 60 64 68 72 76 80 84 88 92 96 100 104 108 112 116 120 124 128 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #12942, Octane, 4-methyl- (from NIST14.L) 43 85714157 36 40 44 48 52 56 60 64 68 72 76 80 84 88 92 96 100 104 108 112 116 120 124 128m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #12947, Octane, 2-methyl- (from NIST14.L) 43 57 41 71 56 85 36 40 44 48 52 56 60 64 68 72 76 80 84 88 92 96 100 104 108 112 116 120 124 128 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #12973, Heptane, 2,4-dimethyl- (from NIST14.L) 43 85 57 7141 84 Page 181 of 478 Report Date: 28-Nov-2017 09:23:18 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Octane,3-methyl-2216-33-3 NIST14.L 12944 C9H20 128 91 Heptane,2,5-dimethyl-2216-30-0 NIST14.L 12977 C9H20 128 72 Undecane,6-methyl-17302-33-9 NIST14.L 39991 C12H26 170 53 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 m/z 0 7 14 21 28 35 Y ( X 10 0 0 0 )Raw Spec: Scan 2222(14.84) 57 43 56 98 997139 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170m/z 0 7 14 21 28 35 Y ( X 10 0 0 0 )28034-08[MS SCAN Spec]:Scan 2222(14.84) 57 43 56 98 997139 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #12944, Octane, 3-methyl- (from NIST14.L) 57 43 56 98 9971 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #12977, Heptane, 2,5-dimethyl- (from NIST14.L) 57 43 56 71 99 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #39991, Undecane, 6-methyl- (from NIST14.L) 57 43 985671 Page 182 of 478 Report Date: 28-Nov-2017 09:23:18 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Unknown Pentane,2,2-dimethyl-590-35-2 NIST14.L 4049 C7H16 100 59 Butane,2,2,3-trimethyl-464-06-2 NIST14.L 4061 C7H16 100 53 Heptane,4-ethyl-2216-32-2 NIST14.L 12941 C9H20 128 47 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 4 8 12 16 Y ( X 10 0 0 0 )Raw Spec: Scan 2378(15.67) 57 43 8556 41 84715539 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 4 8 12 16 Y ( X 10 0 0 0 )28034-08[MS SCAN Spec]:Scan 2378(15.67) 57 43 8556 41 84715539 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #4049, Pentane, 2,2-dimethyl- (from NIST14.L) 57 43 41 56 85 39 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #4061, Butane, 2,2,3-trimethyl- (from NIST14.L) 57 43 56 85 39 55 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #12941, Heptane, 4-ethyl- (from NIST14.L) 43 57 85 41 9855 9969 Page 183 of 478 Report Date: 28-Nov-2017 09:23:18 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Octane,3,5-dimethyl-15869-93-9 NIST14.L 19687 C10H22 142 87 Octane,2,5-dimethyl-15869-89-3 NIST14.L 19672 C10H22 142 64 Undecane,5,5-dimethyl-17312-73-1 NIST14.L 51431 C13H28 184 64 30 50 70 90 110 130 150 170 190 210 230 250 m/z 0 5 10 15 20 25 Y ( X 10 0 0 0 )Raw Spec: Scan 2401(15.79) 57 43 71 41 55 85 996939 30 50 70 90 110 130 150 170 190 210 230 250m/z 0 5 10 15 20 25 Y ( X 10 0 0 0 )28034-08[MS SCAN Spec]:Scan 2401(15.79) 57 43 71 41 55 85 996939 30 50 70 90 110 130 150 170 190 210 230 250 m/z 1 19 37 55 73 91 Y ( X 10 0 ) Entry #19687, Octane, 3,5-dimethyl- (from NIST14.L) 57 43 71 7055 39 8569 99 11353 30 50 70 90 110 130 150 170 190 210 230 250 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #19672, Octane, 2,5-dimethyl- (from NIST14.L) 57 43 71 41 995585 30 50 70 90 110 130 150 170 190 210 230 250 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #51431, Undecane, 5,5-dimethyl- (from NIST14.L) 57 43 71 41 998556 12770 Page 184 of 478 Report Date: 28-Nov-2017 09:23:18 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Unknown Decane 124-18-5 NIST14.L 19648 C10H22 142 58 Octane,2,7-dimethyl-1072-16-8 NIST14.L 19680 C10H22 142 50 Hexane,2,5-dimethyl-592-13-2 NIST14.L 7788 C8H18 114 38 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 4 8 12 16 Y ( X 10 0 0 0 )Raw Spec: Scan 2411(15.85) 5743 55 974171 99 8539 12696 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 4 8 12 16 Y ( X 10 0 0 0 )28034-08[MS SCAN Spec]:Scan 2411(15.85) 5743 55 974171 99 8539 12696 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #19648, Decane (from NIST14.L) 57 43 71 85567039 99 14253 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #19680, Octane, 2,7-dimethyl- (from NIST14.L) 43 57 41 71 99563985 69 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 2 20 38 56 74 92 Y ( X 10 0 ) Entry #7788, Hexane, 2,5-dimethyl- (from NIST14.L) 5743 39 997155 112 114 Page 185 of 478 Report Date: 28-Nov-2017 09:23:18 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Unknown Nonane,3-methyl-5911-04-6 NIST14.L 19662 C10H22 142 76 Octane,3,6-dimethyl-15869-94-0 NIST14.L 19677 C10H22 142 64 Hexadecane,2,6,10,14-tetramethyl-638-36-8 NIST14.L 142261 C20H42 282 53 30 50 70 90 110 130 150 170 190 210 230 250 270 290 m/z 0 3 6 9 12 Y ( X 10 0 0 0 )Raw Spec: Scan 2454(16.08) 57 71 43 55 83 113703985 30 50 70 90 110 130 150 170 190 210 230 250 270 290 m/z 0 3 6 9 12 Y ( X 10 0 0 0 )28034-08[MS SCAN Spec]:Scan 2454(16.08) 57 71 43 55 83 113703985 30 50 70 90 110 130 150 170 190 210 230 250 270 290 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #19662, Nonane, 3-methyl- (from NIST14.L) 57 43 71 41 56 39 11370 30 50 70 90 110 130 150 170 190 210 230 250 270 290m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #19677, Octane, 3,6-dimethyl- (from NIST14.L) 57 7143 41 56 11339 30 50 70 90 110 130 150 170 190 210 230 250 270 290 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #142261, Hexadecane, 2,6,10,14-tetramethyl- (from NIST14.L) 57 71 43 854155 1137099 127 Page 186 of 478 Report Date: 28-Nov-2017 09:23:19 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Nonane,2-methyl-871-83-0 NIST14.L 19660 C10H22 142 91 Tetradecane 629-59-4 NIST14.L 63624 C14H30 198 72 Silane,trichlorooctadecyl-112-04-9 NIST14.L 230698 C18H37Cl3Si 386 72 30 50 70 90 110 130 150 170 190 210 230 250 270 290 310 330 350 370 390 m/z 0 12 24 36 48 60 Y ( X 10 0 0 0 )Raw Spec: Scan 2517(16.41) 57 71 85 30 50 70 90 110 130 150 170 190 210 230 250 270 290 310 330 350 370 390m/z 0 12 24 36 48 60 Y ( X 10 0 0 0 )28034-08[MS SCAN Spec]:Scan 2517(16.41) 57 71 85 30 50 70 90 110 130 150 170 190 210 230 250 270 290 310 330 350 370 390 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #19660, Nonane, 2-methyl- (from NIST14.L) 43 57 71 98 30 50 70 90 110 130 150 170 190 210 230 250 270 290 310 330 350 370 390 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #63624, Tetradecane (from NIST14.L) 57 43 71 85 99 30 50 70 90 110 130 150 170 190 210 230 250 270 290 310 330 350 370 390 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #230698, Silane, trichlorooctadecyl- (from NIST14.L) 57 71 85 99 135 Page 187 of 478 Report Date: 28-Nov-2017 09:23:19 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Nonane,3-methyl-5911-04-6 NIST14.L 19659 C10H22 142 94 Octane,3,6-dimethyl-15869-94-0 NIST14.L 19677 C10H22 142 90 Octane,2,6-dimethyl-2051-30-1 NIST14.L 19673 C10H22 142 78 30 50 70 90 110 130 150 170 190 210 230 250 270 m/z 0 12 24 36 48 60 Y ( X 10 0 0 0 )Raw Spec: Scan 2541(16.54) 57 71 43 56 11255 113703985 30 50 70 90 110 130 150 170 190 210 230 250 270m/z 0 12 24 36 48 60 Y ( X 10 0 0 0 )28034-08[MS SCAN Spec]:Scan 2541(16.54) 57 71 43 56 11255 113703985 30 50 70 90 110 130 150 170 190 210 230 250 270 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #19659, Nonane, 3-methyl- (from NIST14.L) 57 7143 5641 112 11355398570 30 50 70 90 110 130 150 170 190 210 230 250 270 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #19677, Octane, 3,6-dimethyl- (from NIST14.L) 57 7143 41 56 11339 30 50 70 90 110 130 150 170 190 210 230 250 270 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #19673, Octane, 2,6-dimethyl- (from NIST14.L) 57 43 71 5641 113558539 Page 188 of 478 Report Date: 28-Nov-2017 09:23:19 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-08.D Injection Date: 24-Nov-2017 15:47:30 Instrument ID: CHB.i Lims ID: 200-41113-A-1 Lab Sample ID: 200-41113-1 Client ID: SV-3 Operator ID: VTP ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Decane 124-18-5 NIST14.L 19650 C10H22 142 90 Carbonic acid,prop-1-en-2-yl tetradecyl ester 1000382-90-9 NIST14.L 157798 C18H34O3 298 78 Tetradecane 629-59-4 NIST14.L 63624 C14H30 198 72 30 50 70 90 110 130 150 170 190 210 230 250 270 m/z 0 16 32 48 64 80 Y ( X 10 0 0 0 )Raw Spec: Scan 2615(16.94) 5743 7141 85567039 99 30 50 70 90 110 130 150 170 190 210 230 250 270m/z 0 16 32 48 64 80 Y ( X 10 0 0 0 )28034-08[MS SCAN Spec]:Scan 2615(16.94) 5743 7141 85567039 99 30 50 70 90 110 130 150 170 190 210 230 250 270 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #19650, Decane (from NIST14.L) 43 57 41 71 85567039 30 50 70 90 110 130 150 170 190 210 230 250 270 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #157798, Carbonic acid, prop-1-en-2-yl tetradecyl ester (from NIST14.L) 57 43 714155 85 9739 111 30 50 70 90 110 130 150 170 190 210 230 250 270 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #63624, Tetradecane (from NIST14.L) 57 43 7141 85 55 7039 9984 Page 189 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: SV-2 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-2 TestAmerica Burlington Matrix:28034-09.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 13:34 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:2.98 Level: (low/med)Low 67(mL) 0.32(mm) Date Analyzed:11/24/2017 16:40 ID:RTX-624 Analysis Batch No.:123710 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 120.9175-71-8 Dichlorodifluoromethane 1.5 U 1.5 86.4775-45-6 Freon 22 1.5 U 1.5 170.9276-14-2 1,2-Dichlorotetrafluoroe thane 0.60 U 0.60 50.4974-87-3 Chloromethane 1.5 U 1.5 58.12106-97-8 n-Butane 17 1.5 62.5075-01-4 Vinyl chloride 0.10 U 0.10 54.09106-99-0 1,3-Butadiene 2.2 0.60 94.9474-83-9 Bromomethane 0.60 U 0.60 64.5275-00-3 Chloroethane 1.5 U 1.5 106.96593-60-2 Bromoethene(Vinyl Bromide) 0.60 U 0.60 137.3775-69-4 Trichlorofluoromethane 0.60 U 0.60 187.3876-13-1 Freon TF 0.60 U 0.60 96.9475-35-4 1,1-Dichloroethene 0.10 U 0.10 58.0867-64-1 Acetone 38 15 60.1067-63-0 Isopropyl alcohol 15 U 15 76.1475-15-0 Carbon disulfide 5.1 1.5 76.53107-05-1 3-Chloropropene 1.5 U 1.5 84.9375-09-2 Methylene Chloride 1.5 U 1.5 74.1275-65-0 tert-Butyl alcohol 15 U 15 88.151634-04-4 Methyl tert-butyl ether 0.60 U 0.60 96.94156-60-5 trans-1,2-Dichloroethene 0.60 U 0.60 86.17110-54-3 n-Hexane 1.3 0.60 98.9675-34-3 1,1-Dichloroethane 0.60 U 0.60 72.1178-93-3 Methyl Ethyl Ketone 6.0 1.5 96.94156-59-2 cis-1,2-Dichloroethene 0.10 U 0.10 96.94540-59-0 1,2-Dichloroethene, Total 1.2 U 1.2 119.3867-66-3 Chloroform 5.3 0.60 72.11109-99-9 Tetrahydrofuran 15 U 15 133.4171-55-6 1,1,1-Trichloroethane 0.60 U 0.60 84.16110-82-7 Cyclohexane 0.60 U 0.60 153.8156-23-5 Carbon tetrachloride 0.10 U 0.10 114.23540-84-1 2,2,4-Trimethylpentane 20 0.60 78.1171-43-2 Benzene 1.4 0.60 98.96107-06-2 1,2-Dichloroethane 0.60 U 0.60 FORM I TO-15 Page 190 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: SV-2 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-2 TestAmerica Burlington Matrix:28034-09.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 13:34 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:2.98 Level: (low/med)Low 67(mL) 0.32(mm) Date Analyzed:11/24/2017 16:40 ID:RTX-624 Analysis Batch No.:123710 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 100.21142-82-5 n-Heptane 0.71 0.60 131.3979-01-6 Trichloroethene 0.10 U 0.10 100.1280-62-6 Methyl methacrylate 1.5 U 1.5 112.9978-87-5 1,2-Dichloropropane 0.60 U 0.60 88.11123-91-1 1,4-Dioxane 15 U 15 163.8375-27-4 Bromodichloromethane 0.60 U 0.60 110.9710061-01-5 cis-1,3-Dichloropropene 0.60 U 0.60 100.16108-10-1 methyl isobutyl ketone 1.5 U 1.5 92.14108-88-3 Toluene 5.0 0.60 110.9710061-02-6 trans-1,3-Dichloropropen e 0.60 U 0.60 133.4179-00-5 1,1,2-Trichloroethane 0.60 U 0.60 165.83127-18-4 Tetrachloroethene 0.60 U 0.60 100.20591-78-6 Methyl Butyl Ketone (2-Hexanone) 1.5 U 1.5 208.29124-48-1 Dibromochloromethane 0.60 U 0.60 187.87106-93-4 1,2-Dibromoethane 0.60 U 0.60 112.56108-90-7 Chlorobenzene 0.60 U 0.60 106.17100-41-4 Ethylbenzene 37 0.60 106.17179601-23-1 m,p-Xylene 140 1.5 106.1795-47-6 Xylene, o-46 0.60 106.171330-20-7 Xylene (total)190 2.1 104.15100-42-5 Styrene 0.60 U 0.60 252.7575-25-2 Bromoform 0.60 U 0.60 120.1998-82-8 Cumene 0.67 0.60 167.8579-34-5 1,1,2,2-Tetrachloroethan e 0.60 U 0.60 120.19103-65-1 n-Propylbenzene 0.60 U 0.60 120.20622-96-8 4-Ethyltoluene 0.60 U 0.60 120.20108-67-8 1,3,5-Trimethylbenzene 0.60 U 0.60 126.5995-49-8 2-Chlorotoluene 0.60 U 0.60 134.2298-06-6 tert-Butylbenzene 0.60 U 0.60 120.2095-63-6 1,2,4-Trimethylbenzene 0.75 0.60 134.22135-98-8 sec-Butylbenzene 0.60 U 0.60 134.2299-87-6 4-Isopropyltoluene 0.60 U 0.60 147.00541-73-1 1,3-Dichlorobenzene 0.60 U 0.60 147.00106-46-7 1,4-Dichlorobenzene 0.60 U 0.60 FORM I TO-15 Page 191 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: SV-2 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-2 TestAmerica Burlington Matrix:28034-09.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 13:34 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:2.98 Level: (low/med)Low 67(mL) 0.32(mm) Date Analyzed:11/24/2017 16:40 ID:RTX-624 Analysis Batch No.:123710 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 126.58100-44-7 Benzyl chloride 0.60 U 0.60 134.22104-51-8 n-Butylbenzene 0.60 U 0.60 147.0095-50-1 1,2-Dichlorobenzene 0.60 U 0.60 181.45120-82-1 1,2,4-Trichlorobenzene 1.5 U 1.5 260.7687-68-3 Hexachlorobutadiene 0.60 U 0.60 128.1791-20-3 Naphthalene 1.5 U 1.5 FORM I TO-15 Page 192 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: SV-2 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-2 TestAmerica Burlington Matrix:28034-09.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 13:34 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:2.98 Level: (low/med)Low 67(mL) 0.32(mm) Date Analyzed:11/24/2017 16:40 ID:RTX-624 Analysis Batch No.:123710 ug/m3Units: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 120.9175-71-8 Dichlorodifluoromethane 7.4 U 7.4 86.4775-45-6 Freon 22 5.3 U 5.3 170.9276-14-2 1,2-Dichlorotetrafluoroe thane 4.2 U 4.2 50.4974-87-3 Chloromethane 3.1 U 3.1 58.12106-97-8 n-Butane 40 3.5 62.5075-01-4 Vinyl chloride 0.27 U 0.27 54.09106-99-0 1,3-Butadiene 4.9 1.3 94.9474-83-9 Bromomethane 2.3 U 2.3 64.5275-00-3 Chloroethane 3.9 U 3.9 106.96593-60-2 Bromoethene(Vinyl Bromide) 2.6 U 2.6 137.3775-69-4 Trichlorofluoromethane 3.3 U 3.3 187.3876-13-1 Freon TF 4.6 U 4.6 96.9475-35-4 1,1-Dichloroethene 0.41 U 0.41 58.0867-64-1 Acetone 90 35 60.1067-63-0 Isopropyl alcohol 37 U 37 76.1475-15-0 Carbon disulfide 16 4.6 76.53107-05-1 3-Chloropropene 4.7 U 4.7 84.9375-09-2 Methylene Chloride 5.2 U 5.2 74.1275-65-0 tert-Butyl alcohol 45 U 45 88.151634-04-4 Methyl tert-butyl ether 2.1 U 2.1 96.94156-60-5 trans-1,2-Dichloroethene 2.4 U 2.4 86.17110-54-3 n-Hexane 4.5 2.1 98.9675-34-3 1,1-Dichloroethane 2.4 U 2.4 72.1178-93-3 Methyl Ethyl Ketone 18 4.4 96.94156-59-2 cis-1,2-Dichloroethene 0.41 U 0.41 96.94540-59-0 1,2-Dichloroethene, Total 4.7 U 4.7 119.3867-66-3 Chloroform 26 2.9 72.11109-99-9 Tetrahydrofuran 44 U 44 133.4171-55-6 1,1,1-Trichloroethane 3.3 U 3.3 84.16110-82-7 Cyclohexane 2.1 U 2.1 153.8156-23-5 Carbon tetrachloride 0.66 U 0.66 114.23540-84-1 2,2,4-Trimethylpentane 93 2.8 78.1171-43-2 Benzene 4.3 1.9 98.96107-06-2 1,2-Dichloroethane 2.4 U 2.4 FORM I TO-15 Page 193 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: SV-2 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-2 TestAmerica Burlington Matrix:28034-09.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 13:34 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:2.98 Level: (low/med)Low 67(mL) 0.32(mm) Date Analyzed:11/24/2017 16:40 ID:RTX-624 Analysis Batch No.:123710 ug/m3Units: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 100.21142-82-5 n-Heptane 2.9 2.4 131.3979-01-6 Trichloroethene 0.56 U 0.56 100.1280-62-6 Methyl methacrylate 6.1 U 6.1 112.9978-87-5 1,2-Dichloropropane 2.8 U 2.8 88.11123-91-1 1,4-Dioxane 54 U 54 163.8375-27-4 Bromodichloromethane 4.0 U 4.0 110.9710061-01-5 cis-1,3-Dichloropropene 2.7 U 2.7 100.16108-10-1 methyl isobutyl ketone 6.1 U 6.1 92.14108-88-3 Toluene 19 2.2 110.9710061-02-6 trans-1,3-Dichloropropen e 2.7 U 2.7 133.4179-00-5 1,1,2-Trichloroethane 3.3 U 3.3 165.83127-18-4 Tetrachloroethene 4.0 U 4.0 100.20591-78-6 Methyl Butyl Ketone (2-Hexanone) 6.1 U 6.1 208.29124-48-1 Dibromochloromethane 5.1 U 5.1 187.87106-93-4 1,2-Dibromoethane 4.6 U 4.6 112.56108-90-7 Chlorobenzene 2.7 U 2.7 106.17100-41-4 Ethylbenzene 160 2.6 106.17179601-23-1 m,p-Xylene 620 6.5 106.1795-47-6 Xylene, o-200 2.6 106.171330-20-7 Xylene (total)810 9.1 104.15100-42-5 Styrene 2.5 U 2.5 252.7575-25-2 Bromoform 6.2 U 6.2 120.1998-82-8 Cumene 3.3 2.9 167.8579-34-5 1,1,2,2-Tetrachloroethan e 4.1 U 4.1 120.19103-65-1 n-Propylbenzene 2.9 U 2.9 120.20622-96-8 4-Ethyltoluene 2.9 U 2.9 120.20108-67-8 1,3,5-Trimethylbenzene 2.9 U 2.9 126.5995-49-8 2-Chlorotoluene 3.1 U 3.1 134.2298-06-6 tert-Butylbenzene 3.3 U 3.3 120.2095-63-6 1,2,4-Trimethylbenzene 3.7 2.9 134.22135-98-8 sec-Butylbenzene 3.3 U 3.3 134.2299-87-6 4-Isopropyltoluene 3.3 U 3.3 147.00541-73-1 1,3-Dichlorobenzene 3.6 U 3.6 147.00106-46-7 1,4-Dichlorobenzene 3.6 U 3.6 FORM I TO-15 Page 194 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: SV-2 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-2 TestAmerica Burlington Matrix:28034-09.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 13:34 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:2.98 Level: (low/med)Low 67(mL) 0.32(mm) Date Analyzed:11/24/2017 16:40 ID:RTX-624 Analysis Batch No.:123710 ug/m3Units: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 126.58100-44-7 Benzyl chloride 3.1 U 3.1 134.22104-51-8 n-Butylbenzene 3.3 U 3.3 147.0095-50-1 1,2-Dichlorobenzene 3.6 U 3.6 181.45120-82-1 1,2,4-Trichlorobenzene 11 U 11 260.7687-68-3 Hexachlorobutadiene 6.4 U 6.4 128.1791-20-3 Naphthalene 7.8 U 7.8 FORM I TO-15 Page 195 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS Client Sample ID: Lab Name:Job No.: SV-2 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-2 TestAmerica Burlington Matrix:28034-09.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 13:34 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:2.98 Level: (low/med)Low 67(mL) 0.32(mm) Date Analyzed:11/24/2017 16:40 ID:RTX-624 Analysis Batch No.:123710 ppb v/vUnits: Number TICs Found:TIC Result Total:36610 QRTCOMPOUND NAME RESULTCAS NO.MATCH QUALITY 13.03 J N638-04-0 Cyclohexane, 1,3-dimethyl-, cis-48 97% 13.72 J N2207-04-7 Cyclohexane, 1,4-dimethyl-, trans-27 97% 14.26 J N1839-63-0 Cyclohexane, 1,3,5-trimethyl-25 97% 14.39 J N1678-91-7 Cyclohexane, ethyl-33 95% 14.44 J N3073-66-3 Cyclohexane, 1,1,3-trimethyl-51 94% 14.68 JUnknown47 14.76 J N7667-60-9 Cyclohexane, 1,2,4-trimethyl-, (1.alpha.,2.beta.,4.beta.)- 41 94% 14.84 J N2216-33-3 Octane, 3-methyl-42 90% 15.28 J N2234-75-5 Cyclohexane, 1,2,4-trimethyl-26 93% 15.85 JUnknown26 FORM I-TIC TO-15 Page 196 of 478 Report Date: 28-Nov-2017 09:30:40 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Target Compound Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Lims ID: 200-41113-A-2 Client ID: SV-2 Sample Type: Client Inject. Date: 24-Nov-2017 16:40:30 ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Sample Info: 200-0028034-009 Misc. Info.: 41113-02 Operator ID: VTP Instrument ID: CHB.i Method:\\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\TO15_LLNJ_TO3.m Limit Group: AI_TO15_ICAL Last Update: 28-Nov-2017 09:30:39 Calib Date: 07-Nov-2017 01:49:30 Integrator: RTE ID Type: Deconvolution ID Quant Method: Internal/External Standard Quant By: Initial Calibration Last ICal File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-13.D Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host:XAWRK022 First Level Reviewer: puangmaleek Date:28-Nov-2017 09:30:39 Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response OnCol Amt ppb v/v Flags 2 Dichlorodifluoromethane 85 3.193 3.193 0.000 98 10007 0.1252 3 Chlorodifluoromethane 51 3.225 ND 4 1,2-Dichloro-1,1,2,2-tetra 85 3.412 ND 5 Chloromethane 50 3.540 3.540 0.005 37 3533 0.1239 7 6 Butane 43 3.716 3.711 0.005 98 276844 5.62 7 Vinyl chloride 62 3.748 ND 8 Butadiene 54 3.812 3.812 0.000 96 18850 0.7488 10 Bromomethane 94 4.479 ND 11 Chloroethane 64 4.709 ND 13 Vinyl bromide 106 5.120 ND 14 Trichlorofluoromethane 101 5.221 5.221 0.005 1 4894 0.0574 7 19 1,1,2-Trichloro-1,2,2-trif 101 6.246 ND 20 1,1-Dichloroethene 96 6.315 ND 21 Acetone 43 6.464 6.465 -0.001 96 682450 12.7 22 Isopropyl alcohol 45 6.683 ND 23 Carbon disulfide 76 6.747 6.748 -0.001 98 173080 1.72 24 3-Chloro-1-propene 41 7.014 ND 27 Methylene Chloride 49 7.281 7.281 0.005 58 4448 0.1034 7 28 2-Methyl-2-propanol 59 7.409 7.409 0.026 62 10601 0.1350 7 29 Methyl tert-butyl ether 73 7.660 7.623 0.037 95 19223 0.1797 30 trans-1,2-Dichloroethene 61 7.687 ND 32 Hexane 57 8.012 8.012 0.000 80 28076 0.4285 33 1,1-Dichloroethane 63 8.423 ND 36 2-Butanone (MEK) 72 9.325 9.315 0.010 100 42511 2.01 37 cis-1,2-Dichloroethene 96 9.331 ND * 39 Chlorobromomethane 128 9.699 9.699 0.000 93 360978 10.0 38 Tetrahydrofuran 42 9.710 ND 40 Chloroform 83 9.773 9.774 -0.001 94 137759 1.77 S 41 1,2-Dichloroethene, Total 61 10.000 ND 42 1,1,1-Trichloroethane 97 10.030 ND 43 Cyclohexane 84 10.046 ND Page 197 of 478 Report Date: 28-Nov-2017 09:30:40 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response OnCol Amt ppb v/v Flags 44 Carbon tetrachloride 117 10.238 ND 45 Isooctane 57 10.515 10.521 -0.006 100 1449166 6.68 46 Benzene 78 10.563 10.563 0.000 92 60673 0.4535 47 1,2-Dichloroethane 62 10.659 ND 48 n-Heptane 43 10.771 10.771 -0.001 1 19677 0.2373 M * 50 1,4-Difluorobenzene 114 11.102 11.102 0.000 94 1819209 10.0 53 Trichloroethene 95 11.476 ND 54 1,2-Dichloropropane 63 11.839 ND 55 Methyl methacrylate 69 11.876 ND 56 1,4-Dioxane 88 11.967 ND 58 Dichlorobromomethane 83 12.202 ND 60 cis-1,3-Dichloropropene 75 12.826 ND 61 4-Methyl-2-pentanone (MIBK 43 12.976 ND 64 Toluene 92 13.258 13.259 -0.001 93 154631 1.68 66 trans-1,3-Dichloropropene 75 13.621 ND 67 1,1,2-Trichloroethane 83 13.888 ND 68 Tetrachloroethene 166 14.032 ND 69 2-Hexanone 43 14.150 ND 70 Chlorodibromomethane 129 14.449 ND 71 Ethylene Dibromide 107 14.646 ND * 72 Chlorobenzene-d5 117 15.212 15.212 0.000 84 1541512 10.0 73 Chlorobenzene 112 15.249 ND 74 Ethylbenzene 91 15.318 15.319 -0.001 98 2515217 12.5 76 m-Xylene & p-Xylene 106 15.462 15.468 -0.006 0 3802772 47.8 78 o-Xylene 106 15.980 15.975 0.005 99 1232225 15.6 S 77 Xylenes, Total 106 0 63.4 79 Styrene 104 16.002 ND 80 Bromoform 173 16.295 ND 81 Isopropylbenzene 105 16.391 16.391 0.000 1 50209 0.2246 M 83 1,1,2,2-Tetrachloroethane 83 16.797 ND 84 N-Propylbenzene 91 16.871 16.871 0.005 1 29960 0.1087 M 87 4-Ethyltoluene 105 16.994 16.994 0.000 1 21393 0.0976 M 88 2-Chlorotoluene 91 17.037 ND 89 1,3,5-Trimethylbenzene 105 17.058 17.058 0.000 1 17610 0.0972 M 91 tert-Butylbenzene 119 17.437 ND 92 1,2,4-Trimethylbenzene 105 17.506 17.507 -0.001 98 45195 0.2524 93 sec-Butylbenzene 105 17.694 ND 94 4-Isopropyltoluene 119 17.848 17.848 0.005 1 2980 0.0133 7 95 1,3-Dichlorobenzene 146 17.923 ND 96 1,4-Dichlorobenzene 146 18.035 ND 97 Benzyl chloride 91 18.185 ND 99 n-Butylbenzene 91 18.350 ND 100 1,2-Dichlorobenzene 146 18.521 ND 103 1,2,4-Trichlorobenzene 180 20.880 ND 104 Hexachlorobutadiene 225 21.045 ND 105 Naphthalene 128 21.360 21.360 0.000 1 3643 0.0248 7 Page 198 of 478 Report Date: 28-Nov-2017 09:30:40 Chrom Revision: 2.2 13-Nov-2017 17:19:06 QC Flag Legend Processing Flags 7 - Failed Limit of Detection Review Flags M - Manually Integrated Reagents: ATTO15BISs_00006 Amount Added: 20.00 Units: mL Run Reagent Page 199 of 478 Report Date: 28-Nov-2017 09:30:40 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Tentatively Identified Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Lims ID: 200-41113-A-2 Client ID: SV-2 Sample Type: Client Inject. Date: 24-Nov-2017 16:40:30 ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol:200.000 mL Dil. Factor: 2.9800 Sample Info: 200-0028034-009 Misc. Info.: 41113-02 Operator ID: VTP Instrument ID: CHB.i Method:\\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\TO15_LLNJ_TO3.m Limit Group: AI_TO15_ICAL Last Update: 28-Nov-2017 09:30:39 Calib Date: 07-Nov-2017 01:49:30 Tic RT Window: 0.000 -0.000 Response: area Quant By: Nearest ISTD Quant LOD: 10.00000 MS Library: \\ChromNA\Burlington\Database\NIST14.L Min. Match: 1 Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host:XAWRK022 First Level Reviewer: puangmaleek Date:28-Nov-2017 09:30:39 Tentative Identified Compound Results RT Area Amount ppb v/v Quant Cpnd Qual Lib Entry Molecular Formula Mol. Weight Flags 638-04-0 Cyclohexane, 1,3-dimethyl-, cis- 13.034 6214673 16.1 50 97 6931 C8H16 112 2207-04-7 Cyclohexane, 1,4-dimethyl-, trans- 13.717 4057895 9.00 72 97 6940 C8H16 112 1839-63-0 Cyclohexane, 1,3,5-trimethyl- 14.262 3813965 8.46 72 97 11834 C9H18 126 1678-91-7 Cyclohexane, ethyl- 14.390 4950998 11.0 72 95 6791 C8H16 112 3073-66-3 Cyclohexane, 1,1,3-trimethyl- 14.443 7728441 17.1 72 94 11835 C9H18 126 Unknown 14.678 7130703 15.8 72 0 0 0 7667-60-9 Cyclohexane, 1,2,4-trimethyl-, (1.alpha.,2.beta.,4.beta.)- 14.758 6256474 13.9 72 94 11870 C9H18 126 2216-33-3 Octane, 3-methyl- 14.843 6327568 14.0 72 90 12944 C9H20 128 2234-75-5 Cyclohexane, 1,2,4-trimethyl- 15.276 3938376 8.73 72 93 11819 C9H18 126 Unknown 15.847 3975620 8.82 72 0 0 0 Page 200 of 478 Report Date: 28-Nov-2017 09:30:40 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Quantitation Compounds Compound RT Area Amount ppb v/v * 50 1,4-Difluorobenzene 11.102 3866151 10.0 * 72 Chlorobenzene-d5 15.212 4509544 10.0 QC Flag Legend Processing Flags Reagents: ATTO15BISs_00006 Amount Added: 20.00 Units: mL Run Reagent Page 201 of 478 Report Date: 28-Nov-2017 09:30:40 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Operator ID: VTP Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Worklist Smp#: 38 Client ID: SV-2 Purge Vol: 200.000 mL Dil. Factor: 2.9800 ALS Bottle#: 9 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Y Scaling: Method Defined: Scale to the Nth Largest Target: 1 2.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 18.0 20.0 22.0 24.0 Min 0 1 2 3 4 5 6 7 8 9 10 11 12 Y ( X 10 0 0 0 0 0 ) 28034-09[MS SCAN Chro]:Total * C h l o r o b r o m o m e t h a n e ( 9 . 6 9 9 ) * 1 ,4- D i f lu o r o b e n z en e ( 1 1 . 1 0 2 ) * C h l o r o b e n z en e - d 5( 1 5 .2 1 2 ) Page 202 of 478 Report Date: 28-Nov-2017 09:30:40 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 6 Butane, CAS: 106-97-8 37 41 45 49 53 57 m/z 0 2 4 6 8 10 12 14 Y ( X 10 0 0 0 ) Raw Spec:Scan 138(3.72) 43 41 5839 44 37 41 45 49 53 57m/z 0 2 4 6 8 10 12 14 Y ( X 10 0 0 0 ) Enhanced Spec:Scan 138(3.72), Qvalue=98 43 41 5839 44 37 41 45 49 53 57 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 6 Butane (DATA) 43 41 39 58 37 41 45 49 53 57 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 138 @ 3.716 min.(Qvalue: 98) 41 5842 3.2 3.5 3.8 4.1 Min 0 2 4 6 8 10 12 14 Y ( X 10 0 0 0 ) m/z 43.0 3 . 7 1 6 3.1 3.4 3.7 4.0Min 0 2 4 6 8 10 12 14 Y ( X 10 0 0 0 ) m/z 41.0 3 . 6 8 4 3.2 3.5 3.8 4.1 Min 0 3 6 9 12 15 18 Y ( X 10 0 0 ) m/z 58.0 3 . 7 1 6 3.1 3.4 3.7 4.0 4.3 Min 0 3 6 9 12 15 Y ( X 10 0 0 0 ) m/z 43.0 m/z 41.0 m/z 58.0 Page 203 of 478 Report Date: 28-Nov-2017 09:30:40 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 8 Butadiene, CAS: 106-99-0 36 40 44 48 52 56 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Raw Spec:Scan 156(3.81) 57 39 54 53 41 44 51 49 5538 36 40 44 48 52 56m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 156(3.81), Qvalue=96 5439 53 51 4938 55 36 40 44 48 52 56 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 8 Butadiene (DATA) 39 54 53 50 51 4938 36 40 44 48 52 56 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 3.810 min.(Qvalue: 96) 51 54 3.3 3.6 3.9 4.2 Min 0 12 24 36 48 60 72 84 Y ( X 10 0 ) m/z 54.0 3 . 8 1 2 Page 204 of 478 Report Date: 28-Nov-2017 09:30:41 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 21 Acetone, CAS: 67-64-1 36 40 44 48 52 56 60 m/z 0 3 6 9 12 15 18 21 24 Y ( X 10 0 0 0 ) Raw Spec:Scan 653(6.46) 43 5844 42 36 40 44 48 52 56 60m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 653(6.46), Qvalue=96 43 58 42 36 40 44 48 52 56 60 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 21 Acetone (NIST) 43 58 42 36 40 44 48 52 56 60 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 6.470 min.(Qvalue: 96) 58 5.9 6.2 6.5 6.8 Min 0 3 6 9 12 15 18 21 24 Y ( X 10 0 0 0 ) m/z 43.0 6 . 4 6 4 5.9 6.2 6.5 6.8Min 0 12 24 36 48 60 72 84 Y ( X 10 0 0 ) m/z 58.0 6 . 4 7 0 5.9 6.2 6.5 6.8 Min 0 4 8 12 16 20 24 Y ( X 10 0 0 0 ) m/z 43.0 m/z 58.0 Page 205 of 478 Report Date: 28-Nov-2017 09:30:41 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 23 Carbon disulfide, CAS: 75-15-0 38 42 46 50 54 58 62 66 70 74 78 m/z 0 9 18 27 36 45 54 63 Y ( X 10 0 0 ) Raw Spec:Scan 706(6.75) 76 44 38 42 46 50 54 58 62 66 70 74 78m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Amdis Enhanced Spec: Scan 706(6.75), Qvalue=98 76 44 67 68 38 42 46 50 54 58 62 66 70 74 78 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 23 Carbon disulfide (NIST) 76 44 38 42 46 50 54 58 62 66 70 74 78 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 6.730 min.(Qvalue: 98) 67 78 6.2 6.5 6.8 7.1 Min 0 9 18 27 36 45 54 63 Y ( X 10 0 0 ) m/z 76.0 6 . 7 4 7 Page 206 of 478 Report Date: 28-Nov-2017 09:30:41 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 32 Hexane, CAS: 110-54-3 37 41 45 49 53 57 61 65 69 73 77 81 85 m/z 0 2 4 6 8 10 12 14 16 Y ( X 10 0 0 ) Raw Spec:Scan 943(8.01) 43 41 57 7256 865544 37 41 45 49 53 57 61 65 69 73 77 81 85m/z 0 2 4 6 8 10 12 14 16 Y ( X 10 0 ) Amdis Enhanced Spec: Scan 943(8.01), Qvalue=80 43 41 57 56 8655 37 41 45 49 53 57 61 65 69 73 77 81 85 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 32 Hexane (NIST) 57 43 56 86 55 37 41 45 49 53 57 61 65 69 73 77 81 85 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 8.020 min.(Qvalue: 80) 43 7.5 7.8 8.1 8.4 Min 0 12 24 36 48 60 72 84 96 Y ( X 10 0 ) m/z 57.0 8 . 0 1 2 7.5 7.8 8.1 8.4Min 0 3 6 9 12 15 18 Y ( X 10 0 ) m/z 86.0 8 . 0 1 7 7.5 7.8 8.1 8.4 Min 0 14 28 42 56 70 84 Y ( X 10 0 ) m/z 57.0 m/z 86.0 Page 207 of 478 Report Date: 28-Nov-2017 09:30:41 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 36 2-Butanone (MEK), CAS: 78-93-3 30 50 70 90 110 130 150 m/z 0 8 16 24 32 40 48 56 Y ( X 10 0 0 ) Raw Spec:Scan 1189(9.32) 43 72 5742 30 50 70 90 110 130 150m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 1189(9.32), Qvalue=100 43 72 5742 30 50 70 90 110 130 150 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 36 2-Butanone (MEK) (DATA) 43 72 57 30 50 70 90 110 130 150 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 9.320 min.(Qvalue:100) 42 72 8.8 9.1 9.4 9.7 Min 0 3 6 9 12 15 Y ( X 10 0 0 ) m/z 72.0 9 . 3 2 5 8.8 9.1 9.4 9.7Min 0 8 16 24 32 40 48 56 Y ( X 10 0 0 ) m/z 43.0 9 . 3 2 0 8.8 9.1 9.4 9.7 Min 0 9 18 27 36 45 54 Y ( X 10 0 0 ) m/z 72.0 m/z 43.0 Page 208 of 478 Report Date: 28-Nov-2017 09:30:41 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 40 Chloroform, CAS: 67-66-3 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 103107111115119123127 m/z 0 7 14 21 28 35 42 49 56 Y ( X 10 0 0 ) Raw Spec:Scan 1273(9.77) 83 85 47 8748 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 103107111115119123127m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 1273(9.77), Qvalue=94 83 85 47 8748 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 103107111115119123127 m/z 0 13 26 39 52 65 78 91 Y ( X 10 0 ) Ref Spec: 40 Chloroform (NIST) 83 85 47 48 87 82 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 103107111115119123127 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 9.770 min.(Qvalue: 94) 9.2 9.5 9.8 10.1 Min 0 7 14 21 28 35 42 49 56 Y ( X 10 0 0 ) m/z 83.0 9 . 7 7 3 9.2 9.5 9.8 10.1Min 0 5 10 15 20 25 30 35 Y ( X 10 0 0 ) m/z 85.0 9 . 7 7 3 9.2 9.5 9.8 10.1 Min 0 8 16 24 32 40 48 56 Y ( X 10 0 0 ) m/z 83.0 m/z 85.0 Page 209 of 478 Report Date: 28-Nov-2017 09:30:41 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 45 Isooctane, CAS: 540-84-1 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 m/z 0 6 12 18 24 30 36 42 Y ( X 10 0 0 0 ) Raw Spec:Scan 1412(10.52) 57 56 41 43 99 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 1412(10.52), Qvalue=100 57 56 41 43 99 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 45 Isooctane (NIST) 57 56 41 43 99 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 10.520 min.(Qvalue:100) 10.0 10.3 10.6 10.9 Min 0 6 12 18 24 30 36 42 Y ( X 10 0 0 0 ) m/z 57.0 1 0 . 5 1 5 10.0 10.3 10.6 10.9Min 0 12 24 36 48 60 72 84 96 Y ( X 10 0 0 ) m/z 41.0 1 0 . 5 20 10.0 10.3 10.6 10.9 Min 0 10 20 30 40 50 60 70 Y ( X 10 0 0 ) m/z 43.0 1 0 . 5 20 10.0 10.3 10.6 10.9 Min 0 7 14 21 28 35 42 Y ( X 10 0 0 0 ) m/z 57.0 m/z 41.0 m/z 43.0 Page 210 of 478 Report Date: 28-Nov-2017 09:30:41 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 46 Benzene, CAS: 71-43-2 36 40 44 48 52 56 60 64 68 72 76 80 84 88 92 96 100 m/z 0 7 14 21 28 35 42 49 Y ( X 10 0 0 ) Raw Spec:Scan 1421(10.56) 57 78 56 41 43 7752 99 36 40 44 48 52 56 60 64 68 72 76 80 84 88 92 96 100m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 1421(10.56), Qvalue=92 78 77 52 76 36 40 44 48 52 56 60 64 68 72 76 80 84 88 92 96 100 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 46 Benzene (DATA) 78 775152 7974 36 40 44 48 52 56 60 64 68 72 76 80 84 88 92 96 100 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 10.560 min.(Qvalue: 92) 10.0 10.3 10.6 10.9 Min 0 4 8 12 16 20 24 Y ( X 10 0 0 ) m/z 78.0 1 0 . 5 63 10.0 10.3 10.6 10.9Min 0 8 16 24 32 40 48 56 Y ( X 10 0 ) m/z 77.0 1 0 . 5 63 10.0 10.3 10.6 10.9 Min 0 4 8 12 16 20 24 Y ( X 10 0 0 ) m/z 78.0 m/z 77.0 Page 211 of 478 Report Date: 28-Nov-2017 09:30:41 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 48 n-Heptane, CAS: 142-82-5 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 m/z 0 10 20 30 40 50 60 70 80 Y ( X 10 0 ) Raw Spec:Scan 1460(10.77) 43 71 57 56 704455 10058 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99m/z 0 10 20 30 40 50 60 70 80 Y ( X 10 0 ) Enhanced Spec:Scan 1460(10.77), Qvalue=1 43 71 57 56 704455 10058 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 48 n-Heptane (NIST) 43 57 71 56 70 10055 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1460 @ 10.771 min.(Qvalue: 1) 714458 10.2 10.5 10.8 11.1 Min -1 2 5 8 11 14 Y ( X 10 0 0 ) m/z 43.0 1 0 . 7 7 1 10.2 10.5 10.8 11.1Min -1 6 13 20 27 34 41 48 Y ( X 10 0 ) m/z 71.0 1 0 . 7 7 1 10.2 10.5 10.8 11.1 Min 0 11 22 33 44 55 66 Y ( X 10 0 0 ) m/z 43.0 m/z 71.0 Page 212 of 478 Report Date: 28-Nov-2017 09:30:41 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 64 Toluene, CAS: 108-88-3 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 m/z 0 3 6 9 12 15 18 Y ( X 10 0 0 0 ) Raw Spec:Scan 1926(13.26) 43 91 85 57 927156 8465 114 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 1926(13.26), Qvalue=93 91 92 65 8351 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 64 Toluene (NIST) 91 92 6551 93 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 13.260 min.(Qvalue: 93) 83 12.7 13.0 13.3 13.6 Min 0 9 18 27 36 45 54 63 Y ( X 10 0 0 ) m/z 92.0 1 3 . 2 5 8 12.7 13.0 13.3 13.6Min 0 2 4 6 8 10 12 Y ( X 10 0 0 0 ) m/z 91.0 1 3 . 2 5 8 12.7 13.0 13.3 13.6 Min 0 2 4 6 8 10 12 Y ( X 10 0 0 0 ) m/z 92.0 m/z 91.0 Page 213 of 478 Report Date: 28-Nov-2017 09:30:41 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 74 Ethylbenzene, CAS: 100-41-4 30 50 70 90 110 130 150 170 190 210 m/z 0 2 4 6 8 10 12 Y ( X 10 0 0 0 0 ) Raw Spec:Scan 2312(15.32) 91 106 51 55 77 78 105 30 50 70 90 110 130 150 170 190 210m/z 0 2 4 6 8 10 12 Y ( X 10 0 0 0 0 ) Enhanced Spec:Scan 2312(15.32), Qvalue=98 91 106 51 55 77 78 105 30 50 70 90 110 130 150 170 190 210 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 74 Ethylbenzene (NIST) 91 106 51 65 77 78 105 30 50 70 90 110 130 150 170 190 210 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 2312 @ 15.318 min.(Qvalue: 98) 5543 106 14.8 15.1 15.4 15.7 Min 0 5 10 15 20 25 30 35 Y ( X 10 0 0 0 0 ) m/z 91.0 1 5 .3 1 8 14.8 15.1 15.4 15.7Min 0 3 6 9 12 15 18 Y ( X 10 0 0 0 0 ) m/z 106.0 1 5 .3 1 8 14.8 15.1 15.4 15.7 Min 0 6 12 18 24 30 36 Y ( X 10 0 0 0 0 ) m/z 91.0 m/z 106.0 Page 214 of 478 Report Date: 28-Nov-2017 09:30:41 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 76 m-Xylene & p-Xylene, CAS: 179601-23-1 30 50 70 90 110 130 150 170 190 210 m/z 0 5 10 15 20 25 30 35 Y ( X 10 0 0 0 0 ) Raw Spec:Scan 2339(15.46) 91 106 105 7751 7965 30 50 70 90 110 130 150 170 190 210m/z 0 5 10 15 20 25 30 35 Y ( X 10 0 0 0 0 ) Enhanced Spec:Scan 2339(15.46), Qvalue=0 91 106 105 7751 7965 14.9 15.2 15.5 15.8 Min 0 3 6 9 12 15 18 Y ( X 10 0 0 0 0 ) m/z 106.0 1 5 .4 6 2 14.9 15.2 15.5 15.8Min 0 5 10 15 20 25 30 35 Y ( X 10 0 0 0 0 ) m/z 91.0 1 5 .4 6 2 14.9 15.2 15.5 15.8 Min 0 6 12 18 24 30 36 Y ( X 10 0 0 0 0 ) m/z 106.0 m/z 91.0 Page 215 of 478 Report Date: 28-Nov-2017 09:30:42 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 78 o-Xylene, CAS: 95-47-6 30 50 70 90 110 130 150 170 190 210 230 250 m/z 0 2 4 6 8 10 12 14 Y ( X 10 0 0 0 0 ) Raw Spec:Scan 2436(15.98) 91 106 7751 30 50 70 90 110 130 150 170 190 210 230 250m/z 0 10 20 30 40 50 60 70 Y ( X 10 0 ) Amdis Enhanced Spec: Scan 2436(15.98), Qvalue=99 91 106 57 77 30 50 70 90 110 130 150 170 190 210 230 250 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 78 o-Xylene (NIST) 91 106 7751 30 50 70 90 110 130 150 170 190 210 230 250 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 15.960 min.(Qvalue: 99) 57 15.4 15.7 16.0 16.3 Min 0 2 4 6 8 10 Y ( X 10 0 0 0 0 ) m/z 106.0 1 5 .9 8 0 15.4 15.7 16.0 16.3Min 0 3 6 9 12 15 18 21 Y ( X 10 0 0 0 0 ) m/z 91.0 1 5 .9 8 0 15.4 15.7 16.0 16.3 Min 0 3 6 9 12 15 18 21 Y ( X 10 0 0 0 0 ) m/z 106.0 m/z 91.0 Page 216 of 478 Report Date: 28-Nov-2017 09:30:42 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 81 Isopropylbenzene, CAS: 98-82-8 30 50 70 90 110 130 150 170 190 210 230 250 m/z 0 5 10 15 20 25 30 35 Y ( X 10 0 0 ) Raw Spec:Scan 2513(16.39) 57 10543 70 98 120 125 30 50 70 90 110 130 150 170 190 210 230 250m/z 0 5 10 15 20 25 30 35 Y ( X 10 0 0 ) Enhanced Spec:Scan 2513(16.39), Qvalue=1 57 10543 70 98 120 125 30 50 70 90 110 130 150 170 190 210 230 250 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 81 Isopropylbenzene (NIST) 105 120777951 30 50 70 90 110 130 150 170 190 210 230 250 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 2513 @ 16.391 min.(Qvalue: 1) 57 43 70 98 15.8 16.1 16.4 16.7 Min 0 7 14 21 28 35 42 49 Y ( X 10 0 0 ) m/z 105.0 1 6 . 3 9 1 15.8 16.1 16.4 16.7Min 0 9 18 27 36 45 54 63 72 Y ( X 10 0 ) m/z 120.0 1 6 . 3 9 1 15.8 16.1 16.4 16.7 Min 0 3 6 9 12 15 Y ( X 10 0 0 0 ) m/z 77.0 15.8 16.1 16.4 16.7 Min 0 5 10 15 20 25 Y ( X 10 0 0 0 ) m/z 105.0 m/z 120.0 m/z 77.0 Page 217 of 478 Report Date: 28-Nov-2017 09:30:42 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 92 1,2,4-Trimethylbenzene, CAS: 95-63-6 30 50 70 90 110 130 150 170 190 210 230 250 m/z 0 4 8 12 16 20 24 Y ( X 10 0 0 ) Raw Spec:Scan 2722(17.51) 105 120 57 77 121 30 50 70 90 110 130 150 170 190 210 230 250m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 2722(17.51), Qvalue=98 105 120 77 51 121 30 50 70 90 110 130 150 170 190 210 230 250 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 92 1,2,4-Trimethylbenzene (NIST) 105 120 77 30 50 70 90 110 130 150 170 190 210 230 250 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 17.510 min.(Qvalue: 98) 120 17.0 17.3 17.6 17.9 Min 0 4 8 12 16 20 24 Y ( X 10 0 0 ) m/z 105.0 1 7 . 5 06 17.0 17.3 17.6 17.9Min 0 2 4 6 8 10 12 Y ( X 10 0 0 ) m/z 120.0 1 7 . 5 06 17.0 17.3 17.6 17.9 Min 0 4 8 12 16 20 24 Y ( X 10 0 0 ) m/z 105.0 m/z 120.0 Page 218 of 478 Report Date: 28-Nov-2017 09:30:41 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#:38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 48 n-Heptane, CAS: 142-82-5 Signal: 1 Processing Integration Results Not Detected Expected RT: 10.77 10.4 10.6 10.8 11.0 Min 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 Y ( X 10 0 0 ) m/z 43.0 Manual Integration Results RT: 10.77 Area: 19677 Amount: 0.237259 Amount Units: ppb v/v 10.4 10.6 10.8 11.0 Min -1 1 3 5 7 9 11 13 15 Y ( X 10 0 0 ) m/z 43.0 1 0 . 7 7 1 Reviewer: puangmaleek, 28-Nov-2017 09:26:30 Audit Action: Assigned Compound ID Audit Reason: Assign Peak Page 219 of 478 Report Date: 28-Nov-2017 09:30:41 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#:38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 48 n-Heptane, CAS: 142-82-5 Signal: 1 Processing Integration Results Not Detected Expected RT: 10.77 10.4 10.6 10.8 11.0Min 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 Y ( X 10 0 0 ) m/z 43.0 Manual Integration Results RT: 10.77 Area: 19677 Amount: 0.237259 Amount Units: ppb v/v 10.4 10.6 10.8 11.0 Min -1 1 3 5 7 9 11 13 15 Y ( X 10 0 0 ) m/z 43.0 1 0 . 7 7 1 Reviewer: puangmaleek, 28-Nov-2017 09:26:43 Audit Action: Manually Integrated Audit Reason: Assign Peak Page 220 of 478 Report Date: 28-Nov-2017 09:30:41 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#:38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 48 n-Heptane, CAS: 142-82-5 Signal: 2 Processing Integration Results Not Detected Expected RT: 10.77 10.4 10.6 10.8 11.0Min 0 4 8 12 16 20 24 28 32 36 40 44 48 52 Y ( X 10 0 ) m/z 71.0 Manual Integration Results RT: 10.77 Area: 11033 Amount: 0.237259 Amount Units: ppb v/v 10.4 10.6 10.8 11.0 Min -1 3 7 11 15 19 23 27 31 35 39 43 47 51 Y ( X 10 0 ) m/z 71.0 1 0 . 7 7 1 Reviewer: puangmaleek, 28-Nov-2017 09:26:56 Audit Action: Manually Integrated Audit Reason: Assign Peak Page 221 of 478 Report Date: 28-Nov-2017 09:30:42 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#:38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 81 Isopropylbenzene, CAS: 98-82-8 Signal: 1 Processing Integration Results Not Detected Expected RT: 16.39 16.0 16.2 16.4 16.6 Min 0 2 4 6 8 10 12 14 16 18 20 22 24 26 Y ( X 10 0 0 ) m/z 105.0 Manual Integration Results RT: 16.39 Area: 50209 Amount: 0.224564 Amount Units: ppb v/v 16.0 16.2 16.4 16.6 Min 0 2 4 6 8 10 12 14 16 18 20 22 24 26 Y ( X 10 0 0 ) m/z 105.0 1 6 . 3 9 1 Reviewer: puangmaleek, 28-Nov-2017 09:27:50 Audit Action: Assigned Compound ID Audit Reason: Assign Peak Page 222 of 478 Report Date: 28-Nov-2017 09:30:42 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#:38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 81 Isopropylbenzene, CAS: 98-82-8 Signal: 1 Processing Integration Results Not Detected Expected RT: 16.39 16.0 16.2 16.4 16.6Min 0 2 4 6 8 10 12 14 16 18 20 22 24 26 Y ( X 10 0 0 ) m/z 105.0 Manual Integration Results RT: 16.39 Area: 50209 Amount: 0.224564 Amount Units: ppb v/v 16.0 16.2 16.4 16.6 Min 0 2 4 6 8 10 12 14 16 18 20 22 24 26 Y ( X 10 0 0 ) m/z 105.0 1 6 . 3 9 1 Reviewer: puangmaleek, 28-Nov-2017 09:27:56 Audit Action: Manually Integrated Audit Reason: Assign Peak Page 223 of 478 Report Date: 28-Nov-2017 09:30:42 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#:38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 84 N-Propylbenzene, CAS: 103-65-1 Signal: 1 Processing Integration Results Not Detected Expected RT: 16.87 16.5 16.7 16.9 17.1 Min 0 2 4 6 8 10 12 14 16 Y ( X 10 0 0 ) m/z 91.0 Manual Integration Results RT: 16.87 Area: 29960 Amount: 0.108748 Amount Units: ppb v/v 16.5 16.7 16.9 17.1 Min 0 2 4 6 8 10 12 14 16 Y ( X 10 0 0 ) m/z 91.0 1 6 . 8 7 1 Reviewer: puangmaleek, 28-Nov-2017 09:28:13 Audit Action: Assigned Compound ID Audit Reason: Assign Peak Page 224 of 478 Report Date: 28-Nov-2017 09:30:42 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#:38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 84 N-Propylbenzene, CAS: 103-65-1 Signal: 1 Processing Integration Results Not Detected Expected RT: 16.87 16.5 16.7 16.9 17.1Min 0 2 4 6 8 10 12 14 16 Y ( X 10 0 0 ) m/z 91.0 Manual Integration Results RT: 16.87 Area: 29960 Amount: 0.108748 Amount Units: ppb v/v 16.5 16.7 16.9 17.1 Min 0 2 4 6 8 10 12 14 16 Y ( X 10 0 0 ) m/z 91.0 1 6 . 8 7 1 Reviewer: puangmaleek, 28-Nov-2017 09:28:18 Audit Action: Manually Integrated Audit Reason: Assign Peak Page 225 of 478 Report Date: 28-Nov-2017 09:30:42 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#:38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 87 4-Ethyltoluene, CAS: 622-96-8 Signal: 1 Processing Integration Results Not Detected Expected RT: 16.99 16.7 16.9 17.1 Min 0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 Y ( X 10 0 0 ) m/z 105.0 Manual Integration Results RT: 16.99 Area: 21393 Amount: 0.097601 Amount Units: ppb v/v 16.7 16.9 17.1 Min -1 1 3 5 7 9 11 13 15 17 19 21 23 25 27 Y ( X 10 0 0 ) m/z 105.0 1 6 . 9 9 4 Reviewer: puangmaleek, 28-Nov-2017 09:28:27 Audit Action: Assigned Compound ID Audit Reason: Assign Peak Page 226 of 478 Report Date: 28-Nov-2017 09:30:42 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#:38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 87 4-Ethyltoluene, CAS: 622-96-8 Signal: 1 Processing Integration Results Not Detected Expected RT: 16.99 16.7 16.9 17.1Min 0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 Y ( X 10 0 0 ) m/z 105.0 Manual Integration Results RT: 16.99 Area: 21393 Amount: 0.097601 Amount Units: ppb v/v 16.7 16.9 17.1 Min -1 1 3 5 7 9 11 13 15 17 19 21 23 25 27 Y ( X 10 0 0 ) m/z 105.0 1 6 . 9 9 4 Reviewer: puangmaleek, 28-Nov-2017 09:28:35 Audit Action: Manually Integrated Audit Reason: Assign Peak Page 227 of 478 Report Date: 28-Nov-2017 09:30:42 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#:38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 89 1,3,5-Trimethylbenzene, CAS: 108-67-8 Signal: 1 Processing Integration Results Not Detected Expected RT: 17.06 16.7 16.9 17.1 17.3 Min 0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 Y ( X 10 0 0 ) m/z 105.0 Manual Integration Results RT: 17.06 Area: 17610 Amount: 0.097182 Amount Units: ppb v/v 16.7 16.9 17.1 17.3 Min -1 1 3 5 7 9 11 13 15 17 19 21 23 25 27 Y ( X 10 0 0 ) m/z 105.0 1 7 . 0 5 8 Reviewer: puangmaleek, 28-Nov-2017 09:28:49 Audit Action: Assigned Compound ID Audit Reason: Assign Peak Page 228 of 478 Report Date: 28-Nov-2017 09:30:42 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#:38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 89 1,3,5-Trimethylbenzene, CAS: 108-67-8 Signal: 1 Processing Integration Results Not Detected Expected RT: 17.06 16.7 16.9 17.1 17.3Min 0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 Y ( X 10 0 0 ) m/z 105.0 Manual Integration Results RT: 17.06 Area: 17610 Amount: 0.097182 Amount Units: ppb v/v 16.7 16.9 17.1 17.3 Min -1 1 3 5 7 9 11 13 15 17 19 21 23 25 27 Y ( X 10 0 0 ) m/z 105.0 1 7 . 0 5 8 Reviewer: puangmaleek, 28-Nov-2017 09:28:53 Audit Action: Manually Integrated Audit Reason: Assign Peak Page 229 of 478 Report Date: 28-Nov-2017 09:30:42 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Cyclohexane,1,3-dimethyl-,cis-638-04-0 NIST14.L 6931 C8H16 112 97 Cyclohexane,1,3-dimethyl-591-21-9 NIST14.L 6866 C8H16 112 91 Cyclohexane,1,4-dimethyl-589-90-2 NIST14.L 6863 C8H16 112 91 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 m/z 0 10 20 30 40 50 Y ( X 10 0 0 0 )Raw Spec: Scan 1884(13.03) 97 55 11241695642709883 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113m/z 0 10 20 30 40 50 Y ( X 10 0 0 0 )28034-09[MS SCAN Spec]:Scan 1884(13.03) 97 55 11241695642709883 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #6931, Cyclohexane, 1,3-dimethyl-, cis- (from NIST14.L) 9755 41 112566942987053 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #6866, Cyclohexane, 1,3-dimethyl- (from NIST14.L) 9755 41 112695642709853 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #6863, Cyclohexane, 1,4-dimethyl- (from NIST14.L) 55 97 11241 56 6942 70 83 96 9884 Page 230 of 478 Report Date: 28-Nov-2017 09:30:43 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Cyclohexane,1,4-dimethyl-,trans-2207-04-7 NIST14.L 6940 C8H16 112 97 Cyclohexane,1,4-dimethyl-589-90-2 NIST14.L 6869 C8H16 112 95 Cyclohexane,1,4-dimethyl-,cis-624-29-3 NIST14.L 6922 C8H16 112 94 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 m/z 0 6 12 18 24 Y ( X 10 0 0 0 )Raw Spec: Scan 2012(13.72) 9755 11256416942709683988453 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113m/z 0 6 12 18 24 Y ( X 10 0 0 0 )28034-09[MS SCAN Spec]:Scan 2012(13.72) 9755 11256416942709683988453 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #6940, Cyclohexane, 1,4-dimethyl-, trans- (from NIST14.L) 55 97 41 112 56 6942 967083 985384 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #6869, Cyclohexane, 1,4-dimethyl- (from NIST14.L) 55 97 41 1125669427096538398 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #6922, Cyclohexane, 1,4-dimethyl-, cis- (from NIST14.L) 55 97 41 112564269708396849853 Page 231 of 478 Report Date: 28-Nov-2017 09:30:43 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Cyclohexane,1,3,5-trimethyl-1839-63-0 NIST14.L 11834 C9H18 126 97 Cyclohexane,1,3,5-trimethyl-, (1.alpha.,3.alpha 1795-27-3 NIST14.L 11879 C9H18 126 94 Cyclohexane,1,3,5-trimethyl-, (1.alpha.,3.alpha 1795-26-2 NIST14.L 11876 C9H18 126 60 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 117 121 125 129 m/z 0 7 14 21 28 Y ( X 10 0 0 0 )Raw Spec: Scan 2114(14.26) 69 111 55 41 126567068421128384 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 117 121 125 129m/z 0 7 14 21 28 Y ( X 10 0 0 0 )28034-09[MS SCAN Spec]:Scan 2114(14.26) 69 111 55 41 126567068421128384 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 117 121 125 129 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11834, Cyclohexane, 1,3,5-trimethyl- (from NIST14.L) 11169 55 41 12656704311283 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 117 121 125 129 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11879, Cyclohexane, 1,3,5-trimethyl-, (1.alpha.,3.alpha.,5.alpha.)- (from NIST14.L) 69 111 55 41 126 5642 7067 11253 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 117 121 125 129 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11876, Cyclohexane, 1,3,5-trimethyl-, (1.alpha.,3.alpha.,5.beta.)- (from NIST14.L) 69 11155 41 1264256 7053 83 1126784 Page 232 of 478 Report Date: 28-Nov-2017 09:30:43 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Cyclohexane,ethyl-1678-91-7 NIST14.L 6791 C8H16 112 95 3,4-Dimethyl-2-hexene 2213-37-8 NIST14.L 6819 C8H16 112 76 Cyclohexane,propyl-1678-92-8 NIST14.L 11775 C9H18 126 64 36 40 44 48 52 56 60 64 68 72 76 80 84 88 92 96 100 104 108 112 116 120 124 128 m/z 0 10 20 30 40 50 Y ( X 10 0 0 0 )Raw Spec: Scan 2138(14.39) 8355 82 41 11256676984429754 36 40 44 48 52 56 60 64 68 72 76 80 84 88 92 96 100 104 108 112 116 120 124 128m/z 0 10 20 30 40 50 Y ( X 10 0 0 0 )28034-09[MS SCAN Spec]:Scan 2138(14.39) 8355 82 41 11256676984429754 36 40 44 48 52 56 60 64 68 72 76 80 84 88 92 96 100 104 108 112 116 120 124 128 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #6791, Cyclohexane, ethyl- (from NIST14.L) 83 55 82 41 1125667426984 36 40 44 48 52 56 60 64 68 72 76 80 84 88 92 96 100 104 108 112 116 120 124 128 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #6819, 3,4-Dimethyl-2-hexene (from NIST14.L) 55 83 41 112 43 69 845653 97 36 40 44 48 52 56 60 64 68 72 76 80 84 88 92 96 100 104 108 112 116 120 124 128 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11775, Cyclohexane, propyl- (from NIST14.L) 83 55 82 41 126675669844354 Page 233 of 478 Report Date: 28-Nov-2017 09:30:44 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Cyclohexane,1,1,3-trimethyl-3073-66-3 NIST14.L 11835 C9H18 126 94 Cyclohexane,1,3,5-trimethyl-, (1.alpha.,3.alpha 1795-27-3 NIST14.L 11878 C9H18 126 64 Cyclohexane,1,2,4-trimethyl-2234-75-5 NIST14.L 11819 C9H18 126 50 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 117 121 125 129 m/z 0 12 24 36 48 60 Y ( X 10 0 0 0 )Raw Spec: Scan 2148(14.44) 11169 55 41 56 837043 84 112976753 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 117 121 125 129m/z 0 12 24 36 48 60 Y ( X 10 0 0 0 )28034-09[MS SCAN Spec]:Scan 2148(14.44) 11169 55 41 56 837043 84 112976753 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 117 121 125 129 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11835, Cyclohexane, 1,1,3-trimethyl- (from NIST14.L) 111 69 5541 8356 43 70 1125367 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 117 121 125 129 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11878, Cyclohexane, 1,3,5-trimethyl-, (1.alpha.,3.alpha.,5.alpha.)- (from NIST14.L) 11169 55 41 1264256701125367 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 117 121 125 129 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11819, Cyclohexane, 1,2,4-trimethyl- (from NIST14.L) 69 111 55 41 1265670844367539711257 Page 234 of 478 Report Date: 28-Nov-2017 09:30:44 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Unknown Octane,4-methyl-2216-34-4 NIST14.L 12942 C9H20 128 72 Hexane,3-ethyl-619-99-8 NIST14.L 7761 C8H18 114 64 Octane,2-methyl-3221-61-2 NIST14.L 12950 C9H20 128 64 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 15 30 45 60 75 Y ( X 10 0 0 0 )Raw Spec: Scan 2192(14.68) 43 57 71 85417056 39 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 15 30 45 60 75 Y ( X 10 0 0 0 )28034-09[MS SCAN Spec]:Scan 2192(14.68) 43 57 71 85417056 39 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #12942, Octane, 4-methyl- (from NIST14.L) 43 85714157 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #7761, Hexane, 3-ethyl- (from NIST14.L) 43 85417157 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #12950, Octane, 2-methyl- (from NIST14.L) 43 57 71 8541 56 1133969 128 Page 235 of 478 Report Date: 28-Nov-2017 09:30:44 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Cyclohexane,1,2,4-trimethyl-, (1.alpha.,2.beta.7667-60-9 NIST14.L 11870 C9H18 126 94 Cyclohexane,1,3,5-trimethyl-, (1.alpha.,3.alpha 1795-26-2 NIST14.L 11876 C9H18 126 90 Cyclohexane,1,2,4-trimethyl-2234-75-5 NIST14.L 11829 C9H18 126 90 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 11 22 33 44 55 Y ( X 10 0 0 0 )Raw Spec: Scan 2207(14.76) 11169 55 126415670438411297 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210m/z 0 11 22 33 44 55 Y ( X 10 0 0 0 )28034-09[MS SCAN Spec]:Scan 2207(14.76) 11169 55 126415670438411297 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11870, Cyclohexane, 1,2,4-trimethyl-, (1.alpha.,2.beta.,4.beta.)- (from NIST14.L) 69 111 55 41 126395670428411297 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11876, Cyclohexane, 1,3,5-trimethyl-, (1.alpha.,3.alpha.,5.beta.)- (from NIST14.L) 69 11155 41 39 1264256 70 83 112 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11829, Cyclohexane, 1,2,4-trimethyl- (from NIST14.L) 6955 11141 5643 126397084976753112 Page 236 of 478 Report Date: 28-Nov-2017 09:30:44 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Octane,3-methyl-2216-33-3 NIST14.L 12944 C9H20 128 90 Heptane,2,5-dimethyl-2216-30-0 NIST14.L 12977 C9H20 128 72 Heptane,4-(1-methylethyl)-52896-87-4 NIST14.L 19714 C10H22 142 59 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 2 4 6 8 10 Y ( X 10 0 0 0 0 )Raw Spec: Scan 2223(14.84) 57 43 56 98 9971 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210m/z 0 2 4 6 8 10 Y ( X 10 0 0 0 0 )28034-09[MS SCAN Spec]:Scan 2223(14.84) 57 43 56 98 9971 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #12944, Octane, 3-methyl- (from NIST14.L) 57 43 56 98 9971 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #12977, Heptane, 2,5-dimethyl- (from NIST14.L) 57 43 56 71 99 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #19714, Heptane, 4-(1-methylethyl)- (from NIST14.L) 57 43 98 5639 69 9970 Page 237 of 478 Report Date: 28-Nov-2017 09:30:44 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Cyclohexane,1,2,4-trimethyl-2234-75-5 NIST14.L 11819 C9H18 126 93 Cyclohexane,1,2,3-trimethyl-, (1.alpha.,2.beta.1678-81-5 NIST14.L 11873 C9H18 126 93 Cyclohexane,1,1,2-trimethyl-7094-26-0 NIST14.L 11825 C9H18 126 74 30 50 70 90 110 130 150 170 190 210 230 250 m/z 0 6 12 18 24 30 Y ( X 10 0 0 0 )Raw Spec: Scan 2304(15.28) 69 11155 5641 70 126824339975771112 30 50 70 90 110 130 150 170 190 210 230 250m/z 0 6 12 18 24 30 Y ( X 10 0 0 0 )28034-09[MS SCAN Spec]:Scan 2304(15.28) 69 11155 5641 70 126824339975771112 30 50 70 90 110 130 150 170 190 210 230 250 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11819, Cyclohexane, 1,2,4-trimethyl- (from NIST14.L) 69 111 55 41 12656397084436797112 30 50 70 90 110 130 150 170 190 210 230 250 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11873, Cyclohexane, 1,2,3-trimethyl-, (1.alpha.,2.beta.,3.alpha.)- (from NIST14.L) 69 55 11141 56 70 126833943678297112 30 50 70 90 110 130 150 170 190 210 230 250 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11825, Cyclohexane, 1,1,2-trimethyl- (from NIST14.L) 69 41 56 111 39 57 7043 126836798 Page 238 of 478 Report Date: 28-Nov-2017 09:30:45 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-09.D Injection Date: 24-Nov-2017 16:40:30 Instrument ID: CHB.i Lims ID: 200-41113-A-2 Lab Sample ID: 200-41113-2 Client ID: SV-2 Operator ID: VTP ALS Bottle#: 9 Worklist Smp#: 38 Purge Vol: 200.000 mL Dil. Factor: 2.9800 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Unknown 2-Hexene,3,4,4-trimethyl-53941-19-8 NIST14.L 11806 C9H18 126 81 Cyclohexane,1-ethyl-2-methyl-3728-54-9 NIST14.L 11840 C9H18 126 80 1-Ethyl-4-methylcyclohexane 3728-56-1 NIST14.L 11812 C9H18 126 76 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 5 10 15 20 25 Y ( X 10 0 0 0 )Raw Spec: Scan 2411(15.85) 9755 6941 1267043579698 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 5 10 15 20 25 Y ( X 10 0 0 0 )28034-09[MS SCAN Spec]:Scan 2411(15.85) 9755 6941 1267043579698 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11806, 2-Hexene, 3,4,4-trimethyl- (from NIST14.L) 9755 41 69 4339 1265798 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11840, Cyclohexane, 1-ethyl-2-methyl- (from NIST14.L) 9755 41 69 96 126984270 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11812, 1-Ethyl-4-methylcyclohexane (from NIST14.L) 9755 41 69 12696984381 Page 239 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: SV-1 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-3 TestAmerica Burlington Matrix:28034-10.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 00:00 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:2.5 Level: (low/med)Low 80(mL) 0.32(mm) Date Analyzed:11/24/2017 17:32 ID:RTX-624 Analysis Batch No.:123710 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 120.9175-71-8 Dichlorodifluoromethane 1.3 U 1.3 86.4775-45-6 Freon 22 1.3 U 1.3 170.9276-14-2 1,2-Dichlorotetrafluoroe thane 0.50 U 0.50 50.4974-87-3 Chloromethane 1.3 U 1.3 58.12106-97-8 n-Butane 44 1.3 62.5075-01-4 Vinyl chloride 0.088 U 0.088 54.09106-99-0 1,3-Butadiene 3.3 0.50 94.9474-83-9 Bromomethane 0.50 U 0.50 64.5275-00-3 Chloroethane 1.3 U 1.3 106.96593-60-2 Bromoethene(Vinyl Bromide) 0.50 U 0.50 137.3775-69-4 Trichlorofluoromethane 0.50 U 0.50 187.3876-13-1 Freon TF 0.50 U 0.50 96.9475-35-4 1,1-Dichloroethene 0.088 U 0.088 58.0867-64-1 Acetone 13 U 13 60.1067-63-0 Isopropyl alcohol 13 U 13 76.1475-15-0 Carbon disulfide 5.2 1.3 76.53107-05-1 3-Chloropropene 1.3 U 1.3 84.9375-09-2 Methylene Chloride 1.3 U 1.3 74.1275-65-0 tert-Butyl alcohol 13 U 13 88.151634-04-4 Methyl tert-butyl ether 0.50 U 0.50 96.94156-60-5 trans-1,2-Dichloroethene 0.50 U 0.50 86.17110-54-3 n-Hexane 1.5 0.50 98.9675-34-3 1,1-Dichloroethane 0.50 U 0.50 72.1178-93-3 Methyl Ethyl Ketone 1.4 1.3 96.94156-59-2 cis-1,2-Dichloroethene 0.088 U 0.088 96.94540-59-0 1,2-Dichloroethene, Total 1.0 U 1.0 119.3867-66-3 Chloroform 2.3 0.50 72.11109-99-9 Tetrahydrofuran 13 U 13 133.4171-55-6 1,1,1-Trichloroethane 0.50 U 0.50 84.16110-82-7 Cyclohexane 0.73 0.50 153.8156-23-5 Carbon tetrachloride 0.088 U 0.088 114.23540-84-1 2,2,4-Trimethylpentane 0.50 U 0.50 78.1171-43-2 Benzene 1.6 0.50 98.96107-06-2 1,2-Dichloroethane 0.50 U 0.50 FORM I TO-15 Page 240 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: SV-1 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-3 TestAmerica Burlington Matrix:28034-10.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 00:00 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:2.5 Level: (low/med)Low 80(mL) 0.32(mm) Date Analyzed:11/24/2017 17:32 ID:RTX-624 Analysis Batch No.:123710 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 100.21142-82-5 n-Heptane 0.74 0.50 131.3979-01-6 Trichloroethene 0.088 U 0.088 100.1280-62-6 Methyl methacrylate 1.3 U 1.3 112.9978-87-5 1,2-Dichloropropane 0.50 U 0.50 88.11123-91-1 1,4-Dioxane 13 U 13 163.8375-27-4 Bromodichloromethane 0.50 U 0.50 110.9710061-01-5 cis-1,3-Dichloropropene 0.50 U 0.50 100.16108-10-1 methyl isobutyl ketone 1.3 U 1.3 92.14108-88-3 Toluene 4.4 0.50 110.9710061-02-6 trans-1,3-Dichloropropen e 0.50 U 0.50 133.4179-00-5 1,1,2-Trichloroethane 0.50 U 0.50 165.83127-18-4 Tetrachloroethene 0.50 U 0.50 100.20591-78-6 Methyl Butyl Ketone (2-Hexanone) 1.3 U 1.3 208.29124-48-1 Dibromochloromethane 0.50 U 0.50 187.87106-93-4 1,2-Dibromoethane 0.50 U 0.50 112.56108-90-7 Chlorobenzene 0.50 U 0.50 106.17100-41-4 Ethylbenzene 9.1 0.50 106.17179601-23-1 m,p-Xylene 36 1.3 106.1795-47-6 Xylene, o-12 0.50 106.171330-20-7 Xylene (total)48 1.8 104.15100-42-5 Styrene 0.50 U 0.50 252.7575-25-2 Bromoform 0.50 U 0.50 120.1998-82-8 Cumene 0.50 U 0.50 167.8579-34-5 1,1,2,2-Tetrachloroethan e 0.50 U 0.50 120.19103-65-1 n-Propylbenzene 0.50 U 0.50 120.20622-96-8 4-Ethyltoluene 0.50 U 0.50 120.20108-67-8 1,3,5-Trimethylbenzene 0.50 U 0.50 126.5995-49-8 2-Chlorotoluene 0.50 U 0.50 134.2298-06-6 tert-Butylbenzene 0.50 U 0.50 120.2095-63-6 1,2,4-Trimethylbenzene 0.93 0.50 134.22135-98-8 sec-Butylbenzene 0.50 U 0.50 134.2299-87-6 4-Isopropyltoluene 0.50 U 0.50 147.00541-73-1 1,3-Dichlorobenzene 0.50 U 0.50 147.00106-46-7 1,4-Dichlorobenzene 0.50 U 0.50 FORM I TO-15 Page 241 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: SV-1 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-3 TestAmerica Burlington Matrix:28034-10.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 00:00 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:2.5 Level: (low/med)Low 80(mL) 0.32(mm) Date Analyzed:11/24/2017 17:32 ID:RTX-624 Analysis Batch No.:123710 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 126.58100-44-7 Benzyl chloride 0.50 U 0.50 134.22104-51-8 n-Butylbenzene 0.50 U 0.50 147.0095-50-1 1,2-Dichlorobenzene 0.50 U 0.50 181.45120-82-1 1,2,4-Trichlorobenzene 1.3 U 1.3 260.7687-68-3 Hexachlorobutadiene 0.50 U 0.50 128.1791-20-3 Naphthalene 1.3 U 1.3 FORM I TO-15 Page 242 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: SV-1 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-3 TestAmerica Burlington Matrix:28034-10.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 00:00 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:2.5 Level: (low/med)Low 80(mL) 0.32(mm) Date Analyzed:11/24/2017 17:32 ID:RTX-624 Analysis Batch No.:123710 ug/m3Units: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 120.9175-71-8 Dichlorodifluoromethane 6.2 U 6.2 86.4775-45-6 Freon 22 4.4 U 4.4 170.9276-14-2 1,2-Dichlorotetrafluoroe thane 3.5 U 3.5 50.4974-87-3 Chloromethane 2.6 U 2.6 58.12106-97-8 n-Butane 110 3.0 62.5075-01-4 Vinyl chloride 0.22 U 0.22 54.09106-99-0 1,3-Butadiene 7.3 1.1 94.9474-83-9 Bromomethane 1.9 U 1.9 64.5275-00-3 Chloroethane 3.3 U 3.3 106.96593-60-2 Bromoethene(Vinyl Bromide) 2.2 U 2.2 137.3775-69-4 Trichlorofluoromethane 2.8 U 2.8 187.3876-13-1 Freon TF 3.8 U 3.8 96.9475-35-4 1,1-Dichloroethene 0.35 U 0.35 58.0867-64-1 Acetone 30 U 30 60.1067-63-0 Isopropyl alcohol 31 U 31 76.1475-15-0 Carbon disulfide 16 3.9 76.53107-05-1 3-Chloropropene 3.9 U 3.9 84.9375-09-2 Methylene Chloride 4.3 U 4.3 74.1275-65-0 tert-Butyl alcohol 38 U 38 88.151634-04-4 Methyl tert-butyl ether 1.8 U 1.8 96.94156-60-5 trans-1,2-Dichloroethene 2.0 U 2.0 86.17110-54-3 n-Hexane 5.4 1.8 98.9675-34-3 1,1-Dichloroethane 2.0 U 2.0 72.1178-93-3 Methyl Ethyl Ketone 4.2 3.7 96.94156-59-2 cis-1,2-Dichloroethene 0.35 U 0.35 96.94540-59-0 1,2-Dichloroethene, Total 4.0 U 4.0 119.3867-66-3 Chloroform 11 2.4 72.11109-99-9 Tetrahydrofuran 37 U 37 133.4171-55-6 1,1,1-Trichloroethane 2.7 U 2.7 84.16110-82-7 Cyclohexane 2.5 1.7 153.8156-23-5 Carbon tetrachloride 0.55 U 0.55 114.23540-84-1 2,2,4-Trimethylpentane 2.3 U 2.3 78.1171-43-2 Benzene 5.1 1.6 98.96107-06-2 1,2-Dichloroethane 2.0 U 2.0 FORM I TO-15 Page 243 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: SV-1 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-3 TestAmerica Burlington Matrix:28034-10.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 00:00 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:2.5 Level: (low/med)Low 80(mL) 0.32(mm) Date Analyzed:11/24/2017 17:32 ID:RTX-624 Analysis Batch No.:123710 ug/m3Units: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 100.21142-82-5 n-Heptane 3.1 2.0 131.3979-01-6 Trichloroethene 0.47 U 0.47 100.1280-62-6 Methyl methacrylate 5.1 U 5.1 112.9978-87-5 1,2-Dichloropropane 2.3 U 2.3 88.11123-91-1 1,4-Dioxane 45 U 45 163.8375-27-4 Bromodichloromethane 3.4 U 3.4 110.9710061-01-5 cis-1,3-Dichloropropene 2.3 U 2.3 100.16108-10-1 methyl isobutyl ketone 5.1 U 5.1 92.14108-88-3 Toluene 17 1.9 110.9710061-02-6 trans-1,3-Dichloropropen e 2.3 U 2.3 133.4179-00-5 1,1,2-Trichloroethane 2.7 U 2.7 165.83127-18-4 Tetrachloroethene 3.4 U 3.4 100.20591-78-6 Methyl Butyl Ketone (2-Hexanone) 5.1 U 5.1 208.29124-48-1 Dibromochloromethane 4.3 U 4.3 187.87106-93-4 1,2-Dibromoethane 3.8 U 3.8 112.56108-90-7 Chlorobenzene 2.3 U 2.3 106.17100-41-4 Ethylbenzene 40 2.2 106.17179601-23-1 m,p-Xylene 150 5.4 106.1795-47-6 Xylene, o-53 2.2 106.171330-20-7 Xylene (total)210 7.6 104.15100-42-5 Styrene 2.1 U 2.1 252.7575-25-2 Bromoform 5.2 U 5.2 120.1998-82-8 Cumene 2.5 U 2.5 167.8579-34-5 1,1,2,2-Tetrachloroethan e 3.4 U 3.4 120.19103-65-1 n-Propylbenzene 2.5 U 2.5 120.20622-96-8 4-Ethyltoluene 2.5 U 2.5 120.20108-67-8 1,3,5-Trimethylbenzene 2.5 U 2.5 126.5995-49-8 2-Chlorotoluene 2.6 U 2.6 134.2298-06-6 tert-Butylbenzene 2.7 U 2.7 120.2095-63-6 1,2,4-Trimethylbenzene 4.6 2.5 134.22135-98-8 sec-Butylbenzene 2.7 U 2.7 134.2299-87-6 4-Isopropyltoluene 2.7 U 2.7 147.00541-73-1 1,3-Dichlorobenzene 3.0 U 3.0 147.00106-46-7 1,4-Dichlorobenzene 3.0 U 3.0 FORM I TO-15 Page 244 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: SV-1 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-3 TestAmerica Burlington Matrix:28034-10.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 00:00 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:2.5 Level: (low/med)Low 80(mL) 0.32(mm) Date Analyzed:11/24/2017 17:32 ID:RTX-624 Analysis Batch No.:123710 ug/m3Units: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 126.58100-44-7 Benzyl chloride 2.6 U 2.6 134.22104-51-8 n-Butylbenzene 2.7 U 2.7 147.0095-50-1 1,2-Dichlorobenzene 3.0 U 3.0 181.45120-82-1 1,2,4-Trichlorobenzene 9.3 U 9.3 260.7687-68-3 Hexachlorobutadiene 5.3 U 5.3 128.1791-20-3 Naphthalene 6.6 U 6.6 FORM I TO-15 Page 245 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS Client Sample ID: Lab Name:Job No.: SV-1 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-3 TestAmerica Burlington Matrix:28034-10.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 00:00 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:2.5 Level: (low/med)Low 80(mL) 0.32(mm) Date Analyzed:11/24/2017 17:32 ID:RTX-624 Analysis Batch No.:123710 ppb v/vUnits: Number TICs Found:TIC Result Total:94.610 QRTCOMPOUND NAME RESULTCAS NO.MATCH QUALITY 3.44 J N75-28-5 Isobutane 9.4 86% 13.04 J N624-29-3 Cyclohexane, 1,4-dimethyl-, cis-13 91% 13.72 J N2207-04-7 Cyclohexane, 1,4-dimethyl-, trans-6.6 97% 14.39 J N1678-91-7 Cyclohexane, ethyl-8.2 95% 14.44 J N3073-66-3 Cyclohexane, 1,1,3-trimethyl-12 94% 14.67 JUnknown12 14.75 J N7667-60-9 Cyclohexane, 1,2,4-trimethyl-, (1.alpha.,2.beta.,4.beta.)- 8.9 94% 14.84 J N2216-33-3 Octane, 3-methyl-10 90% 15.27 J N1678-81-5 Cyclohexane, 1,2,3-trimethyl-, (1.alpha.,2.beta.,3.alpha.)- 6.6 93% 15.85 JUnknown7.9 FORM I-TIC TO-15 Page 246 of 478 Report Date: 28-Nov-2017 09:36:53 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Target Compound Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Lims ID: 200-41113-A-3 Client ID: SV-1 Sample Type: Client Inject. Date: 24-Nov-2017 17:32:30 ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol:200.000 mL Dil. Factor: 2.5000 Sample Info: 200-0028034-010 Misc. Info.: 41113-03 Operator ID: VTP Instrument ID: CHB.i Method:\\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\TO15_LLNJ_TO3.m Limit Group: AI_TO15_ICAL Last Update: 28-Nov-2017 09:36:51 Calib Date: 07-Nov-2017 01:49:30 Integrator: RTE ID Type: Deconvolution ID Quant Method: Internal/External Standard Quant By: Initial Calibration Last ICal File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-13.D Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host:XAWRK022 First Level Reviewer: puangmaleek Date:28-Nov-2017 09:36:50 Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response OnCol Amt ppb v/v Flags 2 Dichlorodifluoromethane 85 3.199 3.193 0.006 98 12364 0.1476 3 Chlorodifluoromethane 51 3.231 3.225 0.006 95 3964 0.0832 4 1,2-Dichloro-1,1,2,2-tetra 85 3.412 ND 5 Chloromethane 50 3.535 3.535 0.000 25 2428 0.0813 7 6 Butane 43 3.711 3.711 0.000 99 912847 17.7 7 Vinyl chloride 62 3.748 ND 8 Butadiene 54 3.812 3.812 0.000 95 34572 1.31 10 Bromomethane 94 4.479 ND 11 Chloroethane 64 4.709 ND 13 Vinyl bromide 106 5.120 ND 14 Trichlorofluoromethane 101 5.227 5.227 0.011 1 5564 0.0623 7M 19 1,1,2-Trichloro-1,2,2-trif 101 6.246 ND 20 1,1-Dichloroethene 96 6.315 ND 21 Acetone 43 6.475 6.465 0.010 96 170872 3.04 22 Isopropyl alcohol 45 6.683 ND 23 Carbon disulfide 76 6.742 6.748 -0.006 100 220512 2.09 24 3-Chloro-1-propene 41 7.014 ND 27 Methylene Chloride 49 7.271 7.271 -0.005 15 2704 0.0600 7 28 2-Methyl-2-propanol 59 7.383 ND 29 Methyl tert-butyl ether 73 7.623 ND 30 trans-1,2-Dichloroethene 61 7.687 ND 32 Hexane 57 8.018 8.012 0.006 95 41999 0.6120 33 1,1-Dichloroethane 63 8.423 ND 36 2-Butanone (MEK) 72 9.320 9.315 0.005 99 12573 0.5681 37 cis-1,2-Dichloroethene 96 9.331 ND * 39 Chlorobromomethane 128 9.694 9.699 -0.005 92 378133 10.0 38 Tetrahydrofuran 42 9.710 ND 40 Chloroform 83 9.768 9.774 -0.006 94 74318 0.9119 S 41 1,2-Dichloroethene, Total 61 10.000 ND 42 1,1,1-Trichloroethane 97 10.030 ND 43 Cyclohexane 84 10.046 10.046 0.000 96 17415 0.2926 Page 247 of 478 Report Date: 28-Nov-2017 09:36:53 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response OnCol Amt ppb v/v Flags 44 Carbon tetrachloride 117 10.227 10.227 -0.011 1 893 0.0119 7 45 Isooctane 57 10.521 ND 46 Benzene 78 10.558 10.563 -0.005 94 89132 0.6415 47 1,2-Dichloroethane 62 10.659 ND 48 n-Heptane 43 10.772 10.772 0.000 92 25642 0.2977 * 50 1,4-Difluorobenzene 114 11.103 11.102 0.001 94 1889521 10.0 53 Trichloroethene 95 11.476 ND 54 1,2-Dichloropropane 63 11.839 ND 55 Methyl methacrylate 69 11.876 ND 56 1,4-Dioxane 88 11.967 ND 58 Dichlorobromomethane 83 12.197 12.202 -0.005 63 9280 0.0994 60 cis-1,3-Dichloropropene 75 12.826 ND 61 4-Methyl-2-pentanone (MIBK 43 12.976 ND 64 Toluene 92 13.253 13.259 -0.006 93 169137 1.77 66 trans-1,3-Dichloropropene 75 13.621 ND 67 1,1,2-Trichloroethane 83 13.888 ND 68 Tetrachloroethene 166 14.032 ND 69 2-Hexanone 43 14.150 ND 70 Chlorodibromomethane 129 14.449 ND 71 Ethylene Dibromide 107 14.646 ND * 72 Chlorobenzene-d5 117 15.212 15.212 0.000 84 1601689 10.0 73 Chlorobenzene 112 15.249 ND 74 Ethylbenzene 91 15.319 15.319 0.000 98 765899 3.65 76 m-Xylene & p-Xylene 106 15.463 15.468 -0.005 0 1178281 14.3 78 o-Xylene 106 15.975 15.975 0.000 99 397596 4.84 S 77 Xylenes, Total 106 0 19.1 79 Styrene 104 16.002 ND 80 Bromoform 173 16.295 ND 81 Isopropylbenzene 105 16.386 16.391 -0.005 87 31875 0.1372 83 1,1,2,2-Tetrachloroethane 83 16.797 ND 84 N-Propylbenzene 91 16.866 16.866 0.000 1 32379 0.1131 M 87 4-Ethyltoluene 105 16.989 16.994 -0.005 76 32067 0.1408 88 2-Chlorotoluene 91 17.037 ND 89 1,3,5-Trimethylbenzene 105 17.059 17.059 0.001 65 23905 0.1270 M 91 tert-Butylbenzene 119 17.437 ND 92 1,2,4-Trimethylbenzene 105 17.502 17.507 -0.005 98 69360 0.3729 93 sec-Butylbenzene 105 17.688 17.688 -0.006 57 9362 0.0331 7 94 4-Isopropyltoluene 119 17.843 17.843 0.000 37 5701 0.0245 7 95 1,3-Dichlorobenzene 146 17.923 ND 96 1,4-Dichlorobenzene 146 18.035 ND 97 Benzyl chloride 91 18.185 ND 99 n-Butylbenzene 91 18.350 ND 100 1,2-Dichlorobenzene 146 18.521 ND 103 1,2,4-Trichlorobenzene 180 20.880 ND 104 Hexachlorobutadiene 225 21.045 ND 105 Naphthalene 128 21.365 21.365 0.005 1 4291 0.0281 7 Page 248 of 478 Report Date: 28-Nov-2017 09:36:53 Chrom Revision: 2.2 13-Nov-2017 17:19:06 QC Flag Legend Processing Flags 7 - Failed Limit of Detection Review Flags M - Manually Integrated Reagents: ATTO15BISs_00006 Amount Added: 20.00 Units: mL Run Reagent Page 249 of 478 Report Date: 28-Nov-2017 09:36:53 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Tentatively Identified Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Lims ID: 200-41113-A-3 Client ID: SV-1 Sample Type: Client Inject. Date: 24-Nov-2017 17:32:30 ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Sample Info: 200-0028034-010 Misc. Info.: 41113-03 Operator ID: VTP Instrument ID: CHB.i Method:\\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\TO15_LLNJ_TO3.m Limit Group: AI_TO15_ICAL Last Update: 28-Nov-2017 09:36:51 Calib Date: 07-Nov-2017 01:49:30 Tic RT Window: 0.000 -0.000 Response: area Quant By: Nearest ISTD Quant LOD: 10.00000 MS Library: \\ChromNA\Burlington\Database\NIST14.L Min. Match: 1 Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host:XAWRK022 First Level Reviewer: puangmaleek Date:28-Nov-2017 09:36:50 Tentative Identified Compound Results RT Area Amount ppb v/v Quant Cpnd Qual Lib Entry Molecular Formula Mol. Weight Flags 75-28-5 Isobutane 3.439 890117 3.74 39 86 237 C4H10 58 624-29-3 Cyclohexane, 1,4-dimethyl-, cis- 13.035 2057499 5.17 50 91 6928 C8H16 112 2207-04-7 Cyclohexane, 1,4-dimethyl-, trans- 13.718 1201884 2.64 72 97 6940 C8H16 112 1678-91-7 Cyclohexane, ethyl- 14.385 1493783 3.28 72 95 6789 C8H16 112 3073-66-3 Cyclohexane, 1,1,3-trimethyl- 14.443 2172862 4.77 72 94 11835 C9H18 126 Unknown 14.673 2143465 4.70 72 0 0 0 7667-60-9 Cyclohexane, 1,2,4-trimethyl-, (1.alpha.,2.beta.,4.beta.)- 14.753 1620061 3.56 72 94 11871 C9H18 126 2216-33-3 Octane, 3-methyl- 14.838 1832983 4.02 72 90 12944 C9H20 128 1678-81-5 Cyclohexane, 1,2,3-trimethyl-, (1.alpha.,2.beta.,3.alpha.)- 15.271 1196910 2.63 72 93 11873 C9H18 126 Unknown 15.847 1445540 3.17 72 0 0 0 Page 250 of 478 Report Date: 28-Nov-2017 09:36:53 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Quantitation Compounds Compound RT Area Amount ppb v/v * 39 Chlorobromomethane 9.694 2377702 10.0 * 50 1,4-Difluorobenzene 11.097 3977074 10.0 * 72 Chlorobenzene-d5 15.212 4555972 10.0 QC Flag Legend Processing Flags Reagents: ATTO15BISs_00006 Amount Added: 20.00 Units: mL Run Reagent Page 251 of 478 Report Date: 28-Nov-2017 09:36:53 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Operator ID: VTP Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Worklist Smp#: 39 Client ID: SV-1 Purge Vol: 200.000 mL Dil. Factor: 2.5000 ALS Bottle#: 10 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Y Scaling: Method Defined: Scale to the Nth Largest Target: 1 2.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 18.0 20.0 22.0 24.0 Min 0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 Y ( X 10 0 0 0 0 ) 28034-10[MS SCAN Chro]:Total * C h l o r o b r o m o m e t h a n e ( 9 . 6 9 4 ) * 1 ,4- D i f lu o r o b e n z en e ( 1 1 . 0 9 7 ) * C h l o r o b e n z en e - d 5 ( 1 5 . 2 1 2 ) Page 252 of 478 Report Date: 28-Nov-2017 09:36:53 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 6 Butane, CAS: 106-97-8 35 39 43 47 51 55 59 63 67 71 75 m/z 0 6 12 18 24 30 36 42 Y ( X 10 0 0 0 ) Raw Spec:Scan 137(3.71) 43 41 5839 35 39 43 47 51 55 59 63 67 71 75m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 137(3.71), Qvalue=99 43 41 5839 35 39 43 47 51 55 59 63 67 71 75 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 6 Butane (DATA) 43 41 39 58 35 39 43 47 51 55 59 63 67 71 75 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 3.710 min.(Qvalue: 99) 58 42 3.2 3.5 3.8 4.1 Min 0 6 12 18 24 30 36 42 Y ( X 10 0 0 0 ) m/z 43.0 3 . 7 1 1 3.1 3.4 3.7 4.0Min 0 3 6 9 12 15 18 21 Y ( X 10 0 0 0 ) m/z 41.0 3 . 6 8 4 3.2 3.5 3.8 4.1 Min 0 9 18 27 36 45 54 63 Y ( X 10 0 0 ) m/z 58.0 3 . 7 1 1 3.1 3.4 3.7 4.0 4.3 Min 0 8 16 24 32 40 Y ( X 10 0 0 0 ) m/z 43.0 m/z 41.0 m/z 58.0 Page 253 of 478 Report Date: 28-Nov-2017 09:36:53 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 8 Butadiene, CAS: 106-99-0 30 50 70 90 110 130 150 170 190 210 m/z 0 3 6 9 12 15 18 Y ( X 10 0 0 ) Raw Spec:Scan 156(3.81) 54 53 57 30 50 70 90 110 130 150 170 190 210m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 156(3.81), Qvalue=95 54 53 57 30 50 70 90 110 130 150 170 190 210 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 8 Butadiene (DATA) 54 53 30 50 70 90 110 130 150 170 190 210 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 3.820 min.(Qvalue: 95) 57 54 3.3 3.6 3.9 4.2 Min 0 3 6 9 12 15 18 Y ( X 10 0 0 ) m/z 54.0 3 . 8 1 2 Page 254 of 478 Report Date: 28-Nov-2017 09:36:53 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 23 Carbon disulfide, CAS: 75-15-0 30 50 70 90 110 130 150 170 190 210 m/z 0 11 22 33 44 55 66 77 Y ( X 10 0 0 ) Raw Spec:Scan 705(6.74) 76 44 78 30 50 70 90 110 130 150 170 190 210m/z 0 11 22 33 44 55 66 77 Y ( X 10 0 0 ) Enhanced Spec:Scan 705(6.74), Qvalue=100 76 44 78 30 50 70 90 110 130 150 170 190 210 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 23 Carbon disulfide (NIST) 76 44 78 30 50 70 90 110 130 150 170 190 210 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 705 @ 6.742 min.(Qvalue:100) 78 6.2 6.5 6.8 7.1 Min 0 11 22 33 44 55 66 77 Y ( X 10 0 0 ) m/z 76.0 6 . 7 4 2 Page 255 of 478 Report Date: 28-Nov-2017 09:36:54 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 32 Hexane, CAS: 110-54-3 39 43 47 51 55 59 63 67 71 75 79 83 87 m/z 0 2 4 6 8 10 12 14 Y ( X 10 0 0 ) Raw Spec:Scan 944(8.02) 57 43 56 86 55 71 72 39 43 47 51 55 59 63 67 71 75 79 83 87m/z 0 2 4 6 8 10 12 14 Y ( X 10 0 0 ) Enhanced Spec:Scan 944(8.02), Qvalue=95 57 43 56 86 55 71 72 39 43 47 51 55 59 63 67 71 75 79 83 87 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 32 Hexane (NIST) 57 43 56 86 55 39 43 47 51 55 59 63 67 71 75 79 83 87 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 944 @ 8.018 min.(Qvalue: 95) 5641 86 7.5 7.8 8.1 8.4 Min 0 2 4 6 8 10 12 14 Y ( X 10 0 0 ) m/z 57.0 8 . 0 1 8 7.5 7.8 8.1 8.4Min 0 4 8 12 16 20 24 Y ( X 10 0 ) m/z 86.0 8 . 0 1 8 7.5 7.8 8.1 8.4 Min 0 3 6 9 12 15 Y ( X 10 0 0 ) m/z 57.0 m/z 86.0 Page 256 of 478 Report Date: 28-Nov-2017 09:36:54 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 36 2-Butanone (MEK), CAS: 78-93-3 39 43 47 51 55 59 63 67 71 m/z 0 3 6 9 12 15 Y ( X 10 0 0 ) Raw Spec:Scan 1188(9.32) 43 72 57 39 43 47 51 55 59 63 67 71m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 1188(9.32), Qvalue=99 43 72 57 39 43 47 51 55 59 63 67 71 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 36 2-Butanone (MEK) (DATA) 43 72 57 39 43 47 51 55 59 63 67 71 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 9.330 min.(Qvalue: 99) 7242 8.8 9.1 9.4 9.7 Min 0 7 14 21 28 35 42 49 Y ( X 10 0 ) m/z 72.0 9 . 3 2 0 8.8 9.1 9.4 9.7Min 0 3 6 9 12 15 18 Y ( X 10 0 0 ) m/z 43.0 9 . 3 2 5 8.8 9.1 9.4 9.7 Min 0 3 6 9 12 15 18 Y ( X 10 0 0 ) m/z 72.0 m/z 43.0 Page 257 of 478 Report Date: 28-Nov-2017 09:36:54 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 40 Chloroform, CAS: 67-66-3 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 103107111115119123127 m/z 0 4 8 12 16 20 24 28 Y ( X 10 0 0 ) Raw Spec:Scan 1272(9.77) 83 85 47 87498267 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 103107111115119123127m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 1272(9.77), Qvalue=94 83 85 47 87488267 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 103107111115119123127 m/z 0 13 26 39 52 65 78 91 Y ( X 10 0 ) Ref Spec: 40 Chloroform (NIST) 83 85 47 48 87 82 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 103107111115119123127 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 9.770 min.(Qvalue: 94) 9.2 9.5 9.8 10.1 Min 0 4 8 12 16 20 24 28 Y ( X 10 0 0 ) m/z 83.0 9 . 7 6 8 9.2 9.5 9.8 10.1Min 0 3 6 9 12 15 18 Y ( X 10 0 0 ) m/z 85.0 9 . 7 6 8 9.2 9.5 9.8 10.1 Min 0 5 10 15 20 25 30 Y ( X 10 0 0 ) m/z 83.0 m/z 85.0 Page 258 of 478 Report Date: 28-Nov-2017 09:36:54 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 43 Cyclohexane, CAS: 110-82-7 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 m/z 0 13 26 39 52 65 78 91 Y ( X 10 0 ) Raw Spec:Scan 1324(10.05) 56 84 41 55 6943 57 67 83445471 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 1324(10.05), Qvalue=96 56 84 41 55 69 42 6754 83 85 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 43 Cyclohexane (NIST) 56 84 41 55 69 42 54 8583 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 10.040 min.(Qvalue: 96) 55 6942 9.5 9.8 10.1 10.4 Min 0 8 16 24 32 40 48 56 Y ( X 10 0 ) m/z 84.0 1 0 . 0 4 6 9.5 9.8 10.1 10.4Min 0 13 26 39 52 65 78 91 Y ( X 10 0 ) m/z 56.0 1 0 . 0 4 6 9.5 9.8 10.1 10.4 Min 0 14 28 42 56 70 84 98 Y ( X 10 0 ) m/z 84.0 m/z 56.0 Page 259 of 478 Report Date: 28-Nov-2017 09:36:55 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 46 Benzene, CAS: 71-43-2 36 40 44 48 52 56 60 64 68 72 76 m/z 0 5 10 15 20 25 30 35 Y ( X 10 0 0 ) Raw Spec:Scan 1420(10.56) 78 775152 39 36 40 44 48 52 56 60 64 68 72 76m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 1420(10.56), Qvalue=94 78 77 52 39 76 36 40 44 48 52 56 60 64 68 72 76 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 46 Benzene (DATA) 78 775152 39 74 36 40 44 48 52 56 60 64 68 72 76 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 10.560 min.(Qvalue: 94) 10.0 10.3 10.6 10.9 Min 0 5 10 15 20 25 30 35 Y ( X 10 0 0 ) m/z 78.0 1 0 . 5 5 8 10.0 10.3 10.6 10.9Min 0 11 22 33 44 55 66 77 Y ( X 10 0 ) m/z 77.0 1 0 . 5 5 3 10.0 10.3 10.6 10.9 Min 0 6 12 18 24 30 36 Y ( X 10 0 0 ) m/z 78.0 m/z 77.0 Page 260 of 478 Report Date: 28-Nov-2017 09:36:55 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 48 n-Heptane, CAS: 142-82-5 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Raw Spec:Scan 1460(10.77) 43 71 57 56 70 1005544 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 1460(10.77), Qvalue=92 43 71 57 56 70 1005544 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 48 n-Heptane (NIST) 43 57 71 56 70 10055 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 10.780 min.(Qvalue: 92) 71 10057 10.2 10.5 10.8 11.1 Min 0 2 4 6 8 10 Y ( X 10 0 0 ) m/z 43.0 1 0 . 7 7 2 10.2 10.5 10.8 11.1Min 0 8 16 24 32 40 48 56 64 Y ( X 10 0 ) m/z 71.0 1 0 . 7 7 2 10.2 10.5 10.8 11.1 Min 0 2 4 6 8 10 Y ( X 10 0 0 ) m/z 43.0 m/z 71.0 Page 261 of 478 Report Date: 28-Nov-2017 09:36:55 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 64 Toluene, CAS: 108-88-3 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 m/z 0 2 4 6 8 10 12 Y ( X 10 0 0 0 ) Raw Spec:Scan 1925(13.25) 91 43 92 855771 55 65 84 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113m/z 0 4 8 12 16 20 24 28 Y ( X 10 0 ) Amdis Enhanced Spec: Scan 1925(13.25), Qvalue=93 91 43 92 8557 71 56 65 84 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 64 Toluene (NIST) 91 92 6551 93 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 13.250 min.(Qvalue: 93) 43 855771 12.7 13.0 13.3 13.6 Min 0 10 20 30 40 50 60 70 Y ( X 10 0 0 ) m/z 92.0 1 3 . 2 5 3 12.7 13.0 13.3 13.6Min 0 2 4 6 8 10 12 Y ( X 10 0 0 0 ) m/z 91.0 1 3 . 2 5 9 12.7 13.0 13.3 13.6 Min 0 2 4 6 8 10 12 Y ( X 10 0 0 0 ) m/z 92.0 m/z 91.0 Page 262 of 478 Report Date: 28-Nov-2017 09:36:55 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 74 Ethylbenzene, CAS: 100-41-4 30 50 70 90 110 130 150 170 190 210 m/z 0 5 10 15 20 25 30 35 40 Y ( X 10 0 0 0 ) Raw Spec:Scan 2312(15.32) 91 106 43 57 77 78 105 30 50 70 90 110 130 150 170 190 210m/z 0 5 10 15 20 25 30 35 40 Y ( X 10 0 0 0 ) Enhanced Spec:Scan 2312(15.32), Qvalue=98 91 106 43 57 77 78 105 30 50 70 90 110 130 150 170 190 210 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 74 Ethylbenzene (NIST) 91 106 51 65 77 78 105 30 50 70 90 110 130 150 170 190 210 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 2312 @ 15.319 min.(Qvalue: 98) 43 57 106 14.8 15.1 15.4 15.7 Min 0 2 4 6 8 10 12 Y ( X 10 0 0 0 0 ) m/z 91.0 1 5 . 3 1 9 14.8 15.1 15.4 15.7Min 0 8 16 24 32 40 48 56 Y ( X 10 0 0 0 ) m/z 106.0 1 5 . 3 1 9 14.8 15.1 15.4 15.7 Min 0 2 4 6 8 10 12 Y ( X 10 0 0 0 0 ) m/z 91.0 m/z 106.0 Page 263 of 478 Report Date: 28-Nov-2017 09:36:55 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 76 m-Xylene & p-Xylene, CAS: 179601-23-1 30 50 70 90 110 130 150 170 190 210 m/z 0 2 4 6 8 10 12 Y ( X 10 0 0 0 0 ) Raw Spec:Scan 2339(15.46) 91 106 105 7751 7965 30 50 70 90 110 130 150 170 190 210m/z 0 2 4 6 8 10 12 Y ( X 10 0 0 0 0 ) Enhanced Spec:Scan 2339(15.46), Qvalue=0 91 106 105 7751 7965 14.9 15.2 15.5 15.8 Min 0 8 16 24 32 40 48 56 Y ( X 10 0 0 0 ) m/z 106.0 1 5 . 4 6 3 14.9 15.2 15.5 15.8Min 0 2 4 6 8 10 12 Y ( X 10 0 0 0 0 ) m/z 91.0 1 5 . 4 6 3 14.9 15.2 15.5 15.8 Min 0 2 4 6 8 10 12 Y ( X 10 0 0 0 0 ) m/z 106.0 m/z 91.0 Page 264 of 478 Report Date: 28-Nov-2017 09:36:55 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 78 o-Xylene, CAS: 95-47-6 30 50 70 90 110 130 150 170 190 210 230 250 m/z 0 6 12 18 24 30 36 42 Y ( X 10 0 0 0 ) Raw Spec:Scan 2435(15.98) 91 106 7751 30 50 70 90 110 130 150 170 190 210 230 250m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 2435(15.98), Qvalue=99 91 106 7751 30 50 70 90 110 130 150 170 190 210 230 250 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 78 o-Xylene (NIST) 91 106 7751 30 50 70 90 110 130 150 170 190 210 230 250 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 15.980 min.(Qvalue: 99) 15.4 15.7 16.0 16.3 Min 0 6 12 18 24 30 36 Y ( X 10 0 0 0 ) m/z 106.0 1 5 . 9 7 5 15.4 15.7 16.0 16.3Min 0 10 20 30 40 50 60 70 Y ( X 10 0 0 0 ) m/z 91.0 1 5 . 9 7 5 15.4 15.7 16.0 16.3 Min 0 11 22 33 44 55 66 Y ( X 10 0 0 0 ) m/z 106.0 m/z 91.0 Page 265 of 478 Report Date: 28-Nov-2017 09:36:56 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 92 1,2,4-Trimethylbenzene, CAS: 95-63-6 30 50 70 90 110 130 150 170 190 210 230 250 m/z 0 5 10 15 20 25 30 35 40 Y ( X 10 0 0 ) Raw Spec:Scan 2721(17.50) 105 120 7757 121 30 50 70 90 110 130 150 170 190 210 230 250m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 2721(17.50), Qvalue=98 105 120 77 121 30 50 70 90 110 130 150 170 190 210 230 250 m/z 0 2 4 6 8 10 Y ( X 10 0 0 ) Ref Spec: 92 1,2,4-Trimethylbenzene (NIST) 105 120 77 30 50 70 90 110 130 150 170 190 210 230 250 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 17.500 min.(Qvalue: 98) 120 16.9 17.2 17.5 17.8 18.1 Min 0 5 10 15 20 25 30 35 40 Y ( X 10 0 0 ) m/z 105.0 1 7 . 5 0 2 17.0 17.3 17.6 17.9Min 0 3 6 9 12 15 18 Y ( X 10 0 0 ) m/z 120.0 1 7 . 5 0 7 16.9 17.2 17.5 17.8 18.1 Min 0 6 12 18 24 30 36 Y ( X 10 0 0 ) m/z 105.0 m/z 120.0 Page 266 of 478 Report Date: 28-Nov-2017 09:36:53 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 14 Trichlorofluoromethane, CAS: 75-69-4 Signal: 1 Processing Integration Results RT: 5.23 Area: 2649 Amount: 0.029639 Amount Units: ppb v/v 4.9 5.1 5.3 5.5 Min 0 2 4 6 8 10 12 14 16 18 Y ( X 10 0 ) m/z 101.0 5 . 2 2 7 Manual Integration Results RT: 5.23 Area: 5564 Amount: 0.062255 Amount Units: ppb v/v 4.9 5.1 5.3 5.5 Min 0 2 4 6 8 10 12 14 16 18 Y ( X 10 0 ) m/z 101.0 5 . 2 2 7 Reviewer: puangmaleek, 28-Nov-2017 09:31:44 Audit Action: Assigned Compound ID Audit Reason: Assign Peak Page 267 of 478 Report Date: 28-Nov-2017 09:36:53 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 14 Trichlorofluoromethane, CAS: 75-69-4 Signal: 1 Processing Integration Results RT: 5.23 Area: 2649 Amount: 0.029639 Amount Units: ppb v/v 4.9 5.1 5.3 5.5Min 0 2 4 6 8 10 12 14 16 18 Y ( X 10 0 ) m/z 101.0 5 . 2 2 7 Manual Integration Results RT: 5.23 Area: 5564 Amount: 0.062255 Amount Units: ppb v/v 4.9 5.1 5.3 5.5 Min 0 2 4 6 8 10 12 14 16 18 Y ( X 10 0 ) m/z 101.0 5 . 2 2 7 Reviewer: puangmaleek, 28-Nov-2017 09:31:54 Audit Action: Manually Integrated Audit Reason: Assign Peak Page 268 of 478 Report Date: 28-Nov-2017 09:36:55 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 84 N-Propylbenzene, CAS: 103-65-1 Signal: 1 Processing Integration Results Not Detected Expected RT: 16.87 16.5 16.7 16.9 17.1 Min 0 2 4 6 8 10 12 14 16 18 Y ( X 10 0 0 ) m/z 91.0 Manual Integration Results RT: 16.87 Area: 32379 Amount: 0.113113 Amount Units: ppb v/v 16.5 16.7 16.9 17.1 Min 0 2 4 6 8 10 12 14 16 18 Y ( X 10 0 0 ) m/z 91.0 1 6 . 8 6 6 Reviewer: puangmaleek, 28-Nov-2017 09:34:17 Audit Action: Assigned Compound ID Audit Reason: Assign Peak Page 269 of 478 Report Date: 28-Nov-2017 09:36:55 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 84 N-Propylbenzene, CAS: 103-65-1 Signal: 1 Processing Integration Results Not Detected Expected RT: 16.87 16.5 16.7 16.9 17.1Min 0 2 4 6 8 10 12 14 16 18 Y ( X 10 0 0 ) m/z 91.0 Manual Integration Results RT: 16.87 Area: 32379 Amount: 0.113113 Amount Units: ppb v/v 16.5 16.7 16.9 17.1 Min 0 2 4 6 8 10 12 14 16 18 Y ( X 10 0 0 ) m/z 91.0 1 6 . 8 6 6 Reviewer: puangmaleek, 28-Nov-2017 09:34:27 Audit Action: Manually Integrated Audit Reason: Assign Peak Page 270 of 478 Report Date: 28-Nov-2017 09:36:56 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 89 1,3,5-Trimethylbenzene, CAS: 108-67-8 Signal: 1 Processing Integration Results RT: 16.99 Area: 32067 Amount: 0.170316 Amount Units: ppb v/v 16.7 16.9 17.1 17.3 Min 0 3 6 9 12 15 18 21 24 27 30 33 36 Y ( X 10 0 0 ) m/z 105.0 1 6 . 9 8 9 Manual Integration Results RT: 17.06 Area: 23905 Amount: 0.126965 Amount Units: ppb v/v 16.7 16.9 17.1 17.3 Min 0 3 6 9 12 15 18 21 24 27 30 33 36 Y ( X 10 0 0 ) m/z 105.0 1 7 . 0 5 9 Reviewer: puangmaleek, 28-Nov-2017 09:34:48 Audit Action: Assigned Compound ID Audit Reason: Assign Peak Page 271 of 478 Report Date: 28-Nov-2017 09:36:56 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 89 1,3,5-Trimethylbenzene, CAS: 108-67-8 Signal: 1 Processing Integration Results RT: 16.99 Area: 32067 Amount: 0.170316 Amount Units: ppb v/v 16.7 16.9 17.1 17.3Min 0 3 6 9 12 15 18 21 24 27 30 33 36 Y ( X 10 0 0 ) m/z 105.0 1 6 . 9 8 9 Manual Integration Results RT: 17.06 Area: 23905 Amount: 0.126965 Amount Units: ppb v/v 16.7 16.9 17.1 17.3 Min 0 3 6 9 12 15 18 21 24 27 30 33 36 Y ( X 10 0 0 ) m/z 105.0 1 7 . 0 5 9 Reviewer: puangmaleek, 28-Nov-2017 09:34:52 Audit Action: Manually Integrated Audit Reason: Assign Peak Page 272 of 478 Report Date: 28-Nov-2017 09:36:56 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Isobutane 75-28-5 NIST14.L 237 C4H10 58 86 Isopropylsulfonyl chloride 10147-37-2 NIST14.L 19769 C3H7ClO2S 142 9 Cyclobutylamine 2516-34-9 NIST14.L 615 C4H9N 71 9 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 m/z 0 4 8 12 16 20 Y ( X 10 0 0 0 )Raw Spec: Scan 86(3.44) 43 41 39 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99m/z 0 4 8 12 16 20 Y ( X 10 0 0 0 )28034-10[MS SCAN Spec]:Scan 86(3.44) 43 41 39 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #237, Isobutane (from NIST14.L) 43 41 39 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #19769, Isopropylsulfonyl chloride (from NIST14.L) 43 41 39 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #615, Cyclobutylamine (from NIST14.L) 43 42 41 Page 273 of 478 Report Date: 28-Nov-2017 09:36:57 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Cyclohexane,1,4-dimethyl-,cis-624-29-3 NIST14.L 6928 C8H16 112 91 Cyclohexane,1,3-dimethyl-,cis-638-04-0 NIST14.L 6931 C8H16 112 91 Cyclohexane,1,3-dimethyl-591-21-9 NIST14.L 6866 C8H16 112 91 36 40 44 48 52 56 60 64 68 72 76 80 84 88 92 96 100 104 108 112 m/z 0 4 8 12 16 Y ( X 10 0 0 0 )Raw Spec: Scan 1884(13.03) 97 55 112415669427098 36 40 44 48 52 56 60 64 68 72 76 80 84 88 92 96 100 104 108 112m/z 0 4 8 12 16 Y ( X 10 0 0 0 )28034-10[MS SCAN Spec]:Scan 1884(13.03) 97 55 112415669427098 36 40 44 48 52 56 60 64 68 72 76 80 84 88 92 96 100 104 108 112 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #6928, Cyclohexane, 1,4-dimethyl-, cis- (from NIST14.L) 55 97 11241 56 6942 96837084 9853 36 40 44 48 52 56 60 64 68 72 76 80 84 88 92 96 100 104 108 112 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #6931, Cyclohexane, 1,3-dimethyl-, cis- (from NIST14.L) 9755 41 112566942987053 36 40 44 48 52 56 60 64 68 72 76 80 84 88 92 96 100 104 108 112 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #6866, Cyclohexane, 1,3-dimethyl- (from NIST14.L) 9755 41 112695642709853 Page 274 of 478 Report Date: 28-Nov-2017 09:36:57 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Cyclohexane,1,4-dimethyl-,trans-2207-04-7 NIST14.L 6940 C8H16 112 97 Cyclohexane,1,4-dimethyl-589-90-2 NIST14.L 6863 C8H16 112 97 Cyclohexane,1,4-dimethyl-,cis-624-29-3 NIST14.L 6922 C8H16 112 95 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 m/z 0 16 32 48 64 80 Y ( X 10 0 0 ) Raw Spec: Scan 2012(13.72) 9755 11256416970429683988453 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113m/z 0 16 32 48 64 80 Y ( X 10 0 0 ) 28034-10[MS SCAN Spec]:Scan 2012(13.72) 9755 11256416970429683988453 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #6940, Cyclohexane, 1,4-dimethyl-, trans- (from NIST14.L) 55 97 41 112 56 6942 967083 985384 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #6863, Cyclohexane, 1,4-dimethyl- (from NIST14.L) 55 97 11241 56 6942 70 83 96 9884 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #6922, Cyclohexane, 1,4-dimethyl-, cis- (from NIST14.L) 55 97 41 112564269708396849853 Page 275 of 478 Report Date: 28-Nov-2017 09:36:58 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Cyclohexane,ethyl-1678-91-7 NIST14.L 6789 C8H16 112 95 Cyclohexane,propyl-1678-92-8 NIST14.L 11775 C9H18 126 78 3,4-Dimethyl-2-hexene 2213-37-8 NIST14.L 6819 C8H16 112 76 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 3 6 9 12 15 Y ( X 10 0 0 0 )Raw Spec: Scan 2137(14.38) 83 55 82 41 1126769843942 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210m/z 0 3 6 9 12 15 Y ( X 10 0 0 0 )28034-10[MS SCAN Spec]:Scan 2137(14.38) 83 55 82 41 1126769843942 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #6789, Cyclohexane, ethyl- (from NIST14.L) 83 55 8241 112 56 673942 84 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11775, Cyclohexane, propyl- (from NIST14.L) 83 55 82 41 1266739698443 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #6819, 3,4-Dimethyl-2-hexene (from NIST14.L) 55 83 41 11239436984 Page 276 of 478 Report Date: 28-Nov-2017 09:36:58 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Cyclohexane,1,1,3-trimethyl-3073-66-3 NIST14.L 11835 C9H18 126 94 Cyclohexane,1,3,5-trimethyl-, (1.alpha.,3.alpha 1795-27-3 NIST14.L 11878 C9H18 126 64 Cyclohexane,1,2,4-trimethyl-2234-75-5 NIST14.L 11819 C9H18 126 49 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 117 121 125 129 m/z 0 4 8 12 16 Y ( X 10 0 0 0 )Raw Spec: Scan 2148(14.44) 111 69 55 41 835670 8443 1129767 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 117 121 125 129m/z 0 4 8 12 16 Y ( X 10 0 0 0 )28034-10[MS SCAN Spec]:Scan 2148(14.44) 111 69 55 41 835670 8443 1129767 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 117 121 125 129 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11835, Cyclohexane, 1,1,3-trimethyl- (from NIST14.L) 111 69 5541 8356 43 70 1125367 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 117 121 125 129 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11878, Cyclohexane, 1,3,5-trimethyl-, (1.alpha.,3.alpha.,5.alpha.)- (from NIST14.L) 11169 55 41 1264256701125367 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 117 121 125 129 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11819, Cyclohexane, 1,2,4-trimethyl- (from NIST14.L) 69 111 55 41 1265670844367539711257 Page 277 of 478 Report Date: 28-Nov-2017 09:36:58 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Unknown Heptane,2,4-dimethyl-2213-23-2 NIST14.L 12971 C9H20 128 72 Hexane,2,3,4-trimethyl-921-47-1 NIST14.L 12982 C9H20 128 64 Octane,4-methyl-2216-34-4 NIST14.L 12942 C9H20 128 64 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 5 10 15 20 Y ( X 10 0 0 0 )Raw Spec: Scan 2191(14.67) 43 57 71 85417056 39 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 5 10 15 20 Y ( X 10 0 0 0 )28034-10[MS SCAN Spec]:Scan 2191(14.67) 43 57 71 85417056 39 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #12971, Heptane, 2,4-dimethyl- (from NIST14.L) 43 85415771 84 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #12982, Hexane, 2,3,4-trimethyl- (from NIST14.L) 43 41 7157 85 39 69 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #12942, Octane, 4-methyl- (from NIST14.L) 43 85714157 Page 278 of 478 Report Date: 28-Nov-2017 09:36:58 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Cyclohexane,1,2,4-trimethyl-, (1.alpha.,2.beta.7667-60-9 NIST14.L 11871 C9H18 126 94 Cyclohexane,1,3,5-trimethyl-, (1.alpha.,3.alpha 1795-26-2 NIST14.L 11876 C9H18 126 90 Cyclohexane,1,2,4-trimethyl-2234-75-5 NIST14.L 11819 C9H18 126 90 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 117 121 125 m/z 0 3 6 9 12 15 Y ( X 10 0 0 0 )Raw Spec: Scan 2206(14.75) 11169 55 41 12656704384112679753 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 117 121 125m/z 0 3 6 9 12 15 Y ( X 10 0 0 0 )28034-10[MS SCAN Spec]:Scan 2206(14.75) 11169 55 41 12656704384112679753 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 117 121 125 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11871, Cyclohexane, 1,2,4-trimethyl-, (1.alpha.,2.beta.,4.beta.)- (from NIST14.L) 1116955 41 56 12643708453112675797 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 117 121 125 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11876, Cyclohexane, 1,3,5-trimethyl-, (1.alpha.,3.alpha.,5.beta.)- (from NIST14.L) 69 11155 41 1264256 7053 83 1126784 37 41 45 49 53 57 61 65 69 73 77 81 85 89 93 97 101 105 109 113 117 121 125 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11819, Cyclohexane, 1,2,4-trimethyl- (from NIST14.L) 69 111 55 41 1265670844367539711257 Page 279 of 478 Report Date: 28-Nov-2017 09:36:58 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Octane,3-methyl-2216-33-3 NIST14.L 12944 C9H20 128 90 Heptane,2,5-dimethyl-2216-30-0 NIST14.L 12977 C9H20 128 72 Decane,2,6,6-trimethyl-62108-24-1 NIST14.L 51451 C13H28 184 53 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 6 12 18 24 30 Y ( X 10 0 0 0 )Raw Spec: Scan 2222(14.84) 57 43 56 98 997139 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210m/z 0 6 12 18 24 30 Y ( X 10 0 0 0 )28034-10[MS SCAN Spec]:Scan 2222(14.84) 57 43 56 98 997139 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #12944, Octane, 3-methyl- (from NIST14.L) 57 43 56 98 9971 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #12977, Heptane, 2,5-dimethyl- (from NIST14.L) 57 43 56 71 99 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #51451, Decane, 2,6,6-trimethyl- (from NIST14.L) 57 43 714156 998570 127 Page 280 of 478 Report Date: 28-Nov-2017 09:36:58 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Cyclohexane,1,2,3-trimethyl-, (1.alpha.,2.beta.1678-81-5 NIST14.L 11873 C9H18 126 93 Cyclohexane,1,2,4-trimethyl-2234-75-5 NIST14.L 11831 C9H18 126 70 3-Heptene,2,6-dimethyl-2738-18-3 NIST14.L 11788 C9H18 126 60 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 15 30 45 60 75 Y ( X 10 0 0 ) Raw Spec: Scan 2303(15.27) 69 11155 5641 70 126824339975781112 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210m/z 0 15 30 45 60 75 Y ( X 10 0 0 ) 28034-10[MS SCAN Spec]:Scan 2303(15.27) 69 11155 5641 70 126824339975781112 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11873, Cyclohexane, 1,2,3-trimethyl-, (1.alpha.,2.beta.,3.alpha.)- (from NIST14.L) 69 55 11141 56 70 126833943678297112 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11831, Cyclohexane, 1,2,4-trimethyl- (from NIST14.L) 69 11155 41 12656703997844267112 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11788, 3-Heptene, 2,6-dimethyl- (from NIST14.L) 55 69 5641 43 70 12657833953 Page 281 of 478 Report Date: 28-Nov-2017 09:36:58 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-10.D Injection Date: 24-Nov-2017 17:32:30 Instrument ID: CHB.i Lims ID: 200-41113-A-3 Lab Sample ID: 200-41113-3 Client ID: SV-1 Operator ID: VTP ALS Bottle#: 10 Worklist Smp#: 39 Purge Vol: 200.000 mL Dil. Factor: 2.5000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column:Detector MS SCAN Library Search Compound Match CAS#Library Entry Formula Weight Q Unknown 1-Ethyl-4-methylcyclohexane 3728-56-1 NIST14.L 11812 C9H18 126 76 Cyclohexane,1-ethyl-2-methyl-,trans-4923-78-8 NIST14.L 11861 C9H18 126 68 3,5-Dimethyl-3-heptene 59643-68-4 NIST14.L 11784 C9H18 126 62 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 16 32 48 64 80 Y ( X 10 0 0 ) Raw Spec: Scan 2411(15.85) 9755 694143 70 1263996986753 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 16 32 48 64 80 Y ( X 10 0 0 ) 28034-10[MS SCAN Spec]:Scan 2411(15.85) 9755 694143 70 1263996986753 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11812, 1-Ethyl-4-methylcyclohexane (from NIST14.L) 9755 41 69 12696984381 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11861, Cyclohexane, 1-ethyl-2-methyl-, trans- (from NIST14.L) 9755 41 69 126984281 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 18 36 54 72 90 Y ( X 10 0 ) Entry #11784, 3,5-Dimethyl-3-heptene (from NIST14.L) 9755 69 12641 984356 Page 282 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: AA-1 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-4 TestAmerica Burlington Matrix:28034-11.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 00:00 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/24/2017 18:24 ID:RTX-624 Analysis Batch No.:123710 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 120.9175-71-8 Dichlorodifluoromethane 0.50 U 0.50 86.4775-45-6 Freon 22 0.50 U 0.50 170.9276-14-2 1,2-Dichlorotetrafluoroe thane 0.20 U 0.20 50.4974-87-3 Chloromethane 0.50 U 0.50 58.12106-97-8 n-Butane 0.50 U 0.50 62.5075-01-4 Vinyl chloride 0.035 U 0.035 54.09106-99-0 1,3-Butadiene 0.20 U 0.20 94.9474-83-9 Bromomethane 0.20 U 0.20 64.5275-00-3 Chloroethane 0.50 U 0.50 106.96593-60-2 Bromoethene(Vinyl Bromide) 0.20 U 0.20 137.3775-69-4 Trichlorofluoromethane 0.20 U 0.20 187.3876-13-1 Freon TF 0.20 U 0.20 96.9475-35-4 1,1-Dichloroethene 0.035 U 0.035 58.0867-64-1 Acetone 5.0 U 5.0 60.1067-63-0 Isopropyl alcohol 5.0 U 5.0 76.1475-15-0 Carbon disulfide 0.50 U 0.50 76.53107-05-1 3-Chloropropene 0.50 U 0.50 84.9375-09-2 Methylene Chloride 0.50 U 0.50 74.1275-65-0 tert-Butyl alcohol 5.0 U 5.0 88.151634-04-4 Methyl tert-butyl ether 0.20 U 0.20 96.94156-60-5 trans-1,2-Dichloroethene 0.20 U 0.20 86.17110-54-3 n-Hexane 0.20 U 0.20 98.9675-34-3 1,1-Dichloroethane 0.20 U 0.20 72.1178-93-3 Methyl Ethyl Ketone 0.50 U 0.50 96.94156-59-2 cis-1,2-Dichloroethene 0.035 U 0.035 96.94540-59-0 1,2-Dichloroethene, Total 0.40 U 0.40 119.3867-66-3 Chloroform 0.20 U 0.20 72.11109-99-9 Tetrahydrofuran 5.0 U 5.0 133.4171-55-6 1,1,1-Trichloroethane 0.20 U 0.20 84.16110-82-7 Cyclohexane 0.20 U 0.20 153.8156-23-5 Carbon tetrachloride 0.061 0.035 114.23540-84-1 2,2,4-Trimethylpentane 0.20 U 0.20 78.1171-43-2 Benzene 0.20 U 0.20 98.96107-06-2 1,2-Dichloroethane 0.20 U 0.20 FORM I TO-15 Page 283 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: AA-1 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-4 TestAmerica Burlington Matrix:28034-11.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 00:00 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/24/2017 18:24 ID:RTX-624 Analysis Batch No.:123710 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 100.21142-82-5 n-Heptane 0.20 U 0.20 131.3979-01-6 Trichloroethene 0.035 U 0.035 100.1280-62-6 Methyl methacrylate 0.50 U 0.50 112.9978-87-5 1,2-Dichloropropane 0.20 U 0.20 88.11123-91-1 1,4-Dioxane 5.0 U 5.0 163.8375-27-4 Bromodichloromethane 0.20 U 0.20 110.9710061-01-5 cis-1,3-Dichloropropene 0.20 U 0.20 100.16108-10-1 methyl isobutyl ketone 0.50 U 0.50 92.14108-88-3 Toluene 0.20 U 0.20 110.9710061-02-6 trans-1,3-Dichloropropen e 0.20 U 0.20 133.4179-00-5 1,1,2-Trichloroethane 0.20 U 0.20 165.83127-18-4 Tetrachloroethene 0.20 U 0.20 100.20591-78-6 Methyl Butyl Ketone (2-Hexanone) 0.50 U 0.50 208.29124-48-1 Dibromochloromethane 0.20 U 0.20 187.87106-93-4 1,2-Dibromoethane 0.20 U 0.20 112.56108-90-7 Chlorobenzene 0.20 U 0.20 106.17100-41-4 Ethylbenzene 0.20 U 0.20 106.17179601-23-1 m,p-Xylene 0.50 U 0.50 106.1795-47-6 Xylene, o-0.20 U 0.20 106.171330-20-7 Xylene (total)0.70 U 0.70 104.15100-42-5 Styrene 0.20 U 0.20 252.7575-25-2 Bromoform 0.20 U 0.20 120.1998-82-8 Cumene 0.20 U 0.20 167.8579-34-5 1,1,2,2-Tetrachloroethan e 0.20 U 0.20 120.19103-65-1 n-Propylbenzene 0.20 U 0.20 120.20622-96-8 4-Ethyltoluene 0.20 U 0.20 120.20108-67-8 1,3,5-Trimethylbenzene 0.20 U 0.20 126.5995-49-8 2-Chlorotoluene 0.20 U 0.20 134.2298-06-6 tert-Butylbenzene 0.20 U 0.20 120.2095-63-6 1,2,4-Trimethylbenzene 0.20 U 0.20 134.22135-98-8 sec-Butylbenzene 0.20 U 0.20 134.2299-87-6 4-Isopropyltoluene 0.20 U 0.20 147.00541-73-1 1,3-Dichlorobenzene 0.20 U 0.20 147.00106-46-7 1,4-Dichlorobenzene 0.20 U 0.20 FORM I TO-15 Page 284 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: AA-1 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-4 TestAmerica Burlington Matrix:28034-11.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 00:00 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/24/2017 18:24 ID:RTX-624 Analysis Batch No.:123710 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 126.58100-44-7 Benzyl chloride 0.20 U 0.20 134.22104-51-8 n-Butylbenzene 0.20 U 0.20 147.0095-50-1 1,2-Dichlorobenzene 0.20 U 0.20 181.45120-82-1 1,2,4-Trichlorobenzene 0.50 U 0.50 260.7687-68-3 Hexachlorobutadiene 0.20 U 0.20 128.1791-20-3 Naphthalene 0.50 U 0.50 FORM I TO-15 Page 285 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: AA-1 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-4 TestAmerica Burlington Matrix:28034-11.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 00:00 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/24/2017 18:24 ID:RTX-624 Analysis Batch No.:123710 ug/m3Units: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 120.9175-71-8 Dichlorodifluoromethane 2.5 U 2.5 86.4775-45-6 Freon 22 1.8 U 1.8 170.9276-14-2 1,2-Dichlorotetrafluoroe thane 1.4 U 1.4 50.4974-87-3 Chloromethane 1.0 U 1.0 58.12106-97-8 n-Butane 1.2 U 1.2 62.5075-01-4 Vinyl chloride 0.089 U 0.089 54.09106-99-0 1,3-Butadiene 0.44 U 0.44 94.9474-83-9 Bromomethane 0.78 U 0.78 64.5275-00-3 Chloroethane 1.3 U 1.3 106.96593-60-2 Bromoethene(Vinyl Bromide) 0.87 U 0.87 137.3775-69-4 Trichlorofluoromethane 1.1 U 1.1 187.3876-13-1 Freon TF 1.5 U 1.5 96.9475-35-4 1,1-Dichloroethene 0.14 U 0.14 58.0867-64-1 Acetone 12 U 12 60.1067-63-0 Isopropyl alcohol 12 U 12 76.1475-15-0 Carbon disulfide 1.6 U 1.6 76.53107-05-1 3-Chloropropene 1.6 U 1.6 84.9375-09-2 Methylene Chloride 1.7 U 1.7 74.1275-65-0 tert-Butyl alcohol 15 U 15 88.151634-04-4 Methyl tert-butyl ether 0.72 U 0.72 96.94156-60-5 trans-1,2-Dichloroethene 0.79 U 0.79 86.17110-54-3 n-Hexane 0.70 U 0.70 98.9675-34-3 1,1-Dichloroethane 0.81 U 0.81 72.1178-93-3 Methyl Ethyl Ketone 1.5 U 1.5 96.94156-59-2 cis-1,2-Dichloroethene 0.14 U 0.14 96.94540-59-0 1,2-Dichloroethene, Total 1.6 U 1.6 119.3867-66-3 Chloroform 0.98 U 0.98 72.11109-99-9 Tetrahydrofuran 15 U 15 133.4171-55-6 1,1,1-Trichloroethane 1.1 U 1.1 84.16110-82-7 Cyclohexane 0.69 U 0.69 153.8156-23-5 Carbon tetrachloride 0.39 0.22 114.23540-84-1 2,2,4-Trimethylpentane 0.93 U 0.93 78.1171-43-2 Benzene 0.64 U 0.64 98.96107-06-2 1,2-Dichloroethane 0.81 U 0.81 FORM I TO-15 Page 286 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: AA-1 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-4 TestAmerica Burlington Matrix:28034-11.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 00:00 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/24/2017 18:24 ID:RTX-624 Analysis Batch No.:123710 ug/m3Units: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 100.21142-82-5 n-Heptane 0.82 U 0.82 131.3979-01-6 Trichloroethene 0.19 U 0.19 100.1280-62-6 Methyl methacrylate 2.0 U 2.0 112.9978-87-5 1,2-Dichloropropane 0.92 U 0.92 88.11123-91-1 1,4-Dioxane 18 U 18 163.8375-27-4 Bromodichloromethane 1.3 U 1.3 110.9710061-01-5 cis-1,3-Dichloropropene 0.91 U 0.91 100.16108-10-1 methyl isobutyl ketone 2.0 U 2.0 92.14108-88-3 Toluene 0.75 U 0.75 110.9710061-02-6 trans-1,3-Dichloropropen e 0.91 U 0.91 133.4179-00-5 1,1,2-Trichloroethane 1.1 U 1.1 165.83127-18-4 Tetrachloroethene 1.4 U 1.4 100.20591-78-6 Methyl Butyl Ketone (2-Hexanone) 2.0 U 2.0 208.29124-48-1 Dibromochloromethane 1.7 U 1.7 187.87106-93-4 1,2-Dibromoethane 1.5 U 1.5 112.56108-90-7 Chlorobenzene 0.92 U 0.92 106.17100-41-4 Ethylbenzene 0.87 U 0.87 106.17179601-23-1 m,p-Xylene 2.2 U 2.2 106.1795-47-6 Xylene, o-0.87 U 0.87 106.171330-20-7 Xylene (total)3.0 U 3.0 104.15100-42-5 Styrene 0.85 U 0.85 252.7575-25-2 Bromoform 2.1 U 2.1 120.1998-82-8 Cumene 0.98 U 0.98 167.8579-34-5 1,1,2,2-Tetrachloroethan e 1.4 U 1.4 120.19103-65-1 n-Propylbenzene 0.98 U 0.98 120.20622-96-8 4-Ethyltoluene 0.98 U 0.98 120.20108-67-8 1,3,5-Trimethylbenzene 0.98 U 0.98 126.5995-49-8 2-Chlorotoluene 1.0 U 1.0 134.2298-06-6 tert-Butylbenzene 1.1 U 1.1 120.2095-63-6 1,2,4-Trimethylbenzene 0.98 U 0.98 134.22135-98-8 sec-Butylbenzene 1.1 U 1.1 134.2299-87-6 4-Isopropyltoluene 1.1 U 1.1 147.00541-73-1 1,3-Dichlorobenzene 1.2 U 1.2 147.00106-46-7 1,4-Dichlorobenzene 1.2 U 1.2 FORM I TO-15 Page 287 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: AA-1 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-4 TestAmerica Burlington Matrix:28034-11.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 00:00 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/24/2017 18:24 ID:RTX-624 Analysis Batch No.:123710 ug/m3Units: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 126.58100-44-7 Benzyl chloride 1.0 U 1.0 134.22104-51-8 n-Butylbenzene 1.1 U 1.1 147.0095-50-1 1,2-Dichlorobenzene 1.2 U 1.2 181.45120-82-1 1,2,4-Trichlorobenzene 3.7 U 3.7 260.7687-68-3 Hexachlorobutadiene 2.1 U 2.1 128.1791-20-3 Naphthalene 2.6 U 2.6 FORM I TO-15 Page 288 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS Client Sample ID: Lab Name:Job No.: AA-1 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:200-41113-4 TestAmerica Burlington Matrix:28034-11.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/20/2017 00:00 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/24/2017 18:24 ID:RTX-624 Analysis Batch No.:123710 ppb v/vUnits: Number TICs Found:TIC Result Total:00 QRTCOMPOUND NAME RESULTCAS NO.MATCH QUALITY Tentatively Identified Compound None FORM I-TIC TO-15 Page 289 of 478 Report Date: 28-Nov-2017 09:42:10 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Target Compound Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-11.D Lims ID: 200-41113-A-4 Client ID: AA-1 Sample Type: Client Inject. Date: 24-Nov-2017 18:24:30 ALS Bottle#: 11 Worklist Smp#: 40 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Sample Info: 200-0028034-011 Misc. Info.: 41113-04 Operator ID: VTP Instrument ID: CHB.i Method:\\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\TO15_LLNJ_TO3.m Limit Group: AI_TO15_ICAL Last Update: 28-Nov-2017 09:42:09 Calib Date: 07-Nov-2017 01:49:30 Integrator: RTE ID Type: Deconvolution ID Quant Method: Internal/External Standard Quant By: Initial Calibration Last ICal File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-13.D Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host:XAWRK022 First Level Reviewer: puangmaleek Date:28-Nov-2017 09:42:09 Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response OnCol Amt ppb v/v Flags 2 Dichlorodifluoromethane 85 3.193 3.193 0.000 99 31821 0.3648 3 Chlorodifluoromethane 51 3.231 3.225 0.006 97 9337 0.1882 4 1,2-Dichloro-1,1,2,2-tetra 85 3.412 ND 5 Chloromethane 50 3.540 3.540 0.005 83 12580 0.4043 7 6 Butane 43 3.711 3.711 0.000 91 17863 0.3323 7 7 Vinyl chloride 62 3.748 ND 8 Butadiene 54 3.812 ND 10 Bromomethane 94 4.479 ND 11 Chloroethane 64 4.709 ND 13 Vinyl bromide 106 5.120 ND 14 Trichlorofluoromethane 101 5.216 5.216 0.000 97 16252 0.1746 19 1,1,2-Trichloro-1,2,2-trif 101 6.246 6.246 0.000 92 4890 0.0625 20 1,1-Dichloroethene 96 6.315 ND 21 Acetone 43 6.481 6.481 0.016 92 55543 0.9500 7 22 Isopropyl alcohol 45 6.726 6.726 0.043 83 16375 0.2492 7 23 Carbon disulfide 76 6.748 ND 24 3-Chloro-1-propene 41 7.014 ND 27 Methylene Chloride 49 7.276 7.276 0.000 64 5633 0.1201 7 28 2-Methyl-2-propanol 59 7.383 ND 29 Methyl tert-butyl ether 73 7.623 ND 30 trans-1,2-Dichloroethene 61 7.687 ND 32 Hexane 57 8.018 8.012 0.006 94 6148 0.0860 33 1,1-Dichloroethane 63 8.423 ND 36 2-Butanone (MEK) 72 9.336 9.336 0.021 89 2564 0.1112 7 37 cis-1,2-Dichloroethene 96 9.331 ND * 39 Chlorobromomethane 128 9.694 9.699 -0.005 91 393822 10.0 38 Tetrahydrofuran 42 9.710 ND 40 Chloroform 83 9.774 ND S 41 1,2-Dichloroethene, Total 61 10.000 ND 42 1,1,1-Trichloroethane 97 10.030 ND 43 Cyclohexane 84 10.046 ND Page 290 of 478 Report Date: 28-Nov-2017 09:42:10 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-11.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response OnCol Amt ppb v/v Flags 44 Carbon tetrachloride 117 10.233 10.238 -0.005 94 4802 0.0615 45 Isooctane 57 10.521 ND 46 Benzene 78 10.558 10.563 -0.005 96 15384 0.1064 47 1,2-Dichloroethane 62 10.659 ND 48 n-Heptane 43 10.766 10.766 -0.006 24 1811 0.0202 7 * 50 1,4-Difluorobenzene 114 11.103 11.102 0.001 94 1967074 10.0 53 Trichloroethene 95 11.476 ND 54 1,2-Dichloropropane 63 11.839 ND 55 Methyl methacrylate 69 11.876 ND 56 1,4-Dioxane 88 11.967 ND 58 Dichlorobromomethane 83 12.202 ND 60 cis-1,3-Dichloropropene 75 12.826 ND 61 4-Methyl-2-pentanone (MIBK 43 12.976 ND 64 Toluene 92 13.253 13.259 -0.006 92 8019 0.0795 66 trans-1,3-Dichloropropene 75 13.621 ND 67 1,1,2-Trichloroethane 83 13.888 ND 68 Tetrachloroethene 166 14.032 ND 69 2-Hexanone 43 14.150 ND 70 Chlorodibromomethane 129 14.449 ND 71 Ethylene Dibromide 107 14.646 ND * 72 Chlorobenzene-d5 117 15.212 15.212 0.000 84 1688199 10.0 73 Chlorobenzene 112 15.249 ND 74 Ethylbenzene 91 15.324 15.319 0.005 90 6765 0.0306 M 76 m-Xylene & p-Xylene 106 15.463 15.463 -0.005 0 4203 0.0483 7 78 o-Xylene 106 15.981 15.981 0.006 22 2475 0.0286 7 S 77 Xylenes, Total 106 0 0.0768 7 79 Styrene 104 16.002 ND 80 Bromoform 173 16.295 ND 81 Isopropylbenzene 105 16.391 ND 83 1,1,2,2-Tetrachloroethane 83 16.797 ND 84 N-Propylbenzene 91 16.866 ND 87 4-Ethyltoluene 105 16.994 ND 88 2-Chlorotoluene 91 17.037 ND 89 1,3,5-Trimethylbenzene 105 17.058 ND 91 tert-Butylbenzene 119 17.437 ND 92 1,2,4-Trimethylbenzene 105 17.507 17.507 0.000 1 2235 0.0114 7 93 sec-Butylbenzene 105 17.694 ND 94 4-Isopropyltoluene 119 17.843 ND 95 1,3-Dichlorobenzene 146 17.923 ND 96 1,4-Dichlorobenzene 146 18.035 ND 97 Benzyl chloride 91 18.185 ND 99 n-Butylbenzene 91 18.350 ND 100 1,2-Dichlorobenzene 146 18.521 ND 103 1,2,4-Trichlorobenzene 180 20.880 ND 104 Hexachlorobutadiene 225 21.045 ND 105 Naphthalene 128 21.360 ND Page 291 of 478 Report Date: 28-Nov-2017 09:42:10 Chrom Revision: 2.2 13-Nov-2017 17:19:06 QC Flag Legend Processing Flags 7 - Failed Limit of Detection Review Flags M - Manually Integrated Reagents: ATTO15BISs_00006 Amount Added: 20.00 Units: mL Run Reagent Page 292 of 478 Report Date: 28-Nov-2017 09:42:10 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-11.D Injection Date: 24-Nov-2017 18:24:30 Instrument ID: CHB.i Operator ID: VTP Lims ID: 200-41113-A-4 Lab Sample ID: 200-41113-4 Worklist Smp#: 40 Client ID: AA-1 Purge Vol: 200.000 mL Dil. Factor: 1.0000 ALS Bottle#: 11 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Y Scaling: Method Defined: Scale to the Nth Largest Target: 1 2.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 18.0 20.0 22.0 24.0 Min 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 Y ( X 10 0 0 0 0 ) 28034-11[MS SCAN Chro]:Total * C h l o r o b r o m o m e t h a n e ( 9 . 6 9 4 ) * 1 ,4- D i f lu o r o b e n z en e ( 1 1 . 0 9 7 ) * C h l o r o b e n z en e - d 5( 1 5 .2 1 2 ) Page 293 of 478 Report Date: 28-Nov-2017 09:42:10 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-11.D Injection Date: 24-Nov-2017 18:24:30 Instrument ID: CHB.i Lims ID: 200-41113-A-4 Lab Sample ID: 200-41113-4 Client ID: AA-1 Operator ID: VTP ALS Bottle#: 11 Worklist Smp#: 40 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 44 Carbon tetrachloride, CAS: 56-23-5 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 103107111115119123 m/z 0 3 6 9 12 15 18 21 Y ( X 10 0 ) Raw Spec:Scan 1359(10.23) 117 40 8247 84 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 103107111115119123m/z 0 13 26 39 52 65 78 91 Y ( X 10 ) Amdis Enhanced Spec: Scan 1359(10.23), Qvalue=94 117 8247 8449 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 103107111115119123 m/z 0 13 26 39 52 65 78 91 Y ( X 10 0 ) Ref Spec: 44 Carbon tetrachloride (NIST) 117 8247 84 49 35 39 43 47 51 55 59 63 67 71 75 79 83 87 91 95 99 103107111115119123 m/z -100 -75 -50 -25 0 25 50 75 100 Y Differenc Spec:Scan 1 @ 10.240 min.(Qvalue: 94) 9.7 10.0 10.3 10.6 Min 0 3 6 9 12 15 18 21 Y ( X 10 0 ) m/z 117.0 1 0 . 2 3 3 9.7 10.0 10.3 10.6Min 0 3 6 9 12 15 18 Y ( X 10 0 ) m/z 119.0 1 0 . 2 4 3 9.7 10.0 10.3 10.6 Min 0 3 6 9 12 15 18 21 Y ( X 10 0 ) m/z 117.0 m/z 119.0 Page 294 of 478 Report Date: 28-Nov-2017 09:42:10 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-11.D Injection Date: 24-Nov-2017 18:24:30 Instrument ID: CHB.i Lims ID: 200-41113-A-4 Lab Sample ID: 200-41113-4 Client ID: AA-1 Operator ID: VTP ALS Bottle#: 11 Worklist Smp#:40 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 74 Ethylbenzene, CAS: 100-41-4 Signal: 1 Processing Integration Results RT: 15.46 Area: 8025 Amount: 0.036307 Amount Units: ppb v/v 15.0 15.2 15.4 15.6 15.8 Min 0 3 6 9 12 15 18 21 24 27 30 33 36 39 Y ( X 10 0 ) m/z 91.0 1 5 .4 5 8 Manual Integration Results RT: 15.32 Area: 6765 Amount: 0.030607 Amount Units: ppb v/v 15.0 15.2 15.4 15.6 15.8 Min 0 3 6 9 12 15 18 21 24 27 30 33 36 39 Y ( X 10 0 ) m/z 91.0 1 5 .3 2 4 Reviewer: puangmaleek, 28-Nov-2017 09:40:20 Audit Action: Assigned Compound ID Audit Reason: Assign Peak Page 295 of 478 Report Date: 28-Nov-2017 09:42:10 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-11.D Injection Date: 24-Nov-2017 18:24:30 Instrument ID: CHB.i Lims ID: 200-41113-A-4 Lab Sample ID: 200-41113-4 Client ID: AA-1 Operator ID: VTP ALS Bottle#: 11 Worklist Smp#:40 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 74 Ethylbenzene, CAS: 100-41-4 Signal: 1 Processing Integration Results RT: 15.46 Area: 8025 Amount: 0.036307 Amount Units: ppb v/v 15.0 15.2 15.4 15.6 15.8Min 0 3 6 9 12 15 18 21 24 27 30 33 36 39 Y ( X 10 0 ) m/z 91.0 1 5 .4 5 8 Manual Integration Results RT: 15.32 Area: 6765 Amount: 0.030607 Amount Units: ppb v/v 15.0 15.2 15.4 15.6 15.8 Min 0 3 6 9 12 15 18 21 24 27 30 33 36 39 Y ( X 10 0 ) m/z 91.0 1 5 .3 2 4 Reviewer: puangmaleek, 28-Nov-2017 09:40:35 Audit Action: Manually Integrated Audit Reason: Assign Peak Page 296 of 478 Report Date: 28-Nov-2017 09:42:10 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-11.D Injection Date: 24-Nov-2017 18:24:30 Instrument ID: CHB.i Lims ID: 200-41113-A-4 Lab Sample ID: 200-41113-4 Client ID: AA-1 Operator ID: VTP ALS Bottle#: 11 Worklist Smp#:40 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 74 Ethylbenzene, CAS: 100-41-4 Signal: 2 Processing Integration Results RT: 15.46 Area: 4203 Amount: 0.036307 Amount Units: ppb v/v 15.0 15.2 15.4 15.6 15.8Min 0 2 4 6 8 10 12 14 16 18 20 Y ( X 10 0 ) m/z 106.0 1 5 .4 6 3 Manual Integration Results RT: 15.32 Area: 1979 Amount: 0.030607 Amount Units: ppb v/v 15.0 15.2 15.4 15.6 15.8 Min 0 2 4 6 8 10 12 14 16 18 20 Y ( X 10 0 ) m/z 106.0 1 5 .3 1 9 Reviewer: puangmaleek, 28-Nov-2017 09:40:55 Audit Action: Manually Integrated Audit Reason: Assign Peak Page 297 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:GC Column:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-41113-1 200-41113-1 CHB.i Analy Batch No.:122990 38392Calibration Start Date:Calibration End Date:11/06/2017 17:59 N 11/07/2017 01:49 0.32(mm)RTX-624 ID: CURVE EVALUATION Calibration Files: LEVEL: LAB SAMPLE ID:LAB FILE ID: 1Level IC 200-122990/4 27754-04.D 2Level IC 200-122990/5 27754-05.D 3Level IC 200-122990/7 27754-07.D 4Level IC 200-122990/9 27754-09.D 5Level ICIS 200-122990/10 27754-10.D 6Level IC 200-122990/11 27754-11.D 7Level IC 200-122990/12 27754-12.D 8Level IC 200-122990/13 27754-13.D ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 #%RSD # MAX %RSD R^2 OR COD # MIN R^2 OR COD MIN RRF LVL 6 LVL 7 LVL 8 Propylene +++++ +++++ +++++ 0.7829 0.6601 Ave 25.1 0.5500 0.4987 0.4082 30.00.5800 Dichlorodifluoromethane +++++ +++++ 2.2914 2.7246 2.4725 Ave 16.5 2.1237 1.9904 1.6864 30.02.2148 Freon 22 +++++ +++++ 1.4063 1.5983 1.3978 Ave 20.3 1.1791 1.0836 0.8916 30.01.2595 1,2-Dichlorotetrafluoroethane +++++ 2.3883 2.3647 2.7373 2.5495 Ave 12.3 2.2558 2.1389 1.8473 30.02.3260 Chloromethane +++++ +++++ 0.8320 0.9935 0.8838 Ave 18.4 0.7538 0.6929 0.5839 30.00.7900 n-Butane +++++ +++++ 1.5577 1.7267 1.5143 Ave 21.0 1.2772 1.1579 0.9552 30.01.3648 Vinyl chloride 0.8415 0.9491 0.9624 1.1600 1.0764 Ave 13.0 0.9598 0.8952 0.7712 30.00.9520 1,3-Butadiene 0.4740 0.7804 0.7246 0.8751 0.8108 Ave 19.1 0.7033 0.6551 0.5558 30.00.6974 Bromomethane +++++ 0.9656 0.9095 1.0958 1.0710 Ave 8.3 0.9791 0.9705 0.8690 30.00.9801 Chloroethane +++++ +++++ 0.5922 0.6756 0.6360 Ave 10.8 0.5762 0.5621 0.4908 30.00.5888 Isopentane +++++ 1.4077 1.2780 1.4926 1.3533 Ave 16.4 1.1689 1.0797 0.9044 30.01.2407 Bromoethene(Vinyl Bromide)+++++ 0.9161 0.9119 1.1137 1.0842 Ave 8.2 1.0187 1.0226 0.9292 30.00.9995 Trichlorofluoromethane +++++ 2.4078 2.3505 2.7380 2.5386 Ave 10.2 2.3132 2.2262 1.9709 30.02.3636 n-Pentane +++++ +++++ 2.0632 2.3086 2.0528 Ave 17.0 1.7978 1.6824 1.4113 30.01.8860 FORM VI TO-15 Note: The M1 coefficient is the same as Ave RRF for an Ave curve type. Page 298 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:GC Column:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-41113-1 200-41113-1 CHB.i Analy Batch No.:122990 38392Calibration Start Date:Calibration End Date:11/06/2017 17:59 N 11/07/2017 01:49 0.32(mm)RTX-624 ID: CURVE EVALUATION ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 #%RSD # MAX %RSD R^2 OR COD # MIN R^2 OR COD MIN RRF LVL 6 LVL 7 LVL 8 Ethanol +++++ +++++ 0.6459 0.6218 0.5366 Ave 21.6 0.5058 0.4445 0.3466 30.00.5169 Ethyl ether +++++ 0.7385 0.6749 0.8592 0.7904 Ave 11.2 0.7230 0.6955 0.6063 30.00.7268 Acrolein +++++ +++++ +++++ 0.3795 0.3571 Ave 10.7 0.3339 0.3238 0.2846 30.00.3358 Freon TF +++++ 2.0105 1.9215 2.2417 2.0873 Ave 7.6 1.9535 1.9288 1.7570 30.01.9858 1,1-Dichloroethene 1.0767 0.9879 0.9257 1.1220 1.0335 Ave 8.0 0.9715 0.9613 0.8766 30.00.9944 Acetone +++++ +++++ +++++ 1.9671 1.6472 Ave 22.8 1.4241 1.3053 1.0798 30.01.4847 Isopropyl alcohol +++++ +++++ +++++ 2.0939 1.8900 Ave 20.1 1.6265 1.4975 1.2335 30.01.6683 Carbon disulfide +++++ +++++ 2.7115 3.2357 2.9747 Ave 10.3 2.7326 2.6778 2.3910 30.02.7872 3-Chloropropene +++++ 1.2877 1.4743 1.7599 1.5339 Ave 16.3 1.3214 1.2899 1.0459 30.01.3876 Acetonitrile +++++ +++++ +++++ 1.0683 0.9412 Ave 18.6 0.8395 0.7931 0.6435 30.00.8571 Methylene Chloride +++++ +++++ 1.2793 1.4439 1.2974 Ave 15.8 1.1396 1.0774 0.9096 30.01.1912 tert-Butyl alcohol +++++ +++++ +++++ 2.6008 2.4183 Ave 16.2 2.1514 2.0009 1.7033 30.02.1749 Methyl tert-butyl ether +++++ 2.9417 2.9055 3.4433 3.1851 Ave 9.9 2.9313 2.8376 2.4993 30.02.9634 trans-1,2-Dichloroethene +++++ 1.4923 1.5010 1.8046 1.6314 Ave 11.6 1.4696 1.4209 1.2410 30.01.5087 Acrylonitrile +++++ +++++ 0.7556 0.9553 0.8764 Ave 13.3 0.7861 0.7511 0.6518 30.00.7960 n-Hexane +++++ 2.2246 1.8618 2.0543 1.8508 Ave 15.1 1.6778 1.6270 1.4080 30.01.8149 1,1-Dichloroethane 2.0934 2.1348 1.9465 2.3805 2.1550 Ave 11.3 1.9393 1.8669 1.6212 30.02.0172 Vinyl acetate +++++ +++++ +++++ 3.4470 3.0993 Ave 18.7 2.7075 2.5332 2.0968 30.02.7768 Methyl Ethyl Ketone +++++ +++++ 0.5949 0.6707 0.6140 Ave 9.9 0.5758 0.5598 0.4967 30.00.5853 cis-1,2-Dichloroethene 1.0265 1.1079 1.1319 1.3367 1.2420 Ave 8.7 1.1515 1.1465 1.0510 30.01.1492 FORM VI TO-15 Note: The M1 coefficient is the same as Ave RRF for an Ave curve type. Page 299 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:GC Column:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-41113-1 200-41113-1 CHB.i Analy Batch No.:122990 38392Calibration Start Date:Calibration End Date:11/06/2017 17:59 N 11/07/2017 01:49 0.32(mm)RTX-624 ID: CURVE EVALUATION ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 #%RSD # MAX %RSD R^2 OR COD # MIN R^2 OR COD MIN RRF LVL 6 LVL 7 LVL 8 Ethyl acetate +++++ +++++ +++++ 0.1076 0.0996 Ave 7.9 0.0947 0.0943 0.0870 30.00.0966 Tetrahydrofuran +++++ +++++ +++++ 0.3310 0.2952 Ave 18.0 0.2597 0.2427 0.2058 30.00.2669 Chloroform +++++ 2.2341 2.1363 2.5153 2.2926 Ave 10.5 2.0932 2.0258 1.7891 30.02.1552 1,1,1-Trichloroethane +++++ 0.4231 0.4045 0.4843 0.4423 Ave 9.0 0.4138 0.3991 0.3643 30.00.4188 Cyclohexane +++++ 0.3010 0.2998 0.3520 0.3312 Ave 6.5 0.3164 0.3106 0.2936 30.00.3149 Carbon tetrachloride 0.3009 0.3763 0.3778 0.4850 0.4482 Ave 14.1 0.4161 0.4055 0.3660 30.00.3970 2,2,4-Trimethylpentane +++++ 1.1816 1.1319 1.3969 1.2863 Ave 10.0 1.1833 1.1435 1.0224 30.01.1923 Benzene +++++ 0.8467 0.6963 0.8076 0.7509 Ave 9.6 0.7066 0.6947 0.6448 30.00.7354 1,2-Dichloroethane +++++ 0.2685 0.2617 0.3168 0.2819 Ave 12.8 0.2557 0.2403 0.2088 30.00.2620 n-Heptane +++++ 0.5170 0.4567 0.5452 0.4864 Ave 14.9 0.4327 0.4065 0.3467 30.00.4559 n-Butanol +++++ +++++ +++++ 0.1668 0.1519 Ave 12.7 0.1405 0.1330 0.1194 30.00.1423 Trichloroethene 0.2401 0.2996 0.2832 0.3386 0.3170 Ave 9.9 0.2997 0.2937 0.2764 30.00.2935 1,2-Dichloropropane +++++ 0.2687 0.2760 0.3329 0.3048 Ave 9.9 0.2805 0.2727 0.2455 30.00.2830 Methyl methacrylate +++++ +++++ 0.2292 0.3030 0.2824 Ave 10.3 0.2660 0.2614 0.2392 30.00.2636 1,4-Dioxane +++++ +++++ +++++ 0.1611 0.1514 Ave 12.1 0.1361 0.1317 0.1180 30.00.1397 Dibromomethane +++++ 0.2979 0.2699 0.3137 0.3028 Ave 4.9 0.2888 0.2886 0.2816 30.00.2919 Bromodichloromethane +++++ 0.4877 0.4846 0.5765 0.5250 Ave 9.3 0.4841 0.4728 0.4296 30.00.4943 cis-1,3-Dichloropropene +++++ 0.3579 0.3732 0.4671 0.4333 Ave 10.0 0.4057 0.3964 0.3626 30.00.3995 methyl isobutyl ketone +++++ +++++ 0.5274 0.6939 0.6217 Ave 15.7 0.5534 0.5193 0.4418 30.00.5596 n-Octane +++++ 0.7051 0.6394 0.7851 0.7038 Ave 15.8 0.6170 0.5731 0.4739 30.00.6425 FORM VI TO-15 Note: The M1 coefficient is the same as Ave RRF for an Ave curve type. Page 300 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:GC Column:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-41113-1 200-41113-1 CHB.i Analy Batch No.:122990 38392Calibration Start Date:Calibration End Date:11/06/2017 17:59 N 11/07/2017 01:49 0.32(mm)RTX-624 ID: CURVE EVALUATION ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 #%RSD # MAX %RSD R^2 OR COD # MIN R^2 OR COD MIN RRF LVL 6 LVL 7 LVL 8 Toluene +++++ 0.6339 0.5826 0.6554 0.6047 Ave 6.2 0.5799 0.5800 0.5468 30.00.5976 trans-1,3-Dichloropropene +++++ 0.3346 0.3455 0.4525 0.4221 Ave 11.6 0.3925 0.3813 0.3444 30.00.3818 1,1,2-Trichloroethane +++++ 0.2865 0.2877 0.3363 0.3078 Ave 7.4 0.2899 0.2872 0.2669 30.00.2946 Tetrachloroethene 0.4049 0.4856 0.4437 0.5203 0.4923 Ave 7.3 0.4773 0.4824 0.4813 30.00.4735 Methyl Butyl Ketone (2-Hexanone)+++++ +++++ 0.5755 0.7349 0.6543 Ave 15.1 0.5902 0.5522 0.4717 30.00.5965 Dibromochloromethane +++++ 0.4889 0.5130 0.6486 0.5890 Ave 9.3 0.5692 0.5751 0.5502 30.00.5620 1,2-Dibromoethane +++++ 0.4721 0.4869 0.5932 0.5535 Ave 8.0 0.5271 0.5240 0.4978 30.00.5221 Chlorobenzene +++++ 0.7665 0.7498 0.8805 0.8257 Ave 5.6 0.7935 0.7987 0.7640 30.00.7969 Ethylbenzene +++++ 1.3137 1.2635 1.4522 1.3595 Ave 6.1 1.2926 1.2872 1.1962 30.01.3093 n-Nonane +++++ 0.7085 0.6416 0.7816 0.7118 Ave 10.7 0.6581 0.6358 0.5564 30.00.6705 m,p-Xylene +++++ 0.4698 0.4754 0.5680 0.5374 Ave 6.7 0.5223 0.5280 0.5093 30.00.5157 Xylene, o-+++++ 0.5030 0.4818 0.5654 0.5294 Ave 5.4 0.5106 0.5118 0.4895 30.00.5131 Styrene +++++ 0.6356 0.6948 0.8608 0.8308 Ave 10.3 0.8061 0.8054 0.7779 30.00.7731 Bromoform +++++ 0.3603 0.4638 0.6155 0.5331 Ave 16.0 0.5402 0.5618 0.5546 30.00.5185 Cumene +++++ 1.3804 1.3509 1.6284 1.5219 Ave 6.9 1.4541 1.4572 1.3600 30.01.4504 1,1,2,2-Tetrachloroethane +++++ 0.7546 0.7550 0.9074 0.8461 Ave 8.9 0.7893 0.7773 0.6911 30.00.7887 n-Propylbenzene +++++ 1.6752 1.6612 2.0570 1.9213 Ave 9.2 1.8237 1.7852 1.5869 30.01.7872 1,2,3-Trichloropropane +++++ +++++ 0.5846 0.6993 0.6432 Ave 10.7 0.6009 0.5824 0.5077 30.00.6030 n-Decane +++++ +++++ 0.8484 1.0271 0.9342 Ave 13.9 0.8239 0.7681 0.6962 30.00.8496 4-Ethyltoluene +++++ 1.3269 1.3118 1.6058 1.5220 Ave 8.0 1.4553 1.4153 1.3162 30.01.4219 FORM VI TO-15 Note: The M1 coefficient is the same as Ave RRF for an Ave curve type. Page 301 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:GC Column:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-41113-1 200-41113-1 CHB.i Analy Batch No.:122990 38392Calibration Start Date:Calibration End Date:11/06/2017 17:59 N 11/07/2017 01:49 0.32(mm)RTX-624 ID: CURVE EVALUATION ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 #%RSD # MAX %RSD R^2 OR COD # MIN R^2 OR COD MIN RRF LVL 6 LVL 7 LVL 8 2-Chlorotoluene +++++ 1.1452 1.1011 1.3512 1.2650 Ave 8.2 1.1948 1.1561 1.0727 30.01.1837 1,3,5-Trimethylbenzene +++++ 1.1098 1.0937 1.3356 1.2640 Ave 7.9 1.1903 1.1241 1.1109 30.01.1755 Alpha Methyl Styrene +++++ 0.4546 0.5151 0.6583 0.6358 Ave 12.2 0.6062 0.5804 0.5793 30.00.5757 tert-Butylbenzene +++++ 1.0989 1.0603 1.3058 1.2158 Ave 8.1 1.1321 1.0879 1.0585 30.01.1370 1,2,4-Trimethylbenzene +++++ 1.0658 1.0879 1.3456 1.2681 Ave 9.1 1.1601 1.1076 1.0949 30.01.1614 sec-Butylbenzene +++++ 1.6931 1.6828 2.0505 1.9037 Ave 8.7 1.7262 1.6672 1.6325 30.01.7651 4-Isopropyltoluene +++++ 1.3427 1.3572 1.6854 1.5692 Ave 8.8 1.3920 1.3924 1.4166 30.01.4508 1,3-Dichlorobenzene +++++ 0.6309 0.7114 0.8725 0.8442 Ave 10.6 0.7987 0.7574 0.7891 30.00.7721 1,4-Dichlorobenzene +++++ 0.5716 0.7094 0.8557 0.8331 Ave 12.6 0.7836 0.7400 0.7911 30.00.7549 Benzyl chloride +++++ 0.5174 0.7780 1.0518 1.0220 Ave 20.7 0.9241 0.8764 0.8708 30.00.8629 n-Undecane +++++ +++++ +++++ 1.1078 0.9638 Ave 14.0 0.9189 0.8755 0.7541 30.00.9240 n-Butylbenzene +++++ 1.2292 1.2726 1.5850 1.4294 Ave 9.7 1.2744 1.2827 1.2539 30.01.3325 1,2-Dichlorobenzene +++++ 0.6255 0.6790 0.8309 0.7888 Ave 9.5 0.7182 0.6983 0.7406 30.00.7259 n-Dodecane +++++ +++++ +++++ 0.8750 0.7977 Ave 27.8 0.7950 0.7338 0.3703 30.00.7144 1,2,4-Trichlorobenzene +++++ +++++ 0.3683 0.4341 0.4634 Ave 10.9 0.5095 0.4881 0.4409 30.00.4507 Hexachlorobutadiene +++++ 0.4594 0.4545 0.5337 0.4879 Ave 9.8 0.4986 0.4985 0.3880 30.00.4744 Naphthalene +++++ +++++ 0.8313 0.8572 0.9553 Ave 10.8 1.1083 1.0204 0.9401 30.00.9521 1,2,3-Trichlorobenzene +++++ +++++ 0.3347 0.3923 0.4117 Ave 13.2 0.4480 0.4344 0.3232 30.00.3907 FORM VI TO-15 Note: The M1 coefficient is the same as Ave RRF for an Ave curve type. Page 302 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-41113-1 200-41113-1 CHB.i Analy Batch No.:122990 38392Calibration Start Date:Calibration End Date:11/06/2017 17:59 N 11/07/2017 01:49 GC Column:RTX-624 ID:0.32(mm) RESPONSE AND CONCENTRATION Calibration Files: LEVEL: LAB SAMPLE ID:LAB FILE ID: Level 1 IC 200-122990/4 27754-04.D Level 2 IC 200-122990/5 27754-05.D Level 3 IC 200-122990/7 27754-07.D Level 4 IC 200-122990/9 27754-09.D Level 5 ICIS 200-122990/10 27754-10.D Level 6 IC 200-122990/11 27754-11.D Level 7 IC 200-122990/12 27754-12.D Level 8 IC 200-122990/13 27754-13.D ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (PPB V/V) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 6 LVL 7 LVL 8 Propylene AveBCM +++++ +++++ +++++ 94270 178752 262308 350917 666801 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Dichlorodifluoromethane AveBCM +++++ +++++ 27637 328049 669500 1012917 1400515 2754680 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Freon 22 AveBCM +++++ +++++ 16962 192442 378485 562365 762497 1456389 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 1,2-Dichlorotetrafluoroethane AveBCM +++++ 11568 28521 329585 690355 1075928 1504994 3017555 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Chloromethane AveBCM +++++ +++++ 10035 119627 239308 359553 487565 953781 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 n-Butane AveBCM +++++ +++++ 18787 207906 410042 609191 814735 1560254 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Vinyl chloride AveBCM 687 4597 11608 139669 291466 457798 629881 1259739 0.0351 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,3-Butadiene AveBCM 387 3780 8740 105361 219553 335437 460938 907836 0.0351 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Bromomethane AveBCM +++++ 4677 10970 131944 290018 466967 682895 1419547 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Chloroethane AveBCM +++++ +++++ 7142 81341 172230 274839 395487 801767 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Isopentane AveBCM +++++ 6818 15414 179718 366461 557524 759706 1477241 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Bromoethene(Vinyl Bromide)AveBCM +++++ 4437 10998 134098 293593 485880 719528 1517808 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Trichlorofluoromethane AveBCM +++++ 11662 28350 329662 687404 1103290 1566416 3219338 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Pentane AveBCM +++++ +++++ 24884 277962 555873 857492 1183796 2305350 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Ethanol AveBCM +++++ +++++ 78001 149824 218031 322355 625643 1415524 +++++ +++++ 5.01 9.99 15.0 20.0 40.0 100.0 FORM VI TO-15 Page 303 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-41113-1 200-41113-1 CHB.i Analy Batch No.:122990 38392Calibration Start Date:Calibration End Date:11/06/2017 17:59 N 11/07/2017 01:49 GC Column:RTX-624 ID:0.32(mm) RESPONSE AND CONCENTRATION ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (PPB V/V) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 6 LVL 7 LVL 8 Ethyl ether AveBCM +++++ 3577 8140 103447 214038 344829 489381 990383 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Acrolein AveBCM +++++ +++++ +++++ 45692 96696 159278 227859 464860 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Freon TF AveBCM +++++ 9738 23175 269917 565202 931730 1357192 2870018 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,1-Dichloroethene AveBCM 879 4785 11165 135100 279844 463386 676409 1431915 0.0351 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Acetone AveBCM +++++ +++++ +++++ 236842 446021 679222 918444 1763733 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Isopropyl alcohol AveBCM +++++ +++++ +++++ 252112 511783 775787 1053695 2014852 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Carbon disulfide AveBCM +++++ +++++ 32704 389595 805496 1303321 1884193 3905659 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 3-Chloropropene AveBCM +++++ 6237 17782 211903 415357 630248 907636 1708448 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Acetonitrile AveBCM +++++ +++++ +++++ 128629 254873 400394 558071 1051183 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Methylene Chloride AveBCM +++++ +++++ 15430 173856 351310 543530 758104 1485831 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 tert-Butyl alcohol AveBCM +++++ +++++ +++++ 313150 654836 1026121 1407939 2782228 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Methyl tert-butyl ether AveBCM +++++ 14248 35044 414586 862467 1398096 1996655 4082553 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 trans-1,2-Dichloroethene AveBCM +++++ 7228 18104 217279 441740 700935 999814 2027160 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Acrylonitrile AveBCM +++++ +++++ 9113 115020 237313 374931 528510 1064673 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 n-Hexane AveBCM +++++ 10775 22455 247350 501161 800225 1144849 2299897 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,1-Dichloroethane AveBCM 1709 10340 23477 286623 583546 924957 1313600 2648188 0.0351 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Vinyl acetate AveBCM +++++ +++++ +++++ 415040 839222 1291360 1782446 3425006 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Methyl Ethyl Ketone AveBCM +++++ +++++ 7175 80752 166254 274656 393924 811284 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 cis-1,2-Dichloroethene AveBCM 838 5366 13652 160947 336303 549204 806754 1716713 0.0351 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Ethyl acetate AveBCM +++++ +++++ +++++ 12961 26960 45156 66363 142076 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Tetrahydrofuran AveDFBZ +++++ +++++ +++++ 202420 402366 611226 842926 1611154 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 FORM VI TO-15 Page 304 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-41113-1 200-41113-1 CHB.i Analy Batch No.:122990 38392Calibration Start Date:Calibration End Date:11/06/2017 17:59 N 11/07/2017 01:49 GC Column:RTX-624 ID:0.32(mm) RESPONSE AND CONCENTRATION ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (PPB V/V) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 6 LVL 7 LVL 8 Chloroform AveBCM +++++ 10821 25766 302854 620796 998358 1425408 2922350 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,1,1-Trichloroethane AveDFBZ +++++ 10372 24994 296136 602834 973905 1386002 2851804 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Cyclohexane AveDFBZ +++++ 7379 18527 215268 451412 744741 1078684 2298205 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Carbon tetrachloride AveDFBZ 1233 9225 23344 296544 610969 979389 1408169 2864853 0.0351 0.200 0.500 4.99 10.00 15.0 20.0 40.0 2,2,4-Trimethylpentane AveDFBZ +++++ 28967 69941 854191 1753387 2785353 3971225 8002808 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Benzene AveDFBZ +++++ 20758 43028 493843 1023623 1663189 2412590 5046961 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,2-Dichloroethane AveDFBZ +++++ 6582 16172 193741 384279 601835 834386 1634383 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Heptane AveDFBZ +++++ 12675 28219 333367 663081 1018472 1411728 2713764 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Butanol AveDFBZ +++++ +++++ +++++ 101995 207031 330651 462049 934673 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Trichloroethene AveDFBZ 984 7346 17501 207050 432058 705472 1020053 2163493 0.0351 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,2-Dichloropropane AveDFBZ +++++ 6587 17056 203574 415515 660207 947123 1921446 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Methyl methacrylate AveDFBZ +++++ +++++ 14165 185277 384997 626224 907851 1872327 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 1,4-Dioxane AveDFBZ +++++ +++++ +++++ 98539 206434 320238 457426 923935 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Dibromomethane AveDFBZ +++++ 7303 16681 191845 412753 679826 1002264 2204560 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Bromodichloromethane AveDFBZ +++++ 11957 29942 352531 715566 1139481 1641881 3362489 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 cis-1,3-Dichloropropene AveDFBZ +++++ 8775 23060 285608 590668 955016 1376724 2838418 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 methyl isobutyl ketone AveDFBZ +++++ +++++ 32590 424306 847377 1302488 1803414 3457992 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 n-Octane AveDFBZ +++++ 17287 39510 480047 959417 1452261 1990415 3709404 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Toluene AveCBNZ d5 +++++ 13793 31753 362352 753577 1231696 1809158 3852181 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 trans-1,3-Dichloropropene AveDFBZ +++++ 8203 21348 276675 575307 923761 1324222 2695893 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,1,2-Trichloroethane AveCBNZ d5 +++++ 6233 15678 185969 383516 615856 895676 1880575 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 FORM VI TO-15 Page 305 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-41113-1 200-41113-1 CHB.i Analy Batch No.:122990 38392Calibration Start Date:Calibration End Date:11/06/2017 17:59 N 11/07/2017 01:49 GC Column:RTX-624 ID:0.32(mm) RESPONSE AND CONCENTRATION ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (PPB V/V) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 6 LVL 7 LVL 8 Tetrachloroethene AveCBNZ d5 1459 10565 24183 287651 613429 1013752 1504548 3391200 0.0351 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Methyl Butyl Ketone (2-Hexanone)AveCBNZ d5 +++++ +++++ 31361 406329 815397 1253699 1722537 3323450 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Dibromochloromethane AveCBNZ d5 +++++ 10638 27956 358608 734000 1209039 1793665 3876618 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,2-Dibromoethane AveCBNZ d5 +++++ 10271 26533 327996 689766 1119668 1634580 3507458 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Chlorobenzene AveCBNZ d5 +++++ 16678 40862 486827 1028944 1685338 2491305 5382503 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Ethylbenzene AveCBNZ d5 +++++ 28583 68858 802931 1694195 2745535 4014844 8428186 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Nonane AveCBNZ d5 +++++ 15416 34964 432179 886988 1397898 1983042 3919902 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 m,p-Xylene AveCBNZ d5 +++++ 20444 51820 628058 1339356 2218882 3293994 7176091 +++++ 0.401 1.00 9.99 20.0 30.0 40.0 80.0 Xylene, o-AveCBNZ d5 +++++ 10945 26258 312634 659664 1084561 1596485 3448842 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Styrene AveCBNZ d5 +++++ 13830 37866 475931 1035340 1712264 2512147 5480628 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Bromoform AveCBNZ d5 +++++ 7840 25278 340328 664355 1147379 1752241 3907202 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Cumene AveCBNZ d5 +++++ 30035 73623 900374 1896589 3088484 4545305 9581691 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,1,2,2-Tetrachloroethane AveCBNZ d5 +++++ 16418 41145 501706 1054405 1676500 2424642 4869536 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Propylbenzene AveCBNZ d5 +++++ 36449 90532 1137310 2394240 3873668 5568174 11180756 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,2,3-Trichloropropane AveCBNZ d5 +++++ +++++ 31857 386627 801515 1276362 1816466 3577331 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 n-Decane AveCBNZ d5 +++++ +++++ 46234 567864 1164188 1749982 2395755 4905409 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 4-Ethyltoluene AveCBNZ d5 +++++ 28872 71488 887867 1896619 3091160 4414476 9273522 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 2-Chlorotoluene AveCBNZ d5 +++++ 24918 60006 747078 1576394 2537832 3605957 7557699 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,3,5-Trimethylbenzene AveCBNZ d5 +++++ 24147 59606 738489 1575121 2528343 3506340 7827219 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Alpha Methyl Styrene AveCBNZ d5 +++++ 9891 28073 363985 792287 1287536 1810300 4081481 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 tert-Butylbenzene AveCBNZ d5 +++++ 23910 57783 722005 1515083 2404614 3393419 7457439 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 FORM VI TO-15 Page 306 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-41113-1 200-41113-1 CHB.i Analy Batch No.:122990 38392Calibration Start Date:Calibration End Date:11/06/2017 17:59 N 11/07/2017 01:49 GC Column:RTX-624 ID:0.32(mm) RESPONSE AND CONCENTRATION ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (PPB V/V) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 6 LVL 7 LVL 8 1,2,4-Trimethylbenzene AveCBNZ d5 +++++ 23191 59289 743964 1580281 2464062 3454778 7714438 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 sec-Butylbenzene AveCBNZ d5 +++++ 36838 91707 1133717 2372305 3666512 5200086 11501603 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 4-Isopropyltoluene AveCBNZ d5 +++++ 29214 73963 931887 1955482 2956723 4342966 9980594 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,3-Dichlorobenzene AveCBNZ d5 +++++ 13728 38771 482419 1052014 1696474 2362589 5559940 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,4-Dichlorobenzene AveCBNZ d5 +++++ 12436 38663 473120 1038211 1664444 2308042 5573724 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Benzyl chloride AveCBNZ d5 +++++ 11257 42398 581535 1273643 1962790 2733690 6135081 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Undecane AveCBNZ d5 +++++ +++++ +++++ 612517 1200999 1951866 2730816 5313148 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 n-Butylbenzene AveCBNZ d5 +++++ 26745 69356 876363 1781253 2706883 4000789 8834446 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,2-Dichlorobenzene AveCBNZ d5 +++++ 13609 37002 459422 983042 1525509 2178021 5217884 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Dodecane AveCBNZ d5 +++++ +++++ +++++ 483798 994023 1688580 2288869 2608958 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 1,2,4-Trichlorobenzene AveCBNZ d5 +++++ +++++ 20073 240031 577428 1082245 1522402 3106580 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Hexachlorobutadiene AveCBNZ d5 +++++ 9995 24771 295106 608010 1059150 1555025 2733620 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Naphthalene AveCBNZ d5 +++++ +++++ 45302 473935 1190473 2354157 3182700 6623680 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 1,2,3-Trichlorobenzene AveCBNZ d5 +++++ +++++ 18238 216879 513047 951579 1354997 2277299 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Curve Type Legend: Ave = Average ISTD FORM VI TO-15 Page 307 of 478 Report Date: 07-Nov-2017 13:39:37 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Target Compound Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-04.D Lims ID: ic Client ID: Sample Type: IC Calib Level: 1 Inject. Date: 06-Nov-2017 17:59:30 ALS Bottle#: 4 Worklist Smp#: 4 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Sample Info: 200-0027754-004 Misc. Info.: ic Operator ID: vtp Instrument ID: CHB.i Sublist:chrom-TO15_LLNJ_TO3*sub5 Method:\\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\TO15_LLNJ_TO3.m Limit Group: AI_TO15_ICAL Last Update: 07-Nov-2017 13:39:36 Calib Date: 07-Nov-2017 01:49:30 Integrator: RTE ID Type: Deconvolution ID Quant Method: Internal/External Standard Quant By: Initial Calibration Last ICal File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-13.D Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host:XAWRK022 First Level Reviewer: daiglep Date:07-Nov-2017 08:54:08 Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 1 Propene 41 3.145 3.135 0.010 60 1084 0.0351 0.0803 2 Dichlorodifluoromethane 85 3.199 3.193 0.006 96 1821 0.0351 0.0353 3 Chlorodifluoromethane 51 3.236 3.225 0.011 95 1482 0.0351 0.0506 4 1,2-Dichloro-1,1,2,2-tetra 85 3.417 3.412 0.005 90 1766 0.0351 0.0326 5 Chloromethane 50 3.540 3.535 0.005 1 824 0.0351 0.0448 6 Butane 43 3.716 3.711 0.005 93 2069 0.0351 0.0651 7 Vinyl chloride 62 3.754 3.748 0.006 86 687 0.0351 0.0310 8 Butadiene 54 3.818 3.812 0.006 1 387 0.0351 0.0238 10 Bromomethane 94 4.490 4.479 0.011 1 497 0.0351 0.0218 9 BFB 11 Chloroethane 64 4.709 ND ND 12 2-Methylbutane 43 4.794 4.789 0.005 1 1000 0.0351 0.0346 13 Vinyl bromide 106 5.120 5.120 0.000 1 539 0.0351 0.0232 14 Trichlorofluoromethane 101 5.221 5.216 0.005 1 1623 0.0351 0.0295 15 Pentane 43 5.365 5.355 0.010 94 3076 0.0351 0.0701 16 Ethanol 45 5.702 5.675 0.027 97 1504 0.0702 0.1250 17 Ethyl ether 59 5.830 ND ND 18 Acrolein 56 6.198 ND ND 19 1,1,2-Trichloro-1,2,2-trif 101 6.230 6.246 -0.016 1 1226 0.0351 0.0265 20 1,1-Dichloroethene 96 6.326 6.321 0.005 0 879 0.0351 0.0380 M 21 Acetone 43 6.507 6.470 0.037 97 6717 0.0351 0.1944 22 Isopropyl alcohol 45 6.748 6.684 0.064 63 579 0.0351 0.0149 23 Carbon disulfide 76 6.753 6.748 0.005 94 2114 0.0351 0.0326 24 3-Chloro-1-propene 41 7.025 7.020 0.005 1 1179 0.0351 0.0365 26 Acetonitrile 41 7.025 7.079 -0.054 34 1179 0.0351 0.0591 27 Methylene Chloride 49 7.287 7.276 0.011 91 1215 0.0351 0.0438 28 2-Methyl-2-propanol 59 7.436 7.388 0.048 1 1666 0.0351 0.0329 29 Methyl tert-butyl ether 73 7.687 7.628 0.059 91 1552 0.0351 0.0225 30 trans-1,2-Dichloroethene 61 7.682 7.687 -0.005 0 575 0.0351 0.0164 31 Acrylonitrile 53 7.778 7.756 0.022 1 219 0.0351 0.0118 Page 308 of 478 Report Date: 07-Nov-2017 13:39:37 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-04.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 32 Hexane 57 8.012 8.018 -0.006 94 2859 0.0351 0.0677 33 1,1-Dichloroethane 63 8.418 8.429 -0.011 91 1709 0.0351 0.0364 34 Vinyl acetate 43 8.455 8.434 0.021 60 1650 0.0351 0.0255 36 2-Butanone (MEK) 72 9.347 9.320 0.027 96 426 0.0351 0.0313 37 cis-1,2-Dichloroethene 96 9.331 9.331 0.000 50 838 0.0351 0.0313 M 35 Ethyl acetate 88 9.336 ND ND * 39 Chlorobromomethane 128 9.699 9.699 0.000 96 232740 10.0 10.0 38 Tetrahydrofuran 42 9.758 9.710 0.048 53 1047 0.0351 0.0336 40 Chloroform 83 9.779 9.774 0.005 70 1415 0.0351 0.0282 S 41 1,2-Dichloroethene, Total 61 0 0.0702 0.0477 42 1,1,1-Trichloroethane 97 10.035 10.035 0.000 79 1397 0.0351 0.0286 43 Cyclohexane 84 10.035 10.046 -0.011 1 326 0.0351 0.008860 44 Carbon tetrachloride 117 10.238 10.243 -0.005 83 1233 0.0351 0.0266 45 Isooctane 57 10.521 ND ND 46 Benzene 78 10.558 10.564 -0.006 94 3865 0.0351 0.0450 47 1,2-Dichloroethane 62 10.665 ND ND 48 n-Heptane 43 10.766 10.777 -0.011 88 1972 0.0351 0.0370 A 49 GRO 1 10.865 (4.779-16.951) 0 4176944 0.0351 0 * 50 1,4-Difluorobenzene 114 11.103 11.102 0.000 94 1168258 10.0 10.0 51 n-Butanol 56 11.337 11.289 0.048 83 1075 0.0351 0.0647 53 Trichloroethene 95 11.481 11.476 0.005 83 984 0.0351 0.0287 M 54 1,2-Dichloropropane 63 11.839 11.844 -0.005 90 1133 0.0351 0.0343 55 Methyl methacrylate 69 11.882 ND ND 56 1,4-Dioxane 88 12.020 11.967 0.053 45 468 0.0351 0.0287 57 Dibromomethane 174 12.036 12.031 0.005 94 1449 0.0351 0.0425 58 Dichlorobromomethane 83 12.202 12.202 0.000 87 1830 0.0351 0.0317 A 59 TVOC as Toluene 1 12.485 (3.125-21.845) 0 4497654 0.0351 0 60 cis-1,3-Dichloropropene 75 12.832 12.832 0.000 83 1344 0.0351 0.0288 61 4-Methyl-2-pentanone (MIBK 43 13.002 12.976 0.026 8 2066 0.0351 0.0316 63 n-Octane 43 13.253 13.248 0.005 89 2837 0.0351 0.0378 64 Toluene 92 13.259 13.264 -0.005 91 2668 0.0351 0.0435 66 trans-1,3-Dichloropropene 75 13.616 13.622 -0.006 1 870 0.0351 0.0195 67 1,1,2-Trichloroethane 83 13.894 ND ND 68 Tetrachloroethene 166 14.038 14.038 0.000 92 1459 0.0351 0.0300 M 69 2-Hexanone 43 14.187 14.155 0.032 82 2176 0.0351 0.0355 70 Chlorodibromomethane 129 14.454 14.449 0.005 93 1383 0.0351 0.0240 71 Ethylene Dibromide 107 14.652 14.652 0.000 90 1571 0.0351 0.0293 * 72 Chlorobenzene-d5 117 15.212 15.212 0.000 86 1027167 10.0 10.0 73 Chlorobenzene 112 15.255 15.255 0.000 82 3015 0.0351 0.0368 74 Ethylbenzene 91 15.319 15.319 0.000 96 6627 0.0351 0.0493 75 n-Nonane 57 15.340 15.340 0.000 68 2506 0.0351 0.0364 76 m-Xylene & p-Xylene 106 15.473 15.468 0.005 0 3081 0.0702 0.0582 78 o-Xylene 106 15.980 15.981 -0.001 96 2184 0.0351 0.0414 S 77 Xylenes, Total 106 0 0.1052 0.0996 79 Styrene 104 16.007 16.002 0.005 92 2006 0.0351 0.0253 80 Bromoform 173 16.295 16.295 0.000 89 1032 0.0351 0.0194 81 Isopropylbenzene 105 16.391 16.391 0.000 96 4484 0.0351 0.0301 83 1,1,2,2-Tetrachloroethane 83 16.797 16.797 0.000 90 2657 0.0351 0.0328 84 N-Propylbenzene 91 16.877 16.872 0.005 98 5752 0.0351 0.0313 85 1,2,3-Trichloropropane 75 16.648 16.647 0.001 61 325918 0.0351 5.26 86 n-Decane 57 16.941 16.941 0.000 88 2936 0.0351 0.0336 87 4-Ethyltoluene 105 17.000 16.995 0.005 96 4545 0.0351 0.0311 Page 309 of 478 Report Date: 07-Nov-2017 13:39:37 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-04.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 88 2-Chlorotoluene 91 17.037 17.037 0.000 92 4069 0.0351 0.0335 89 1,3,5-Trimethylbenzene 105 17.064 17.064 0.000 92 3821 0.0351 0.0316 90 Alpha Methyl Styrene 118 17.341 17.336 0.005 79 1387 0.0351 0.0235 91 tert-Butylbenzene 119 17.437 17.437 0.000 92 3760 0.0351 0.0322 92 1,2,4-Trimethylbenzene 105 17.507 17.507 0.000 92 3687 0.0351 0.0309 93 sec-Butylbenzene 105 17.694 17.694 0.000 97 5875 0.0351 0.0324 94 4-Isopropyltoluene 119 17.838 17.848 -0.010 96 4621 0.0351 0.0310 95 1,3-Dichlorobenzene 146 17.928 17.928 0.000 92 2242 0.0351 0.0283 96 1,4-Dichlorobenzene 146 18.040 18.035 0.005 93 2046 0.0351 0.0264 97 Benzyl chloride 91 18.185 18.185 0.000 95 1802 0.0351 0.0203 98 Undecane 57 18.318 18.318 0.000 94 3184 0.0351 0.0335 99 n-Butylbenzene 91 18.355 18.355 0.000 95 4247 0.0351 0.0310 100 1,2-Dichlorobenzene 146 18.526 18.521 0.005 91 2298 0.0351 0.0308 102 Dodecane 57 19.770 19.770 0.000 88 2769 0.0351 0.0377 103 1,2,4-Trichlorobenzene 180 20.880 20.885 -0.005 81 1045 0.0351 0.0226 104 Hexachlorobutadiene 225 21.051 21.051 -0.001 83 1834 0.0351 0.0376 105 Naphthalene 128 21.376 21.360 0.016 93 1534 0.0351 0.0157 106 1,2,3-Trichlorobenzene 180 21.851 21.835 0.016 1 1034 0.0351 0.0258 QC Flag Legend Processing Flags ND - Not Detected or Marked ND Review Flags M - Manually Integrated Reagents: ATTO15CAL1w_00179 Amount Added: 35.00 Units: mL ATTO15BISs_00006 Amount Added: 20.00 Units: mL Run Reagent Page 310 of 478 Report Date: 07-Nov-2017 13:39:37 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-04.D Injection Date: 06-Nov-2017 17:59:30 Instrument ID: CHB.i Operator ID: vtp Lims ID: ic Worklist Smp#: 4 Client ID: Purge Vol: 200.000 mL Dil. Factor: 1.0000 ALS Bottle#: 4 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Y Scaling: Method Defined: Scale to the Nth Largest Target: 1 2.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 18.0 20.0 22.0 24.0 Min 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 Y ( X 10 0 0 0 0 ) 27754-04[MS SCAN Chro]:Total * C h l o r o b r o m o m e t h a n e ( 9 . 6 9 9 ) * 1 ,4- D i f lu o r o b e n z en e ( 1 1 . 1 0 3 ) * C h l o r o b e n z en e - d 5 ( 1 5 . 2 1 2 )+ Page 311 of 478 Report Date: 07-Nov-2017 13:39:37 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-04.D Injection Date: 06-Nov-2017 17:59:30 Instrument ID: CHB.i Lims ID: ic Client ID: Operator ID: vtp ALS Bottle#: 4 Worklist Smp#:4 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 20 1,1-Dichloroethene, CAS: 75-35-4 Signal: 1 Processing Integration Results Not Detected Expected RT: 6.32 6.0 6.2 6.4 6.6 Min 0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 Y ( X 10 ) m/z 96.0 Manual Integration Results RT: 6.33 Area: 879 Amount: 0.037980 Amount Units: ppb v/v 6.0 6.2 6.4 6.6 Min 0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 Y ( X 10 ) m/z 96.0 6 . 3 2 6 Reviewer: daiglep, 07-Nov-2017 08:53:49 Audit Action: Manually Integrated Audit Reason: Missed Peak Page 312 of 478 Report Date: 07-Nov-2017 13:39:37 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-04.D Injection Date: 06-Nov-2017 17:59:30 Instrument ID: CHB.i Lims ID: ic Client ID: Operator ID: vtp ALS Bottle#: 4 Worklist Smp#:4 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 20 1,1-Dichloroethene, CAS: 75-35-4 Signal: 2 Processing Integration Results Not Detected Expected RT: 6.32 6.0 6.2 6.4 6.6Min 0 4 8 12 16 20 24 28 32 36 40 44 48 52 Y ( X 10 ) m/z 61.0 Manual Integration Results RT: 6.33 Area: 879 Amount: 0.037980 Amount Units: ppb v/v 6.0 6.2 6.4 6.6 Min 0 4 8 12 16 20 24 28 32 36 40 44 48 52 Y ( X 10 ) m/z 61.0 6 . 3 2 6 Reviewer: daiglep, 07-Nov-2017 08:55:25 Audit Action: Manually Integrated Audit Reason: Missed Peak Page 313 of 478 Report Date: 07-Nov-2017 13:39:37 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-04.D Injection Date: 06-Nov-2017 17:59:30 Instrument ID: CHB.i Lims ID: ic Client ID: Operator ID: vtp ALS Bottle#: 4 Worklist Smp#:4 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 20 1,1-Dichloroethene, CAS: 75-35-4 Signal: 3 Processing Integration Results Not Detected Expected RT: 6.32 6.0 6.2 6.4 6.6Min 0 2 4 6 8 10 12 14 16 18 20 22 24 Y ( X 10 ) m/z 63.0 Manual Integration Results RT: 6.33 Area: 152 Amount: 0.037980 Amount Units: ppb v/v 6.0 6.2 6.4 6.6 Min 0 2 4 6 8 10 12 14 16 18 20 22 24 Y ( X 10 ) m/z 63.0 6 . 3 2 6 Reviewer: daiglep, 07-Nov-2017 08:55:27 Audit Action: Manually Integrated Audit Reason: Missed Peak Page 314 of 478 Report Date: 07-Nov-2017 13:39:37 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-04.D Injection Date: 06-Nov-2017 17:59:30 Instrument ID: CHB.i Lims ID: ic Client ID: Operator ID: vtp ALS Bottle#: 4 Worklist Smp#:4 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 37 cis-1,2-Dichloroethene, CAS: 156-59-2 Signal: 1 Processing Integration Results RT: 9.34 Area: 330 Amount: 0.012152 Amount Units: ppb v/v 9.0 9.2 9.4 9.6 Min 0 4 8 12 16 20 24 28 32 36 40 44 48 52 56 Y ( X 10 ) m/z 96.0 9 . 3 4 1 Manual Integration Results RT: 9.33 Area: 838 Amount: 0.031330 Amount Units: ppb v/v 9.0 9.2 9.4 9.6 Min 0 4 8 12 16 20 24 28 32 36 40 44 48 52 56 Y ( X 10 ) m/z 96.0 9 . 3 3 1 Reviewer: daiglep, 07-Nov-2017 08:55:46 Audit Action: Manually Integrated Audit Reason: Incomplete Integration Page 315 of 478 Report Date: 07-Nov-2017 13:39:37 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-04.D Injection Date: 06-Nov-2017 17:59:30 Instrument ID: CHB.i Lims ID: ic Client ID: Operator ID: vtp ALS Bottle#: 4 Worklist Smp#:4 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 37 cis-1,2-Dichloroethene, CAS: 156-59-2 Signal: 2 Processing Integration Results RT: 9.34 Area: 296 Amount: 0.012152 Amount Units: ppb v/v 9.0 9.2 9.4 9.6Min 0 2 4 6 8 10 12 14 16 18 20 22 24 26 Y ( X 10 ) m/z 98.0 9 . 3 3 6 Manual Integration Results RT: 9.35 Area: 380 Amount: 0.031330 Amount Units: ppb v/v 9.0 9.2 9.4 9.6 Min 0 2 4 6 8 10 12 14 16 18 20 22 24 26 Y ( X 10 ) m/z 98.0 9 . 3 4 7 Reviewer: daiglep, 07-Nov-2017 08:55:48 Audit Action: Manually Integrated Audit Reason: Incomplete Integration Page 316 of 478 Report Date: 07-Nov-2017 13:39:37 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-04.D Injection Date: 06-Nov-2017 17:59:30 Instrument ID: CHB.i Lims ID: ic Client ID: Operator ID: vtp ALS Bottle#: 4 Worklist Smp#:4 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 53 Trichloroethene, CAS: 79-01-6 Signal: 1 Processing Integration Results RT: 11.48 Area: 795 Amount: 0.023646 Amount Units: ppb v/v 11.1 11.3 11.5 11.7 Min 0 4 8 12 16 20 24 28 32 36 40 44 48 52 56 Y ( X 10 ) m/z 95.0 1 1 . 4 8 1 Manual Integration Results RT: 11.48 Area: 984 Amount: 0.028693 Amount Units: ppb v/v 11.1 11.3 11.5 11.7 Min 0 4 8 12 16 20 24 28 32 36 40 44 48 52 56 Y ( X 10 ) m/z 95.0 1 1 . 4 8 1 Reviewer: daiglep, 07-Nov-2017 08:56:01 Audit Action: Manually Integrated Audit Reason: Incomplete Integration Page 317 of 478 Report Date: 07-Nov-2017 13:39:37 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-04.D Injection Date: 06-Nov-2017 17:59:30 Instrument ID: CHB.i Lims ID: ic Client ID: Operator ID: vtp ALS Bottle#: 4 Worklist Smp#:4 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 53 Trichloroethene, CAS: 79-01-6 Signal: 2 Processing Integration Results RT: 11.48 Area: 0 Amount: 0.023646 Amount Units: ppb v/v 2.9 3.9 4.9 5.9 6.9 7.9 8.9 9.9 10.9Min 0 1 2 3 4 5 6 7 8 9 10 11 12 13 Y ( X 10 0 0 0 ) m/z 130.0 Manual Integration Results RT: 11.48 Area: 1071 Amount: 0.028693 Amount Units: ppb v/v 2.9 3.9 4.9 5.9 6.9 7.9 8.9 9.9 10.9 Min 0 1 2 3 4 5 6 7 8 9 10 11 Y ( X 10 0 ) m/z 130.0 1 1 . 4 7 6 Reviewer: daiglep, 07-Nov-2017 08:56:03 Audit Action: Manually Integrated Audit Reason: Incomplete Integration Page 318 of 478 Report Date: 07-Nov-2017 13:39:37 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-04.D Injection Date: 06-Nov-2017 17:59:30 Instrument ID: CHB.i Lims ID: ic Client ID: Operator ID: vtp ALS Bottle#: 4 Worklist Smp#:4 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 68 Tetrachloroethene, CAS: 127-18-4 Signal: 1 Processing Integration Results RT: 14.04 Area: 1169 Amount: 0.024559 Amount Units: ppb v/v 13.7 13.9 14.1 14.3 Min 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 Y ( X 10 ) m/z 166.0 1 4 . 0 3 8 Manual Integration Results RT: 14.04 Area: 1459 Amount: 0.030000 Amount Units: ppb v/v 13.7 13.9 14.1 14.3 Min 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 Y ( X 10 ) m/z 166.0 1 4 . 0 3 8 Reviewer: daiglep, 07-Nov-2017 08:56:12 Audit Action: Manually Integrated Audit Reason: Incomplete Integration Page 319 of 478 Report Date: 07-Nov-2017 13:39:37 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-04.D Injection Date: 06-Nov-2017 17:59:30 Instrument ID: CHB.i Lims ID: ic Client ID: Operator ID: vtp ALS Bottle#: 4 Worklist Smp#:4 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 68 Tetrachloroethene, CAS: 127-18-4 Signal: 2 Processing Integration Results RT: 14.04 Area: 599 Amount: 0.024559 Amount Units: ppb v/v 13.7 13.9 14.1 14.3Min 0 3 6 9 12 15 18 21 24 27 30 33 36 39 42 Y ( X 10 ) m/z 168.0 1 4 . 0 4 3 Manual Integration Results RT: 14.04 Area: 703 Amount: 0.030000 Amount Units: ppb v/v 13.7 13.9 14.1 14.3 Min 0 3 6 9 12 15 18 21 24 27 30 33 36 39 42 Y ( X 10 ) m/z 168.0 1 4 . 0 4 3 Reviewer: daiglep, 07-Nov-2017 08:56:14 Audit Action: Manually Integrated Audit Reason: Incomplete Integration Page 320 of 478 Report Date: 07-Nov-2017 13:39:39 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Target Compound Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-05.D Lims ID: ic Client ID: Sample Type: IC Calib Level: 2 Inject. Date: 06-Nov-2017 18:52:30 ALS Bottle#: 5 Worklist Smp#: 5 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Sample Info: 200-0027754-005 Misc. Info.: ic Operator ID: vtp Instrument ID: CHB.i Sublist:chrom-TO15_LLNJ_TO3*sub5 Method:\\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\TO15_LLNJ_TO3.m Limit Group: AI_TO15_ICAL Last Update: 07-Nov-2017 13:39:39 Calib Date: 07-Nov-2017 01:49:30 Integrator: RTE ID Type: Deconvolution ID Quant Method: Internal/External Standard Quant By: Initial Calibration Last ICal File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-13.D Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host:XAWRK022 First Level Reviewer: daiglep Date:07-Nov-2017 08:57:46 Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 1 Propene 41 3.140 3.135 0.005 50 4736 0.2004 0.3379 2 Dichlorodifluoromethane 85 3.193 3.193 0.000 99 11681 0.2004 0.2183 3 Chlorodifluoromethane 51 3.230 3.225 0.005 96 8186 0.2004 0.2690 4 1,2-Dichloro-1,1,2,2-tetra 85 3.412 3.412 0.000 88 11568 0.2004 0.2058 5 Chloromethane 50 3.540 3.535 0.005 99 4805 0.2004 0.2517 6 Butane 43 3.716 3.711 0.005 98 9877 0.2004 0.2995 7 Vinyl chloride 62 3.748 3.748 0.000 96 4597 0.2004 0.1998 8 Butadiene 54 3.817 3.812 0.005 96 3780 0.2004 0.2243 9 BFB 10 Bromomethane 94 4.485 4.479 0.006 98 4677 0.2004 0.1975 11 Chloroethane 64 4.703 4.709 -0.006 43 2778 0.2004 0.1952 12 2-Methylbutane 43 4.799 4.789 0.010 97 6818 0.2004 0.2274 13 Vinyl bromide 106 5.125 5.120 0.005 98 4437 0.2004 0.1837 14 Trichlorofluoromethane 101 5.216 5.216 0.000 98 11662 0.2004 0.2042 15 Pentane 43 5.360 5.355 0.005 97 12480 0.2004 0.2738 16 Ethanol 45 5.691 5.675 0.016 100 7428 0.4009 0.5947 17 Ethyl ether 59 5.840 5.830 0.010 91 3577 0.2004 0.2037 18 Acrolein 56 6.203 6.198 0.005 52 2573 0.2004 0.3171 19 1,1,2-Trichloro-1,2,2-trif 101 6.256 6.246 0.010 95 9738 0.2004 0.2029 20 1,1-Dichloroethene 96 6.320 6.321 -0.001 96 4785 0.2004 0.1991 21 Acetone 43 6.481 6.470 0.011 97 36770 0.2004 1.02 22 Isopropyl alcohol 45 6.710 6.684 0.026 98 10339 0.2004 0.2565 23 Carbon disulfide 76 6.747 6.748 -0.001 98 13784 0.2004 0.2047 24 3-Chloro-1-propene 41 7.009 7.020 -0.011 92 6237 0.2004 0.1860 26 Acetonitrile 41 7.084 7.079 0.005 98 5436 0.2004 0.2625 27 Methylene Chloride 49 7.276 7.276 0.000 92 6991 0.2004 0.2429 28 2-Methyl-2-propanol 59 7.409 7.388 0.021 94 11135 0.2004 0.2119 29 Methyl tert-butyl ether 73 7.665 7.628 0.037 97 14248 0.2004 0.1990 30 trans-1,2-Dichloroethene 61 7.687 7.687 0.000 97 7228 0.2004 0.1983 31 Acrylonitrile 53 7.761 7.756 0.005 87 3821 0.2004 0.1986 Page 321 of 478 Report Date: 07-Nov-2017 13:39:39 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-05.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 32 Hexane 57 8.012 8.018 -0.006 93 10775 0.2004 0.2457 33 1,1-Dichloroethane 63 8.423 8.429 -0.006 98 10340 0.2004 0.2121 34 Vinyl acetate 43 8.445 8.434 0.011 100 12490 0.2004 0.1861 36 2-Butanone (MEK) 72 9.336 9.320 0.016 97 4450 0.2004 0.3146 37 cis-1,2-Dichloroethene 96 9.325 9.331 -0.006 54 5366 0.2004 0.1932 35 Ethyl acetate 88 9.336 ND ND * 39 Chlorobromomethane 128 9.699 9.699 0.000 96 241645 10.0 10.0 38 Tetrahydrofuran 42 9.725 9.710 0.015 95 7217 0.2004 0.2211 40 Chloroform 83 9.773 9.774 -0.001 92 10821 0.2004 0.2078 S 41 1,2-Dichloroethene, Total 61 0 0.4009 0.3915 42 1,1,1-Trichloroethane 97 10.030 10.035 -0.005 94 10372 0.2004 0.2025 43 Cyclohexane 84 10.046 10.046 0.000 98 7379 0.2004 0.1916 44 Carbon tetrachloride 117 10.232 10.243 -0.011 94 9225 0.2004 0.1900 45 Isooctane 57 10.521 10.521 0.000 98 28967 0.2004 0.1986 46 Benzene 78 10.558 10.564 -0.006 95 20758 0.2004 0.2308 47 1,2-Dichloroethane 62 10.665 10.665 0.000 97 6582 0.2004 0.2054 48 n-Heptane 43 10.771 10.777 -0.006 93 12675 0.2004 0.2273 A 49 GRO 1 10.865 (4.779-16.951) 0 6852122 0.2004 0 * 50 1,4-Difluorobenzene 114 11.102 11.102 0.000 94 1223095 10.0 10.0 51 n-Butanol 56 11.321 11.289 0.032 89 7643 0.2004 0.4391 53 Trichloroethene 95 11.476 11.476 0.000 97 7346 0.2004 0.2046 54 1,2-Dichloropropane 63 11.844 11.844 0.000 83 6587 0.2004 0.1903 55 Methyl methacrylate 69 11.892 11.882 0.010 94 5690 0.2004 0.1765 56 1,4-Dioxane 88 11.988 11.967 0.021 91 3786 0.2004 0.2216 57 Dibromomethane 174 12.026 12.031 -0.005 97 7303 0.2004 0.2045 58 Dichlorobromomethane 83 12.196 12.202 -0.006 95 11957 0.2004 0.1978 A 59 TVOC as Toluene 1 12.485 (3.125-21.845) 0 8365975 0.2004 0 60 cis-1,3-Dichloropropene 75 12.831 12.832 -0.001 92 8775 0.2004 0.1796 61 4-Methyl-2-pentanone (MIBK 43 12.992 12.976 0.016 97 13433 0.2004 0.1963 63 n-Octane 43 13.242 13.248 -0.006 92 17287 0.2004 0.2200 64 Toluene 92 13.258 13.264 -0.006 94 13793 0.2004 0.2126 66 trans-1,3-Dichloropropene 75 13.621 13.622 -0.001 98 8203 0.2004 0.1757 67 1,1,2-Trichloroethane 83 13.899 13.894 0.005 57 6233 0.2004 0.1949 M 68 Tetrachloroethene 166 14.032 14.038 -0.006 97 10565 0.2004 0.2056 69 2-Hexanone 43 14.171 14.155 0.016 94 15208 0.2004 0.2349 70 Chlorodibromomethane 129 14.449 14.449 0.000 96 10638 0.2004 0.1744 71 Ethylene Dibromide 107 14.646 14.652 -0.006 99 10271 0.2004 0.1812 * 72 Chlorobenzene-d5 117 15.212 15.212 0.000 85 1085526 10.0 10.0 73 Chlorobenzene 112 15.254 15.255 -0.001 91 16678 0.2004 0.1928 74 Ethylbenzene 91 15.318 15.319 -0.001 98 28583 0.2004 0.2011 75 n-Nonane 57 15.340 15.340 0.000 94 15416 0.2004 0.2118 76 m-Xylene & p-Xylene 106 15.468 15.468 0.000 0 20444 0.4009 0.3652 78 o-Xylene 106 15.980 15.981 -0.001 97 10945 0.2004 0.1965 S 77 Xylenes, Total 106 0 0.6013 0.5617 79 Styrene 104 16.002 16.002 0.000 98 13830 0.2004 0.1648 80 Bromoform 173 16.290 16.295 -0.005 95 7840 0.2004 0.1393 81 Isopropylbenzene 105 16.386 16.391 -0.005 96 30035 0.2004 0.1908 85 1,2,3-Trichloropropane 75 16.877 16.647 0.230 98 12655 0.2004 0.1933 83 1,1,2,2-Tetrachloroethane 83 16.797 16.797 0.000 97 16418 0.2004 0.1918 84 N-Propylbenzene 91 16.872 16.872 0.000 99 36449 0.2004 0.1879 86 n-Decane 57 16.936 16.941 -0.005 89 19233 0.2004 0.2085 87 4-Ethyltoluene 105 16.994 16.995 -0.001 99 28872 0.2004 0.1871 Page 322 of 478 Report Date: 07-Nov-2017 13:39:39 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-05.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 88 2-Chlorotoluene 91 17.037 17.037 0.000 97 24918 0.2004 0.1939 89 1,3,5-Trimethylbenzene 105 17.058 17.064 -0.006 93 24147 0.2004 0.1892 90 Alpha Methyl Styrene 118 17.330 17.336 -0.006 88 9891 0.2004 0.1583 91 tert-Butylbenzene 119 17.432 17.437 -0.005 94 23910 0.2004 0.1937 92 1,2,4-Trimethylbenzene 105 17.507 17.507 0.000 97 23191 0.2004 0.1839 93 sec-Butylbenzene 105 17.693 17.694 -0.001 99 36838 0.2004 0.1923 94 4-Isopropyltoluene 119 17.848 17.848 0.000 97 29214 0.2004 0.1855 95 1,3-Dichlorobenzene 146 17.923 17.928 -0.005 97 13728 0.2004 0.1638 96 1,4-Dichlorobenzene 146 18.035 18.035 0.000 92 12436 0.2004 0.1518 97 Benzyl chloride 91 18.190 18.185 0.005 99 11257 0.2004 0.1202 98 Undecane 57 18.312 18.318 -0.006 96 20829 0.2004 0.2077 99 n-Butylbenzene 91 18.350 18.355 -0.005 98 26745 0.2004 0.1849 100 1,2-Dichlorobenzene 146 18.521 18.521 0.000 97 13609 0.2004 0.1727 102 Dodecane 57 19.769 19.770 -0.001 96 16899 0.2004 0.2179 103 1,2,4-Trichlorobenzene 180 20.885 20.885 0.000 90 5646 0.2004 0.1154 104 Hexachlorobutadiene 225 21.040 21.051 -0.011 96 9995 0.2004 0.1941 105 Naphthalene 128 21.365 21.360 0.005 99 11209 0.2004 0.1085 106 1,2,3-Trichlorobenzene 180 21.835 21.835 0.000 93 6230 0.2004 0.1469 QC Flag Legend Processing Flags ND - Not Detected or Marked ND Review Flags M - Manually Integrated Reagents: ATTO15CAL1w_00179 Amount Added: 200.00 Units: mL ATTO15BISs_00006 Amount Added: 20.00 Units: mL Run Reagent Page 323 of 478 Report Date: 07-Nov-2017 13:39:39 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-05.D Injection Date: 06-Nov-2017 18:52:30 Instrument ID: CHB.i Operator ID: vtp Lims ID: ic Worklist Smp#: 5 Client ID: Purge Vol: 200.000 mL Dil. Factor: 1.0000 ALS Bottle#: 5 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Y Scaling: Method Defined: Scale to the Nth Largest Target: 1 2.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 18.0 20.0 22.0 24.0 Min 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 Y ( X 10 0 0 0 0 ) 27754-05[MS SCAN Chro]:Total * C h l o r o b r o m o m e t h a n e ( 9 . 6 9 3 )+ * 1 ,4- D i f lu o r o b e n z en e ( 1 1 . 1 0 2 ) * C h l o r o b e n z en e - d 5 ( 1 5 . 2 1 2 )+ Page 324 of 478 Report Date: 07-Nov-2017 13:39:39 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-05.D Injection Date: 06-Nov-2017 18:52:30 Instrument ID: CHB.i Lims ID: ic Client ID: Operator ID: vtp ALS Bottle#: 5 Worklist Smp#:5 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 67 1,1,2-Trichloroethane, CAS: 79-00-5 Signal: 1 Processing Integration Results RT: 13.90 Area: 3201 Amount: 0.107345 Amount Units: ppb v/v 13.6 13.8 14.0 Min 0 2 4 6 8 10 12 14 16 18 20 22 24 26 Y ( X 10 0 ) m/z 83.0 1 3 . 8 9 9 Manual Integration Results RT: 13.90 Area: 6233 Amount: 0.194899 Amount Units: ppb v/v 13.6 13.8 14.0 Min 0 2 4 6 8 10 12 14 16 18 20 22 24 26 Y ( X 10 0 ) m/z 83.0 1 3 . 8 9 9 Reviewer: daiglep, 07-Nov-2017 09:04:29 Audit Action: Manually Integrated Audit Reason: Incomplete Integration Page 325 of 478 Report Date: 07-Nov-2017 13:39:39 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-05.D Injection Date: 06-Nov-2017 18:52:30 Instrument ID: CHB.i Lims ID: ic Client ID: Operator ID: vtp ALS Bottle#: 5 Worklist Smp#:5 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 67 1,1,2-Trichloroethane, CAS: 79-00-5 Signal: 2 Processing Integration Results RT: 13.89 Area: 0 Amount: 0.107345 Amount Units: ppb v/v 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0Min 0 3 6 9 12 15 18 21 24 27 30 33 36 39 Y ( X 10 0 ) m/z 97.0 Manual Integration Results RT: 13.89 Area: 7230 Amount: 0.194899 Amount Units: ppb v/v 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0 Min 0 3 6 9 12 15 18 21 24 27 30 33 36 39 Y ( X 10 0 ) m/z 97.0 1 3 . 8 8 8 Reviewer: daiglep, 07-Nov-2017 09:04:31 Audit Action: Manually Integrated Audit Reason: Incomplete Integration Page 326 of 478 Report Date: 07-Nov-2017 13:39:40 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Manual Integration/User Assign Peak Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-05.D Injection Date: 06-Nov-2017 18:52:30 Instrument ID: CHB.i Lims ID: ic Client ID: Operator ID: vtp ALS Bottle#: 5 Worklist Smp#:5 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Detector MS SCAN 67 1,1,2-Trichloroethane, CAS: 79-00-5 Signal: 3 Processing Integration Results RT: 13.90 Area: 2112 Amount: 0.107345 Amount Units: ppb v/v 13.6 13.8 14.0Min 0 2 4 6 8 10 12 14 16 18 Y ( X 10 0 ) m/z 85.0 1 3 . 8 9 9 Manual Integration Results RT: 13.90 Area: 3982 Amount: 0.194899 Amount Units: ppb v/v 13.6 13.8 14.0 Min 0 2 4 6 8 10 12 14 16 18 Y ( X 10 0 ) m/z 85.0 1 3 . 8 9 9 Reviewer: daiglep, 07-Nov-2017 09:04:33 Audit Action: Manually Integrated Audit Reason: Incomplete Integration Page 327 of 478 Report Date: 07-Nov-2017 13:39:47 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Target Compound Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-07.D Lims ID: ic Client ID: Sample Type: IC Calib Level: 3 Inject. Date: 06-Nov-2017 20:36:30 ALS Bottle#: 7 Worklist Smp#: 7 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Sample Info: 200-0027754-007 Misc. Info.: ic Operator ID: vtp Instrument ID: CHB.i Sublist:chrom-TO15_LLNJ_TO3*sub5 Method:\\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\TO15_LLNJ_TO3.m Limit Group: AI_TO15_ICAL Last Update: 07-Nov-2017 13:39:46 Calib Date: 07-Nov-2017 01:49:30 Integrator: RTE ID Type: Deconvolution ID Quant Method: Internal/External Standard Quant By: Initial Calibration Last ICal File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-13.D Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host:XAWRK022 First Level Reviewer: daiglep Date:07-Nov-2017 08:58:36 Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 1 Propene 41 3.140 3.135 0.005 96 9005 0.5005 0.6442 2 Dichlorodifluoromethane 85 3.199 3.193 0.006 99 27637 0.5005 0.5178 3 Chlorodifluoromethane 51 3.231 3.225 0.006 97 16962 0.5005 0.5588 4 1,2-Dichloro-1,1,2,2-tetra 85 3.412 3.412 0.000 91 28521 0.5005 0.5088 5 Chloromethane 50 3.540 3.535 0.005 98 10035 0.5005 0.5271 6 Butane 43 3.711 3.711 0.000 98 18787 0.5005 0.5712 7 Vinyl chloride 62 3.748 3.748 0.000 97 11608 0.5005 0.5060 8 Butadiene 54 3.823 3.812 0.011 96 8740 0.5005 0.5200 10 Bromomethane 94 4.479 4.479 0.000 96 10970 0.5005 0.4644 9 BFB 11 Chloroethane 64 4.709 4.709 0.000 96 7142 0.5005 0.5033 12 2-Methylbutane 43 4.794 4.789 0.005 94 15414 0.5005 0.5155 13 Vinyl bromide 106 5.120 5.120 0.000 97 10998 0.5005 0.4566 14 Trichlorofluoromethane 101 5.216 5.216 0.000 98 28350 0.5005 0.4977 15 Pentane 43 5.360 5.355 0.005 97 24884 0.5005 0.5475 16 Ethanol 45 5.675 5.675 0.000 98 78001 5.01 6.26 17 Ethyl ether 59 5.851 5.830 0.021 89 8140 0.5005 0.4647 18 Acrolein 56 6.209 6.198 0.011 65 5099 0.5005 0.6301 19 1,1,2-Trichloro-1,2,2-trif 101 6.241 6.246 -0.005 95 23175 0.5005 0.4842 20 1,1-Dichloroethene 96 6.315 6.321 -0.006 96 11165 0.5005 0.4659 21 Acetone 43 6.481 6.470 0.011 97 39306 0.5005 1.10 22 Isopropyl alcohol 45 6.705 6.684 0.021 99 20154 0.5005 0.5013 23 Carbon disulfide 76 6.748 6.748 0.000 98 32704 0.5005 0.4869 24 3-Chloro-1-propene 41 7.020 7.020 0.000 94 17782 0.5005 0.5317 26 Acetonitrile 41 7.084 7.079 0.005 96 11438 0.5005 0.5537 27 Methylene Chloride 49 7.271 7.276 -0.005 97 15430 0.5005 0.5375 28 2-Methyl-2-propanol 59 7.409 7.388 0.021 94 24805 0.5005 0.4732 29 Methyl tert-butyl ether 73 7.644 7.628 0.016 98 35044 0.5005 0.4907 30 trans-1,2-Dichloroethene 61 7.687 7.687 0.000 99 18104 0.5005 0.4979 31 Acrylonitrile 53 7.767 7.756 0.011 94 9113 0.5005 0.4750 Page 328 of 478 Report Date: 07-Nov-2017 13:39:47 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-07.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 32 Hexane 57 8.012 8.018 -0.006 95 22455 0.5005 0.5134 33 1,1-Dichloroethane 63 8.423 8.429 -0.006 99 23477 0.5005 0.4829 34 Vinyl acetate 43 8.439 8.434 0.005 100 32250 0.5005 0.4819 36 2-Butanone (MEK) 72 9.331 9.320 0.011 96 7175 0.5005 0.5086 37 cis-1,2-Dichloroethene 96 9.331 9.331 0.000 62 13652 0.5005 0.4929 35 Ethyl acetate 88 9.336 ND ND * 39 Chlorobromomethane 128 9.699 9.699 0.000 97 241003 10.0 10.0 38 Tetrahydrofuran 42 9.726 9.710 0.016 96 16890 0.5005 0.5125 40 Chloroform 83 9.774 9.774 0.000 96 25766 0.5005 0.4961 S 41 1,2-Dichloroethene, Total 61 0 1.00 0.99 42 1,1,1-Trichloroethane 97 10.030 10.035 -0.005 95 24994 0.5005 0.4834 43 Cyclohexane 84 10.041 10.046 -0.005 98 18527 0.5005 0.4764 44 Carbon tetrachloride 117 10.233 10.243 -0.010 96 23344 0.5005 0.4763 45 Isooctane 57 10.521 10.521 0.000 99 69941 0.5005 0.4751 46 Benzene 78 10.564 10.564 0.000 96 43028 0.5005 0.4739 47 1,2-Dichloroethane 62 10.660 10.665 -0.005 95 16172 0.5005 0.5000 48 n-Heptane 43 10.772 10.777 -0.005 95 28219 0.5005 0.5013 A 49 GRO 1 10.865 (4.779-16.951) 0 9755312 0.5005 0 * 50 1,4-Difluorobenzene 114 11.103 11.102 0.001 94 1234746 10.0 10.0 51 n-Butanol 56 11.321 11.289 0.032 92 9644 0.5005 0.5488 53 Trichloroethene 95 11.476 11.476 0.000 98 17501 0.5005 0.4828 54 1,2-Dichloropropane 63 11.839 11.844 -0.005 90 17056 0.5005 0.4881 55 Methyl methacrylate 69 11.882 11.882 0.000 97 14165 0.5005 0.4353 56 1,4-Dioxane 88 11.983 11.967 0.016 97 7977 0.5005 0.4625 57 Dibromomethane 174 12.026 12.031 -0.005 95 16681 0.5005 0.4628 58 Dichlorobromomethane 83 12.202 12.202 0.000 97 29942 0.5005 0.4906 A 59 TVOC as Toluene 1 12.485 (3.125-21.845) 0 13333275 0.5005 0 60 cis-1,3-Dichloropropene 75 12.826 12.832 -0.006 92 23060 0.5005 0.4675 61 4-Methyl-2-pentanone (MIBK 43 12.986 12.976 0.010 97 32590 0.5005 0.4717 63 n-Octane 43 13.243 13.248 -0.005 94 39510 0.5005 0.4980 64 Toluene 92 13.259 13.264 -0.005 93 31753 0.5005 0.4879 66 trans-1,3-Dichloropropene 75 13.622 13.622 0.000 98 21348 0.5005 0.4528 67 1,1,2-Trichloroethane 83 13.894 13.894 0.000 96 15678 0.5005 0.4887 68 Tetrachloroethene 166 14.033 14.038 -0.005 97 24183 0.5005 0.4690 69 2-Hexanone 43 14.161 14.155 0.006 95 31361 0.5005 0.4828 70 Chlorodibromomethane 129 14.449 14.449 0.000 99 27956 0.5005 0.4568 71 Ethylene Dibromide 107 14.646 14.652 -0.006 99 26533 0.5005 0.4667 * 72 Chlorobenzene-d5 117 15.212 15.212 0.000 86 1088970 10.0 10.0 73 Chlorobenzene 112 15.249 15.255 -0.006 96 40862 0.5005 0.4708 74 Ethylbenzene 91 15.319 15.319 0.000 98 68858 0.5005 0.4830 75 n-Nonane 57 15.335 15.340 -0.005 95 34964 0.5005 0.4788 76 m-Xylene & p-Xylene 106 15.463 15.468 -0.005 0 51820 1.00 0.9227 78 o-Xylene 106 15.975 15.981 -0.006 97 26258 0.5005 0.4700 S 77 Xylenes, Total 106 0 1.50 1.39 79 Styrene 104 16.002 16.002 0.000 98 37866 0.5005 0.4498 80 Bromoform 173 16.295 16.295 0.000 97 25278 0.5005 0.4477 81 Isopropylbenzene 105 16.386 16.391 -0.005 96 73623 0.5005 0.4661 85 1,2,3-Trichloropropane 75 16.882 16.647 0.235 97 31857 0.5005 0.4851 83 1,1,2,2-Tetrachloroethane 83 16.797 16.797 0.000 97 41145 0.5005 0.4791 84 N-Propylbenzene 91 16.866 16.872 -0.006 99 90532 0.5005 0.4652 86 n-Decane 57 16.936 16.941 -0.005 89 46234 0.5005 0.4997 87 4-Ethyltoluene 105 16.995 16.995 0.000 98 71488 0.5005 0.4617 Page 329 of 478 Report Date: 07-Nov-2017 13:39:47 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-07.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 88 2-Chlorotoluene 91 17.032 17.037 -0.005 97 60006 0.5005 0.4655 89 1,3,5-Trimethylbenzene 105 17.059 17.064 -0.005 92 59606 0.5005 0.4656 90 Alpha Methyl Styrene 118 17.331 17.336 -0.005 88 28073 0.5005 0.4478 91 tert-Butylbenzene 119 17.432 17.437 -0.005 95 57783 0.5005 0.4667 92 1,2,4-Trimethylbenzene 105 17.502 17.507 -0.005 98 59289 0.5005 0.4688 93 sec-Butylbenzene 105 17.688 17.694 -0.006 99 91707 0.5005 0.4771 94 4-Isopropyltoluene 119 17.843 17.848 -0.005 98 73963 0.5005 0.4682 95 1,3-Dichlorobenzene 146 17.923 17.928 -0.005 98 38771 0.5005 0.4612 96 1,4-Dichlorobenzene 146 18.035 18.035 0.000 96 38663 0.5005 0.4703 97 Benzyl chloride 91 18.185 18.185 0.000 98 42398 0.5005 0.4512 98 Undecane 57 18.318 18.318 0.000 97 48082 0.5005 0.4778 99 n-Butylbenzene 91 18.350 18.355 -0.005 98 69356 0.5005 0.4780 100 1,2-Dichlorobenzene 146 18.521 18.521 0.000 96 37002 0.5005 0.4681 102 Dodecane 57 19.770 19.770 0.000 95 40649 0.5005 0.5225 103 1,2,4-Trichlorobenzene 180 20.880 20.885 -0.005 93 20073 0.5005 0.4090 104 Hexachlorobutadiene 225 21.040 21.051 -0.011 97 24771 0.5005 0.4795 105 Naphthalene 128 21.365 21.360 0.005 99 45302 0.5005 0.4369 106 1,2,3-Trichlorobenzene 180 21.835 21.835 0.000 94 18238 0.5005 0.4287 QC Flag Legend Processing Flags ND - Not Detected or Marked ND Reagents: ATTO15CAL2w_00245 Amount Added: 200.00 Units: mL ATTO15BISs_00006 Amount Added: 20.00 Units: mL Run Reagent Page 330 of 478 Report Date: 07-Nov-2017 13:39:47 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-07.D Injection Date: 06-Nov-2017 20:36:30 Instrument ID: CHB.i Operator ID: vtp Lims ID: ic Worklist Smp#: 7 Client ID: Purge Vol: 200.000 mL Dil. Factor: 1.0000 ALS Bottle#: 7 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Y Scaling: Method Defined: Scale to the Nth Largest Target: 1 2.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 18.0 20.0 22.0 24.0 Min 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 Y ( X 10 0 0 0 0 ) 27754-07[MS SCAN Chro]:Total * C h l o r o b r o m o m e t h a n e ( 9 . 6 9 4 )+ * 1 ,4- D i f lu o r o b e n z en e ( 1 1 . 1 0 3 ) * C h l o r o b e n z en e - d 5 ( 1 5 . 2 1 2 )+ Page 331 of 478 Report Date: 07-Nov-2017 13:39:54 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Target Compound Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-09.D Lims ID: ic Client ID: Sample Type: IC Calib Level: 4 Inject. Date: 06-Nov-2017 22:20:30 ALS Bottle#: 9 Worklist Smp#: 9 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Sample Info: 200-0027754-009 Misc. Info.: ic Operator ID: vtp Instrument ID: CHB.i Sublist:chrom-TO15_LLNJ_TO3*sub5 Method:\\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\TO15_LLNJ_TO3.m Limit Group: AI_TO15_ICAL Last Update: 07-Nov-2017 13:39:53 Calib Date: 07-Nov-2017 01:49:30 Integrator: RTE ID Type: Deconvolution ID Quant Method: Internal/External Standard Quant By: Initial Calibration Last ICal File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-13.D Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host:XAWRK022 First Level Reviewer: daiglep Date:07-Nov-2017 08:59:12 Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 1 Propene 41 3.135 3.135 0.000 99 94270 4.99 6.74 2 Dichlorodifluoromethane 85 3.193 3.193 0.000 99 328049 4.99 6.14 3 Chlorodifluoromethane 51 3.231 3.225 0.006 97 192442 4.99 6.34 4 1,2-Dichloro-1,1,2,2-tetra 85 3.412 3.412 0.000 90 329585 4.99 5.88 5 Chloromethane 50 3.540 3.535 0.005 99 119627 4.99 6.28 6 Butane 43 3.711 3.711 0.000 99 207906 4.99 6.32 7 Vinyl chloride 62 3.748 3.748 0.000 98 139669 4.99 6.08 8 Butadiene 54 3.818 3.812 0.006 98 105361 4.99 6.26 9 BFB 10 Bromomethane 94 4.485 4.479 0.006 99 131944 4.99 5.58 11 Chloroethane 64 4.709 4.709 0.000 100 81341 4.99 5.73 12 2-Methylbutane 43 4.794 4.789 0.005 95 179718 4.99 6.01 13 Vinyl bromide 106 5.120 5.120 0.000 99 134098 4.99 5.56 14 Trichlorofluoromethane 101 5.221 5.216 0.005 98 329662 4.99 5.78 15 Pentane 43 5.355 5.355 0.000 96 277962 4.99 6.11 16 Ethanol 45 5.675 5.675 0.000 99 149824 10.0 12.0 17 Ethyl ether 59 5.835 5.830 0.005 94 103447 4.99 5.90 18 Acrolein 56 6.198 6.198 0.000 96 45692 4.99 5.64 19 1,1,2-Trichloro-1,2,2-trif 101 6.246 6.246 0.000 96 269917 4.99 5.64 20 1,1-Dichloroethene 96 6.315 6.321 -0.006 96 135100 4.99 5.63 21 Acetone 43 6.470 6.470 0.000 98 236842 4.99 6.61 22 Isopropyl alcohol 45 6.684 6.684 0.000 100 252112 4.99 6.27 23 Carbon disulfide 76 6.748 6.748 0.000 99 389595 4.99 5.80 24 3-Chloro-1-propene 41 7.015 7.020 -0.006 93 211903 4.99 6.33 26 Acetonitrile 41 7.079 7.079 0.000 99 128629 4.99 6.22 27 Methylene Chloride 49 7.276 7.276 0.000 97 173856 4.99 6.05 28 2-Methyl-2-propanol 59 7.383 7.388 -0.005 94 313150 4.99 5.97 29 Methyl tert-butyl ether 73 7.628 7.628 0.000 98 414586 4.99 5.80 30 trans-1,2-Dichloroethene 61 7.687 7.687 0.000 98 217279 4.99 5.97 31 Acrylonitrile 53 7.756 7.756 0.000 96 115020 4.99 5.99 Page 332 of 478 Report Date: 07-Nov-2017 13:39:54 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-09.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 32 Hexane 57 8.018 8.018 0.000 95 247350 4.99 5.65 33 1,1-Dichloroethane 63 8.429 8.429 0.000 99 286623 4.99 5.89 34 Vinyl acetate 43 8.434 8.434 0.000 100 415040 4.99 6.20 36 2-Butanone (MEK) 72 9.315 9.320 -0.005 100 80752 4.99 5.72 37 cis-1,2-Dichloroethene 96 9.331 9.331 0.000 95 160947 4.99 5.81 35 Ethyl acetate 88 9.331 9.336 -0.005 92 12961 4.99 5.56 * 39 Chlorobromomethane 128 9.699 9.699 0.000 97 241168 10.0 10.0 38 Tetrahydrofuran 42 9.715 9.710 0.005 97 202420 4.99 6.19 40 Chloroform 83 9.774 9.774 0.000 95 302854 4.99 5.83 S 41 1,2-Dichloroethene, Total 61 0 9.99 11.8 42 1,1,1-Trichloroethane 97 10.035 10.035 0.000 96 296136 4.99 5.77 43 Cyclohexane 84 10.046 10.046 0.000 98 215268 4.99 5.58 44 Carbon tetrachloride 117 10.238 10.243 -0.005 98 296544 4.99 6.10 45 Isooctane 57 10.521 10.521 0.000 99 854191 4.99 5.85 46 Benzene 78 10.564 10.564 0.000 96 493843 4.99 5.48 47 1,2-Dichloroethane 62 10.660 10.665 -0.005 96 193741 4.99 6.04 48 n-Heptane 43 10.772 10.777 -0.005 94 333367 4.99 5.97 A 49 GRO 1 10.865 (4.779-16.951) 0 67780240 4.99 0 * 50 1,4-Difluorobenzene 114 11.103 11.102 0.001 94 1224793 10.0 10.0 51 n-Butanol 56 11.289 11.289 0.000 88 101995 4.99 5.85 53 Trichloroethene 95 11.476 11.476 0.000 98 207050 4.99 5.76 54 1,2-Dichloropropane 63 11.844 11.844 0.000 95 203574 4.99 5.87 55 Methyl methacrylate 69 11.882 11.882 0.000 96 185277 4.99 5.74 56 1,4-Dioxane 88 11.972 11.967 0.005 95 98539 4.99 5.76 57 Dibromomethane 174 12.031 12.031 0.000 98 191845 4.99 5.37 58 Dichlorobromomethane 83 12.202 12.202 0.000 98 352531 4.99 5.82 A 59 TVOC as Toluene 1 12.485 (3.125-21.845) 0 108224039 4.99 0 60 cis-1,3-Dichloropropene 75 12.832 12.832 0.000 92 285608 4.99 5.84 61 4-Methyl-2-pentanone (MIBK 43 12.976 12.976 0.000 97 424306 4.99 6.19 63 n-Octane 43 13.248 13.248 0.000 94 480047 4.99 6.10 64 Toluene 92 13.259 13.264 -0.005 93 362352 4.99 5.47 66 trans-1,3-Dichloropropene 75 13.622 13.622 0.000 97 276675 4.99 5.92 67 1,1,2-Trichloroethane 83 13.894 13.894 0.000 96 185969 4.99 5.70 68 Tetrachloroethene 166 14.033 14.038 -0.005 98 287651 4.99 5.49 69 2-Hexanone 43 14.155 14.155 0.000 94 406329 4.99 6.15 70 Chlorodibromomethane 129 14.449 14.449 0.000 99 358608 4.99 5.76 71 Ethylene Dibromide 107 14.652 14.652 0.000 98 327996 4.99 5.67 * 72 Chlorobenzene-d5 117 15.212 15.212 0.000 86 1107460 10.0 10.0 73 Chlorobenzene 112 15.249 15.255 -0.006 95 486827 4.99 5.52 74 Ethylbenzene 91 15.319 15.319 0.000 98 802931 4.99 5.54 75 n-Nonane 57 15.340 15.340 0.000 95 432179 4.99 5.82 76 m-Xylene & p-Xylene 106 15.468 15.468 0.000 0 628058 9.99 11.0 78 o-Xylene 106 15.981 15.981 0.000 98 312634 4.99 5.50 S 77 Xylenes, Total 106 0 15.0 16.5 79 Styrene 104 16.002 16.002 0.000 99 475931 4.99 5.56 80 Bromoform 173 16.295 16.295 0.000 97 340328 4.99 5.93 81 Isopropylbenzene 105 16.391 16.391 0.000 96 900374 4.99 5.61 85 1,2,3-Trichloropropane 75 16.877 16.647 0.230 98 386627 4.99 5.79 83 1,1,2,2-Tetrachloroethane 83 16.797 16.797 0.000 97 501706 4.99 5.74 84 N-Propylbenzene 91 16.866 16.872 -0.006 99 1137310 4.99 5.75 86 n-Decane 57 16.936 16.941 -0.005 88 567864 4.99 6.04 87 4-Ethyltoluene 105 16.995 16.995 0.000 98 887867 4.99 5.64 Page 333 of 478 Report Date: 07-Nov-2017 13:39:54 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-09.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 88 2-Chlorotoluene 91 17.037 17.037 0.000 96 747078 4.99 5.70 89 1,3,5-Trimethylbenzene 105 17.059 17.064 -0.005 93 738489 4.99 5.67 90 Alpha Methyl Styrene 118 17.331 17.336 -0.005 89 363985 4.99 5.71 91 tert-Butylbenzene 119 17.437 17.437 0.000 96 722005 4.99 5.73 92 1,2,4-Trimethylbenzene 105 17.507 17.507 0.000 97 743964 4.99 5.78 93 sec-Butylbenzene 105 17.694 17.694 0.000 99 1133717 4.99 5.80 94 4-Isopropyltoluene 119 17.843 17.848 -0.005 98 931887 4.99 5.80 95 1,3-Dichlorobenzene 146 17.923 17.928 -0.005 98 482419 4.99 5.64 96 1,4-Dichlorobenzene 146 18.035 18.035 0.000 95 473120 4.99 5.66 97 Benzyl chloride 91 18.185 18.185 0.000 99 581535 4.99 6.09 98 Undecane 57 18.318 18.318 0.000 97 612517 4.99 5.99 99 n-Butylbenzene 91 18.350 18.355 -0.005 98 876363 4.99 5.94 100 1,2-Dichlorobenzene 146 18.521 18.521 0.000 96 459422 4.99 5.71 102 Dodecane 57 19.770 19.770 0.000 96 483798 4.99 6.12 103 1,2,4-Trichlorobenzene 180 20.880 20.885 -0.005 94 240031 4.99 4.81 104 Hexachlorobutadiene 225 21.051 21.051 0.000 98 295106 4.99 5.62 105 Naphthalene 128 21.360 21.360 0.000 99 473935 4.99 4.49 106 1,2,3-Trichlorobenzene 180 21.835 21.835 0.000 95 216879 4.99 5.01 Reagents: ATTO15CAL3w_00188 Amount Added: 200.00 Units: mL ATTO15BISs_00006 Amount Added: 20.00 Units: mL Run Reagent Page 334 of 478 Report Date: 07-Nov-2017 13:39:54 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-09.D Injection Date: 06-Nov-2017 22:20:30 Instrument ID: CHB.i Operator ID: vtp Lims ID: ic Worklist Smp#: 9 Client ID: Purge Vol: 200.000 mL Dil. Factor: 1.0000 ALS Bottle#: 9 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Y Scaling: Method Defined: Scale to the Nth Largest Target: 1 2.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 18.0 20.0 22.0 24.0 Min 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 Y ( X 10 0 0 0 0 ) 27754-09[MS SCAN Chro]:Total * C h l o r o b r o m o m e t h a n e ( 9 . 7 0 4 )+ * 1 ,4- D i f lu o r o b e n z en e ( 1 1 . 1 0 3 ) * C h l o r o b e n z en e - d 5 ( 1 5 . 2 1 2 )+ Page 335 of 478 Report Date: 07-Nov-2017 13:39:56 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Target Compound Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-10.D Lims ID: icis Client ID: Sample Type: ICIS Calib Level: 5 Inject. Date: 06-Nov-2017 23:12:30 ALS Bottle#: 10 Worklist Smp#: 10 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Sample Info: 200-0027754-010 Misc. Info.: icis Operator ID: vtp Instrument ID: CHB.i Sublist:chrom-TO15_LLNJ_TO3*sub5 Method:\\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\TO15_LLNJ_TO3.m Limit Group: AI_TO15_ICAL Last Update: 07-Nov-2017 13:39:55 Calib Date: 07-Nov-2017 01:49:30 Integrator: RTE ID Type: Deconvolution ID Quant Method: Internal/External Standard Quant By: Initial Calibration Last ICal File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-13.D Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host:XAWRK022 First Level Reviewer: daiglep Date:07-Nov-2017 08:52:42 Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 1 Propene 41 3.135 3.135 0.000 99 178752 10.0 11.4 2 Dichlorodifluoromethane 85 3.193 3.193 0.000 99 669500 10.0 11.2 3 Chlorodifluoromethane 51 3.225 3.225 0.000 97 378485 10.0 11.1 4 1,2-Dichloro-1,1,2,2-tetra 85 3.412 3.412 0.000 89 690355 10.0 11.0 5 Chloromethane 50 3.535 3.535 0.000 99 239308 10.0 11.2 6 Butane 43 3.711 3.711 0.000 99 410042 10.0 11.1 7 Vinyl chloride 62 3.748 3.748 0.000 98 291466 10.0 11.3 8 Butadiene 54 3.812 3.812 0.000 96 219553 10.0 11.6 10 Bromomethane 94 4.479 4.479 0.000 99 290018 10.0 10.9 9 BFB 11 Chloroethane 64 4.709 4.709 0.000 100 172230 10.0 10.8 12 2-Methylbutane 43 4.789 4.789 0.000 95 366461 10.0 10.9 13 Vinyl bromide 106 5.120 5.120 0.000 100 293593 10.0 10.8 14 Trichlorofluoromethane 101 5.216 5.216 0.000 98 687404 10.0 10.7 15 Pentane 43 5.355 5.355 0.000 96 555873 10.0 10.9 16 Ethanol 45 5.675 5.675 0.000 99 218031 15.0 15.6 17 Ethyl ether 59 5.830 5.830 0.000 94 214038 10.0 10.9 18 Acrolein 56 6.198 6.198 0.000 95 96696 10.0 10.6 19 1,1,2-Trichloro-1,2,2-trif 101 6.246 6.246 0.000 97 565202 10.0 10.5 20 1,1-Dichloroethene 96 6.321 6.321 0.000 97 279844 10.0 10.4 21 Acetone 43 6.470 6.470 0.000 97 446021 10.0 11.1 22 Isopropyl alcohol 45 6.684 6.684 0.000 99 511783 10.0 11.3 23 Carbon disulfide 76 6.748 6.748 0.000 99 805496 10.0 10.7 24 3-Chloro-1-propene 41 7.020 7.020 0.000 93 415357 10.0 11.1 26 Acetonitrile 41 7.079 7.079 0.000 99 254873 10.0 11.0 27 Methylene Chloride 49 7.276 7.276 0.000 96 351310 10.0 10.9 28 2-Methyl-2-propanol 59 7.388 7.388 0.000 93 654836 10.0 11.1 29 Methyl tert-butyl ether 73 7.628 7.628 0.000 98 862467 10.0 10.7 30 trans-1,2-Dichloroethene 61 7.687 7.687 0.000 99 441740 10.0 10.8 31 Acrylonitrile 53 7.756 7.756 0.000 96 237313 10.0 11.0 Page 336 of 478 Report Date: 07-Nov-2017 13:39:56 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-10.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 32 Hexane 57 8.018 8.018 0.000 94 501161 10.0 10.2 33 1,1-Dichloroethane 63 8.429 8.429 0.000 99 583546 10.0 10.7 34 Vinyl acetate 43 8.434 8.434 0.000 100 839222 10.0 11.2 36 2-Butanone (MEK) 72 9.320 9.320 0.000 100 166254 10.0 10.5 37 cis-1,2-Dichloroethene 96 9.331 9.331 0.000 96 336303 10.0 10.8 35 Ethyl acetate 88 9.336 9.336 0.000 92 26960 10.0 10.3 * 39 Chlorobromomethane 128 9.704 9.704 0.000 97 270834 10.0 10.0 38 Tetrahydrofuran 42 9.710 9.710 0.000 96 402366 10.0 11.1 40 Chloroform 83 9.774 9.774 0.000 96 620796 10.0 10.6 S 41 1,2-Dichloroethene, Total 61 0 20.0 21.6 42 1,1,1-Trichloroethane 97 10.035 10.035 0.000 96 602834 10.0 10.6 43 Cyclohexane 84 10.046 10.046 0.000 98 451412 10.0 10.5 44 Carbon tetrachloride 117 10.243 10.243 0.000 98 610969 10.0 11.3 45 Isooctane 57 10.521 10.521 0.000 99 1753387 10.0 10.8 46 Benzene 78 10.564 10.564 0.000 96 1023623 10.0 10.2 47 1,2-Dichloroethane 62 10.665 10.665 0.000 96 384279 10.0 10.8 48 n-Heptane 43 10.777 10.777 0.000 93 663081 10.0 10.7 A 49 GRO 1 10.865 (4.779-16.951) 0 135949929 10.0 0 * 50 1,4-Difluorobenzene 114 11.108 11.108 0.000 94 1363371 10.0 10.0 51 n-Butanol 56 11.289 11.289 0.000 89 207031 10.0 10.7 53 Trichloroethene 95 11.476 11.476 0.000 98 432058 10.0 10.8 54 1,2-Dichloropropane 63 11.844 11.844 0.000 94 415515 10.0 10.8 55 Methyl methacrylate 69 11.882 11.882 0.000 96 384997 10.0 10.7 56 1,4-Dioxane 88 11.967 11.967 0.000 94 206434 10.0 10.8 57 Dibromomethane 174 12.031 12.031 0.000 97 412753 10.0 10.4 58 Dichlorobromomethane 83 12.202 12.202 0.000 97 715566 10.0 10.6 A 59 TVOC as Toluene 1 12.485 (3.125-21.845) 0 221248223 10.0 0 60 cis-1,3-Dichloropropene 75 12.832 12.832 0.000 91 590668 10.0 10.8 61 4-Methyl-2-pentanone (MIBK 43 12.976 12.976 0.000 96 847377 10.0 11.1 63 n-Octane 43 13.248 13.248 0.000 93 959417 10.0 11.0 64 Toluene 92 13.264 13.264 0.000 93 753577 10.0 10.1 66 trans-1,3-Dichloropropene 75 13.622 13.622 0.000 96 575307 10.0 11.1 67 1,1,2-Trichloroethane 83 13.894 13.894 0.000 95 383516 10.0 10.4 68 Tetrachloroethene 166 14.038 14.038 0.000 98 613429 10.0 10.4 69 2-Hexanone 43 14.155 14.155 0.000 94 815397 10.0 11.0 70 Chlorodibromomethane 129 14.449 14.449 0.000 98 734000 10.0 10.5 71 Ethylene Dibromide 107 14.652 14.652 0.000 98 689766 10.0 10.6 * 72 Chlorobenzene-d5 117 15.212 15.212 0.000 87 1246413 10.0 10.0 73 Chlorobenzene 112 15.255 15.255 0.000 95 1028944 10.0 10.4 74 Ethylbenzene 91 15.319 15.319 0.000 98 1694195 10.0 10.4 75 n-Nonane 57 15.340 15.340 0.000 93 886988 10.0 10.6 76 m-Xylene & p-Xylene 106 15.468 15.468 0.000 0 1339356 20.0 20.8 78 o-Xylene 106 15.981 15.981 0.000 98 659664 10.0 10.3 S 77 Xylenes, Total 106 0 30.0 31.2 79 Styrene 104 16.002 16.002 0.000 98 1035340 10.0 10.7 80 Bromoform 173 16.295 16.295 0.000 98 664355 10.0 10.3 81 Isopropylbenzene 105 16.391 16.391 0.000 95 1896589 10.0 10.5 85 1,2,3-Trichloropropane 75 16.882 16.882 0.000 98 801515 10.0 10.7 83 1,1,2,2-Tetrachloroethane 83 16.797 16.797 0.000 97 1054405 10.0 10.7 84 N-Propylbenzene 91 16.872 16.872 0.000 99 2394240 10.0 10.7 86 n-Decane 57 16.941 16.941 0.000 89 1164188 10.0 11.0 87 4-Ethyltoluene 105 16.995 16.995 0.000 98 1896619 10.0 10.7 Page 337 of 478 Report Date: 07-Nov-2017 13:39:56 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-10.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 88 2-Chlorotoluene 91 17.037 17.037 0.000 97 1576394 10.0 10.7 89 1,3,5-Trimethylbenzene 105 17.064 17.064 0.000 93 1575121 10.0 10.8 90 Alpha Methyl Styrene 118 17.336 17.336 0.000 90 792287 10.0 11.0 91 tert-Butylbenzene 119 17.437 17.437 0.000 95 1515083 10.0 10.7 92 1,2,4-Trimethylbenzene 105 17.507 17.507 0.000 97 1580281 10.0 10.9 93 sec-Butylbenzene 105 17.694 17.694 0.000 99 2372305 10.0 10.8 94 4-Isopropyltoluene 119 17.848 17.848 0.000 98 1955482 10.0 10.8 95 1,3-Dichlorobenzene 146 17.928 17.928 0.000 97 1052014 10.0 10.9 96 1,4-Dichlorobenzene 146 18.035 18.035 0.000 96 1038211 10.0 11.0 97 Benzyl chloride 91 18.185 18.185 0.000 99 1273643 10.0 11.8 98 Undecane 57 18.318 18.318 0.000 97 1200999 10.0 10.4 99 n-Butylbenzene 91 18.355 18.355 0.000 98 1781253 10.0 10.7 100 1,2-Dichlorobenzene 146 18.521 18.521 0.000 97 983042 10.0 10.9 102 Dodecane 57 19.770 19.770 0.000 96 994023 10.0 11.2 103 1,2,4-Trichlorobenzene 180 20.885 20.885 0.000 94 577428 10.0 10.3 104 Hexachlorobutadiene 225 21.051 21.051 0.000 99 608010 10.0 10.3 105 Naphthalene 128 21.360 21.360 0.000 99 1190473 10.0 10.0 106 1,2,3-Trichlorobenzene 180 21.835 21.835 0.000 95 513047 10.0 10.5 Reagents: ATTO15CAL4w_00645 Amount Added: 200.00 Units: mL ATTO15BISs_00006 Amount Added: 20.00 Units: mL Run Reagent Page 338 of 478 Report Date: 07-Nov-2017 13:39:56 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-10.D Injection Date: 06-Nov-2017 23:12:30 Instrument ID: CHB.i Operator ID: vtp Lims ID: icis Worklist Smp#: 10 Client ID: Purge Vol: 200.000 mL Dil. Factor: 1.0000 ALS Bottle#: 10 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Y Scaling: Method Defined: Scale to the Nth Largest Target: 1 2.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 18.0 20.0 22.0 24.0 Min 0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 Y ( X 10 0 0 0 0 ) 27754-10[MS SCAN Chro]:Total * C h l o r o b r o m o m e t h a n e ( 9 . 7 0 4 )+ * 1 ,4- D i f lu o r o b e n z en e ( 1 1 . 1 0 8 ) * C h l o r o b e n z en e - d 5 ( 1 5 . 2 1 2 ) Page 339 of 478 Report Date: 07-Nov-2017 13:39:58 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Target Compound Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-11.D Lims ID: ic Client ID: Sample Type: IC Calib Level: 6 Inject. Date: 07-Nov-2017 00:05:30 ALS Bottle#: 11 Worklist Smp#: 11 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Sample Info: 200-0027754-011 Misc. Info.: ic Operator ID: vtp Instrument ID: CHB.i Sublist:chrom-TO15_LLNJ_TO3*sub5 Method:\\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\TO15_LLNJ_TO3.m Limit Group: AI_TO15_ICAL Last Update: 07-Nov-2017 13:39:57 Calib Date: 07-Nov-2017 01:49:30 Integrator: RTE ID Type: Deconvolution ID Quant Method: Internal/External Standard Quant By: Initial Calibration Last ICal File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-13.D Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host:XAWRK022 First Level Reviewer: daiglep Date:07-Nov-2017 09:06:12 Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 1 Propene 41 3.135 3.135 0.000 99 262308 15.0 14.2 2 Dichlorodifluoromethane 85 3.193 3.193 0.000 99 1012917 15.0 14.4 3 Chlorodifluoromethane 51 3.231 3.225 0.006 97 562365 15.0 14.0 4 1,2-Dichloro-1,1,2,2-tetra 85 3.412 3.412 0.000 95 1075928 15.0 14.6 5 Chloromethane 50 3.540 3.535 0.005 99 359553 15.0 14.3 6 Butane 43 3.711 3.711 0.000 99 609191 15.0 14.0 7 Vinyl chloride 62 3.748 3.748 0.000 98 457798 15.0 15.1 8 Butadiene 54 3.812 3.812 0.000 95 335437 15.0 15.1 9 BFB 10 Bromomethane 94 4.479 4.479 0.000 99 466967 15.0 15.0 11 Chloroethane 64 4.709 4.709 0.000 99 274839 15.0 14.7 12 2-Methylbutane 43 4.794 4.789 0.005 94 557524 15.0 14.1 13 Vinyl bromide 106 5.120 5.120 0.000 100 485880 15.0 15.3 14 Trichlorofluoromethane 101 5.221 5.216 0.005 98 1103290 15.0 14.7 15 Pentane 43 5.355 5.355 0.000 96 857492 15.0 14.3 16 Ethanol 45 5.680 5.675 0.005 99 322355 20.0 19.6 17 Ethyl ether 59 5.830 5.830 0.000 95 344829 15.0 14.9 18 Acrolein 56 6.198 6.198 0.000 94 159278 15.0 14.9 19 1,1,2-Trichloro-1,2,2-trif 101 6.251 6.246 0.005 98 931730 15.0 14.8 20 1,1-Dichloroethene 96 6.321 6.321 0.000 98 463386 15.0 14.7 21 Acetone 43 6.470 6.470 0.000 97 679222 15.0 14.4 22 Isopropyl alcohol 45 6.689 6.684 0.005 99 775787 15.0 14.6 23 Carbon disulfide 76 6.753 6.748 0.005 98 1303321 15.0 14.7 24 3-Chloro-1-propene 41 7.020 7.020 0.000 94 630248 15.0 14.3 26 Acetonitrile 41 7.079 7.079 0.000 100 400394 15.0 14.7 27 Methylene Chloride 49 7.281 7.276 0.005 94 543530 15.0 14.4 28 2-Methyl-2-propanol 59 7.388 7.388 0.000 93 1026121 15.0 14.8 29 Methyl tert-butyl ether 73 7.628 7.628 0.000 97 1398096 15.0 14.8 30 trans-1,2-Dichloroethene 61 7.687 7.687 0.000 98 700935 15.0 14.6 31 Acrylonitrile 53 7.756 7.756 0.000 95 374931 15.0 14.8 Page 340 of 478 Report Date: 07-Nov-2017 13:39:58 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-11.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 32 Hexane 57 8.018 8.018 0.000 93 800225 15.0 13.9 33 1,1-Dichloroethane 63 8.429 8.429 0.000 99 924957 15.0 14.4 34 Vinyl acetate 43 8.434 8.434 0.000 100 1291360 15.0 14.6 36 2-Butanone (MEK) 72 9.320 9.320 0.000 100 274656 15.0 14.8 37 cis-1,2-Dichloroethene 96 9.336 9.331 0.005 95 549204 15.0 15.0 35 Ethyl acetate 88 9.336 9.336 0.000 93 45156 15.0 14.7 * 39 Chlorobromomethane 128 9.704 9.704 0.000 95 317897 10.0 10.0 38 Tetrahydrofuran 42 9.710 9.710 0.000 95 611226 15.0 14.6 40 Chloroform 83 9.774 9.774 0.000 95 998358 15.0 14.6 S 41 1,2-Dichloroethene, Total 61 0 30.0 29.6 42 1,1,1-Trichloroethane 97 10.035 10.035 0.000 95 973905 15.0 14.8 43 Cyclohexane 84 10.051 10.046 0.005 98 744741 15.0 15.1 44 Carbon tetrachloride 117 10.243 10.243 0.000 97 979389 15.0 15.7 45 Isooctane 57 10.521 10.521 0.000 100 2785353 15.0 14.9 46 Benzene 78 10.564 10.564 0.000 95 1663189 15.0 14.4 47 1,2-Dichloroethane 62 10.665 10.665 0.000 96 601835 15.0 14.6 48 n-Heptane 43 10.777 10.777 0.000 92 1018472 15.0 14.2 A 49 GRO 1 10.865 (4.779-16.951) 0 212504719 15.0 0 * 50 1,4-Difluorobenzene 114 11.108 11.108 0.000 94 1568827 10.0 10.0 51 n-Butanol 56 11.289 11.289 0.000 86 330651 15.0 14.8 53 Trichloroethene 95 11.476 11.476 0.000 98 705472 15.0 15.3 54 1,2-Dichloropropane 63 11.844 11.844 0.000 93 660207 15.0 14.9 55 Methyl methacrylate 69 11.882 11.882 0.000 97 626224 15.0 15.1 56 1,4-Dioxane 88 11.972 11.967 0.005 93 320238 15.0 14.6 57 Dibromomethane 174 12.031 12.031 0.000 96 679826 15.0 14.8 58 Dichlorobromomethane 83 12.207 12.202 0.005 98 1139481 15.0 14.7 A 59 TVOC as Toluene 1 12.485 (3.125-21.845) 0 348003400 15.0 0 60 cis-1,3-Dichloropropene 75 12.832 12.832 0.000 90 955016 15.0 15.2 61 4-Methyl-2-pentanone (MIBK 43 12.976 12.976 0.000 95 1302488 15.0 14.8 63 n-Octane 43 13.248 13.248 0.000 91 1452261 15.0 14.4 64 Toluene 92 13.264 13.264 0.000 93 1231696 15.0 14.6 66 trans-1,3-Dichloropropene 75 13.622 13.622 0.000 95 923761 15.0 15.4 67 1,1,2-Trichloroethane 83 13.894 13.894 0.000 95 615856 15.0 14.8 68 Tetrachloroethene 166 14.038 14.038 0.000 98 1013752 15.0 15.1 69 2-Hexanone 43 14.155 14.155 0.000 94 1253699 15.0 14.8 70 Chlorodibromomethane 129 14.449 14.449 0.000 98 1209039 15.0 15.2 71 Ethylene Dibromide 107 14.652 14.652 0.000 98 1119668 15.0 15.1 * 72 Chlorobenzene-d5 117 15.217 15.212 0.005 84 1415692 10.0 10.0 73 Chlorobenzene 112 15.255 15.255 0.000 96 1685338 15.0 14.9 74 Ethylbenzene 91 15.324 15.319 0.005 98 2745535 15.0 14.8 75 n-Nonane 57 15.340 15.340 0.000 94 1397898 15.0 14.7 76 m-Xylene & p-Xylene 106 15.468 15.468 0.000 0 2218882 30.0 30.4 78 o-Xylene 106 15.981 15.981 -0.001 99 1084561 15.0 14.9 S 77 Xylenes, Total 106 0 45.0 45.3 79 Styrene 104 16.002 16.002 0.000 98 1712264 15.0 15.6 80 Bromoform 173 16.295 16.295 0.000 98 1147379 15.0 15.6 81 Isopropylbenzene 105 16.391 16.391 0.000 95 3088484 15.0 15.0 85 1,2,3-Trichloropropane 75 16.882 16.882 0.000 98 1276362 15.0 15.0 83 1,1,2,2-Tetrachloroethane 83 16.797 16.797 0.000 97 1676500 15.0 15.0 84 N-Propylbenzene 91 16.872 16.872 0.000 99 3873668 15.0 15.3 86 n-Decane 57 16.941 16.941 0.000 89 1749982 15.0 14.5 87 4-Ethyltoluene 105 16.995 16.995 0.000 98 3091160 15.0 15.4 Page 341 of 478 Report Date: 07-Nov-2017 13:39:58 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-11.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 88 2-Chlorotoluene 91 17.037 17.037 0.000 97 2537832 15.0 15.1 89 1,3,5-Trimethylbenzene 105 17.064 17.064 0.000 93 2528343 15.0 15.2 90 Alpha Methyl Styrene 118 17.336 17.336 0.000 90 1287536 15.0 15.8 91 tert-Butylbenzene 119 17.437 17.437 0.000 95 2404614 15.0 14.9 92 1,2,4-Trimethylbenzene 105 17.507 17.507 0.000 97 2464062 15.0 15.0 93 sec-Butylbenzene 105 17.694 17.694 0.000 99 3666512 15.0 14.7 94 4-Isopropyltoluene 119 17.848 17.848 0.000 98 2956723 15.0 14.4 95 1,3-Dichlorobenzene 146 17.928 17.928 0.000 97 1696474 15.0 15.5 96 1,4-Dichlorobenzene 146 18.041 18.035 0.006 96 1664444 15.0 15.6 97 Benzyl chloride 91 18.190 18.185 0.005 99 1962790 15.0 16.1 98 Undecane 57 18.318 18.318 0.000 96 1951866 15.0 14.9 99 n-Butylbenzene 91 18.355 18.355 0.000 98 2706883 15.0 14.3 100 1,2-Dichlorobenzene 146 18.521 18.521 0.000 97 1525509 15.0 14.8 102 Dodecane 57 19.770 19.770 0.000 97 1688580 15.0 16.7 103 1,2,4-Trichlorobenzene 180 20.885 20.885 0.000 94 1082245 15.0 17.0 104 Hexachlorobutadiene 225 21.051 21.051 0.000 98 1059150 15.0 15.8 105 Naphthalene 128 21.360 21.360 0.000 100 2354157 15.0 17.5 106 1,2,3-Trichlorobenzene 180 21.835 21.835 0.000 96 951579 15.0 17.2 Reagents: ATTO15CAL5w_00069 Amount Added: 200.00 Units: mL ATTO15BISs_00006 Amount Added: 20.00 Units: mL Run Reagent Page 342 of 478 Report Date: 07-Nov-2017 13:39:58 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-11.D Injection Date: 07-Nov-2017 00:05:30 Instrument ID: CHB.i Operator ID: vtp Lims ID: ic Worklist Smp#: 11 Client ID: Purge Vol: 200.000 mL Dil. Factor: 1.0000 ALS Bottle#: 11 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Y Scaling: Method Defined: Scale to the Nth Largest Target: 1 2.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 18.0 20.0 22.0 24.0 Min 0 3 6 9 12 15 18 21 24 27 30 33 36 39 42 45 48 51 54 57 60 Y ( X 10 0 0 0 0 ) 27754-11[MS SCAN Chro]:Total * C h l o r o b r o m o m e t h a n e ( 9 . 7 0 4 )+ * 1 ,4- D i f lu o r o b e n z en e ( 1 1 . 1 0 8 ) * C h l o r o b e n z en e - d 5 ( 1 5 . 2 1 7 ) Page 343 of 478 Report Date: 07-Nov-2017 13:40:00 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Target Compound Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-12.D Lims ID: ic Client ID: Sample Type: IC Calib Level: 7 Inject. Date: 07-Nov-2017 00:57:30 ALS Bottle#: 12 Worklist Smp#: 12 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Sample Info: 200-0027754-012 Misc. Info.: ic Operator ID: vtp Instrument ID: CHB.i Sublist:chrom-TO15_LLNJ_TO3*sub5 Method:\\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\TO15_LLNJ_TO3.m Limit Group: AI_TO15_ICAL Last Update: 07-Nov-2017 13:40:00 Calib Date: 07-Nov-2017 01:49:30 Integrator: RTE ID Type: Deconvolution ID Quant Method: Internal/External Standard Quant By: Initial Calibration Last ICal File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-13.D Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host:XAWRK022 First Level Reviewer: daiglep Date:07-Nov-2017 09:06:56 Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 1 Propene 41 3.135 3.135 0.000 99 350917 20.0 17.2 2 Dichlorodifluoromethane 85 3.193 3.193 0.000 99 1400515 20.0 18.0 3 Chlorodifluoromethane 51 3.231 3.225 0.006 97 762497 20.0 17.2 4 1,2-Dichloro-1,1,2,2-tetra 85 3.412 3.412 0.000 98 1504994 20.0 18.4 5 Chloromethane 50 3.540 3.535 0.005 99 487565 20.0 17.5 6 Butane 43 3.711 3.711 0.000 98 814735 20.0 17.0 7 Vinyl chloride 62 3.748 3.748 0.000 98 629881 20.0 18.8 8 Butadiene 54 3.812 3.812 0.000 94 460938 20.0 18.8 10 Bromomethane 94 4.479 4.479 0.000 99 682895 20.0 19.8 9 BFB 11 Chloroethane 64 4.709 4.709 0.000 99 395487 20.0 19.1 12 2-Methylbutane 43 4.794 4.789 0.005 93 759706 20.0 17.4 13 Vinyl bromide 106 5.125 5.120 0.005 100 719528 20.0 20.5 14 Trichlorofluoromethane 101 5.221 5.216 0.005 98 1566416 20.0 18.8 15 Pentane 43 5.360 5.355 0.005 96 1183796 20.0 17.8 16 Ethanol 45 5.686 5.675 0.011 98 625643 40.0 34.4 17 Ethyl ether 59 5.830 5.830 0.000 95 489381 20.0 19.1 18 Acrolein 56 6.198 6.198 0.000 95 227859 20.0 19.3 19 1,1,2-Trichloro-1,2,2-trif 101 6.251 6.246 0.005 98 1357192 20.0 19.4 20 1,1-Dichloroethene 96 6.321 6.321 0.000 97 676409 20.0 19.3 21 Acetone 43 6.470 6.470 0.000 96 918444 20.0 17.6 22 Isopropyl alcohol 45 6.694 6.684 0.010 99 1053695 20.0 17.9 23 Carbon disulfide 76 6.753 6.748 0.005 98 1884193 20.0 19.2 24 3-Chloro-1-propene 41 7.020 7.020 0.000 93 907636 20.0 18.6 26 Acetonitrile 41 7.079 7.079 0.000 100 558071 20.0 18.5 27 Methylene Chloride 49 7.281 7.276 0.005 93 758104 20.0 18.1 28 2-Methyl-2-propanol 59 7.393 7.388 0.005 92 1407939 20.0 18.4 29 Methyl tert-butyl ether 73 7.628 7.628 0.000 97 1996655 20.0 19.1 30 trans-1,2-Dichloroethene 61 7.692 7.687 0.005 98 999814 20.0 18.8 31 Acrylonitrile 53 7.756 7.756 0.000 96 528510 20.0 18.9 Page 344 of 478 Report Date: 07-Nov-2017 13:40:00 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-12.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 32 Hexane 57 8.018 8.018 0.000 91 1144849 20.0 17.9 33 1,1-Dichloroethane 63 8.429 8.429 0.000 99 1313600 20.0 18.5 34 Vinyl acetate 43 8.434 8.434 0.000 100 1782446 20.0 18.2 36 2-Butanone (MEK) 72 9.320 9.320 0.000 99 393924 20.0 19.1 37 cis-1,2-Dichloroethene 96 9.336 9.331 0.005 96 806754 20.0 19.9 35 Ethyl acetate 88 9.336 9.336 0.000 94 66363 20.0 19.5 * 39 Chlorobromomethane 128 9.704 9.704 0.000 93 351888 10.0 10.0 38 Tetrahydrofuran 42 9.715 9.710 0.005 94 842926 20.0 18.2 40 Chloroform 83 9.779 9.774 0.005 95 1425408 20.0 18.8 S 41 1,2-Dichloroethene, Total 61 0 40.0 38.8 42 1,1,1-Trichloroethane 97 10.035 10.035 0.000 95 1386002 20.0 19.1 43 Cyclohexane 84 10.051 10.046 0.005 97 1078684 20.0 19.7 44 Carbon tetrachloride 117 10.243 10.243 0.000 97 1408169 20.0 20.4 45 Isooctane 57 10.526 10.521 0.005 100 3971225 20.0 19.2 46 Benzene 78 10.569 10.564 0.005 95 2412590 20.0 18.9 47 1,2-Dichloroethane 62 10.665 10.665 0.000 96 834386 20.0 18.3 48 n-Heptane 43 10.777 10.777 0.000 91 1411728 20.0 17.8 A 49 GRO 1 10.865 (4.779-16.951) 0 302904769 20.0 0 * 50 1,4-Difluorobenzene 114 11.108 11.108 0.000 94 1736810 10.0 10.0 51 n-Butanol 56 11.289 11.289 0.000 85 462049 20.0 18.7 53 Trichloroethene 95 11.476 11.476 0.000 98 1020053 20.0 20.0 54 1,2-Dichloropropane 63 11.844 11.844 0.000 95 947123 20.0 19.3 55 Methyl methacrylate 69 11.882 11.882 0.000 98 907851 20.0 19.8 56 1,4-Dioxane 88 11.973 11.967 0.005 93 457426 20.0 18.9 57 Dibromomethane 174 12.037 12.031 0.006 96 1002264 20.0 19.8 58 Dichlorobromomethane 83 12.207 12.202 0.005 97 1641881 20.0 19.1 A 59 TVOC as Toluene 1 12.485 (3.125-21.845) 0 492329729 20.0 0 60 cis-1,3-Dichloropropene 75 12.832 12.832 0.000 89 1376724 20.0 19.8 61 4-Methyl-2-pentanone (MIBK 43 12.981 12.976 0.005 94 1803414 20.0 18.6 63 n-Octane 43 13.248 13.248 0.000 90 1990415 20.0 17.8 64 Toluene 92 13.264 13.264 0.000 93 1809158 20.0 19.4 66 trans-1,3-Dichloropropene 75 13.622 13.622 0.000 94 1324222 20.0 20.0 67 1,1,2-Trichloroethane 83 13.894 13.894 0.000 94 895676 20.0 19.5 68 Tetrachloroethene 166 14.038 14.038 0.000 98 1504548 20.0 20.4 69 2-Hexanone 43 14.155 14.155 0.000 95 1722537 20.0 18.5 70 Chlorodibromomethane 129 14.449 14.449 0.000 98 1793665 20.0 20.5 71 Ethylene Dibromide 107 14.652 14.652 0.000 98 1634580 20.0 20.1 * 72 Chlorobenzene-d5 117 15.217 15.212 0.005 85 1559872 10.0 10.0 73 Chlorobenzene 112 15.255 15.255 0.000 97 2491305 20.0 20.0 74 Ethylbenzene 91 15.324 15.319 0.005 97 4014844 20.0 19.7 75 n-Nonane 57 15.345 15.340 0.005 92 1983042 20.0 19.0 76 m-Xylene & p-Xylene 106 15.468 15.468 0.000 0 3293994 40.0 40.9 78 o-Xylene 106 15.981 15.981 0.000 99 1596485 20.0 19.9 S 77 Xylenes, Total 106 0 60.0 60.9 79 Styrene 104 16.007 16.002 0.005 97 2512147 20.0 20.8 80 Bromoform 173 16.295 16.295 0.000 99 1752241 20.0 21.7 81 Isopropylbenzene 105 16.391 16.391 0.000 95 4545305 20.0 20.1 83 1,1,2,2-Tetrachloroethane 83 16.802 16.797 0.005 97 2424642 20.0 19.7 84 N-Propylbenzene 91 16.872 16.872 0.000 100 5568174 20.0 20.0 85 1,2,3-Trichloropropane 75 16.882 16.882 0.000 97 1816466 20.0 19.3 86 n-Decane 57 16.941 16.941 0.000 90 2395755 20.0 18.1 87 4-Ethyltoluene 105 17.000 16.995 0.005 98 4414476 20.0 19.9 Page 345 of 478 Report Date: 07-Nov-2017 13:40:00 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-12.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 88 2-Chlorotoluene 91 17.037 17.037 0.000 96 3605957 20.0 19.5 89 1,3,5-Trimethylbenzene 105 17.064 17.064 0.000 94 3506340 20.0 19.1 90 Alpha Methyl Styrene 118 17.336 17.336 0.000 91 1810300 20.0 20.2 91 tert-Butylbenzene 119 17.438 17.437 0.001 96 3393419 20.0 19.1 92 1,2,4-Trimethylbenzene 105 17.512 17.507 0.005 96 3454778 20.0 19.1 93 sec-Butylbenzene 105 17.699 17.694 0.005 99 5200086 20.0 18.9 94 4-Isopropyltoluene 119 17.848 17.848 0.000 98 4342966 20.0 19.2 95 1,3-Dichlorobenzene 146 17.929 17.928 0.000 96 2362589 20.0 19.6 96 1,4-Dichlorobenzene 146 18.041 18.035 0.006 96 2308042 20.0 19.6 97 Benzyl chloride 91 18.190 18.185 0.005 100 2733690 20.0 20.3 98 Undecane 57 18.318 18.318 0.000 95 2730816 20.0 18.9 99 n-Butylbenzene 91 18.355 18.355 0.000 98 4000789 20.0 19.2 100 1,2-Dichlorobenzene 146 18.526 18.521 0.005 98 2178021 20.0 19.2 102 Dodecane 57 19.775 19.770 0.005 97 2288869 20.0 20.5 103 1,2,4-Trichlorobenzene 180 20.885 20.885 0.000 94 1522402 20.0 21.7 104 Hexachlorobutadiene 225 21.051 21.051 0.000 98 1555025 20.0 21.0 105 Naphthalene 128 21.365 21.360 0.005 100 3182700 20.0 21.4 106 1,2,3-Trichlorobenzene 180 21.840 21.835 0.005 96 1354997 20.0 22.2 Reagents: ATTO15CAL6w_00144 Amount Added: 200.00 Units: mL ATTO15BISs_00006 Amount Added: 20.00 Units: mL Run Reagent Page 346 of 478 Report Date: 07-Nov-2017 13:40:00 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-12.D Injection Date: 07-Nov-2017 00:57:30 Instrument ID: CHB.i Operator ID: vtp Lims ID: ic Worklist Smp#: 12 Client ID: Purge Vol: 200.000 mL Dil. Factor: 1.0000 ALS Bottle#: 12 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Y Scaling: Method Defined: Scale to the Nth Largest Target: 1 2.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 18.0 20.0 22.0 24.0 Min 0 3 6 9 12 15 18 21 24 27 30 33 36 39 42 45 48 51 54 57 60 63 66 69 72 75 78 81 84 87 Y ( X 10 0 0 0 0 ) 27754-12[MS SCAN Chro]:Total * C h l o r o b r o m o m e t h a n e ( 9 . 7 1 0 )+ * 1 ,4- D i f lu o r o b e n z en e ( 1 1 . 1 0 8 ) * C h l o r o b e n z en e - d 5 ( 1 5 . 2 1 7 ) Page 347 of 478 Report Date: 07-Nov-2017 13:40:03 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Target Compound Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-13.D Lims ID: ic Client ID: Sample Type: IC Calib Level: 8 Inject. Date: 07-Nov-2017 01:49:30 ALS Bottle#: 13 Worklist Smp#: 13 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Sample Info: 200-0027754-013 Misc. Info.: ic Operator ID: vtp Instrument ID: CHB.i Sublist:chrom-TO15_LLNJ_TO3*sub5 Method:\\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\TO15_LLNJ_TO3.m Limit Group: AI_TO15_ICAL Last Update: 07-Nov-2017 13:40:02 Calib Date: 07-Nov-2017 01:49:30 Integrator: RTE ID Type: Deconvolution ID Quant Method: Internal/External Standard Quant By: Initial Calibration Last ICal File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-13.D Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host:XAWRK022 First Level Reviewer: daiglep Date:07-Nov-2017 09:07:40 Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 1 Propene 41 3.135 3.135 0.000 98 666801 40.0 28.1 2 Dichlorodifluoromethane 85 3.193 3.193 0.000 99 2754680 40.0 30.5 3 Chlorodifluoromethane 51 3.231 3.225 0.006 97 1456389 40.0 28.3 4 1,2-Dichloro-1,1,2,2-tetra 85 3.417 3.412 0.005 97 3017555 40.0 31.8 5 Chloromethane 50 3.540 3.535 0.005 99 953781 40.0 29.6 6 Butane 43 3.716 3.711 0.005 99 1560254 40.0 28.0 7 Vinyl chloride 62 3.748 3.748 0.000 98 1259739 40.0 32.4 8 Butadiene 54 3.818 3.812 0.006 94 907836 40.0 31.9 9 BFB 10 Bromomethane 94 4.485 4.479 0.006 100 1419547 40.0 35.5 11 Chloroethane 64 4.714 4.709 0.005 99 801767 40.0 33.3 12 2-Methylbutane 43 4.800 4.789 0.011 93 1477241 40.0 29.2 13 Vinyl bromide 106 5.125 5.120 0.005 100 1517808 40.0 37.2 14 Trichlorofluoromethane 101 5.227 5.216 0.011 98 3219338 40.0 33.3 15 Pentane 43 5.360 5.355 0.005 96 2305350 40.0 29.9 16 Ethanol 45 5.696 5.675 0.021 98 1415524 100.0 67.1 17 Ethyl ether 59 5.835 5.830 0.005 95 990383 40.0 33.4 18 Acrolein 56 6.198 6.198 0.000 94 464860 40.0 33.9 19 1,1,2-Trichloro-1,2,2-trif 101 6.257 6.246 0.011 99 2870018 40.0 35.4 20 1,1-Dichloroethene 96 6.326 6.321 0.005 95 1431915 40.0 35.3 21 Acetone 43 6.470 6.470 0.000 95 1763733 40.0 29.1 22 Isopropyl alcohol 45 6.710 6.684 0.026 99 2014852 40.0 29.6 23 Carbon disulfide 76 6.753 6.748 0.005 98 3905659 40.0 34.3 24 3-Chloro-1-propene 41 7.025 7.020 0.005 92 1708448 40.0 30.1 26 Acetonitrile 41 7.084 7.079 0.005 99 1051183 40.0 30.0 27 Methylene Chloride 49 7.281 7.276 0.005 90 1485831 40.0 30.5 28 2-Methyl-2-propanol 59 7.410 7.388 0.022 92 2782228 40.0 31.3 29 Methyl tert-butyl ether 73 7.628 7.628 0.000 97 4082553 40.0 33.7 30 trans-1,2-Dichloroethene 61 7.692 7.687 0.005 97 2027160 40.0 32.9 31 Acrylonitrile 53 7.762 7.756 0.006 96 1064673 40.0 32.7 Page 348 of 478 Report Date: 07-Nov-2017 13:40:03 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-13.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 32 Hexane 57 8.023 8.018 0.005 90 2299897 40.0 31.0 33 1,1-Dichloroethane 63 8.434 8.429 0.005 99 2648188 40.0 32.1 34 Vinyl acetate 43 8.440 8.434 0.006 100 3425006 40.0 30.2 36 2-Butanone (MEK) 72 9.325 9.320 0.005 98 811284 40.0 33.9 37 cis-1,2-Dichloroethene 96 9.336 9.331 0.005 95 1716713 40.0 36.6 35 Ethyl acetate 88 9.341 9.336 0.005 94 142076 40.0 36.0 * 39 Chlorobromomethane 128 9.710 9.704 0.006 90 408442 10.0 10.0 38 Tetrahydrofuran 42 9.715 9.710 0.005 93 1611154 40.0 30.8 40 Chloroform 83 9.784 9.774 0.010 94 2922350 40.0 33.2 S 41 1,2-Dichloroethene, Total 61 0 80.0 69.5 42 1,1,1-Trichloroethane 97 10.041 10.035 0.006 95 2851804 40.0 34.8 43 Cyclohexane 84 10.051 10.046 0.005 95 2298205 40.0 37.3 44 Carbon tetrachloride 117 10.243 10.243 0.000 97 2864853 40.0 36.9 45 Isooctane 57 10.526 10.521 0.005 99 8002808 40.0 34.3 46 Benzene 78 10.569 10.564 0.005 94 5046961 40.0 35.1 47 1,2-Dichloroethane 62 10.670 10.665 0.005 96 1634383 40.0 31.9 48 n-Heptane 43 10.782 10.777 0.005 88 2713764 40.0 30.4 A 49 GRO 1 10.865 (4.779-16.951) 0 613108146 40.0 0 * 50 1,4-Difluorobenzene 114 11.113 11.108 0.005 93 1957289 10.0 10.0 51 n-Butanol 56 11.300 11.289 0.011 84 934673 40.0 33.6 53 Trichloroethene 95 11.482 11.476 0.006 96 2163493 40.0 37.7 54 1,2-Dichloropropane 63 11.850 11.844 0.006 95 1921446 40.0 34.7 55 Methyl methacrylate 69 11.887 11.882 0.005 97 1872327 40.0 36.3 56 1,4-Dioxane 88 11.978 11.967 0.011 91 923935 40.0 33.8 57 Dibromomethane 174 12.037 12.031 0.006 95 2204560 40.0 38.6 58 Dichlorobromomethane 83 12.207 12.202 0.005 97 3362489 40.0 34.8 A 59 TVOC as Toluene 1 12.485 (3.125-21.845) 0 1002856430 40.0 0 60 cis-1,3-Dichloropropene 75 12.837 12.832 0.005 88 2838418 40.0 36.3 61 4-Methyl-2-pentanone (MIBK 43 12.987 12.976 0.011 93 3457992 40.0 31.6 63 n-Octane 43 13.253 13.248 0.005 87 3709404 40.0 29.5 64 Toluene 92 13.269 13.264 0.005 93 3852181 40.0 36.6 66 trans-1,3-Dichloropropene 75 13.627 13.622 0.005 94 2695893 40.0 36.1 67 1,1,2-Trichloroethane 83 13.899 13.894 0.005 94 1880575 40.0 36.2 68 Tetrachloroethene 166 14.043 14.038 0.005 96 3391200 40.0 40.7 69 2-Hexanone 43 14.161 14.155 0.006 97 3323450 40.0 31.6 70 Chlorodibromomethane 129 14.454 14.449 0.005 98 3876618 40.0 39.2 71 Ethylene Dibromide 107 14.657 14.652 0.005 98 3507458 40.0 38.1 * 72 Chlorobenzene-d5 117 15.217 15.212 0.005 82 1761738 10.0 10.0 73 Chlorobenzene 112 15.260 15.255 0.005 98 5382503 40.0 38.3 74 Ethylbenzene 91 15.324 15.319 0.005 97 8428186 40.0 36.5 75 n-Nonane 57 15.345 15.340 0.005 86 3919902 40.0 33.2 76 m-Xylene & p-Xylene 106 15.474 15.468 0.006 0 7176091 80.0 79.0 78 o-Xylene 106 15.986 15.981 0.005 98 3448842 40.0 38.2 S 77 Xylenes, Total 106 0 120.0 117.1 79 Styrene 104 16.007 16.002 0.005 97 5480628 40.0 40.2 80 Bromoform 173 16.301 16.295 0.006 99 3907202 40.0 42.8 81 Isopropylbenzene 105 16.397 16.391 0.006 94 9581691 40.0 37.5 83 1,1,2,2-Tetrachloroethane 83 16.802 16.797 0.005 97 4869536 40.0 35.0 84 N-Propylbenzene 91 16.877 16.872 0.005 100 11180756 40.0 35.5 85 1,2,3-Trichloropropane 75 16.888 16.882 0.006 96 3577331 40.0 33.7 86 n-Decane 57 16.947 16.941 0.006 89 4905409 40.0 32.8 87 4-Ethyltoluene 105 17.000 16.995 0.005 98 9273522 40.0 37.0 Page 349 of 478 Report Date: 07-Nov-2017 13:40:03 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-13.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 88 2-Chlorotoluene 91 17.043 17.037 0.006 95 7557699 40.0 36.2 89 1,3,5-Trimethylbenzene 105 17.069 17.064 0.005 94 7827219 40.0 37.8 90 Alpha Methyl Styrene 118 17.341 17.336 0.005 92 4081481 40.0 40.2 91 tert-Butylbenzene 119 17.443 17.437 0.006 96 7457439 40.0 37.2 92 1,2,4-Trimethylbenzene 105 17.512 17.507 0.005 96 7714438 40.0 37.7 93 sec-Butylbenzene 105 17.699 17.694 0.005 99 11501603 40.0 37.0 94 4-Isopropyltoluene 119 17.854 17.848 0.006 98 9980594 40.0 39.0 95 1,3-Dichlorobenzene 146 17.934 17.928 0.006 95 5559940 40.0 40.9 96 1,4-Dichlorobenzene 146 18.041 18.035 0.006 97 5573724 40.0 41.9 97 Benzyl chloride 91 18.190 18.185 0.005 100 6135081 40.0 40.4 98 Undecane 57 18.323 18.318 0.005 93 5313148 40.0 32.6 99 n-Butylbenzene 91 18.361 18.355 0.006 98 8834446 40.0 37.6 100 1,2-Dichlorobenzene 146 18.526 18.521 0.005 99 5217884 40.0 40.8 102 Dodecane 57 19.775 19.770 0.005 97 2608958 40.0 20.7 103 1,2,4-Trichlorobenzene 180 20.885 20.885 0.000 93 3106580 40.0 39.1 104 Hexachlorobutadiene 225 21.051 21.051 0.000 96 2733620 40.0 32.7 105 Naphthalene 128 21.366 21.360 0.006 100 6623680 40.0 39.5 106 1,2,3-Trichlorobenzene 180 21.841 21.835 0.005 95 2277299 40.0 33.1 Reagents: ATTO15CAL7w_00071 Amount Added: 200.00 Units: mL ATTO15BISs_00006 Amount Added: 20.00 Units: mL Run Reagent Page 350 of 478 Report Date: 07-Nov-2017 13:40:03 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-13.D Injection Date: 07-Nov-2017 01:49:30 Instrument ID: CHB.i Operator ID: vtp Lims ID: ic Worklist Smp#: 13 Client ID: Purge Vol: 200.000 mL Dil. Factor: 1.0000 ALS Bottle#: 13 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Y Scaling: Method Defined: Scale to the Nth Largest Target: 1 2.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 18.0 20.0 22.0 24.0 Min 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 Y ( X 10 0 0 0 0 0 ) 27754-13[MS SCAN Chro]:Total * C h l o r o b r o m o m e t h a n e ( 9 . 7 1 0 )+ * 1 ,4- D i f lu o r o b e n z en e ( 1 1 . 1 1 3 ) * C h l o r o b e n z en e - d 5 ( 1 5 . 2 2 3 ) Page 351 of 478 FORM VII Lab Name:Job No.: SDG No.: Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID: Calib End Date:GC Column: ID: AIR - GC/MS VOA CONTINUING CALIBRATION DATA 0.32(mm) 200-41113-1 200-41113-1 CHB.i 11/07/2017 12:25 11/06/2017 17:59 11/07/2017 01:49 ICV 200-122990/24 RTX-624 TestAmerica Burlington Lab File ID:27754-24.D Heated Purge: (Y/N)NConc. Units:ppb v/v ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNT AMOUNT %D AVE RRF RRF MIN RRF Propylene 0.58150.5800 10.0 10.0 0.3 30.0Ave Dichlorodifluoromethane 2.2512.215 10.2 10.0 1.6 30.0Ave Freon 22 1.2501.259 9.92 10.0 -0.7 30.0Ave 1,2-Dichlorotetrafluoroethan e 2.3882.326 10.3 10.0 2.7 30.0Ave Chloromethane 0.79950.7900 10.1 10.0 1.2 30.0Ave n-Butane 1.3331.365 9.77 10.0 -2.3 30.0Ave Vinyl chloride 1.0070.9520 10.6 10.0 5.8 30.0Ave 1,3-Butadiene 0.73680.6974 10.6 10.0 5.6 30.0Ave Bromomethane 1.0360.9801 10.6 10.0 5.7 30.0Ave Chloroethane 0.60940.5888 10.3 10.0 3.5 30.0Ave Isopentane 1.2181.241 9.82 10.0 -1.8 30.0Ave Bromoethene(Vinyl Bromide)1.0710.999 10.7 10.0 7.2 30.0Ave Trichlorofluoromethane 2.4122.364 10.2 10.0 2.0 30.0Ave n-Pentane 1.8831.886 9.98 10.0 -0.2 30.0Ave Ethanol 0.51500.5169 14.9 15.0 -0.4 30.0Ave Ethyl ether 0.75840.7268 10.4 10.0 4.3 30.0Ave Acrolein 0.34300.3358 10.2 10.0 2.1 30.0Ave Freon TF 2.0501.986 10.3 10.0 3.2 30.0Ave 1,1-Dichloroethene 1.0180.9944 10.2 10.0 2.4 30.0Ave Acetone 1.5091.485 10.2 10.0 1.6 30.0Ave Isopropyl alcohol 1.7901.668 10.7 10.0 7.3 30.0Ave Carbon disulfide 2.9122.787 10.4 10.0 4.5 30.0Ave 3-Chloropropene 1.4011.388 10.1 10.0 1.0 30.0Ave Acetonitrile 0.87750.8571 10.2 10.0 2.4 30.0Ave Methylene Chloride 1.2191.191 10.2 10.0 2.3 30.0Ave tert-Butyl alcohol 2.3282.175 10.7 10.0 7.0 30.0Ave Methyl tert-butyl ether 3.0382.963 10.3 10.0 2.5 30.0Ave trans-1,2-Dichloroethene 1.5591.509 10.3 10.0 3.3 30.0Ave Acrylonitrile 0.83880.7960 10.5 10.0 5.4 30.0Ave n-Hexane 1.7701.815 9.75 10.0 -2.5 30.0Ave 1,1-Dichloroethane 2.0532.017 10.2 10.0 1.8 30.0Ave Vinyl acetate 2.8352.777 10.2 10.0 2.1 30.0Ave Methyl Ethyl Ketone 0.59330.5853 10.1 10.0 1.4 30.0Ave Ethyl acetate 0.09850.0966 10.2 10.0 1.9 30.0Ave cis-1,2-Dichloroethene 1.2081.149 10.5 10.0 5.1 30.0Ave Tetrahydrofuran 0.27570.2669 10.3 10.0 3.3 30.0Ave Chloroform 2.1952.155 10.2 10.0 1.9 30.0Ave 1,1,1-Trichloroethane 0.42650.4188 10.2 10.0 1.9 30.0Ave Cyclohexane 0.32750.3149 10.4 10.0 4.0 30.0Ave Carbon tetrachloride 0.43110.3970 10.9 10.0 8.6 30.0Ave FORM VII TO-15 Page 352 of 478 FORM VII Lab Name:Job No.: SDG No.: Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID: Calib End Date:GC Column: ID: AIR - GC/MS VOA CONTINUING CALIBRATION DATA 0.32(mm) 200-41113-1 200-41113-1 CHB.i 11/07/2017 12:25 11/06/2017 17:59 11/07/2017 01:49 ICV 200-122990/24 RTX-624 TestAmerica Burlington Lab File ID:27754-24.D Heated Purge: (Y/N)NConc. Units:ppb v/v ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNT AMOUNT %D AVE RRF RRF MIN RRF 2,2,4-Trimethylpentane 1.2401.192 10.4 10.0 4.0 30.0Ave Benzene 0.73790.7354 10.0 10.0 0.3 30.0Ave 1,2-Dichloroethane 0.26740.2620 10.2 10.0 2.1 30.0Ave n-Heptane 0.45430.4559 9.96 10.0 -0.4 30.0Ave n-Butanol 0.15420.1423 10.8 10.0 8.4 30.0Ave Trichloroethene 0.31110.2935 10.6 10.0 6.0 30.0Ave 1,2-Dichloropropane 0.29790.2830 10.5 10.0 5.2 30.0Ave Methyl methacrylate 0.27590.2636 10.5 10.0 4.7 30.0Ave 1,4-Dioxane 0.15300.1397 10.9 10.0 9.5 30.0Ave Dibromomethane 0.30090.2919 10.3 10.0 3.1 30.0Ave Bromodichloromethane 0.50550.4943 10.2 10.0 2.3 30.0Ave cis-1,3-Dichloropropene 0.41970.3995 10.5 10.0 5.1 30.0Ave methyl isobutyl ketone 0.57840.5596 10.3 10.0 3.4 30.0Ave n-Octane 0.65440.6425 10.2 10.0 1.9 30.0Ave Toluene 0.60480.5976 10.1 10.0 1.2 30.0Ave trans-1,3-Dichloropropene 0.40620.3818 10.6 10.0 6.4 30.0Ave 1,1,2-Trichloroethane 0.30390.2946 10.3 10.0 3.1 30.0Ave Tetrachloroethene 0.49350.4735 10.4 10.0 4.2 30.0Ave Methyl Butyl Ketone (2-Hexanone) 0.61370.5965 10.3 10.0 2.9 30.0Ave Dibromochloromethane 0.58160.5620 10.3 10.0 3.5 30.0Ave 1,2-Dibromoethane 0.54750.5221 10.5 10.0 4.9 30.0Ave Chlorobenzene 0.82180.7969 10.3 10.0 3.1 30.0Ave Ethylbenzene 1.3391.309 10.2 10.0 2.3 30.0Ave n-Nonane 0.69220.6705 10.3 10.0 3.2 30.0Ave m,p-Xylene 0.53460.5157 20.7 20.0 3.6 30.0Ave Xylene, o-0.53030.5131 10.3 10.0 3.4 30.0Ave Styrene 0.82410.7731 10.7 10.0 6.6 30.0Ave Bromoform 0.52710.5185 10.2 10.0 1.7 30.0Ave Cumene 1.5081.450 10.4 10.0 3.9 30.0Ave 1,1,2,2-Tetrachloroethane 0.83110.7887 10.5 10.0 5.4 30.0Ave n-Propylbenzene 1.8781.787 10.5 10.0 5.1 30.0Ave 1,2,3-Trichloropropane 0.62600.6030 10.4 10.0 3.8 30.0Ave n-Decane 0.90650.8496 10.7 10.0 6.7 30.0Ave 4-Ethyltoluene 1.5041.422 10.6 10.0 5.8 30.0Ave 2-Chlorotoluene 1.2341.184 10.4 10.0 4.3 30.0Ave 1,3,5-Trimethylbenzene 1.2491.176 10.6 10.0 6.3 30.0Ave Alpha Methyl Styrene 0.63910.5757 11.1 10.0 11.0 30.0Ave tert-Butylbenzene 1.2101.137 10.6 10.0 6.4 30.0Ave 1,2,4-Trimethylbenzene 1.2491.161 10.7 10.0 7.5 30.0Ave sec-Butylbenzene 1.8891.765 10.7 10.0 7.0 30.0Ave FORM VII TO-15 Page 353 of 478 FORM VII Lab Name:Job No.: SDG No.: Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID: Calib End Date:GC Column: ID: AIR - GC/MS VOA CONTINUING CALIBRATION DATA 0.32(mm) 200-41113-1 200-41113-1 CHB.i 11/07/2017 12:25 11/06/2017 17:59 11/07/2017 01:49 ICV 200-122990/24 RTX-624 TestAmerica Burlington Lab File ID:27754-24.D Heated Purge: (Y/N)NConc. Units:ppb v/v ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNT AMOUNT %D AVE RRF RRF MIN RRF 4-Isopropyltoluene 1.5681.451 10.8 10.0 8.1 30.0Ave 1,3-Dichlorobenzene 0.84390.7721 10.9 10.0 9.3 30.0Ave 1,4-Dichlorobenzene 0.83270.7549 11.0 10.0 10.3 30.0Ave Benzyl chloride 0.9950.8629 11.5 10.0 15.3 30.0Ave n-Undecane 0.95520.9240 10.3 10.0 3.4 30.0Ave n-Butylbenzene 1.4351.332 10.8 10.0 7.7 30.0Ave 1,2-Dichlorobenzene 0.78460.7259 10.8 10.0 8.1 30.0Ave n-Dodecane 0.78090.7144 10.9 10.0 9.3 30.0Ave 1,2,4-Trichlorobenzene 0.43500.4507 9.65 10.0 -3.5 30.0Ave Hexachlorobutadiene 0.45700.4744 9.63 10.0 -3.7 30.0Ave Naphthalene 0.89150.9521 9.36 10.0 -6.4 30.0Ave 1,2,3-Trichlorobenzene 0.38180.3907 9.77 10.0 -2.3 30.0Ave FORM VII TO-15 Page 354 of 478 Report Date: 07-Nov-2017 13:40:38 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Target Compound Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-24.D Lims ID: icv Client ID: Sample Type: ICV Inject. Date: 07-Nov-2017 12:25:30 ALS Bottle#: 24 Worklist Smp#: 24 Purge Vol:200.000 mL Dil. Factor: 1.0000 Sample Info: 200-0027754-024 Operator ID: vtp Instrument ID: CHB.i Sublist: Method:\\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\TO15_LLNJ_TO3.m Limit Group: AI_TO15_ICAL Last Update: 07-Nov-2017 13:40:02 Calib Date: 07-Nov-2017 01:49:30 Integrator: RTE ID Type: Deconvolution ID Quant Method: Internal/External Standard Quant By: Initial Calibration Last ICal File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-13.D Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host:XAWRK022 First Level Reviewer: daiglep Date:07-Nov-2017 13:31:22 Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 1 Propene 41 3.134 3.135 -0.001 98 181047 10.0 10.0 2 Dichlorodifluoromethane 85 3.193 3.193 0.000 99 700839 10.0 10.2 3 Chlorodifluoromethane 51 3.225 3.225 0.000 97 389211 10.0 9.92 4 1,2-Dichloro-1,1,2,2-tetra 85 3.412 3.412 0.000 97 743392 10.0 10.3 5 Chloromethane 50 3.535 3.535 0.000 99 248889 10.0 10.1 6 Butane 43 3.711 3.711 0.000 99 415119 10.0 9.77 7 Vinyl chloride 62 3.748 3.748 0.000 98 313654 10.0 10.6 8 Butadiene 54 3.812 3.812 0.000 96 229374 10.0 10.6 10 Bromomethane 94 4.479 4.479 0.000 99 322525 10.0 10.6 9 BFB 11 Chloroethane 64 4.709 4.709 0.000 99 189727 10.0 10.3 12 2-Methylbutane 43 4.789 4.789 0.000 94 379181 10.0 9.82 13 Vinyl bromide 106 5.114 5.120 -0.006 100 333420 10.0 10.7 14 Trichlorofluoromethane 101 5.221 5.216 0.005 98 750915 10.0 10.2 15 Pentane 43 5.355 5.355 0.000 96 586259 10.0 9.98 16 Ethanol 45 5.680 5.675 0.005 98 240606 15.0 14.9 17 Ethyl ether 59 5.830 5.830 0.000 94 236123 10.0 10.4 18 Acrolein 56 6.198 6.198 0.000 95 106775 10.0 10.2 19 1,1,2-Trichloro-1,2,2-trif 101 6.246 6.246 0.000 98 638129 10.0 10.3 20 1,1-Dichloroethene 96 6.321 6.321 0.000 98 316913 10.0 10.2 21 Acetone 43 6.470 6.470 0.000 96 469731 10.0 10.2 22 Isopropyl alcohol 45 6.689 6.684 0.005 99 557218 10.0 10.7 23 Carbon disulfide 76 6.748 6.748 0.000 99 906656 10.0 10.4 24 3-Chloro-1-propene 41 7.020 7.020 0.000 93 436296 10.0 10.1 26 Acetonitrile 41 7.078 7.079 -0.001 100 273193 10.0 10.2 27 Methylene Chloride 49 7.276 7.276 0.000 94 379401 10.0 10.2 28 2-Methyl-2-propanol 59 7.388 7.388 0.000 93 724780 10.0 10.7 29 Methyl tert-butyl ether 73 7.628 7.628 0.000 98 945886 10.0 10.3 30 trans-1,2-Dichloroethene 61 7.687 7.687 0.000 99 485306 10.0 10.3 31 Acrylonitrile 53 7.756 7.756 0.000 96 261132 10.0 10.5 32 Hexane 57 8.018 8.018 0.000 93 551026 10.0 9.75 Page 355 of 478 Report Date: 07-Nov-2017 13:40:38 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-24.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 33 1,1-Dichloroethane 63 8.429 8.429 0.000 99 639073 10.0 10.2 34 Vinyl acetate 43 8.434 8.434 0.000 100 882685 10.0 10.2 36 2-Butanone (MEK) 72 9.320 9.320 0.000 99 184699 10.0 10.1 37 cis-1,2-Dichloroethene 96 9.336 9.331 0.005 95 376144 10.0 10.5 35 Ethyl acetate 88 9.331 9.336 -0.005 94 30666 10.0 10.2 * 39 Chlorobromomethane 128 9.704 9.704 0.000 95 311386 10.0 10.0 38 Tetrahydrofuran 42 9.715 9.710 0.005 95 424194 10.0 10.3 40 Chloroform 83 9.779 9.774 0.005 95 683454 10.0 10.2 S 41 1,2-Dichloroethene, Total 61 0 20.0 20.8 42 1,1,1-Trichloroethane 97 10.035 10.035 0.000 95 656205 10.0 10.2 43 Cyclohexane 84 10.046 10.046 0.000 98 503835 10.0 10.4 44 Carbon tetrachloride 117 10.243 10.243 0.000 98 663149 10.0 10.9 45 Isooctane 57 10.526 10.521 0.005 100 1907182 10.0 10.4 46 Benzene 78 10.563 10.564 -0.001 95 1135183 10.0 10.0 47 1,2-Dichloroethane 62 10.665 10.665 0.000 96 411406 10.0 10.2 48 n-Heptane 43 10.777 10.777 0.000 91 698841 10.0 9.96 A 49 GRO 1 10.865 (4.779-16.951) 0 147809696 10.0 0 * 50 1,4-Difluorobenzene 114 11.108 11.108 0.000 94 1538738 10.0 10.0 51 n-Butanol 56 11.289 11.289 0.000 87 237289 10.0 10.8 53 Trichloroethene 95 11.476 11.476 0.000 98 478655 10.0 10.6 54 1,2-Dichloropropane 63 11.844 11.844 0.000 95 458255 10.0 10.5 55 Methyl methacrylate 69 11.882 11.882 0.000 97 424511 10.0 10.5 56 1,4-Dioxane 88 11.972 11.967 0.005 93 235313 10.0 10.9 57 Dibromomethane 174 12.031 12.031 0.000 97 462897 10.0 10.3 58 Dichlorobromomethane 83 12.207 12.202 0.005 98 777693 10.0 10.2 A 59 TVOC as Toluene 1 12.485 (3.125-21.845) 0 240152968 10.0 0 60 cis-1,3-Dichloropropene 75 12.832 12.832 0.000 90 645617 10.0 10.5 61 4-Methyl-2-pentanone (MIBK 43 12.976 12.976 0.000 96 889767 10.0 10.3 63 n-Octane 43 13.248 13.248 0.000 92 1006767 10.0 10.2 64 Toluene 92 13.264 13.264 0.000 93 842860 10.0 10.1 66 trans-1,3-Dichloropropene 75 13.621 13.622 -0.001 95 624877 10.0 10.6 67 1,1,2-Trichloroethane 83 13.894 13.894 0.000 95 423500 10.0 10.3 68 Tetrachloroethene 166 14.038 14.038 0.000 98 687718 10.0 10.4 69 2-Hexanone 43 14.150 14.155 -0.005 95 855318 10.0 10.3 70 Chlorodibromomethane 129 14.449 14.449 0.000 98 810571 10.0 10.3 71 Ethylene Dibromide 107 14.651 14.652 -0.001 98 762974 10.0 10.5 * 72 Chlorobenzene-d5 117 15.217 15.212 0.005 84 1393921 10.0 10.0 73 Chlorobenzene 112 15.255 15.255 0.000 96 1145351 10.0 10.3 74 Ethylbenzene 91 15.319 15.319 0.000 98 1865765 10.0 10.2 75 n-Nonane 57 15.340 15.340 0.000 91 964664 10.0 10.3 76 m-Xylene & p-Xylene 106 15.468 15.468 0.000 0 1489987 20.0 20.7 78 o-Xylene 106 15.980 15.981 -0.001 99 739093 10.0 10.3 S 77 Xylenes, Total 106 0 30.0 31.1 79 Styrene 104 16.002 16.002 0.000 98 1148492 10.0 10.7 80 Bromoform 173 16.295 16.295 0.000 98 734520 10.0 10.2 81 Isopropylbenzene 105 16.391 16.391 0.000 95 2100933 10.0 10.4 83 1,1,2,2-Tetrachloroethane 83 16.797 16.797 0.000 97 1158207 10.0 10.5 84 N-Propylbenzene 91 16.872 16.872 0.000 99 2617083 10.0 10.5 85 1,2,3-Trichloropropane 75 16.882 16.882 0.000 97 872384 10.0 10.4 86 n-Decane 57 16.936 16.941 -0.005 89 1263341 10.0 10.7 87 4-Ethyltoluene 105 16.994 16.995 -0.001 98 2096446 10.0 10.6 88 2-Chlorotoluene 91 17.037 17.037 0.000 96 1719854 10.0 10.4 Page 356 of 478 Report Date: 07-Nov-2017 13:40:38 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-24.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 89 1,3,5-Trimethylbenzene 105 17.064 17.064 0.000 93 1741357 10.0 10.6 90 Alpha Methyl Styrene 118 17.336 17.336 0.000 90 890655 10.0 11.1 91 tert-Butylbenzene 119 17.437 17.437 0.000 96 1686362 10.0 10.6 92 1,2,4-Trimethylbenzene 105 17.507 17.507 0.000 97 1740342 10.0 10.7 93 sec-Butylbenzene 105 17.694 17.694 0.000 99 2633043 10.0 10.7 94 4-Isopropyltoluene 119 17.848 17.848 0.000 98 2185801 10.0 10.8 95 1,3-Dichlorobenzene 146 17.923 17.928 -0.005 97 1176103 10.0 10.9 96 1,4-Dichlorobenzene 146 18.035 18.035 0.000 96 1160442 10.0 11.0 97 Benzyl chloride 91 18.185 18.185 -0.001 99 1386864 10.0 11.5 98 Undecane 57 18.318 18.318 0.000 96 1331224 10.0 10.3 99 n-Butylbenzene 91 18.355 18.355 0.000 98 1999979 10.0 10.8 100 1,2-Dichlorobenzene 146 18.521 18.521 0.000 97 1093389 10.0 10.8 102 Dodecane 57 19.770 19.770 0.000 97 1088353 10.0 10.9 103 1,2,4-Trichlorobenzene 180 20.885 20.885 0.000 94 606261 10.0 9.65 104 Hexachlorobutadiene 225 21.050 21.051 -0.001 98 636865 10.0 9.63 105 Naphthalene 128 21.365 21.360 0.005 100 1242371 10.0 9.36 106 1,2,3-Trichlorobenzene 180 21.840 21.835 0.005 95 532115 10.0 9.77 Reagents: ATTO15BISs_00006 Amount Added: 20.00 Units: mL Run Reagent ATTO15LCSW_00712 Amount Added: 200.00 Units: mL Page 357 of 478 Report Date: 07-Nov-2017 13:40:38 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-24.D Injection Date: 07-Nov-2017 12:25:30 Instrument ID: CHB.i Operator ID: vtp Lims ID: icv Worklist Smp#: 24 Client ID: Purge Vol: 200.000 mL Dil. Factor: 1.0000 ALS Bottle#: 24 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Y Scaling: Method Defined: Scale to the Nth Largest Target: 1 2.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 18.0 20.0 22.0 24.0 Min 0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 Y ( X 10 0 0 0 0 ) 27754-24[MS SCAN Chro]:Total * C h l o r o b r o m o m e t h a n e ( 9 . 7 0 4 )+ * 1 ,4- D i f lu o r o b e n z en e ( 1 1 . 1 0 8 ) * C h l o r o b e n z en e - d 5 ( 1 5 . 2 1 7 ) Page 358 of 478 FORM VII Lab Name:Job No.: SDG No.: Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID: Calib End Date:GC Column: ID: AIR - GC/MS VOA CONTINUING CALIBRATION DATA 0.32(mm) 200-41113-1 200-41113-1 CHB.i 11/24/2017 10:33 11/06/2017 17:59 11/07/2017 01:49 CCVIS 200-123710/2 RTX-624 TestAmerica Burlington Lab File ID:28034-02.D Heated Purge: (Y/N)NConc. Units:ppb v/v ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNT AMOUNT %D AVE RRF RRF MIN RRF Propylene 0.52170.5800 8.99 10.0 -10.1 30.0Ave Dichlorodifluoromethane 1.9612.215 8.85 10.0 -11.4 30.0Ave Freon 22 1.0901.259 8.65 10.0 -13.5 30.0Ave 1,2-Dichlorotetrafluoroethan e 2.1592.326 9.28 10.0 -7.2 30.0Ave Chloromethane 0.70780.7900 8.96 10.0 -10.4 30.0Ave n-Butane 1.1681.365 8.56 10.0 -14.4 30.0Ave Vinyl chloride 0.90500.9520 9.50 10.0 -4.9 30.0Ave 1,3-Butadiene 0.66190.6974 9.49 10.0 -5.1 30.0Ave Bromomethane 0.96970.9801 9.89 10.0 -1.1 30.0Ave Chloroethane 0.56730.5888 9.63 10.0 -3.7 30.0Ave Isopentane 1.0851.241 8.74 10.0 -12.6 30.0Ave Bromoethene(Vinyl Bromide)1.0230.999 10.2 10.0 2.4 30.0Ave Trichlorofluoromethane 2.1292.364 9.01 10.0 -9.9 30.0Ave n-Pentane 1.6821.886 8.92 10.0 -10.8 30.0Ave Ethanol 0.44190.5169 12.8 15.0 -14.5 30.0Ave Ethyl ether 0.70230.7268 9.66 10.0 -3.4 30.0Ave Acrolein 0.33210.3358 9.89 10.0 -1.1 30.0Ave Freon TF 1.8991.986 9.56 10.0 -4.4 30.0Ave 1,1-Dichloroethene 0.95830.9944 9.63 10.0 -3.6 30.0Ave Acetone 1.3091.485 8.81 10.0 -11.9 30.0Ave Isopropyl alcohol 1.5301.668 9.17 10.0 -8.3 30.0Ave Carbon disulfide 2.6902.787 9.65 10.0 -3.5 30.0Ave 3-Chloropropene 1.2031.388 8.67 10.0 -13.3 30.0Ave Acetonitrile 0.73330.8571 8.55 10.0 -14.4 30.0Ave Methylene Chloride 1.0651.191 8.94 10.0 -10.6 30.0Ave tert-Butyl alcohol 2.0242.175 9.30 10.0 -7.0 30.0Ave Methyl tert-butyl ether 2.7582.963 9.31 10.0 -6.9 30.0Ave trans-1,2-Dichloroethene 1.4021.509 9.29 10.0 -7.1 30.0Ave Acrylonitrile 0.73970.7960 9.29 10.0 -7.1 30.0Ave n-Hexane 1.6051.815 8.84 10.0 -11.6 30.0Ave 1,1-Dichloroethane 1.8252.017 9.05 10.0 -9.5 30.0Ave Vinyl acetate 2.4452.777 8.80 10.0 -12.0 30.0Ave Methyl Ethyl Ketone 0.55020.5853 9.40 10.0 -6.0 30.0Ave cis-1,2-Dichloroethene 1.1161.149 9.71 10.0 -2.9 30.0Ave Ethyl acetate 0.09170.0966 9.49 10.0 -5.1 30.0Ave Tetrahydrofuran 0.23600.2669 8.84 10.0 -11.6 30.0Ave Chloroform 1.9402.155 9.00 10.0 -10.0 30.0Ave 1,1,1-Trichloroethane 0.37330.4188 8.91 10.0 -10.9 30.0Ave Cyclohexane 0.30290.3149 9.62 10.0 -3.8 30.0Ave Carbon tetrachloride 0.37340.3970 9.40 10.0 -5.9 30.0Ave FORM VII TO-15 Page 359 of 478 FORM VII Lab Name:Job No.: SDG No.: Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID: Calib End Date:GC Column: ID: AIR - GC/MS VOA CONTINUING CALIBRATION DATA 0.32(mm) 200-41113-1 200-41113-1 CHB.i 11/24/2017 10:33 11/06/2017 17:59 11/07/2017 01:49 CCVIS 200-123710/2 RTX-624 TestAmerica Burlington Lab File ID:28034-02.D Heated Purge: (Y/N)NConc. Units:ppb v/v ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNT AMOUNT %D AVE RRF RRF MIN RRF 2,2,4-Trimethylpentane 1.1101.192 9.31 10.0 -6.9 30.0Ave Benzene 0.67920.7354 9.23 10.0 -7.6 30.0Ave 1,2-Dichloroethane 0.22180.2620 8.47 10.0 -15.3 30.0Ave n-Heptane 0.39200.4559 8.60 10.0 -14.0 30.0Ave n-Butanol 0.12970.1423 9.11 10.0 -8.9 30.0Ave Trichloroethene 0.28080.2935 9.56 10.0 -4.3 30.0Ave 1,2-Dichloropropane 0.26360.2830 9.31 10.0 -6.9 30.0Ave Methyl methacrylate 0.24980.2636 9.47 10.0 -5.2 30.0Ave 1,4-Dioxane 0.13130.1397 9.40 10.0 -6.0 30.0Ave Dibromomethane 0.27080.2919 9.27 10.0 -7.2 30.0Ave Bromodichloromethane 0.43930.4943 8.89 10.0 -11.1 30.0Ave cis-1,3-Dichloropropene 0.37300.3995 9.33 10.0 -6.6 30.0Ave methyl isobutyl ketone 0.48800.5596 8.72 10.0 -12.8 30.0Ave n-Octane 0.55250.6425 8.60 10.0 -14.0 30.0Ave Toluene 0.55710.5976 9.32 10.0 -6.8 30.0Ave trans-1,3-Dichloropropene 0.35140.3818 9.20 10.0 -8.0 30.0Ave 1,1,2-Trichloroethane 0.27750.2946 9.42 10.0 -5.8 30.0Ave Tetrachloroethene 0.45200.4735 9.54 10.0 -4.5 30.0Ave Methyl Butyl Ketone (2-Hexanone) 0.52410.5965 8.78 10.0 -12.1 30.0Ave Dibromochloromethane 0.52730.5620 9.38 10.0 -6.2 30.0Ave 1,2-Dibromoethane 0.49660.5221 9.51 10.0 -4.9 30.0Ave Chlorobenzene 0.75230.7969 9.44 10.0 -5.6 30.0Ave Ethylbenzene 1.2161.309 9.28 10.0 -7.1 30.0Ave n-Nonane 0.61570.6705 9.18 10.0 -8.2 30.0Ave m,p-Xylene 0.48920.5157 19.0 20.0 -5.1 30.0Ave Xylene, o-0.48000.5131 9.35 10.0 -6.4 30.0Ave Styrene 0.74860.7731 9.68 10.0 -3.2 30.0Ave Bromoform 0.50010.5185 9.64 10.0 -3.5 30.0Ave Cumene 1.3501.450 9.31 10.0 -6.9 30.0Ave 1,1,2,2-Tetrachloroethane 0.73800.7887 9.36 10.0 -6.4 30.0Ave n-Propylbenzene 1.6751.787 9.37 10.0 -6.3 30.0Ave 1,2,3-Trichloropropane 0.54750.6030 9.08 10.0 -9.2 30.0Ave n-Decane 0.78750.8496 9.27 10.0 -7.3 30.0Ave 4-Ethyltoluene 1.3441.422 9.45 10.0 -5.5 30.0Ave 2-Chlorotoluene 1.0881.184 9.19 10.0 -8.1 30.0Ave 1,3,5-Trimethylbenzene 1.1011.176 9.36 10.0 -6.4 30.0Ave Alpha Methyl Styrene 0.56220.5757 9.76 10.0 -2.3 30.0Ave tert-Butylbenzene 1.0581.137 9.30 10.0 -7.0 30.0Ave 1,2,4-Trimethylbenzene 1.0901.161 9.38 10.0 -6.2 30.0Ave sec-Butylbenzene 1.6481.765 9.33 10.0 -6.6 30.0Ave FORM VII TO-15 Page 360 of 478 FORM VII Lab Name:Job No.: SDG No.: Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID: Calib End Date:GC Column: ID: AIR - GC/MS VOA CONTINUING CALIBRATION DATA 0.32(mm) 200-41113-1 200-41113-1 CHB.i 11/24/2017 10:33 11/06/2017 17:59 11/07/2017 01:49 CCVIS 200-123710/2 RTX-624 TestAmerica Burlington Lab File ID:28034-02.D Heated Purge: (Y/N)NConc. Units:ppb v/v ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNT AMOUNT %D AVE RRF RRF MIN RRF 4-Isopropyltoluene 1.3511.451 9.31 10.0 -6.9 30.0Ave 1,3-Dichlorobenzene 0.73470.7721 9.51 10.0 -4.8 30.0Ave 1,4-Dichlorobenzene 0.72730.7549 9.63 10.0 -3.7 30.0Ave Benzyl chloride 0.83780.8629 9.71 10.0 -2.9 30.0Ave n-Undecane 0.79110.9240 8.56 10.0 -14.4 30.0Ave n-Butylbenzene 1.2121.332 9.09 10.0 -9.1 30.0Ave 1,2-Dichlorobenzene 0.68070.7259 9.38 10.0 -6.2 30.0Ave n-Dodecane 0.65550.7144 9.17 10.0 -8.2 30.0Ave 1,2,4-Trichlorobenzene 0.37760.4507 8.38 10.0 -16.2 30.0Ave Hexachlorobutadiene 0.40260.4744 8.48 10.0 -15.1 30.0Ave Naphthalene 0.73380.9521 7.71 10.0 -22.9 30.0Ave 1,2,3-Trichlorobenzene 0.32880.3907 8.41 10.0 -15.8 30.0Ave FORM VII TO-15 Page 361 of 478 Report Date: 28-Nov-2017 09:01:08 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Target Compound Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-02.D Lims ID: ccvis Client ID: Sample Type: CCVIS Inject. Date: 24-Nov-2017 10:33:30 ALS Bottle#: 2 Worklist Smp#: 2 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Sample Info: 200-0028034-002 Operator ID: VTP Instrument ID: CHB.i Sublist:chrom-TO15_LLNJ_TO3*sub5 Method:\\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\TO15_LLNJ_TO3.m Limit Group: AI_TO15_ICAL Last Update: 28-Nov-2017 09:01:07 Calib Date: 07-Nov-2017 01:49:30 Integrator: RTE ID Type: Deconvolution ID Quant Method: Internal/External Standard Quant By: Initial Calibration Last ICal File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-13.D Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host:XAWRK022 First Level Reviewer: puangmaleek Date:28-Nov-2017 09:01:07 Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 1 Propene 41 3.134 3.134 0.000 98 217619 10.0 8.99 2 Dichlorodifluoromethane 85 3.193 3.193 0.000 99 818182 10.0 8.85 3 Chlorodifluoromethane 51 3.225 3.225 0.000 97 454638 10.0 8.65 4 1,2-Dichloro-1,1,2,2-tetra 85 3.412 3.412 0.000 88 900550 10.0 9.28 5 Chloromethane 50 3.535 3.535 0.000 99 295281 10.0 8.96 6 Butane 43 3.711 3.711 0.000 99 487463 10.0 8.56 7 Vinyl chloride 62 3.748 3.748 0.000 98 377534 10.0 9.50 8 Butadiene 54 3.812 3.812 0.000 95 276116 10.0 9.49 10 Bromomethane 94 4.479 4.479 0.000 100 404537 10.0 9.89 9 BFB 11 Chloroethane 64 4.709 4.709 0.000 99 236675 10.0 9.63 12 2-Methylbutane 43 4.789 4.789 0.000 94 452442 10.0 8.74 13 Vinyl bromide 106 5.120 5.120 0.000 100 426801 10.0 10.2 14 Trichlorofluoromethane 101 5.216 5.216 0.000 98 888343 10.0 9.01 15 Pentane 43 5.355 5.355 0.000 96 701667 10.0 8.92 16 Ethanol 45 5.669 5.669 0.000 98 276638 15.0 12.8 17 Ethyl ether 59 5.824 5.824 0.000 95 292987 10.0 9.66 18 Acrolein 56 6.198 6.198 0.000 94 138525 10.0 9.89 19 1,1,2-Trichloro-1,2,2-trif 101 6.246 6.246 0.000 98 792090 10.0 9.56 20 1,1-Dichloroethene 96 6.315 6.315 0.000 96 399780 10.0 9.63 21 Acetone 43 6.465 6.465 0.000 95 545969 10.0 8.81 22 Isopropyl alcohol 45 6.683 6.683 0.000 99 638472 10.0 9.17 23 Carbon disulfide 76 6.748 6.748 0.000 98 1122202 10.0 9.65 24 3-Chloro-1-propene 41 7.014 7.014 0.000 93 501714 10.0 8.67 26 Acetonitrile 41 7.073 7.073 0.000 100 305929 10.0 8.55 27 Methylene Chloride 49 7.276 7.276 0.000 92 444440 10.0 8.94 28 2-Methyl-2-propanol 59 7.383 7.383 0.000 92 844235 10.0 9.30 29 Methyl tert-butyl ether 73 7.623 7.623 0.000 97 1150762 10.0 9.31 30 trans-1,2-Dichloroethene 61 7.687 7.687 0.000 98 584785 10.0 9.29 31 Acrylonitrile 53 7.751 7.751 0.000 96 308587 10.0 9.29 32 Hexane 57 8.012 8.012 0.000 91 669483 10.0 8.84 Page 362 of 478 Report Date: 28-Nov-2017 09:01:08 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-02.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 33 1,1-Dichloroethane 63 8.423 8.423 0.000 99 761361 10.0 9.05 34 Vinyl acetate 43 8.429 8.429 0.000 100 1019935 10.0 8.80 36 2-Butanone (MEK) 72 9.315 9.315 0.000 98 229522 10.0 9.40 37 cis-1,2-Dichloroethene 96 9.331 9.331 0.000 95 465569 10.0 9.71 35 Ethyl acetate 88 9.331 9.331 0.000 94 38269 10.0 9.49 * 39 Chlorobromomethane 128 9.699 9.699 0.000 92 417259 10.0 10.0 38 Tetrahydrofuran 42 9.710 9.710 0.000 94 487030 10.0 8.84 40 Chloroform 83 9.774 9.774 0.000 95 809468 10.0 9.00 S 41 1,2-Dichloroethene, Total 61 0 20.0 19.0 42 1,1,1-Trichloroethane 97 10.030 10.030 0.000 95 770232 10.0 8.91 43 Cyclohexane 84 10.046 10.046 0.000 97 625055 10.0 9.62 44 Carbon tetrachloride 117 10.238 10.238 0.000 97 770506 10.0 9.40 45 Isooctane 57 10.521 10.521 0.000 100 2290586 10.0 9.31 46 Benzene 78 10.563 10.563 0.000 94 1401445 10.0 9.23 47 1,2-Dichloroethane 62 10.659 10.659 0.000 95 457670 10.0 8.47 48 n-Heptane 43 10.772 10.772 0.000 90 808924 10.0 8.60 A 49 GRO 1 10.862 (4.779-16.946) 0 172462754 10.0 0 * 50 1,4-Difluorobenzene 114 11.102 11.102 0.000 93 2063825 10.0 10.0 51 n-Butanol 56 11.284 11.284 0.000 85 267532 10.0 9.11 53 Trichloroethene 95 11.476 11.476 0.000 97 579391 10.0 9.56 54 1,2-Dichloropropane 63 11.839 11.839 0.000 94 543815 10.0 9.31 55 Methyl methacrylate 69 11.876 11.876 0.000 98 515362 10.0 9.47 56 1,4-Dioxane 88 11.967 11.967 0.000 93 270913 10.0 9.40 57 Dibromomethane 174 12.031 12.031 0.000 96 558730 10.0 9.27 58 Dichlorobromomethane 83 12.202 12.202 0.000 97 906515 10.0 8.89 A 59 TVOC as Toluene 1 12.485 (3.124-21.845) 0 274916572 10.0 0 60 cis-1,3-Dichloropropene 75 12.826 12.826 0.000 89 769550 10.0 9.33 61 4-Methyl-2-pentanone (MIBK 43 12.976 12.976 0.000 94 1006892 10.0 8.72 63 n-Octane 43 13.243 13.243 0.000 90 1140099 10.0 8.60 64 Toluene 92 13.259 13.259 0.000 93 1015268 10.0 9.32 66 trans-1,3-Dichloropropene 75 13.621 13.621 0.000 95 725070 10.0 9.20 67 1,1,2-Trichloroethane 83 13.888 13.888 0.000 94 505620 10.0 9.42 68 Tetrachloroethene 166 14.032 14.032 0.000 97 823613 10.0 9.54 69 2-Hexanone 43 14.150 14.150 0.000 96 955115 10.0 8.78 70 Chlorodibromomethane 129 14.449 14.449 0.000 98 960842 10.0 9.38 71 Ethylene Dibromide 107 14.646 14.646 0.000 98 905054 10.0 9.51 * 72 Chlorobenzene-d5 117 15.212 15.212 0.000 84 1822725 10.0 10.0 73 Chlorobenzene 112 15.249 15.249 0.000 96 1370878 10.0 9.44 74 Ethylbenzene 91 15.319 15.319 0.000 97 2215626 10.0 9.28 75 n-Nonane 57 15.340 15.340 0.000 92 1122013 10.0 9.18 76 m-Xylene & p-Xylene 106 15.468 15.468 0.000 0 1783135 20.0 19.0 78 o-Xylene 106 15.975 15.975 0.000 99 874786 10.0 9.35 S 77 Xylenes, Total 106 0 30.0 28.3 79 Styrene 104 16.002 16.002 0.000 97 1364308 10.0 9.68 80 Bromoform 173 16.295 16.295 0.000 98 911421 10.0 9.64 81 Isopropylbenzene 105 16.391 16.391 0.000 95 2460708 10.0 9.31 83 1,1,2,2-Tetrachloroethane 83 16.797 16.797 0.000 97 1344899 10.0 9.36 84 N-Propylbenzene 91 16.866 16.866 0.000 100 3052363 10.0 9.37 85 1,2,3-Trichloropropane 75 16.877 16.877 0.000 98 997650 10.0 9.08 86 n-Decane 57 16.936 16.936 0.000 89 1435082 10.0 9.27 87 4-Ethyltoluene 105 16.994 16.994 0.000 98 2448395 10.0 9.45 88 2-Chlorotoluene 91 17.037 17.037 0.000 96 1982591 10.0 9.19 Page 363 of 478 Report Date: 28-Nov-2017 09:01:08 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-02.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 89 1,3,5-Trimethylbenzene 105 17.058 17.058 0.000 94 2005805 10.0 9.36 90 Alpha Methyl Styrene 118 17.331 17.331 0.000 91 1024571 10.0 9.76 91 tert-Butylbenzene 119 17.437 17.437 0.000 96 1927181 10.0 9.30 92 1,2,4-Trimethylbenzene 105 17.507 17.507 0.000 96 1985613 10.0 9.38 93 sec-Butylbenzene 105 17.694 17.694 0.000 99 3003213 10.0 9.33 94 4-Isopropyltoluene 119 17.843 17.843 0.000 98 2462193 10.0 9.31 95 1,3-Dichlorobenzene 146 17.923 17.923 0.000 96 1338857 10.0 9.51 96 1,4-Dichlorobenzene 146 18.035 18.035 0.000 96 1325341 10.0 9.63 97 Benzyl chloride 91 18.185 18.185 0.000 100 1526860 10.0 9.71 98 Undecane 57 18.318 18.318 0.000 95 1441640 10.0 8.56 99 n-Butylbenzene 91 18.350 18.350 0.000 98 2208197 10.0 9.09 100 1,2-Dichlorobenzene 146 18.521 18.521 0.000 97 1240430 10.0 9.38 102 Dodecane 57 19.770 19.770 0.000 97 1194550 10.0 9.17 103 1,2,4-Trichlorobenzene 180 20.880 20.880 0.000 90 688167 10.0 8.38 104 Hexachlorobutadiene 225 21.045 21.045 0.000 98 733590 10.0 8.48 105 Naphthalene 128 21.360 21.360 0.000 100 1337300 10.0 7.71 106 1,2,3-Trichlorobenzene 180 21.835 21.835 0.000 95 599212 10.0 8.41 Reagents: ATTO15CAL4w_00655 Amount Added: 200.00 Units: mL ATTO15BISs_00006 Amount Added: 20.00 Units: mL Run Reagent Page 364 of 478 Report Date: 28-Nov-2017 09:01:08 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-02.D Injection Date: 24-Nov-2017 10:33:30 Instrument ID: CHB.i Operator ID: VTP Lims ID: ccvis Worklist Smp#: 2 Client ID: Purge Vol: 200.000 mL Dil. Factor: 1.0000 ALS Bottle#: 2 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Y Scaling: Method Defined: Scale to the Nth Largest Target: 1 2.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 18.0 20.0 22.0 24.0 Min 0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 Y ( X 10 0 0 0 0 ) 28034-02[MS SCAN Chro]:Total * C h l o r o b r o m o m e t h a n e ( 9 . 6 9 9 )+ * 1 ,4- D i f lu o r o b e n z en e ( 1 1 . 1 0 2 ) * C h l o r o b e n z en e - d 5( 1 5 .2 1 2 )+ Page 365 of 478 Report Date: 07-Nov-2017 13:39:32 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Target Compound Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-01.D Lims ID: bfb Client ID: Sample Type: BFB Inject. Date: 06-Nov-2017 15:25:30 ALS Bottle#: 1 Worklist Smp#: 1 Injection Vol: 0.0 mL Dil. Factor: 1.0000 Sample Info: 200-0027754-001 Operator ID: vtp Instrument ID: CHB.i Method:\\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\TO15_LLNJ_TO3.m Limit Group: AI_TO15_ICAL Last Update: 07-Nov-2017 13:39:32 Calib Date: 07-Nov-2017 01:49:30 Integrator: RTE ID Type: Deconvolution ID Quant Method: Internal/External Standard Quant By: Initial Calibration Last ICal File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-13.D Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host:XAWRK022 First Level Reviewer: daiglep Date:07-Nov-2017 09:21:09 Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 9 BFB * 39 Chlorobromomethane 128 9.704 10.0 ND * 50 1,4-Difluorobenzene 114 11.108 10.0 ND * 72 Chlorobenzene-d5 117 15.212 10.0 ND Reagents: ATTO15BISs_00006 Amount Added: 20.00 Units: mL Run Reagent Page 366 of 478 Report Date: 07-Nov-2017 13:39:32 Chrom Revision: 2.2 28-Sep-2017 09:29:16 MS Tune Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-01.D Injection Date: 06-Nov-2017 15:25:30 Instrument ID: CHB.i Lims ID: bfb Client ID: Operator ID: vtp ALS Bottle#: 1 Worklist Smp#: 1 Injection Vol: 0.0 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Tune Method: BFB Method TO-15 9 BFB 30 50 70 90 110 130 150 170 190 210 230 250 m/z 0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 Y ( X 10 0 0 0 ) Tune Spec :Average 19-21( 5.68-5.69 ) Bgrd 8( 5.62) 95 174 176 75 50 74 94 96 17751 m/z Ion Abundance Criteria %Relative Abundance 95 Base Peak,100 Percent Relative Abundance 100.0 50 8.0 to 40.0 Percent of m/e 95 16.6 75 30.0 to 66.0 Percent of m/e 95 44.8 96 5.0 to 9.0 Percent of m/e 95 6.6 173 Less than 2.0 Percent of m/e 174 0.0 (0.0) 174 50.0 to 120.0 Percent of m/e 95 88.8 175 4.0 to 9.0 Percent of m/e 174 6.4 (7.2) 176 93.0 to 101.0 Percent of m/e 174 87.0 (98.0) 177 5.0 to 9.0 Percent of m/e 176 5.6 (6.4) Page 367 of 478 Report Date: 07-Nov-2017 13:39:32 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File:\\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-01.D\TO15_LLNJ_TO3.rslt\spectra.d Injection Date: 06-Nov-2017 15:25:30 Spectrum:Tune Spec :Average 19-21( 5.68-5.69 ) Bgrd 8( 5.62) Base Peak:95.00 Minimum % Base Peak: 0 Number of Points: 118 m/z Y m/z Y m/z Y m/z Y 36.00 1897 69.00 24832 107.00 278 147.00 264 37.00 10894 70.00 1972 111.00 161 148.00 632 38.00 9501 71.00 84 112.00 84 149.00 212 39.00 3822 72.00 1271 113.00 144 150.00 207 40.00 68 73.00 9893 115.00 306 152.00 137 41.00 59 74.00 40448 116.00 685 153.00 198 43.00 52 75.00 129448 117.00 1214 154.00 183 44.00 1026 76.00 11364 118.00 721 155.00 638 45.00 1968 77.00 2026 119.00 1035 156.00 156 46.00 175 78.00 972 120.00 13 157.00 432 47.00 4294 79.00 4591 123.00 77 158.00 52 48.00 1209 80.00 1431 124.00 59 159.00 151 49.00 9161 81.00 4782 125.00 53 161.00 345 50.00 47928 82.00 1023 126.00 153 163.00 47 51.00 14954 83.00 53 127.00 50 169.00 43 52.00 603 86.00 188 128.00 881 170.00 54 55.00 635 87.00 13209 129.00 461 171.00 97 56.00 3240 88.00 13034 130.00 1002 172.00 423 57.00 5914 90.00 36 131.00 408 174.00 256640 58.00 51 91.00 765 135.00 258 175.00 18416 59.00 90 92.00 6637 136.00 39 176.00 251456 60.00 2118 93.00 10403 137.00 284 177.00 16157 61.00 10673 94.00 29984 139.00 35 178.00 580 62.00 10425 95.00 289024 140.00 135 192.00 89 63.00 7610 96.00 19120 141.00 2015 195.00 88 64.00 891 97.00 572 142.00 229 205.00 48 65.00 131 103.00 161 143.00 2080 239.00 41 66.00 76 104.00 959 144.00 142 252.00 33 67.00 488 105.00 398 145.00 203 68.00 25544 106.00 849 146.00 332 Page 368 of 478 Report Date: 07-Nov-2017 13:39:32 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-01.D Injection Date: 06-Nov-2017 15:25:30 Instrument ID: CHB.i Operator ID: vtp Lims ID: bfb Worklist Smp#: 1 Client ID: Injection Vol: 0.0 mL Dil. Factor: 1.0000 ALS Bottle#: 1 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Y Scaling: Method Defined: Scale to the Nth Largest Target: 1 5.5 5.8 6.1 6.4 6.7 7.0 7.3 7.6 7.9 8.2 8.5 8.8 Min 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Y ( X 10 0 0 0 0 ) 27754-01[MS SCAN Chro]:Total Page 369 of 478 Report Date: 28-Nov-2017 08:59:56 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Target Compound Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-01.D Lims ID: bfb Client ID: Sample Type: BFB Inject. Date: 24-Nov-2017 09:42:30 ALS Bottle#: 1 Worklist Smp#: 1 Injection Vol: 0.0 mL Dil. Factor: 1.0000 Sample Info: 200-0028034-001 Operator ID:VTP Instrument ID: CHB.i Method:\\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\TO15_LLNJ_TO3.m Limit Group: AI_TO15_ICAL Last Update: 28-Nov-2017 08:59:55 Calib Date: 07-Nov-2017 01:49:30 Integrator: RTE ID Type: Deconvolution ID Quant Method: Internal/External Standard Quant By: Initial Calibration Last ICal File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-13.D Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host:XAWRK022 First Level Reviewer: puangmaleek Date:28-Nov-2017 08:59:55 Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 9 BFB * 39 Chlorobromomethane 128 9.699 10.0 ND * 50 1,4-Difluorobenzene 114 11.102 10.0 ND * 72 Chlorobenzene-d5 117 15.212 10.0 ND Reagents: ATTO15BISs_00006 Amount Added: 20.00 Units: mL Run Reagent Page 370 of 478 Report Date: 28-Nov-2017 08:59:56 Chrom Revision: 2.2 13-Nov-2017 17:19:06 MS Tune Report TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-01.D Injection Date: 24-Nov-2017 09:42:30 Instrument ID: CHB.i Lims ID: bfb Client ID: Operator ID: VTP ALS Bottle#: 1 Worklist Smp#: 1 Injection Vol: 0.0 mL Dil. Factor: 1.0000 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Tune Method: BFB Method TO-15 9 BFB 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 m/z 0 3 6 9 12 15 18 21 24 27 30 33 36 39 42 45 Y ( X 10 0 0 0 ) Tune Spec :Average 18-20( 5.68-5.69 ) Bgrd 8( 5.62) 95 174 176 75 50 74 94 96 177 m/z Ion Abundance Criteria %Relative Abundance 95 Base Peak,100 Percent Relative Abundance 100.0 50 8.0 to 40.0 Percent of m/e 95 14.1 75 30.0 to 66.0 Percent of m/e 95 40.8 96 5.0 to 9.0 Percent of m/e 95 6.6 173 Less than 2.0 Percent of m/e 174 0.0 (0.0) 174 50.0 to 120.0 Percent of m/e 95 91.6 175 4.0 to 9.0 Percent of m/e 174 6.7 (7.3) 176 93.0 to 101.0 Percent of m/e 174 89.5 (97.7) 177 5.0 to 9.0 Percent of m/e 176 5.8 (6.5) Page 371 of 478 Report Date: 28-Nov-2017 08:59:56 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Data File:\\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-01.D\TO15_LLNJ_TO3.rslt\spectra.d Injection Date: 24-Nov-2017 09:42:30 Spectrum:Tune Spec :Average 18-20( 5.68-5.69 ) Bgrd 8( 5.62) Base Peak:95.00 Minimum % Base Peak: 0 Number of Points: 121 m/z Y m/z Y m/z Y m/z Y 36.00 2304 69.00 35520 110.00 149 145.00 237 37.00 13501 70.00 2861 111.00 215 146.00 503 38.00 12453 71.00 129 112.00 120 147.00 270 39.00 4984 72.00 1756 113.00 158 148.00 824 40.00 369 73.00 15199 115.00 327 149.00 296 41.00 96 74.00 56592 116.00 1152 150.00 390 43.00 206 75.00 186368 117.00 1820 152.00 140 44.00 1064 76.00 15929 118.00 1178 153.00 289 45.00 2517 77.00 2565 119.00 1396 154.00 237 46.00 232 78.00 1727 120.00 52 155.00 949 47.00 5962 79.00 5674 122.00 54 156.00 202 48.00 1710 80.00 1835 123.00 130 157.00 600 49.00 12409 81.00 6054 124.00 205 158.00 38 50.00 64488 82.00 1486 125.00 100 159.00 368 51.00 19984 83.00 51 126.00 154 160.00 35 52.00 952 86.00 463 127.00 186 161.00 362 53.00 111 87.00 22624 128.00 1368 163.00 34 55.00 671 88.00 22112 129.00 701 170.00 92 56.00 4106 91.00 1089 130.00 1370 171.00 40 57.00 8247 92.00 9590 131.00 560 172.00 118 58.00 263 93.00 15298 133.00 168 174.00 418752 59.00 42 94.00 44632 134.00 34 175.00 30432 60.00 2748 95.00 457088 135.00 496 176.00 409280 61.00 14362 96.00 30048 136.00 145 177.00 26632 62.00 14235 97.00 933 137.00 514 178.00 699 63.00 10513 103.00 251 139.00 72 193.00 35 64.00 1095 104.00 1176 140.00 193 203.00 36 65.00 93 105.00 536 141.00 2479 207.00 50 66.00 37 106.00 1156 142.00 407 67.00 932 107.00 380 143.00 2763 68.00 35448 108.00 48 144.00 176 Page 372 of 478 Report Date: 28-Nov-2017 08:59:56 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-01.D Injection Date: 24-Nov-2017 09:42:30 Instrument ID: CHB.i Operator ID: VTP Lims ID: bfb Worklist Smp#: 1 Client ID: Injection Vol: 0.0 mL Dil. Factor: 1.0000 ALS Bottle#: 1 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Y Scaling: Method Defined: Scale to the Nth Largest Target: 1 5.5 5.8 6.1 6.4 6.7 7.0 7.3 7.6 7.9 8.2 8.5 8.8 Min 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 Y ( X 10 0 0 0 0 ) 28034-01[MS SCAN Chro]:Total Page 373 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:MB 200-123710/4 TestAmerica Burlington Matrix:28034-04.DLab File ID: Date Collected:TO-15Analysis Method: Air Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/24/2017 12:18 ID:RTX-624 Analysis Batch No.:123710 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 120.9175-71-8 Dichlorodifluoromethane 0.50 U 0.50 86.4775-45-6 Freon 22 0.50 U 0.50 170.9276-14-2 1,2-Dichlorotetrafluoroe thane 0.20 U 0.20 50.4974-87-3 Chloromethane 0.50 U 0.50 58.12106-97-8 n-Butane 0.50 U 0.50 62.5075-01-4 Vinyl chloride 0.035 U 0.035 54.09106-99-0 1,3-Butadiene 0.20 U 0.20 94.9474-83-9 Bromomethane 0.20 U 0.20 64.5275-00-3 Chloroethane 0.50 U 0.50 106.96593-60-2 Bromoethene(Vinyl Bromide) 0.20 U 0.20 137.3775-69-4 Trichlorofluoromethane 0.20 U 0.20 187.3876-13-1 Freon TF 0.20 U 0.20 96.9475-35-4 1,1-Dichloroethene 0.035 U 0.035 58.0867-64-1 Acetone 5.0 U 5.0 60.1067-63-0 Isopropyl alcohol 5.0 U 5.0 76.1475-15-0 Carbon disulfide 0.50 U 0.50 76.53107-05-1 3-Chloropropene 0.50 U 0.50 84.9375-09-2 Methylene Chloride 0.50 U 0.50 74.1275-65-0 tert-Butyl alcohol 5.0 U 5.0 88.151634-04-4 Methyl tert-butyl ether 0.20 U 0.20 96.94156-60-5 trans-1,2-Dichloroethene 0.20 U 0.20 86.17110-54-3 n-Hexane 0.20 U 0.20 98.9675-34-3 1,1-Dichloroethane 0.20 U 0.20 72.1178-93-3 Methyl Ethyl Ketone 0.50 U 0.50 96.94156-59-2 cis-1,2-Dichloroethene 0.035 U 0.035 96.94540-59-0 1,2-Dichloroethene, Total 0.40 U 0.40 119.3867-66-3 Chloroform 0.20 U 0.20 72.11109-99-9 Tetrahydrofuran 5.0 U 5.0 133.4171-55-6 1,1,1-Trichloroethane 0.20 U 0.20 84.16110-82-7 Cyclohexane 0.20 U 0.20 153.8156-23-5 Carbon tetrachloride 0.035 U 0.035 114.23540-84-1 2,2,4-Trimethylpentane 0.20 U 0.20 78.1171-43-2 Benzene 0.20 U 0.20 98.96107-06-2 1,2-Dichloroethane 0.20 U 0.20 FORM I TO-15 Page 374 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:MB 200-123710/4 TestAmerica Burlington Matrix:28034-04.DLab File ID: Date Collected:TO-15Analysis Method: Air Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/24/2017 12:18 ID:RTX-624 Analysis Batch No.:123710 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 100.21142-82-5 n-Heptane 0.20 U 0.20 131.3979-01-6 Trichloroethene 0.035 U 0.035 100.1280-62-6 Methyl methacrylate 0.50 U 0.50 112.9978-87-5 1,2-Dichloropropane 0.20 U 0.20 88.11123-91-1 1,4-Dioxane 5.0 U 5.0 163.8375-27-4 Bromodichloromethane 0.20 U 0.20 110.9710061-01-5 cis-1,3-Dichloropropene 0.20 U 0.20 100.16108-10-1 methyl isobutyl ketone 0.50 U 0.50 92.14108-88-3 Toluene 0.20 U 0.20 110.9710061-02-6 trans-1,3-Dichloropropen e 0.20 U 0.20 133.4179-00-5 1,1,2-Trichloroethane 0.20 U 0.20 165.83127-18-4 Tetrachloroethene 0.20 U 0.20 100.20591-78-6 Methyl Butyl Ketone (2-Hexanone) 0.50 U 0.50 208.29124-48-1 Dibromochloromethane 0.20 U 0.20 187.87106-93-4 1,2-Dibromoethane 0.20 U 0.20 112.56108-90-7 Chlorobenzene 0.20 U 0.20 106.17100-41-4 Ethylbenzene 0.20 U 0.20 106.17179601-23-1 m,p-Xylene 0.50 U 0.50 106.1795-47-6 Xylene, o-0.20 U 0.20 106.171330-20-7 Xylene (total)0.70 U 0.70 104.15100-42-5 Styrene 0.20 U 0.20 252.7575-25-2 Bromoform 0.20 U 0.20 120.1998-82-8 Cumene 0.20 U 0.20 167.8579-34-5 1,1,2,2-Tetrachloroethan e 0.20 U 0.20 120.19103-65-1 n-Propylbenzene 0.20 U 0.20 120.20622-96-8 4-Ethyltoluene 0.20 U 0.20 120.20108-67-8 1,3,5-Trimethylbenzene 0.20 U 0.20 126.5995-49-8 2-Chlorotoluene 0.20 U 0.20 134.2298-06-6 tert-Butylbenzene 0.20 U 0.20 120.2095-63-6 1,2,4-Trimethylbenzene 0.20 U 0.20 134.22135-98-8 sec-Butylbenzene 0.20 U 0.20 134.2299-87-6 4-Isopropyltoluene 0.20 U 0.20 147.00541-73-1 1,3-Dichlorobenzene 0.20 U 0.20 147.00106-46-7 1,4-Dichlorobenzene 0.20 U 0.20 FORM I TO-15 Page 375 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:MB 200-123710/4 TestAmerica Burlington Matrix:28034-04.DLab File ID: Date Collected:TO-15Analysis Method: Air Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/24/2017 12:18 ID:RTX-624 Analysis Batch No.:123710 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 126.58100-44-7 Benzyl chloride 0.20 U 0.20 134.22104-51-8 n-Butylbenzene 0.20 U 0.20 147.0095-50-1 1,2-Dichlorobenzene 0.20 U 0.20 181.45120-82-1 1,2,4-Trichlorobenzene 0.50 U 0.50 260.7687-68-3 Hexachlorobutadiene 0.20 U 0.20 128.1791-20-3 Naphthalene 0.50 U 0.50 FORM I TO-15 Page 376 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:MB 200-123710/4 TestAmerica Burlington Matrix:28034-04.DLab File ID: Date Collected:TO-15Analysis Method: Air Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/24/2017 12:18 ID:RTX-624 Analysis Batch No.:123710 ug/m3Units: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 120.9175-71-8 Dichlorodifluoromethane 2.5 U 2.5 86.4775-45-6 Freon 22 1.8 U 1.8 170.9276-14-2 1,2-Dichlorotetrafluoroe thane 1.4 U 1.4 50.4974-87-3 Chloromethane 1.0 U 1.0 58.12106-97-8 n-Butane 1.2 U 1.2 62.5075-01-4 Vinyl chloride 0.089 U 0.089 54.09106-99-0 1,3-Butadiene 0.44 U 0.44 94.9474-83-9 Bromomethane 0.78 U 0.78 64.5275-00-3 Chloroethane 1.3 U 1.3 106.96593-60-2 Bromoethene(Vinyl Bromide) 0.87 U 0.87 137.3775-69-4 Trichlorofluoromethane 1.1 U 1.1 187.3876-13-1 Freon TF 1.5 U 1.5 96.9475-35-4 1,1-Dichloroethene 0.14 U 0.14 58.0867-64-1 Acetone 12 U 12 60.1067-63-0 Isopropyl alcohol 12 U 12 76.1475-15-0 Carbon disulfide 1.6 U 1.6 76.53107-05-1 3-Chloropropene 1.6 U 1.6 84.9375-09-2 Methylene Chloride 1.7 U 1.7 74.1275-65-0 tert-Butyl alcohol 15 U 15 88.151634-04-4 Methyl tert-butyl ether 0.72 U 0.72 96.94156-60-5 trans-1,2-Dichloroethene 0.79 U 0.79 86.17110-54-3 n-Hexane 0.70 U 0.70 98.9675-34-3 1,1-Dichloroethane 0.81 U 0.81 72.1178-93-3 Methyl Ethyl Ketone 1.5 U 1.5 96.94156-59-2 cis-1,2-Dichloroethene 0.14 U 0.14 96.94540-59-0 1,2-Dichloroethene, Total 1.6 U 1.6 119.3867-66-3 Chloroform 0.98 U 0.98 72.11109-99-9 Tetrahydrofuran 15 U 15 133.4171-55-6 1,1,1-Trichloroethane 1.1 U 1.1 84.16110-82-7 Cyclohexane 0.69 U 0.69 153.8156-23-5 Carbon tetrachloride 0.22 U 0.22 114.23540-84-1 2,2,4-Trimethylpentane 0.93 U 0.93 78.1171-43-2 Benzene 0.64 U 0.64 98.96107-06-2 1,2-Dichloroethane 0.81 U 0.81 FORM I TO-15 Page 377 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:MB 200-123710/4 TestAmerica Burlington Matrix:28034-04.DLab File ID: Date Collected:TO-15Analysis Method: Air Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/24/2017 12:18 ID:RTX-624 Analysis Batch No.:123710 ug/m3Units: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 100.21142-82-5 n-Heptane 0.82 U 0.82 131.3979-01-6 Trichloroethene 0.19 U 0.19 100.1280-62-6 Methyl methacrylate 2.0 U 2.0 112.9978-87-5 1,2-Dichloropropane 0.92 U 0.92 88.11123-91-1 1,4-Dioxane 18 U 18 163.8375-27-4 Bromodichloromethane 1.3 U 1.3 110.9710061-01-5 cis-1,3-Dichloropropene 0.91 U 0.91 100.16108-10-1 methyl isobutyl ketone 2.0 U 2.0 92.14108-88-3 Toluene 0.75 U 0.75 110.9710061-02-6 trans-1,3-Dichloropropen e 0.91 U 0.91 133.4179-00-5 1,1,2-Trichloroethane 1.1 U 1.1 165.83127-18-4 Tetrachloroethene 1.4 U 1.4 100.20591-78-6 Methyl Butyl Ketone (2-Hexanone) 2.0 U 2.0 208.29124-48-1 Dibromochloromethane 1.7 U 1.7 187.87106-93-4 1,2-Dibromoethane 1.5 U 1.5 112.56108-90-7 Chlorobenzene 0.92 U 0.92 106.17100-41-4 Ethylbenzene 0.87 U 0.87 106.17179601-23-1 m,p-Xylene 2.2 U 2.2 106.1795-47-6 Xylene, o-0.87 U 0.87 106.171330-20-7 Xylene (total)3.0 U 3.0 104.15100-42-5 Styrene 0.85 U 0.85 252.7575-25-2 Bromoform 2.1 U 2.1 120.1998-82-8 Cumene 0.98 U 0.98 167.8579-34-5 1,1,2,2-Tetrachloroethan e 1.4 U 1.4 120.19103-65-1 n-Propylbenzene 0.98 U 0.98 120.20622-96-8 4-Ethyltoluene 0.98 U 0.98 120.20108-67-8 1,3,5-Trimethylbenzene 0.98 U 0.98 126.5995-49-8 2-Chlorotoluene 1.0 U 1.0 134.2298-06-6 tert-Butylbenzene 1.1 U 1.1 120.2095-63-6 1,2,4-Trimethylbenzene 0.98 U 0.98 134.22135-98-8 sec-Butylbenzene 1.1 U 1.1 134.2299-87-6 4-Isopropyltoluene 1.1 U 1.1 147.00541-73-1 1,3-Dichlorobenzene 1.2 U 1.2 147.00106-46-7 1,4-Dichlorobenzene 1.2 U 1.2 FORM I TO-15 Page 378 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:MB 200-123710/4 TestAmerica Burlington Matrix:28034-04.DLab File ID: Date Collected:TO-15Analysis Method: Air Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/24/2017 12:18 ID:RTX-624 Analysis Batch No.:123710 ug/m3Units: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 126.58100-44-7 Benzyl chloride 1.0 U 1.0 134.22104-51-8 n-Butylbenzene 1.1 U 1.1 147.0095-50-1 1,2-Dichlorobenzene 1.2 U 1.2 181.45120-82-1 1,2,4-Trichlorobenzene 3.7 U 3.7 260.7687-68-3 Hexachlorobutadiene 2.1 U 2.1 128.1791-20-3 Naphthalene 2.6 U 2.6 FORM I TO-15 Page 379 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS Client Sample ID: Lab Name:Job No.: 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:MB 200-123710/4 TestAmerica Burlington Matrix:28034-04.DLab File ID: Date Collected:TO-15Analysis Method: Air Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/24/2017 12:18 ID:RTX-624 Analysis Batch No.:123710 ppb v/vUnits: Number TICs Found:TIC Result Total:00 QRTCOMPOUND NAME RESULTCAS NO.MATCH QUALITY Tentatively Identified Compound None FORM I-TIC TO-15 Page 380 of 478 Report Date: 28-Nov-2017 09:04:47 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Target Compound Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-04.D Lims ID: mb Client ID: Sample Type: MB Inject. Date: 24-Nov-2017 12:18:30 ALS Bottle#: 4 Worklist Smp#: 4 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Sample Info: 200-0028034-004 Operator ID:VTP Instrument ID: CHB.i Method:\\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\TO15_LLNJ_TO3.m Limit Group: AI_TO15_ICAL Last Update: 28-Nov-2017 09:04:47 Calib Date: 07-Nov-2017 01:49:30 Integrator: RTE ID Type: Deconvolution ID Quant Method: Internal/External Standard Quant By: Initial Calibration Last ICal File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-13.D Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host:XAWRK022 First Level Reviewer: puangmaleek Date:28-Nov-2017 09:04:47 Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 1 Propene 41 3.134 ND 2 Dichlorodifluoromethane 85 3.193 ND 3 Chlorodifluoromethane 51 3.225 ND 4 1,2-Dichloro-1,1,2,2-tetra 85 3.412 ND 5 Chloromethane 50 3.535 ND 6 Butane 43 3.716 3.716 0.005 59 2180 0.0379 7 7 Vinyl chloride 62 3.748 ND 8 Butadiene 54 3.812 ND 10 Bromomethane 94 4.479 ND 11 Chloroethane 64 4.709 ND 12 2-Methylbutane 43 4.789 ND 13 Vinyl bromide 106 5.120 ND 14 Trichlorofluoromethane 101 5.216 ND 15 Pentane 43 5.355 ND 16 Ethanol 45 5.669 ND 17 Ethyl ether 59 5.824 ND 18 Acrolein 56 6.198 ND 19 1,1,2-Trichloro-1,2,2-trif 101 6.246 ND 20 1,1-Dichloroethene 96 6.315 ND 21 Acetone 43 6.465 ND 22 Isopropyl alcohol 45 6.683 ND 23 Carbon disulfide 76 6.748 ND 24 3-Chloro-1-propene 41 7.014 ND 26 Acetonitrile 41 7.073 ND T 25 Methyl Acetate TIC 43 7.200 ND 27 Methylene Chloride 49 7.271 7.271 -0.005 33 1346 0.0268 7 28 2-Methyl-2-propanol 59 7.383 ND 29 Methyl tert-butyl ether 73 7.623 ND 30 trans-1,2-Dichloroethene 61 7.687 ND 31 Acrylonitrile 53 7.751 ND 32 Hexane 57 8.012 ND 33 1,1-Dichloroethane 63 8.423 ND Page 381 of 478 Report Date: 28-Nov-2017 09:04:47 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-04.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 34 Vinyl acetate 43 8.429 ND 36 2-Butanone (MEK) 72 9.315 ND 37 cis-1,2-Dichloroethene 96 9.331 ND 35 Ethyl acetate 88 9.331 ND * 39 Chlorobromomethane 128 9.694 9.699 -0.005 90 421652 10.0 10.0 38 Tetrahydrofuran 42 9.710 ND 40 Chloroform 83 9.774 ND S 41 1,2-Dichloroethene, Total 61 10.000 ND 42 1,1,1-Trichloroethane 97 10.030 ND 43 Cyclohexane 84 10.046 ND 44 Carbon tetrachloride 117 10.238 ND 45 Isooctane 57 10.521 ND 46 Benzene 78 10.563 ND 47 1,2-Dichloroethane 62 10.659 ND 48 n-Heptane 43 10.772 ND A 49 GRO 1 10.862 (4.779-16.946) 0 5254272 0 * 50 1,4-Difluorobenzene 114 11.103 11.102 0.001 93 2106008 10.0 10.0 51 n-Butanol 56 11.284 ND 53 Trichloroethene 95 11.476 ND T 52 Methyl cyclohexane TIC 55 11.500 ND 54 1,2-Dichloropropane 63 11.839 ND 55 Methyl methacrylate 69 11.876 ND 56 1,4-Dioxane 88 11.967 ND 57 Dibromomethane 174 12.031 12.031 0.000 26 988 0.0161 7 58 Dichlorobromomethane 83 12.202 ND A 59 TVOC as Toluene 1 12.485 (3.124-21.845) 0 5566002 0 60 cis-1,3-Dichloropropene 75 12.826 ND 61 4-Methyl-2-pentanone (MIBK 43 12.976 ND 63 n-Octane 43 13.243 ND 64 Toluene 92 13.259 13.259 0.000 20 1510 0.0144 7 66 trans-1,3-Dichloropropene 75 13.621 ND 67 1,1,2-Trichloroethane 83 13.888 ND 68 Tetrachloroethene 166 14.032 ND 69 2-Hexanone 43 14.150 ND 70 Chlorodibromomethane 129 14.449 ND 71 Ethylene Dibromide 107 14.646 ND * 72 Chlorobenzene-d5 117 15.212 15.212 0.000 83 1754551 10.0 10.0 73 Chlorobenzene 112 15.249 ND 74 Ethylbenzene 91 15.313 15.313 -0.006 15 4926 0.0214 7 75 n-Nonane 57 15.340 ND 76 m-Xylene & p-Xylene 106 15.463 15.463 -0.005 0 673 0.007437 7 78 o-Xylene 106 15.975 15.975 0.000 12 1456 0.0162 7 S 77 Xylenes, Total 106 0 0.0236 7 79 Styrene 104 16.002 ND 80 Bromoform 173 16.295 ND 81 Isopropylbenzene 105 16.391 ND 83 1,1,2,2-Tetrachloroethane 83 16.797 ND 84 N-Propylbenzene 91 16.866 ND 85 1,2,3-Trichloropropane 75 16.877 ND 86 n-Decane 57 16.936 ND 87 4-Ethyltoluene 105 16.994 ND 88 2-Chlorotoluene 91 17.037 ND Page 382 of 478 Report Date: 28-Nov-2017 09:04:47 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-04.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 89 1,3,5-Trimethylbenzene 105 17.058 ND 90 Alpha Methyl Styrene 118 17.331 ND 91 tert-Butylbenzene 119 17.437 ND 92 1,2,4-Trimethylbenzene 105 17.507 ND 93 sec-Butylbenzene 105 17.694 ND 94 4-Isopropyltoluene 119 17.843 ND 95 1,3-Dichlorobenzene 146 17.923 ND 96 1,4-Dichlorobenzene 146 18.035 ND 97 Benzyl chloride 91 18.185 ND 98 Undecane 57 18.318 ND 99 n-Butylbenzene 91 18.350 ND 100 1,2-Dichlorobenzene 146 18.521 ND T 101 1,2-Dibromo-3-Chloropropan 75 19.300 ND 102 Dodecane 57 19.770 ND 103 1,2,4-Trichlorobenzene 180 20.880 ND 104 Hexachlorobutadiene 225 21.045 ND 105 Naphthalene 128 21.360 ND 106 1,2,3-Trichlorobenzene 180 21.835 ND T 107 Methyl acetylene TIC 1 0.000 ND T 108 1,1,1,2-Tetrachloroethane 1 0.000 ND T 117 Chlorotrifluoroethene TIC 1 0.000 ND T 118 Difluoroethane TIC 1 0.000 ND T 119 Freon 115 TIC 1 0.000 ND T 120 1,1,1-Trifluoro-2,2-dichlo 1 0.000 ND T 121 1,3-Dichloropropane TIC 1 0.000 ND QC Flag Legend Processing Flags 7 - Failed Limit of Detection Reagents: ATTO15BISs_00006 Amount Added: 20.00 Units: mL Run Reagent Page 383 of 478 Report Date: 28-Nov-2017 09:04:47 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-04.D Injection Date: 24-Nov-2017 12:18:30 Instrument ID: CHB.i Operator ID: VTP Lims ID: mb Worklist Smp#: 4 Client ID: Purge Vol: 200.000 mL Dil. Factor: 1.0000 ALS Bottle#: 4 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Y Scaling: Method Defined: Scale to the Nth Largest Target: 1 2.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 18.0 20.0 22.0 24.0 Min 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 Y ( X 10 0 0 0 0 ) 28034-04[MS SCAN Chro]:Total * C h l o r o b r o m o m e t h a n e ( 9 . 6 9 4 )* 1 ,4- D i f lu o r o b e n z en e ( 1 1 . 0 9 7 )+ * C h l o r o b e n z en e - d 5( 1 5 .2 1 2 )+ Page 384 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:LCS 200-123710/3 TestAmerica Burlington Matrix:28034-03.DLab File ID: Date Collected:TO-15Analysis Method: Air Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/24/2017 11:25 ID:RTX-624 Analysis Batch No.:123710 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 120.9175-71-8 Dichlorodifluoromethane 8.04 0.50 86.4775-45-6 Freon 22 7.83 0.50 170.9276-14-2 1,2-Dichlorotetrafluoroe thane 9.49 0.20 50.4974-87-3 Chloromethane 8.02 0.50 58.12106-97-8 n-Butane 7.93 0.50 62.5075-01-4 Vinyl chloride 8.80 0.035 54.09106-99-0 1,3-Butadiene 8.67 0.20 94.9474-83-9 Bromomethane 9.53 0.20 64.5275-00-3 Chloroethane 9.16 0.50 106.96593-60-2 Bromoethene(Vinyl Bromide) 9.77 0.20 137.3775-69-4 Trichlorofluoromethane 8.64 0.20 187.3876-13-1 Freon TF 9.45 0.20 96.9475-35-4 1,1-Dichloroethene 9.39 0.035 58.0867-64-1 Acetone 8.71 5.0 60.1067-63-0 Isopropyl alcohol 8.35 5.0 76.1475-15-0 Carbon disulfide 10.8 0.50 76.53107-05-1 3-Chloropropene 8.26 0.50 84.9375-09-2 Methylene Chloride 8.61 0.50 74.1275-65-0 tert-Butyl alcohol 8.73 5.0 88.151634-04-4 Methyl tert-butyl ether 9.08 0.20 96.94156-60-5 trans-1,2-Dichloroethene 9.56 0.20 86.17110-54-3 n-Hexane 9.28 0.20 98.9675-34-3 1,1-Dichloroethane 8.97 0.20 72.1178-93-3 Methyl Ethyl Ketone 9.30 0.50 96.94156-59-2 cis-1,2-Dichloroethene 9.44 0.035 96.94540-59-0 1,2-Dichloroethene, Total 19.0 0.40 119.3867-66-3 Chloroform 8.93 0.20 72.11109-99-9 Tetrahydrofuran 8.89 5.0 133.4171-55-6 1,1,1-Trichloroethane 8.87 0.20 84.16110-82-7 Cyclohexane 9.76 0.20 153.8156-23-5 Carbon tetrachloride 9.50 0.035 114.23540-84-1 2,2,4-Trimethylpentane 9.17 0.20 78.1171-43-2 Benzene 9.25 0.20 98.96107-06-2 1,2-Dichloroethane 8.47 0.20 FORM I TO-15 Page 385 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:LCS 200-123710/3 TestAmerica Burlington Matrix:28034-03.DLab File ID: Date Collected:TO-15Analysis Method: Air Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/24/2017 11:25 ID:RTX-624 Analysis Batch No.:123710 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 100.21142-82-5 n-Heptane 8.47 0.20 131.3979-01-6 Trichloroethene 9.67 0.035 100.1280-62-6 Methyl methacrylate 9.66 0.50 112.9978-87-5 1,2-Dichloropropane 9.16 0.20 88.11123-91-1 1,4-Dioxane 9.85 5.0 163.8375-27-4 Bromodichloromethane 8.79 0.20 110.9710061-01-5 cis-1,3-Dichloropropene 9.47 0.20 100.16108-10-1 methyl isobutyl ketone 8.46 0.50 92.14108-88-3 Toluene 9.45 0.20 110.9710061-02-6 trans-1,3-Dichloropropen e 9.47 0.20 133.4179-00-5 1,1,2-Trichloroethane 9.61 0.20 165.83127-18-4 Tetrachloroethene 9.78 0.20 100.20591-78-6 Methyl Butyl Ketone (2-Hexanone) 8.87 0.50 208.29124-48-1 Dibromochloromethane 9.35 0.20 187.87106-93-4 1,2-Dibromoethane 9.67 0.20 112.56108-90-7 Chlorobenzene 9.65 0.20 106.17100-41-4 Ethylbenzene 9.31 0.20 106.17179601-23-1 m,p-Xylene 19.0 0.50 106.1795-47-6 Xylene, o-9.22 0.20 106.171330-20-7 Xylene (total)28.2 0.70 104.15100-42-5 Styrene 9.70 0.20 252.7575-25-2 Bromoform 9.86 0.20 120.1998-82-8 Cumene 9.20 0.20 167.8579-34-5 1,1,2,2-Tetrachloroethan e 9.53 0.20 120.19103-65-1 n-Propylbenzene 9.17 0.20 120.20622-96-8 4-Ethyltoluene 9.47 0.20 120.20108-67-8 1,3,5-Trimethylbenzene 8.93 0.20 126.5995-49-8 2-Chlorotoluene 9.04 0.20 134.2298-06-6 tert-Butylbenzene 8.68 0.20 120.2095-63-6 1,2,4-Trimethylbenzene 8.63 0.20 134.22135-98-8 sec-Butylbenzene 8.52 0.20 134.2299-87-6 4-Isopropyltoluene 8.58 0.20 147.00541-73-1 1,3-Dichlorobenzene 9.01 0.20 147.00106-46-7 1,4-Dichlorobenzene 8.95 0.20 FORM I TO-15 Page 386 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: 200-41113-1SDG No.: 200-41113-1 Lab Sample ID:LCS 200-123710/3 TestAmerica Burlington Matrix:28034-03.DLab File ID: Date Collected:TO-15Analysis Method: Air Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/24/2017 11:25 ID:RTX-624 Analysis Batch No.:123710 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLMOLECULAR WEIGHT 126.58100-44-7 Benzyl chloride 9.03 0.20 134.22104-51-8 n-Butylbenzene 8.73 0.20 147.0095-50-1 1,2-Dichlorobenzene 8.65 0.20 181.45120-82-1 1,2,4-Trichlorobenzene 8.86 0.50 260.7687-68-3 Hexachlorobutadiene 8.73 0.20 128.1791-20-3 Naphthalene 8.33 0.50 FORM I TO-15 Page 387 of 478 Report Date: 28-Nov-2017 09:02:29 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Target Compound Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-03.D Lims ID: lcs Client ID: Sample Type: LCS Inject. Date: 24-Nov-2017 11:25:30 ALS Bottle#: 3 Worklist Smp#: 3 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Sample Info: 200-0028034-003 Operator ID:VTP Instrument ID: CHB.i Method:\\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\TO15_LLNJ_TO3.m Limit Group: AI_TO15_ICAL Last Update: 28-Nov-2017 09:01:07 Calib Date: 07-Nov-2017 01:49:30 Integrator: RTE ID Type: Deconvolution ID Quant Method: Internal/External Standard Quant By: Initial Calibration Last ICal File: \\ChromNA\Burlington\ChromData\CHB.i\20171106-27754.b\27754-13.D Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host:XAWRK022 First Level Reviewer: puangmaleek Date:28-Nov-2017 09:02:27 Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 1 Propene 41 3.145 3.134 0.011 98 185903 10.0 7.66 2 Dichlorodifluoromethane 85 3.209 3.193 0.016 99 745317 10.0 8.04 3 Chlorodifluoromethane 51 3.241 3.225 0.016 98 412994 10.0 7.83 4 1,2-Dichloro-1,1,2,2-tetra 85 3.428 3.412 0.016 96 924132 10.0 9.49 5 Chloromethane 50 3.551 3.535 0.016 99 265230 10.0 8.02 6 Butane 43 3.727 3.711 0.016 99 453279 10.0 7.93 7 Vinyl chloride 62 3.764 3.748 0.016 98 350835 10.0 8.80 8 Butadiene 54 3.833 3.812 0.021 94 253078 10.0 8.67 10 Bromomethane 94 4.495 4.479 0.016 100 390988 10.0 9.53 11 Chloroethane 64 4.730 4.709 0.021 99 225870 10.0 9.16 12 2-Methylbutane 43 4.815 4.789 0.026 95 471706 10.0 9.08 13 Vinyl bromide 106 5.141 5.120 0.021 99 408719 10.0 9.77 14 Trichlorofluoromethane 101 5.242 5.216 0.026 98 854811 10.0 8.64 15 Pentane 43 5.381 5.355 0.026 96 749231 10.0 9.49 16 Ethanol 45 5.723 5.669 0.054 98 247635 15.0 11.4 9 BFB 17 Ethyl ether 59 5.856 5.824 0.032 94 309486 10.0 10.2 18 Acrolein 56 6.219 6.198 0.021 95 167589 10.0 11.9 19 1,1,2-Trichloro-1,2,2-trif 101 6.267 6.246 0.021 99 785730 10.0 9.45 20 1,1-Dichloroethene 96 6.336 6.315 0.021 96 390835 10.0 9.39 21 Acetone 43 6.497 6.465 0.032 96 541265 10.0 8.71 22 Isopropyl alcohol 45 6.731 6.683 0.048 99 583325 10.0 8.35 23 Carbon disulfide 76 6.769 6.748 0.021 98 1260861 10.0 10.8 24 3-Chloro-1-propene 41 7.036 7.014 0.022 92 480111 10.0 8.26 26 Acetonitrile 41 7.100 7.073 0.027 100 351717 10.0 9.80 27 Methylene Chloride 49 7.292 7.276 0.016 92 429284 10.0 8.61 28 2-Methyl-2-propanol 59 7.425 7.383 0.042 92 795070 10.0 8.73 29 Methyl tert-butyl ether 73 7.655 7.623 0.032 97 1126798 10.0 9.08 30 trans-1,2-Dichloroethene 61 7.703 7.687 0.016 98 604127 10.0 9.56 31 Acrylonitrile 53 7.777 7.751 0.026 97 324315 10.0 9.73 32 Hexane 57 8.034 8.012 0.022 90 704750 10.0 9.28 33 1,1-Dichloroethane 63 8.445 8.423 0.022 99 757865 10.0 8.97 Page 388 of 478 Report Date: 28-Nov-2017 09:02:29 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-03.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 34 Vinyl acetate 43 8.455 8.429 0.026 100 1046232 10.0 9.00 36 2-Butanone (MEK) 72 9.336 9.315 0.021 97 227784 10.0 9.30 37 cis-1,2-Dichloroethene 96 9.346 9.331 0.015 95 454081 10.0 9.44 35 Ethyl acetate 88 9.352 9.331 0.021 94 40388 10.0 9.98 * 39 Chlorobromomethane 128 9.715 9.699 0.016 90 418664 10.0 10.0 38 Tetrahydrofuran 42 9.731 9.710 0.021 94 484241 10.0 8.89 40 Chloroform 83 9.789 9.774 0.015 95 805445 10.0 8.93 S 41 1,2-Dichloroethene, Total 61 0 20.0 19.0 42 1,1,1-Trichloroethane 97 10.046 10.030 0.016 95 758340 10.0 8.87 43 Cyclohexane 84 10.056 10.046 0.010 96 627732 10.0 9.76 44 Carbon tetrachloride 117 10.254 10.238 0.016 97 769395 10.0 9.50 45 Isooctane 57 10.531 10.521 0.010 100 2231922 10.0 9.17 46 Benzene 78 10.574 10.563 0.011 95 1388855 10.0 9.25 47 1,2-Dichloroethane 62 10.675 10.659 0.016 96 452984 10.0 8.47 48 n-Heptane 43 10.782 10.772 0.010 90 788498 10.0 8.47 A 49 GRO 1 10.862 (4.779-16.946) 0 165796371 10.0 0 * 50 1,4-Difluorobenzene 114 11.118 11.102 0.016 93 2041262 10.0 10.0 51 n-Butanol 56 11.310 11.284 0.026 84 314982 10.0 10.8 53 Trichloroethene 95 11.487 11.476 0.011 97 579150 10.0 9.67 54 1,2-Dichloropropane 63 11.855 11.839 0.016 94 529350 10.0 9.16 55 Methyl methacrylate 69 11.887 11.876 0.011 98 519622 10.0 9.66 56 1,4-Dioxane 88 11.983 11.967 0.016 92 280887 10.0 9.85 57 Dibromomethane 174 12.042 12.031 0.011 96 549097 10.0 9.21 58 Dichlorobromomethane 83 12.212 12.202 0.010 97 886701 10.0 8.79 A 59 TVOC as Toluene 1 12.485 (3.124-21.845) 0 263934958 10.0 0 60 cis-1,3-Dichloropropene 75 12.837 12.826 0.011 88 771995 10.0 9.47 61 4-Methyl-2-pentanone (MIBK 43 12.986 12.976 0.010 94 966479 10.0 8.46 63 n-Octane 43 13.253 13.243 0.010 90 1113484 10.0 8.49 64 Toluene 92 13.264 13.259 0.005 93 1010013 10.0 9.45 66 trans-1,3-Dichloropropene 75 13.627 13.621 0.006 94 738453 10.0 9.47 67 1,1,2-Trichloroethane 83 13.899 13.888 0.011 94 506658 10.0 9.61 68 Tetrachloroethene 166 14.038 14.032 0.006 98 828276 10.0 9.78 69 2-Hexanone 43 14.160 14.150 0.010 96 946600 10.0 8.87 70 Chlorodibromomethane 129 14.449 14.449 0.000 98 939555 10.0 9.35 71 Ethylene Dibromide 107 14.657 14.646 0.011 98 902784 10.0 9.67 * 72 Chlorobenzene-d5 117 15.217 15.212 0.005 84 1788667 10.0 10.0 73 Chlorobenzene 112 15.254 15.249 0.005 97 1375152 10.0 9.65 74 Ethylbenzene 91 15.324 15.319 0.005 97 2179983 10.0 9.31 75 n-Nonane 57 15.345 15.340 0.005 95 1098472 10.0 9.16 76 m-Xylene & p-Xylene 106 15.468 15.468 0.000 0 1751765 20.0 19.0 78 o-Xylene 106 15.980 15.975 0.005 99 846395 10.0 9.22 S 77 Xylenes, Total 106 0 30.0 28.2 79 Styrene 104 16.002 16.002 0.000 97 1341406 10.0 9.70 80 Bromoform 173 16.295 16.295 0.000 98 914698 10.0 9.86 81 Isopropylbenzene 105 16.391 16.391 0.000 95 2388055 10.0 9.20 83 1,1,2,2-Tetrachloroethane 83 16.797 16.797 0.000 97 1344284 10.0 9.53 84 N-Propylbenzene 91 16.872 16.866 0.006 99 2930931 10.0 9.17 85 1,2,3-Trichloropropane 75 16.882 16.877 0.005 98 967662 10.0 8.97 86 n-Decane 57 16.941 16.936 0.005 89 1305150 10.0 8.59 87 4-Ethyltoluene 105 16.994 16.994 0.000 98 2408691 10.0 9.47 88 2-Chlorotoluene 91 17.037 17.037 0.000 96 1914405 10.0 9.04 89 1,3,5-Trimethylbenzene 105 17.064 17.058 0.006 93 1877507 10.0 8.93 Page 389 of 478 Report Date: 28-Nov-2017 09:02:29 Chrom Revision: 2.2 13-Nov-2017 17:19:06 Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-03.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 90 Alpha Methyl Styrene 118 17.336 17.331 0.005 90 957289 10.0 9.30 91 tert-Butylbenzene 119 17.437 17.437 0.000 96 1765826 10.0 8.68 92 1,2,4-Trimethylbenzene 105 17.507 17.507 0.000 96 1793091 10.0 8.63 93 sec-Butylbenzene 105 17.693 17.694 -0.001 99 2689564 10.0 8.52 94 4-Isopropyltoluene 119 17.848 17.843 0.005 98 2226407 10.0 8.58 95 1,3-Dichlorobenzene 146 17.923 17.923 0.000 97 1244381 10.0 9.01 96 1,4-Dichlorobenzene 146 18.035 18.035 0.000 96 1209031 10.0 8.95 97 Benzyl chloride 91 18.184 18.185 -0.001 100 1393965 10.0 9.03 98 Undecane 57 18.318 18.318 0.000 96 1493920 10.0 9.04 99 n-Butylbenzene 91 18.355 18.350 0.005 98 2080226 10.0 8.73 100 1,2-Dichlorobenzene 146 18.521 18.521 0.000 97 1123377 10.0 8.65 102 Dodecane 57 19.769 19.770 -0.001 97 1152677 10.0 9.02 103 1,2,4-Trichlorobenzene 180 20.880 20.880 0.000 94 714152 10.0 8.86 104 Hexachlorobutadiene 225 21.045 21.045 0.000 98 741181 10.0 8.73 105 Naphthalene 128 21.360 21.360 0.000 100 1418446 10.0 8.33 106 1,2,3-Trichlorobenzene 180 21.835 21.835 0.000 96 599823 10.0 8.58 Reagents: ATTO15LCSW_00723 Amount Added: 200.00 Units: mL ATTO15BISs_00006 Amount Added: 20.00 Units: mL Run Reagent Page 390 of 478 Report Date: 28-Nov-2017 09:02:29 Chrom Revision: 2.2 13-Nov-2017 17:19:06 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHB.i\20171124-28034.b\28034-03.D Injection Date: 24-Nov-2017 11:25:30 Instrument ID: CHB.i Operator ID: VTP Lims ID: lcs Worklist Smp#: 3 Client ID: Purge Vol: 200.000 mL Dil. Factor: 1.0000 ALS Bottle#: 3 Method:TO15_LLNJ_TO3 Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Y Scaling: Method Defined: Scale to the Nth Largest Target: 1 2.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 18.0 20.0 22.0 24.0 Min 0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 Y ( X 10 0 0 0 0 ) 28034-03[MS SCAN Chro]:Total * C h l o r o b r o m o m e t h a n e ( 9 . 7 1 5 )+ * 1 ,4- D i f lu o r o b e n z en e ( 1 1 . 1 1 3 ) * C h l o r o b e n z en e - d 5 ( 1 5 . 2 1 7 ) Page 391 of 478 Lab Name:Job No.: SDG No.: Instrument ID: Analysis Batch Number: AIR - GC/MS VOA ANALYSIS RUN LOG DILUTION FACTOR COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID TestAmerica Burlington 200-41113-1 200-41113-1 CHB.i 122990 Start Date: End Date:11/07/2017 12:25 11/06/2017 15:25 BFB 200-122990/1 RTX-624 0.32(mm)111/06/2017 15:25 27754-01.D VIBLK 200-122990/2 RTX-624 0.32(mm)111/06/2017 16:14 VIBLK 200-122990/3 RTX-624 0.32(mm)111/06/2017 17:07 IC 200-122990/4 RTX-624 0.32(mm)111/06/2017 17:59 27754-04.D IC 200-122990/5 RTX-624 0.32(mm)111/06/2017 18:52 27754-05.D ZZZZZ RTX-624 0.32(mm)111/06/2017 19:44 IC 200-122990/7 RTX-624 0.32(mm)111/06/2017 20:36 27754-07.D ZZZZZ RTX-624 0.32(mm)111/06/2017 21:28 IC 200-122990/9 RTX-624 0.32(mm)111/06/2017 22:20 27754-09.D ICIS 200-122990/10 RTX-624 0.32(mm)111/06/2017 23:12 27754-10.D IC 200-122990/11 RTX-624 0.32(mm)111/07/2017 00:05 27754-11.D IC 200-122990/12 RTX-624 0.32(mm)111/07/2017 00:57 27754-12.D IC 200-122990/13 RTX-624 0.32(mm)111/07/2017 01:49 27754-13.D VIBLK 200-122990/14 RTX-624 0.32(mm)111/07/2017 02:41 VIBLK 200-122990/15 RTX-624 0.32(mm)111/07/2017 03:33 VIBLK 200-122990/16 RTX-624 0.32(mm)111/07/2017 04:25 ZZZZZ RTX-624 0.32(mm)111/07/2017 05:17 ZZZZZ RTX-624 0.32(mm)111/07/2017 06:09 ZZZZZ RTX-624 0.32(mm)111/07/2017 07:01 VIBLK 200-122990/20 RTX-624 0.32(mm)111/07/2017 07:54 VIBLK 200-122990/21 RTX-624 0.32(mm)111/07/2017 09:51 VIBLK 200-122990/22 RTX-624 0.32(mm)111/07/2017 10:41 VIBLK 200-122990/23 RTX-624 0.32(mm)111/07/2017 11:33 ICV 200-122990/24 RTX-624 0.32(mm)111/07/2017 12:25 27754-24.D TO-15 Page 392 of 478 Lab Name:Job No.: SDG No.: Instrument ID: Analysis Batch Number: AIR - GC/MS VOA ANALYSIS RUN LOG DILUTION FACTOR COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID TestAmerica Burlington 200-41113-1 200-41113-1 CHB.i 123710 Start Date: End Date:11/25/2017 01:23 11/24/2017 09:42 BFB 200-123710/1 RTX-624 0.32(mm)111/24/2017 09:42 28034-01.D CCVIS 200-123710/2 RTX-624 0.32(mm)111/24/2017 10:33 28034-02.D LCS 200-123710/3 RTX-624 0.32(mm)111/24/2017 11:25 28034-03.D MB 200-123710/4 RTX-624 0.32(mm)111/24/2017 12:18 28034-04.D ZZZZZ RTX-624 0.32(mm)1011/24/2017 13:10 ZZZZZ RTX-624 0.32(mm)1011/24/2017 14:03 ZZZZZ RTX-624 0.32(mm)1011/24/2017 14:55 200-41113-1 RTX-624 0.32(mm)111/24/2017 15:47 28034-08.D 200-41113-2 RTX-624 0.32(mm)2.9811/24/2017 16:40 28034-09.D 200-41113-3 RTX-624 0.32(mm)2.511/24/2017 17:32 28034-10.D 200-41113-4 RTX-624 0.32(mm)111/24/2017 18:24 28034-11.D ZZZZZ RTX-624 0.32(mm)10.0211/24/2017 19:17 ZZZZZ RTX-624 0.32(mm)82.7711/24/2017 20:09 ZZZZZ RTX-624 0.32(mm)211/24/2017 21:01 ZZZZZ RTX-624 0.32(mm)111/24/2017 21:54 ZZZZZ RTX-624 0.32(mm)111/24/2017 22:46 ZZZZZ RTX-624 0.32(mm)111/24/2017 23:39 ZZZZZ RTX-624 0.32(mm)111/25/2017 00:31 ZZZZZ RTX-624 0.32(mm)311/25/2017 01:23 TO-15 Page 393 of 478 Post-Sampling Air Canister Pressure Check Record Analyst BND Yes N o X X X X Lab ID Pressure1 Anomaly2 ("Hg) (Y/N) 200-41113-A-1 -2.9 N 200-41113-A-2 -2.9 N 200-41113-A-3 -2.6 N 200-41113-A-4 -2.1 N 2 If return pressure is not within criteria, initiate Non-Conformance Memo. 3 Record the ID of the FC used for sampling if information is provided, otherwise leave blank. 4 Record the Flow Controller Set Flow Rate Logbook ID and Page number in which the original FC Check was recorded 1 Criteria: Return Pressure should be between -1 and -10 ("Hg) with the exception of grab samples or those using 100 or 200mL/minute flow controllers. These samples must be returned at no lower than -10"Hg, but have no specific criteria otherwise. 5632-27725 3010 3993 7844 4803 4188 7844 Y Y 5632-27725 4436-27725 5632-2772525375201Y7844 4335 3999 FC FC Check4 FC Return Y Canister ID 7844 (Y/N) (w/ Location Code) 21 (Military)("Hg)(°C) 200-41113 G-24 Post-Sampling Return Pressure Check (4) Is visible sign of damage to canister and/or flow controller (FC) present? If damage observed, list equipment IDs and describe condition: 11/22/17 13:25 Sampling Information and Return Equipment Check Comments ID3 Reference Batch ID Can Cert Pressure (3) MA MCP & NJ DKQP: Check return flow rate for flow controllers Login #Date Time Lab BP Lab Temp (1) Is a Field Test Data Sheet (FTDS) or similar sampling documentation present? Gauge ID Comments 29.8 (2) Is the flow controller ID used for each canister recorded? FSR021:05.10.16:1 TestAmerica Burlington Page 394 of 478 Page 395 of 478 Page 396 of 478 AIR - GC/MS VOA LAB CONTROL SAMPLE RECOVERY FORM III Job No.:Lab Name: SDG No.: Level:Matrix:Low 200-40706-1 Lab File ID:27725_05.DAir Lab ID:LCS 200-122903/5 Client ID: TestAmerica Burlington REC % REC QC LIMITSCONCENTRATION (ppb v/v) SPIKE ADDED (ppb v/v) # LCS LCS COMPOUND Propylene 10.0 11.7 58-129117 Dichlorodifluoromethane 10.0 11.0 68-128110 Freon 22 10.0 11.7 64-128117 1,2-Dichlorotetrafluoroethane 10.0 11.9 78-138119 Chloromethane 10.0 11.2 57-126112 n-Butane 10.0 11.5 56-130115 Vinyl chloride 10.0 10.9 62-125109 1,3-Butadiene 10.0 10.7 59-125107 Bromomethane 10.0 10.4 68-128104 Chloroethane 10.0 10.8 65-125109 Bromoethene(Vinyl Bromide)10.0 10.0 67-127100 Trichlorofluoromethane 10.0 10.5 67-127105 Ethanol 15.0 17.1 28-168114 Freon TF 10.0 10.4 68-128104 1,1-Dichloroethene 10.0 10.1 67-127101 Acetone 10.0 12.2 64-136122 Isopropyl alcohol 10.0 11.2 55-124112 Carbon disulfide 10.0 12.2 81-141122 3-Chloropropene 10.0 9.02 53-13390 Methylene Chloride 10.0 11.6 62-122116 tert-Butyl alcohol 10.0 10.9 64-124109 Methyl tert-butyl ether 10.0 10.8 67-127108 trans-1,2-Dichloroethene 10.0 12.1 72-132121 n-Hexane 10.0 12.0 71-131120 1,1-Dichloroethane 10.0 11.3 66-126113 Vinyl acetate 10.0 12.6 62-130126 Ethyl acetate 10.0 11.1 75-135111 Methyl Ethyl Ketone 10.0 10.5 62-122105 cis-1,2-Dichloroethene 10.0 10.1 67-127101 Chloroform 10.0 10.6 69-129106 Tetrahydrofuran 10.0 12.1 61-136121 1,1,1-Trichloroethane 10.0 10.5 70-130105 Cyclohexane 10.0 10.6 69-129106 Carbon tetrachloride 10.0 10.7 62-143107 2,2,4-Trimethylpentane 10.0 11.1 67-127111 Benzene 10.0 10.5 67-127105 1,2-Dichloroethane 10.0 11.2 67-132112 n-Heptane 10.0 11.3 62-130113 Trichloroethene 10.0 10.2 68-128102 Methyl methacrylate 10.0 10.5 70-130105 1,2-Dichloropropane 10.0 10.7 67-127107 1,4-Dioxane 10.0 9.59 66-13296 FORM III TO-15 # Column to be used to flag recovery and RPD values Page 397 of 478 AIR - GC/MS VOA LAB CONTROL SAMPLE RECOVERY FORM III Job No.:Lab Name: SDG No.: Level:Matrix:Low 200-40706-1 Lab File ID:27725_05.DAir Lab ID:LCS 200-122903/5 Client ID: TestAmerica Burlington REC % REC QC LIMITSCONCENTRATION (ppb v/v) SPIKE ADDED (ppb v/v) # LCS LCS COMPOUND Bromodichloromethane 10.0 10.1 69-129101 cis-1,3-Dichloropropene 10.0 10.6 70-130106 methyl isobutyl ketone 10.0 10.5 62-130105 Toluene 10.0 9.74 67-12797 trans-1,3-Dichloropropene 10.0 9.17 69-12992 1,1,2-Trichloroethane 10.0 10.1 69-129101 Tetrachloroethene 10.0 9.02 70-13090 Methyl Butyl Ketone (2-Hexanone) 10.0 9.69 61-12797 Dibromochloromethane 10.0 8.47 66-13085 1,2-Dibromoethane 10.0 9.74 70-13097 Chlorobenzene 10.0 9.51 68-12895 Ethylbenzene 10.0 9.77 68-12898 m,p-Xylene 20.0 19.3 68-12896 Xylene, o-10.0 9.32 67-12793 Styrene 10.0 9.53 68-12895 Bromoform 10.0 6.70 34-17067 Cumene 10.0 9.50 67-12795 1,1,2,2-Tetrachloroethane 10.0 10.4 69-129104 n-Propylbenzene 10.0 9.86 67-12799 4-Ethyltoluene 10.0 10.5 69-129105 1,3,5-Trimethylbenzene 10.0 9.81 65-12598 2-Chlorotoluene 10.0 10.4 67-127104 tert-Butylbenzene 10.0 9.61 63-12596 1,2,4-Trimethylbenzene 10.0 9.92 65-12599 sec-Butylbenzene 10.0 9.91 66-12699 4-Isopropyltoluene 10.0 10.0 67-129100 1,3-Dichlorobenzene 10.0 9.67 67-12797 1,4-Dichlorobenzene 10.0 9.55 66-12695 Benzyl chloride 10.0 9.97 54-135100 n-Butylbenzene 10.0 10.6 67-127106 1,2-Dichlorobenzene 10.0 9.63 67-12796 1,2,4-Trichlorobenzene 10.0 8.81 59-12688 Hexachlorobutadiene 10.0 9.08 62-13091 Naphthalene 10.0 9.38 50-12194 FORM III TO-15 # Column to be used to flag recovery and RPD values Page 398 of 478 AIR - GC/MS VOA LAB CONTROL SAMPLE RECOVERY FORM III Job No.:Lab Name: SDG No.: Level:Matrix:Low 200-40725-1 Lab File ID:27725_05.DAir Lab ID:LCS 200-122903/5 Client ID: TestAmerica Burlington REC % REC QC LIMITSCONCENTRATION (ppb v/v) SPIKE ADDED (ppb v/v) # LCS LCS COMPOUND Propylene 10.0 11.7 58-129117 Dichlorodifluoromethane 10.0 11.0 68-128110 Freon 22 10.0 11.7 64-128117 1,2-Dichlorotetrafluoroethane 10.0 11.9 78-138119 Chloromethane 10.0 11.2 57-126112 n-Butane 10.0 11.5 56-130115 Vinyl chloride 10.0 10.9 62-125109 1,3-Butadiene 10.0 10.7 59-125107 Bromomethane 10.0 10.4 68-128104 Chloroethane 10.0 10.8 65-125109 Bromoethene(Vinyl Bromide)10.0 10.0 67-127100 Trichlorofluoromethane 10.0 10.5 67-127105 Ethanol 15.0 17.1 28-168114 Freon TF 10.0 10.4 68-128104 1,1-Dichloroethene 10.0 10.1 67-127101 Acetone 10.0 12.2 64-136122 Isopropyl alcohol 10.0 11.2 55-124112 Carbon disulfide 10.0 12.2 81-141122 3-Chloropropene 10.0 9.02 53-13390 Methylene Chloride 10.0 11.6 62-122116 tert-Butyl alcohol 10.0 10.9 64-124109 Methyl tert-butyl ether 10.0 10.8 67-127108 trans-1,2-Dichloroethene 10.0 12.1 72-132121 n-Hexane 10.0 12.0 71-131120 1,1-Dichloroethane 10.0 11.3 66-126113 Vinyl acetate 10.0 12.6 62-130126 Ethyl acetate 10.0 11.1 75-135111 Methyl Ethyl Ketone 10.0 10.5 62-122105 cis-1,2-Dichloroethene 10.0 10.1 67-127101 Chloroform 10.0 10.6 69-129106 Tetrahydrofuran 10.0 12.1 61-136121 1,1,1-Trichloroethane 10.0 10.5 70-130105 Cyclohexane 10.0 10.6 69-129106 Carbon tetrachloride 10.0 10.7 62-143107 2,2,4-Trimethylpentane 10.0 11.1 67-127111 Benzene 10.0 10.5 67-127105 1,2-Dichloroethane 10.0 11.2 67-132112 n-Heptane 10.0 11.3 62-130113 Trichloroethene 10.0 10.2 68-128102 Methyl methacrylate 10.0 10.5 70-130105 1,2-Dichloropropane 10.0 10.7 67-127107 1,4-Dioxane 10.0 9.59 66-13296 FORM III TO-15 # Column to be used to flag recovery and RPD values Page 399 of 478 AIR - GC/MS VOA LAB CONTROL SAMPLE RECOVERY FORM III Job No.:Lab Name: SDG No.: Level:Matrix:Low 200-40725-1 Lab File ID:27725_05.DAir Lab ID:LCS 200-122903/5 Client ID: TestAmerica Burlington REC % REC QC LIMITSCONCENTRATION (ppb v/v) SPIKE ADDED (ppb v/v) # LCS LCS COMPOUND Bromodichloromethane 10.0 10.1 69-129101 cis-1,3-Dichloropropene 10.0 10.6 70-130106 methyl isobutyl ketone 10.0 10.5 62-130105 Toluene 10.0 9.74 67-12797 trans-1,3-Dichloropropene 10.0 9.17 69-12992 1,1,2-Trichloroethane 10.0 10.1 69-129101 Tetrachloroethene 10.0 9.02 70-13090 Methyl Butyl Ketone (2-Hexanone) 10.0 9.69 61-12797 Dibromochloromethane 10.0 8.47 66-13085 1,2-Dibromoethane 10.0 9.74 70-13097 Chlorobenzene 10.0 9.51 68-12895 Ethylbenzene 10.0 9.77 68-12898 m,p-Xylene 20.0 19.3 68-12896 Xylene, o-10.0 9.32 67-12793 Styrene 10.0 9.53 68-12895 Bromoform 10.0 6.70 34-17067 Cumene 10.0 9.50 67-12795 1,1,2,2-Tetrachloroethane 10.0 10.4 69-129104 n-Propylbenzene 10.0 9.86 67-12799 4-Ethyltoluene 10.0 10.5 69-129105 1,3,5-Trimethylbenzene 10.0 9.81 65-12598 2-Chlorotoluene 10.0 10.4 67-127104 tert-Butylbenzene 10.0 9.61 63-12596 1,2,4-Trimethylbenzene 10.0 9.92 65-12599 sec-Butylbenzene 10.0 9.91 66-12699 4-Isopropyltoluene 10.0 10.0 67-129100 1,3-Dichlorobenzene 10.0 9.67 67-12797 1,4-Dichlorobenzene 10.0 9.55 66-12695 Benzyl chloride 10.0 9.97 54-135100 n-Butylbenzene 10.0 10.6 67-127106 1,2-Dichlorobenzene 10.0 9.63 67-12796 1,2,4-Trichlorobenzene 10.0 8.81 59-12688 Hexachlorobutadiene 10.0 9.08 62-13091 Naphthalene 10.0 9.38 50-12194 FORM III TO-15 # Column to be used to flag recovery and RPD values Page 400 of 478 FORM IV AIR - GC/MS VOA METHOD BLANK SUMMARY Lab Name: SDG No.: Job No.:200-40706-1TestAmerica Burlington Date Analyzed: GC Column:ID: Instrument ID:11/03/2017 13:47 RTX-624 NHeated Purge:(Y/N) CHX.i 27725_06.DLab File ID:Lab Sample ID:MB 200-122903/6 AirMatrix: 0.32(mm) THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES: LAB SAMPLE ID LAB FILE ID DATE ANALYZEDCLIENT SAMPLE ID 11/03/2017 12:5727725_05.DLCS 200-122903/5 11/03/2017 15:4327725_08.D200-40706-65632 FORM IV TO-15 Page 401 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: SDG No.: 200-40706-1 Lab Sample ID:MB 200-122903/6 TestAmerica Burlington Matrix:27725_06.DLab File ID: Date Collected:TO-15Analysis Method: Air Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/03/2017 13:47 ID:RTX-624 Analysis Batch No.:122903 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLRL 5.0 5.0U115-07-1 Propylene 5.0 0.50 0.50U75-71-8 Dichlorodifluoromethane 0.50 0.50 0.50U75-45-6 Freon 22 0.50 0.20 0.20U76-14-2 1,2-Dichlorotetrafluoroethane 0.20 0.50 0.50U74-87-3 Chloromethane 0.50 0.50 0.50U106-97-8 n-Butane 0.50 0.20 0.20U75-01-4 Vinyl chloride 0.20 0.20 0.20U106-99-0 1,3-Butadiene 0.20 0.20 0.20U74-83-9 Bromomethane 0.20 0.50 0.50U75-00-3 Chloroethane 0.50 0.20 0.20U593-60-2 Bromoethene(Vinyl Bromide)0.20 0.20 0.20U75-69-4 Trichlorofluoromethane 0.20 5.0 5.0U64-17-5 Ethanol 5.0 0.20 0.20U76-13-1 Freon TF 0.20 0.20 0.20U75-35-4 1,1-Dichloroethene 0.20 5.0 5.0U67-64-1 Acetone 5.0 5.0 5.0U67-63-0 Isopropyl alcohol 5.0 0.50 0.50U75-15-0 Carbon disulfide 0.50 0.50 0.50U107-05-1 3-Chloropropene 0.50 0.50 0.50U75-09-2 Methylene Chloride 0.50 5.0 5.0U75-65-0 tert-Butyl alcohol 5.0 0.20 0.20U1634-04-4 Methyl tert-butyl ether 0.20 0.20 0.20U156-60-5 trans-1,2-Dichloroethene 0.20 0.20 0.20U110-54-3 n-Hexane 0.20 0.20 0.20U75-34-3 1,1-Dichloroethane 0.20 5.0 5.0U108-05-4 Vinyl acetate 5.0 5.0 5.0U141-78-6 Ethyl acetate 5.0 0.50 0.50U78-93-3 Methyl Ethyl Ketone 0.50 0.20 0.20U156-59-2 cis-1,2-Dichloroethene 0.20 0.40 0.40U540-59-0 1,2-Dichloroethene, Total 0.40 0.20 0.20U67-66-3 Chloroform 0.20 5.0 5.0U109-99-9 Tetrahydrofuran 5.0 0.20 0.20U71-55-6 1,1,1-Trichloroethane 0.20 0.20 0.20U110-82-7 Cyclohexane 0.20 0.20 0.20U56-23-5 Carbon tetrachloride 0.20 0.20 0.20U540-84-1 2,2,4-Trimethylpentane 0.20 FORM I TO-15 Page 402 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: SDG No.: 200-40706-1 Lab Sample ID:MB 200-122903/6 TestAmerica Burlington Matrix:27725_06.DLab File ID: Date Collected:TO-15Analysis Method: Air Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/03/2017 13:47 ID:RTX-624 Analysis Batch No.:122903 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLRL 0.20 0.20U71-43-2 Benzene 0.20 0.20 0.20U107-06-2 1,2-Dichloroethane 0.20 0.20 0.20U142-82-5 n-Heptane 0.20 0.20 0.20U79-01-6 Trichloroethene 0.20 0.50 0.50U80-62-6 Methyl methacrylate 0.50 0.20 0.20U78-87-5 1,2-Dichloropropane 0.20 5.0 5.0U123-91-1 1,4-Dioxane 5.0 0.20 0.20U75-27-4 Bromodichloromethane 0.20 0.20 0.20U10061-01-5 cis-1,3-Dichloropropene 0.20 0.50 0.50U108-10-1 methyl isobutyl ketone 0.50 0.20 0.20U108-88-3 Toluene 0.20 0.20 0.20U10061-02-6 trans-1,3-Dichloropropene 0.20 0.20 0.20U79-00-5 1,1,2-Trichloroethane 0.20 0.20 0.20U127-18-4 Tetrachloroethene 0.20 0.50 0.50U591-78-6 Methyl Butyl Ketone (2-Hexanone)0.50 0.20 0.20U124-48-1 Dibromochloromethane 0.20 0.20 0.20U106-93-4 1,2-Dibromoethane 0.20 0.20 0.20U108-90-7 Chlorobenzene 0.20 0.20 0.20U100-41-4 Ethylbenzene 0.20 0.50 0.50U179601-23-1 m,p-Xylene 0.50 0.20 0.20U95-47-6 Xylene, o-0.20 0.70 0.70U1330-20-7 Xylene (total)0.70 0.20 0.20U100-42-5 Styrene 0.20 0.20 0.20U75-25-2 Bromoform 0.20 0.20 0.20U98-82-8 Cumene 0.20 0.20 0.20U79-34-5 1,1,2,2-Tetrachloroethane 0.20 0.20 0.20U103-65-1 n-Propylbenzene 0.20 0.20 0.20U622-96-8 4-Ethyltoluene 0.20 0.20 0.20U108-67-8 1,3,5-Trimethylbenzene 0.20 0.20 0.20U95-49-8 2-Chlorotoluene 0.20 0.20 0.20U98-06-6 tert-Butylbenzene 0.20 0.20 0.20U95-63-6 1,2,4-Trimethylbenzene 0.20 0.20 0.20U135-98-8 sec-Butylbenzene 0.20 0.20 0.20U99-87-6 4-Isopropyltoluene 0.20 0.20 0.20U541-73-1 1,3-Dichlorobenzene 0.20 0.20 0.20U106-46-7 1,4-Dichlorobenzene 0.20 FORM I TO-15 Page 403 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: SDG No.: 200-40706-1 Lab Sample ID:MB 200-122903/6 TestAmerica Burlington Matrix:27725_06.DLab File ID: Date Collected:TO-15Analysis Method: Air Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/03/2017 13:47 ID:RTX-624 Analysis Batch No.:122903 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLRL 0.20 0.20U100-44-7 Benzyl chloride 0.20 0.20 0.20U104-51-8 n-Butylbenzene 0.20 0.20 0.20U95-50-1 1,2-Dichlorobenzene 0.20 0.50 0.50U120-82-1 1,2,4-Trichlorobenzene 0.50 0.20 0.20U87-68-3 Hexachlorobutadiene 0.20 0.50 0.50U91-20-3 Naphthalene 0.50 FORM I TO-15 Page 404 of 478 Report Date: 06-Nov-2017 08:47:53 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Target Compound Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHX.i\20171103-27725.b\27725_06.D Lims ID: mb Client ID: Sample Type: MB Inject. Date: 03-Nov-2017 13:47:30 ALS Bottle#: 6 Worklist Smp#: 6 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Sample Info: 200-0027725-006 Operator ID: pad Instrument ID: CHX.i Method:\\ChromNA\Burlington\ChromData\CHX.i\20171103-27725.b\TO15_MasterMethod_X.m.m Limit Group: AI_TO15_ICAL Last Update: 06-Nov-2017 08:47:52 Calib Date: 24-Oct-2017 00:08:30 Integrator: RTE ID Type: Deconvolution ID Quant Method: Internal Standard Quant By: Initial Calibration Last ICal File: \\ChromNA\Burlington\ChromData\CHX.i\20171023-27547.b\27547_12.D Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host: XAWRK013 First Level Reviewer: puangmaleek Date:06-Nov-2017 08:47:52 Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 1 Propene 41 3.044 ND 2 Dichlorodifluoromethane 85 3.108 ND 3 Chlorodifluoromethane 51 3.156 ND 4 1,2-Dichloro-1,1,2,2-tetra 85 3.354 ND 5 Chloromethane 50 3.488 ND 6 Butane 43 3.670 ND 7 Vinyl chloride 62 3.712 ND 8 Butadiene 54 3.782 ND 10 Bromomethane 94 4.419 ND 11 Chloroethane 64 4.638 ND 12 2-Methylbutane 43 4.702 ND 13 Vinyl bromide 106 5.007 ND 14 Trichlorofluoromethane 101 5.098 ND 16 Pentane 43 5.226 ND 17 Ethanol 45 5.692 5.654 0.038 98 2996 0.2075 18 Ethyl ether 59 5.729 ND 20 1,1,2-Trichloro-1,2,2-trif 101 6.120 ND 19 Acrolein 56 6.120 ND 21 1,1-Dichloroethene 96 6.173 ND 22 Acetone 43 6.468 6.468 0.043 26 3171 0.0785 7 23 Carbon disulfide 76 6.564 ND 24 Isopropyl alcohol 45 6.762 6.708 0.054 97 4820 0.0999 25 3-Chloro-1-propene 41 6.949 ND 26 Acetonitrile 41 7.104 ND 27 Methylene Chloride 49 7.243 ND 28 2-Methyl-2-propanol 59 7.479 ND 29 Methyl tert-butyl ether 73 7.645 ND 31 trans-1,2-Dichloroethene 61 7.677 ND 32 Acrylonitrile 53 7.853 ND 33 Hexane 57 8.046 ND 34 1,1-Dichloroethane 63 8.565 ND 35 Vinyl acetate 43 8.645 ND Page 405 of 478 Report Date: 06-Nov-2017 08:47:53 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File: \\ChromNA\Burlington\ChromData\CHX.i\20171103-27725.b\27725_06.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags S 30 1,2-Dichloroethene, Total 61 9.665 ND 37 cis-1,2-Dichloroethene 96 9.699 ND 38 2-Butanone (MEK) 72 9.768 ND 39 Ethyl acetate 88 9.806 ND * 40 Chlorobromomethane 128 10.180 10.186 -0.006 97 332462 10.0 10.0 41 Tetrahydrofuran 42 10.202 ND 42 Chloroform 83 10.325 ND 43 Cyclohexane 84 10.560 ND 44 1,1,1-Trichloroethane 97 10.603 ND 45 Carbon tetrachloride 117 10.854 ND 46 Isooctane 57 11.309 ND 47 Benzene 78 11.363 ND 48 1,2-Dichloroethane 62 11.566 ND 49 n-Heptane 43 11.726 ND * 50 1,4-Difluorobenzene 114 12.261 12.267 -0.006 95 1717793 10.0 10.0 52 n-Butanol 56 12.721 ND 53 Trichloroethene 95 12.759 ND A 51 GRO 1 13.211 (4.692-21.730) 0 5483485 0 54 1,2-Dichloropropane 63 13.358 ND 55 Methyl methacrylate 69 13.545 ND 56 1,4-Dioxane 88 13.609 ND 57 Dibromomethane 174 13.625 ND 58 Dichlorobromomethane 83 13.941 ND 60 cis-1,3-Dichloropropene 75 14.920 ND A 59 TVOC as Toluene 92 15.118 (3.034-27.202) 0 5534858 0 61 4-Methyl-2-pentanone (MIBK 43 15.241 ND 65 Toluene 92 15.530 ND 64 n-Octane 43 15.583 ND 66 trans-1,3-Dichloropropene 75 16.177 ND 67 1,1,2-Trichloroethane 83 16.568 ND 68 Tetrachloroethene 166 16.659 ND 69 2-Hexanone 43 17.055 ND 71 Chlorodibromomethane 129 17.365 ND 72 Ethylene Dibromide 107 17.648 ND * 74 Chlorobenzene-d5 117 18.595 18.595 0.000 88 1512641 10.0 10.0 75 Chlorobenzene 112 18.660 ND 76 Ethylbenzene 91 18.820 ND 77 n-Nonane 57 18.954 ND 78 m-Xylene & p-Xylene 106 19.088 ND S 73 Xylenes, Total 106 19.600 ND 79 o-Xylene 106 19.981 ND 80 Styrene 104 20.045 ND 81 Bromoform 173 20.511 ND 82 Isopropylbenzene 105 20.741 ND 84 1,1,2,2-Tetrachloroethane 83 21.468 ND 85 N-Propylbenzene 91 21.527 ND 86 1,2,3-Trichloropropane 75 21.564 ND 87 n-Decane 57 21.720 ND 88 4-Ethyltoluene 105 21.730 ND 89 2-Chlorotoluene 91 21.736 ND 90 1,3,5-Trimethylbenzene 105 21.848 ND 91 Alpha Methyl Styrene 118 22.238 ND Page 406 of 478 Report Date: 06-Nov-2017 08:47:53 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File: \\ChromNA\Burlington\ChromData\CHX.i\20171103-27725.b\27725_06.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 92 tert-Butylbenzene 119 22.367 ND 93 1,2,4-Trimethylbenzene 105 22.469 ND 94 sec-Butylbenzene 105 22.709 ND 95 4-Isopropyltoluene 119 22.923 ND 96 1,3-Dichlorobenzene 146 22.950 ND 97 1,4-Dichlorobenzene 146 23.094 ND 98 Benzyl chloride 91 23.303 ND 100 n-Butylbenzene 91 23.517 ND 99 Undecane 57 23.544 ND 101 1,2-Dichlorobenzene 146 23.645 ND 102 Dodecane 57 25.175 ND 103 1,2,4-Trichlorobenzene 180 26.213 ND 104 Hexachlorobutadiene 225 26.401 ND 105 Naphthalene 128 26.711 ND 106 1,2,3-Trichlorobenzene 180 27.192 ND T 118 Chlorotrifluoroethene TIC 1 0.000 ND T 107 Methyl acetylene TIC 1 0.000 ND T 119 Difluoroethane TIC 1 0.000 ND T 121 1,1,1-Trifluoro-2,2-dichlo 1 0.000 ND T 120 Freon 115 TIC 1 0.000 ND T 36 Methyl cyclohexane TIC 55 0.000 ND T 15 Methyl Acetate TIC 43 0.000 ND T 70 1,2-Dibromo-3-Chloropropan 75 0.000 ND T 108 1,1,1,2-Tetrachloroethane 1 0.000 ND T 109 1,3-Dichloropropane TIC 1 0.000 ND QC Flag Legend Processing Flags 7 - Failed Limit of Detection Reagents: ATTO15XISs_00002 Amount Added: 20.00 Units: mL Run Reagent Page 407 of 478 Report Date: 06-Nov-2017 08:47:53 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHX.i\20171103-27725.b\27725_06.D Injection Date: 03-Nov-2017 13:47:30 Instrument ID: CHX.i Operator ID: pad Lims ID: mb Worklist Smp#: 6 Client ID: Purge Vol: 200.000 mL Dil. Factor: 1.0000 ALS Bottle#: 6 Method:TO15_MasterMethod_X.m Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Y Scaling: Method Defined: Scale to the Nth Largest Target: 1 2.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 18.0 20.0 22.0 24.0 26.0 28.0 30.0 Min 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 Y ( X 1 0 0 0 0 0 ) 27725_06[MS SCAN Chro]:Total * C h l o r o b r o m o m e t h a n e ( 1 0 . 1 8 0 ) * 1 ,4- D i f lu o r o b e n z en e ( 1 2 . 2 6 1 ) * C h l o r o b e n z en e - d 5 ( 1 8 . 5 9 0 )+ Page 408 of 478 FORM IV AIR - GC/MS VOA METHOD BLANK SUMMARY Lab Name: SDG No.: Job No.:200-40725-1TestAmerica Burlington Date Analyzed: GC Column:ID: Instrument ID:11/03/2017 13:47 RTX-624 NHeated Purge:(Y/N) CHX.i 27725_06.DLab File ID:Lab Sample ID:MB 200-122903/6 AirMatrix: 0.32(mm) THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES: LAB SAMPLE ID LAB FILE ID DATE ANALYZEDCLIENT SAMPLE ID 11/03/2017 12:5727725_05.DLCS 200-122903/5 11/03/2017 17:3827725_10.D200-40725-24436 FORM IV TO-15 Page 409 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: SDG No.: 200-40725-1 Lab Sample ID:MB 200-122903/6 TestAmerica Burlington Matrix:27725_06.DLab File ID: Date Collected:TO-15Analysis Method: Air Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/03/2017 13:47 ID:RTX-624 Analysis Batch No.:122903 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLRL 5.0 5.0U115-07-1 Propylene 5.0 0.50 0.50U75-71-8 Dichlorodifluoromethane 0.50 0.50 0.50U75-45-6 Freon 22 0.50 0.20 0.20U76-14-2 1,2-Dichlorotetrafluoroethane 0.20 0.50 0.50U74-87-3 Chloromethane 0.50 0.50 0.50U106-97-8 n-Butane 0.50 0.20 0.20U75-01-4 Vinyl chloride 0.20 0.20 0.20U106-99-0 1,3-Butadiene 0.20 0.20 0.20U74-83-9 Bromomethane 0.20 0.50 0.50U75-00-3 Chloroethane 0.50 0.20 0.20U593-60-2 Bromoethene(Vinyl Bromide)0.20 0.20 0.20U75-69-4 Trichlorofluoromethane 0.20 5.0 5.0U64-17-5 Ethanol 5.0 0.20 0.20U76-13-1 Freon TF 0.20 0.20 0.20U75-35-4 1,1-Dichloroethene 0.20 5.0 5.0U67-64-1 Acetone 5.0 5.0 5.0U67-63-0 Isopropyl alcohol 5.0 0.50 0.50U75-15-0 Carbon disulfide 0.50 0.50 0.50U107-05-1 3-Chloropropene 0.50 0.50 0.50U75-09-2 Methylene Chloride 0.50 5.0 5.0U75-65-0 tert-Butyl alcohol 5.0 0.20 0.20U1634-04-4 Methyl tert-butyl ether 0.20 0.20 0.20U156-60-5 trans-1,2-Dichloroethene 0.20 0.20 0.20U110-54-3 n-Hexane 0.20 0.20 0.20U75-34-3 1,1-Dichloroethane 0.20 5.0 5.0U108-05-4 Vinyl acetate 5.0 5.0 5.0U141-78-6 Ethyl acetate 5.0 0.50 0.50U78-93-3 Methyl Ethyl Ketone 0.50 0.20 0.20U156-59-2 cis-1,2-Dichloroethene 0.20 0.40 0.40U540-59-0 1,2-Dichloroethene, Total 0.40 0.20 0.20U67-66-3 Chloroform 0.20 5.0 5.0U109-99-9 Tetrahydrofuran 5.0 0.20 0.20U71-55-6 1,1,1-Trichloroethane 0.20 0.20 0.20U110-82-7 Cyclohexane 0.20 0.20 0.20U56-23-5 Carbon tetrachloride 0.20 0.20 0.20U540-84-1 2,2,4-Trimethylpentane 0.20 FORM I TO-15 Page 410 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: SDG No.: 200-40725-1 Lab Sample ID:MB 200-122903/6 TestAmerica Burlington Matrix:27725_06.DLab File ID: Date Collected:TO-15Analysis Method: Air Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/03/2017 13:47 ID:RTX-624 Analysis Batch No.:122903 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLRL 0.20 0.20U71-43-2 Benzene 0.20 0.20 0.20U107-06-2 1,2-Dichloroethane 0.20 0.20 0.20U142-82-5 n-Heptane 0.20 0.20 0.20U79-01-6 Trichloroethene 0.20 0.50 0.50U80-62-6 Methyl methacrylate 0.50 0.20 0.20U78-87-5 1,2-Dichloropropane 0.20 5.0 5.0U123-91-1 1,4-Dioxane 5.0 0.20 0.20U75-27-4 Bromodichloromethane 0.20 0.20 0.20U10061-01-5 cis-1,3-Dichloropropene 0.20 0.50 0.50U108-10-1 methyl isobutyl ketone 0.50 0.20 0.20U108-88-3 Toluene 0.20 0.20 0.20U10061-02-6 trans-1,3-Dichloropropene 0.20 0.20 0.20U79-00-5 1,1,2-Trichloroethane 0.20 0.20 0.20U127-18-4 Tetrachloroethene 0.20 0.50 0.50U591-78-6 Methyl Butyl Ketone (2-Hexanone)0.50 0.20 0.20U124-48-1 Dibromochloromethane 0.20 0.20 0.20U106-93-4 1,2-Dibromoethane 0.20 0.20 0.20U108-90-7 Chlorobenzene 0.20 0.20 0.20U100-41-4 Ethylbenzene 0.20 0.50 0.50U179601-23-1 m,p-Xylene 0.50 0.20 0.20U95-47-6 Xylene, o-0.20 0.70 0.70U1330-20-7 Xylene (total)0.70 0.20 0.20U100-42-5 Styrene 0.20 0.20 0.20U75-25-2 Bromoform 0.20 0.20 0.20U98-82-8 Cumene 0.20 0.20 0.20U79-34-5 1,1,2,2-Tetrachloroethane 0.20 0.20 0.20U103-65-1 n-Propylbenzene 0.20 0.20 0.20U622-96-8 4-Ethyltoluene 0.20 0.20 0.20U108-67-8 1,3,5-Trimethylbenzene 0.20 0.20 0.20U95-49-8 2-Chlorotoluene 0.20 0.20 0.20U98-06-6 tert-Butylbenzene 0.20 0.20 0.20U95-63-6 1,2,4-Trimethylbenzene 0.20 0.20 0.20U135-98-8 sec-Butylbenzene 0.20 0.20 0.20U99-87-6 4-Isopropyltoluene 0.20 0.20 0.20U541-73-1 1,3-Dichlorobenzene 0.20 0.20 0.20U106-46-7 1,4-Dichlorobenzene 0.20 FORM I TO-15 Page 411 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: SDG No.: 200-40725-1 Lab Sample ID:MB 200-122903/6 TestAmerica Burlington Matrix:27725_06.DLab File ID: Date Collected:TO-15Analysis Method: Air Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:1 Level: (low/med)Low 200(mL) 0.32(mm) Date Analyzed:11/03/2017 13:47 ID:RTX-624 Analysis Batch No.:122903 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLRL 0.20 0.20U100-44-7 Benzyl chloride 0.20 0.20 0.20U104-51-8 n-Butylbenzene 0.20 0.20 0.20U95-50-1 1,2-Dichlorobenzene 0.20 0.50 0.50U120-82-1 1,2,4-Trichlorobenzene 0.50 0.20 0.20U87-68-3 Hexachlorobutadiene 0.20 0.50 0.50U91-20-3 Naphthalene 0.50 FORM I TO-15 Page 412 of 478 Report Date: 06-Nov-2017 08:47:53 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Target Compound Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHX.i\20171103-27725.b\27725_06.D Lims ID: mb Client ID: Sample Type: MB Inject. Date: 03-Nov-2017 13:47:30 ALS Bottle#: 6 Worklist Smp#: 6 Purge Vol: 200.000 mL Dil. Factor: 1.0000 Sample Info: 200-0027725-006 Operator ID: pad Instrument ID: CHX.i Method:\\ChromNA\Burlington\ChromData\CHX.i\20171103-27725.b\TO15_MasterMethod_X.m.m Limit Group: AI_TO15_ICAL Last Update: 06-Nov-2017 08:47:52 Calib Date: 24-Oct-2017 00:08:30 Integrator: RTE ID Type: Deconvolution ID Quant Method: Internal Standard Quant By: Initial Calibration Last ICal File: \\ChromNA\Burlington\ChromData\CHX.i\20171023-27547.b\27547_12.D Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host: XAWRK013 First Level Reviewer: puangmaleek Date:06-Nov-2017 08:47:52 Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 1 Propene 41 3.044 ND 2 Dichlorodifluoromethane 85 3.108 ND 3 Chlorodifluoromethane 51 3.156 ND 4 1,2-Dichloro-1,1,2,2-tetra 85 3.354 ND 5 Chloromethane 50 3.488 ND 6 Butane 43 3.670 ND 7 Vinyl chloride 62 3.712 ND 8 Butadiene 54 3.782 ND 10 Bromomethane 94 4.419 ND 11 Chloroethane 64 4.638 ND 12 2-Methylbutane 43 4.702 ND 13 Vinyl bromide 106 5.007 ND 14 Trichlorofluoromethane 101 5.098 ND 16 Pentane 43 5.226 ND 17 Ethanol 45 5.692 5.654 0.038 98 2996 0.2075 18 Ethyl ether 59 5.729 ND 20 1,1,2-Trichloro-1,2,2-trif 101 6.120 ND 19 Acrolein 56 6.120 ND 21 1,1-Dichloroethene 96 6.173 ND 22 Acetone 43 6.468 6.468 0.043 26 3171 0.0785 7 23 Carbon disulfide 76 6.564 ND 24 Isopropyl alcohol 45 6.762 6.708 0.054 97 4820 0.0999 25 3-Chloro-1-propene 41 6.949 ND 26 Acetonitrile 41 7.104 ND 27 Methylene Chloride 49 7.243 ND 28 2-Methyl-2-propanol 59 7.479 ND 29 Methyl tert-butyl ether 73 7.645 ND 31 trans-1,2-Dichloroethene 61 7.677 ND 32 Acrylonitrile 53 7.853 ND 33 Hexane 57 8.046 ND 34 1,1-Dichloroethane 63 8.565 ND 35 Vinyl acetate 43 8.645 ND Page 413 of 478 Report Date: 06-Nov-2017 08:47:53 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File: \\ChromNA\Burlington\ChromData\CHX.i\20171103-27725.b\27725_06.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags S 30 1,2-Dichloroethene, Total 61 9.665 ND 37 cis-1,2-Dichloroethene 96 9.699 ND 38 2-Butanone (MEK) 72 9.768 ND 39 Ethyl acetate 88 9.806 ND * 40 Chlorobromomethane 128 10.180 10.186 -0.006 97 332462 10.0 10.0 41 Tetrahydrofuran 42 10.202 ND 42 Chloroform 83 10.325 ND 43 Cyclohexane 84 10.560 ND 44 1,1,1-Trichloroethane 97 10.603 ND 45 Carbon tetrachloride 117 10.854 ND 46 Isooctane 57 11.309 ND 47 Benzene 78 11.363 ND 48 1,2-Dichloroethane 62 11.566 ND 49 n-Heptane 43 11.726 ND * 50 1,4-Difluorobenzene 114 12.261 12.267 -0.006 95 1717793 10.0 10.0 52 n-Butanol 56 12.721 ND 53 Trichloroethene 95 12.759 ND A 51 GRO 1 13.211 (4.692-21.730) 0 5483485 0 54 1,2-Dichloropropane 63 13.358 ND 55 Methyl methacrylate 69 13.545 ND 56 1,4-Dioxane 88 13.609 ND 57 Dibromomethane 174 13.625 ND 58 Dichlorobromomethane 83 13.941 ND 60 cis-1,3-Dichloropropene 75 14.920 ND A 59 TVOC as Toluene 92 15.118 (3.034-27.202) 0 5534858 0 61 4-Methyl-2-pentanone (MIBK 43 15.241 ND 65 Toluene 92 15.530 ND 64 n-Octane 43 15.583 ND 66 trans-1,3-Dichloropropene 75 16.177 ND 67 1,1,2-Trichloroethane 83 16.568 ND 68 Tetrachloroethene 166 16.659 ND 69 2-Hexanone 43 17.055 ND 71 Chlorodibromomethane 129 17.365 ND 72 Ethylene Dibromide 107 17.648 ND * 74 Chlorobenzene-d5 117 18.595 18.595 0.000 88 1512641 10.0 10.0 75 Chlorobenzene 112 18.660 ND 76 Ethylbenzene 91 18.820 ND 77 n-Nonane 57 18.954 ND 78 m-Xylene & p-Xylene 106 19.088 ND S 73 Xylenes, Total 106 19.600 ND 79 o-Xylene 106 19.981 ND 80 Styrene 104 20.045 ND 81 Bromoform 173 20.511 ND 82 Isopropylbenzene 105 20.741 ND 84 1,1,2,2-Tetrachloroethane 83 21.468 ND 85 N-Propylbenzene 91 21.527 ND 86 1,2,3-Trichloropropane 75 21.564 ND 87 n-Decane 57 21.720 ND 88 4-Ethyltoluene 105 21.730 ND 89 2-Chlorotoluene 91 21.736 ND 90 1,3,5-Trimethylbenzene 105 21.848 ND 91 Alpha Methyl Styrene 118 22.238 ND Page 414 of 478 Report Date: 06-Nov-2017 08:47:53 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File: \\ChromNA\Burlington\ChromData\CHX.i\20171103-27725.b\27725_06.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response Cal Amt ppb v/v OnCol Amt ppb v/v Flags 92 tert-Butylbenzene 119 22.367 ND 93 1,2,4-Trimethylbenzene 105 22.469 ND 94 sec-Butylbenzene 105 22.709 ND 95 4-Isopropyltoluene 119 22.923 ND 96 1,3-Dichlorobenzene 146 22.950 ND 97 1,4-Dichlorobenzene 146 23.094 ND 98 Benzyl chloride 91 23.303 ND 100 n-Butylbenzene 91 23.517 ND 99 Undecane 57 23.544 ND 101 1,2-Dichlorobenzene 146 23.645 ND 102 Dodecane 57 25.175 ND 103 1,2,4-Trichlorobenzene 180 26.213 ND 104 Hexachlorobutadiene 225 26.401 ND 105 Naphthalene 128 26.711 ND 106 1,2,3-Trichlorobenzene 180 27.192 ND T 118 Chlorotrifluoroethene TIC 1 0.000 ND T 107 Methyl acetylene TIC 1 0.000 ND T 119 Difluoroethane TIC 1 0.000 ND T 121 1,1,1-Trifluoro-2,2-dichlo 1 0.000 ND T 120 Freon 115 TIC 1 0.000 ND T 36 Methyl cyclohexane TIC 55 0.000 ND T 15 Methyl Acetate TIC 43 0.000 ND T 70 1,2-Dibromo-3-Chloropropan 75 0.000 ND T 108 1,1,1,2-Tetrachloroethane 1 0.000 ND T 109 1,3-Dichloropropane TIC 1 0.000 ND QC Flag Legend Processing Flags 7 - Failed Limit of Detection Reagents: ATTO15XISs_00002 Amount Added: 20.00 Units: mL Run Reagent Page 415 of 478 Report Date: 06-Nov-2017 08:47:53 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHX.i\20171103-27725.b\27725_06.D Injection Date: 03-Nov-2017 13:47:30 Instrument ID: CHX.i Operator ID: pad Lims ID: mb Worklist Smp#: 6 Client ID: Purge Vol: 200.000 mL Dil. Factor: 1.0000 ALS Bottle#: 6 Method:TO15_MasterMethod_X.m Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Y Scaling: Method Defined: Scale to the Nth Largest Target: 1 2.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 18.0 20.0 22.0 24.0 26.0 28.0 30.0 Min 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 Y ( X 1 0 0 0 0 0 ) 27725_06[MS SCAN Chro]:Total * C h l o r o b r o m o m e t h a n e ( 1 0 . 1 8 0 ) * 1 ,4- D i f lu o r o b e n z en e ( 1 2 . 2 6 1 ) * C h l o r o b e n z en e - d 5 ( 1 8 . 5 9 0 )+ Page 416 of 478 FORM V Lab Name: SDG No.: Job No.:200-40706-1 Lab File ID: Instrument ID: 27547_01.D CHX.i 10/23/2017 14:57 BFB Injection Date: BFB Injection Time: M/E ION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE Analysis Batch No.:122454 50 8.0 - 40.0% of mass 95 17.5 75 30.0 - 66.0% of mass 95 48.0 95 Base peak, 100% relative abundance 100.0 96 5.0 - 9.0% of mass 95 6.5 173 Less than 2.0% of mass 174 0.7 (0.8) 1 174 50.0 - 120.0% of mass 95 85.9 175 4.0 - 9.0 % of mass 174 6.2 (7.2) 1 176 93.0 - 101.0% of mass 174 83.2 (96.9) 1 177 5.0 - 9.0% of mass 176 5.4 (6.5) 2 1-Value is % mass 174 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS: 2-Value is % mass 176 AIR - GC/MS VOA INSTRUMENT PERFORMANCE CHECK TestAmerica Burlington CLIENT SAMPLE ID LAB FILE IDLAB SAMPLE ID DATE ANALYZED TIME ANALYZED 27547_03.D 10/23/2017 16:35IC 200-122454/3 27547_04.D 10/23/2017 17:25IC 200-122454/4 27547_06.D 10/23/2017 19:06IC 200-122454/6 27547_08.D 10/23/2017 20:46IC 200-122454/8 27547_09.D 10/23/2017 21:37ICIS 200-122454/9 27547_10.D 10/23/2017 22:27IC 200-122454/10 27547_11.D 10/23/2017 23:18IC 200-122454/11 27547_12.D 10/24/2017 00:08IC 200-122454/12 27547_17.D 10/24/2017 04:21ICV 200-122454/17 FORM V TO-15 Page 417 of 478 FORM V Lab Name: SDG No.: Job No.:200-40706-1 Lab File ID: Instrument ID: 27725_01.D CHX.i 11/03/2017 09:29 BFB Injection Date: BFB Injection Time: M/E ION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE Analysis Batch No.:122903 50 8.0 - 40.0% of mass 95 19.7 75 30.0 - 66.0% of mass 95 51.0 95 Base peak, 100% relative abundance 100.0 96 5.0 - 9.0% of mass 95 6.5 173 Less than 2.0% of mass 174 0.6 (0.8) 1 174 50.0 - 120.0% of mass 95 76.9 175 4.0 - 9.0 % of mass 174 5.5 (7.2) 1 176 93.0 - 101.0% of mass 174 74.5 (97.0) 1 177 5.0 - 9.0% of mass 176 4.9 (6.6) 2 1-Value is % mass 174 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS: 2-Value is % mass 176 AIR - GC/MS VOA INSTRUMENT PERFORMANCE CHECK TestAmerica Burlington CLIENT SAMPLE ID LAB FILE IDLAB SAMPLE ID DATE ANALYZED TIME ANALYZED 27725_04.D 11/03/2017 12:06CCVIS 200-122903/4 27725_05.D 11/03/2017 12:57LCS 200-122903/5 27725_06.D 11/03/2017 13:47MB 200-122903/6 5632 27725_08.D 11/03/2017 15:43200-40706-6 FORM V TO-15 Page 418 of 478 FORM V Lab Name: SDG No.: Job No.:200-40725-1 Lab File ID: Instrument ID: 27547_01.D CHX.i 10/23/2017 14:57 BFB Injection Date: BFB Injection Time: M/E ION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE Analysis Batch No.:122454 50 8.0 - 40.0% of mass 95 17.5 75 30.0 - 66.0% of mass 95 48.0 95 Base peak, 100% relative abundance 100.0 96 5.0 - 9.0% of mass 95 6.5 173 Less than 2.0% of mass 174 0.7 (0.8) 1 174 50.0 - 120.0% of mass 95 85.9 175 4.0 - 9.0 % of mass 174 6.2 (7.2) 1 176 93.0 - 101.0% of mass 174 83.2 (96.9) 1 177 5.0 - 9.0% of mass 176 5.4 (6.5) 2 1-Value is % mass 174 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS: 2-Value is % mass 176 AIR - GC/MS VOA INSTRUMENT PERFORMANCE CHECK TestAmerica Burlington CLIENT SAMPLE ID LAB FILE IDLAB SAMPLE ID DATE ANALYZED TIME ANALYZED 27547_03.D 10/23/2017 16:35IC 200-122454/3 27547_04.D 10/23/2017 17:25IC 200-122454/4 27547_06.D 10/23/2017 19:06IC 200-122454/6 27547_08.D 10/23/2017 20:46IC 200-122454/8 27547_09.D 10/23/2017 21:37ICIS 200-122454/9 27547_10.D 10/23/2017 22:27IC 200-122454/10 27547_11.D 10/23/2017 23:18IC 200-122454/11 27547_12.D 10/24/2017 00:08IC 200-122454/12 27547_17.D 10/24/2017 04:21ICV 200-122454/17 FORM V TO-15 Page 419 of 478 FORM V Lab Name: SDG No.: Job No.:200-40725-1 Lab File ID: Instrument ID: 27725_01.D CHX.i 11/03/2017 09:29 BFB Injection Date: BFB Injection Time: M/E ION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE Analysis Batch No.:122903 50 8.0 - 40.0% of mass 95 19.7 75 30.0 - 66.0% of mass 95 51.0 95 Base peak, 100% relative abundance 100.0 96 5.0 - 9.0% of mass 95 6.5 173 Less than 2.0% of mass 174 0.6 (0.8) 1 174 50.0 - 120.0% of mass 95 76.9 175 4.0 - 9.0 % of mass 174 5.5 (7.2) 1 176 93.0 - 101.0% of mass 174 74.5 (97.0) 1 177 5.0 - 9.0% of mass 176 4.9 (6.6) 2 1-Value is % mass 174 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS: 2-Value is % mass 176 AIR - GC/MS VOA INSTRUMENT PERFORMANCE CHECK TestAmerica Burlington CLIENT SAMPLE ID LAB FILE IDLAB SAMPLE ID DATE ANALYZED TIME ANALYZED 27725_04.D 11/03/2017 12:06CCVIS 200-122903/4 27725_05.D 11/03/2017 12:57LCS 200-122903/5 27725_06.D 11/03/2017 13:47MB 200-122903/6 4436 27725_10.D 11/03/2017 17:38200-40725-2 FORM V TO-15 Page 420 of 478 AIR - GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY Lab Name:Job No.: SDG No.: FORM VIII TestAmerica Burlington 200-40706-1 Sample No.:ICIS 200-122454/9 Date Analyzed:10/23/2017 21:37 Lab File ID (Standard):27547_09.D Instrument ID:CHX.i GC Column:RTX-624 ID:0.32(mm) Heated Purge: (Y/N)N Calibration ID:38271 # RT #RT ## RT ## BCM DFBZ CBNZd5 AREA AREA AREA UPPER LIMIT LOWER LIMIT 441008 189004 951749 2220747 841328 1963100 10.19 12.27 18.60INITIAL CALIBRATION MID-POINT 10.52 9.86 12.60 11.94 18.93 18.27 315006 1586248 1402214 LAB SAMPLE ID CLIENT SAMPLE ID ICV 200-122454/17 307663 1542573 1355169 10.19 12.27 18.60 BCM = Bromochloromethane DFBZ = 1,4-Difluorobenzene CBNZd5 = Chlorobenzene-d5 Area Limit = 60%-140% of internal standard area RT Limit = ± 0.33 minutes of internal standard RT # Column used to flag values outside QC limits FORM VIII TO-15 Page 421 of 478 AIR - GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY Lab Name:Job No.: SDG No.: FORM VIII TestAmerica Burlington 200-40706-1 Sample No.:CCVIS 200-122903/4 Date Analyzed:11/03/2017 12:06 Lab File ID (Standard):27725_04.D Instrument ID:CHX.i GC Column:RTX-624 ID:0.32(mm) Heated Purge: (Y/N)N Calibration ID:38271 # RT #RT ## RT ## BCM DFBZ CBNZd5 AREA AREA AREA UPPER LIMIT LOWER LIMIT 468374 200732 1014620 2367448 903787 2108835 10.19 12.27 18.6012/24 HOUR STD 10.52 9.86 12.60 11.94 18.93 18.27 334553 1691034 1506311 LAB SAMPLE ID CLIENT SAMPLE ID LCS 200-122903/5 331131 1672572 1521875 10.19 12.27 18.60 MB 200-122903/6 332462 1717793 1512641 10.18 12.26 18.60 200-40706-6 5632 313748 1594194 1382833 10.19 12.27 18.60 BCM = Bromochloromethane DFBZ = 1,4-Difluorobenzene CBNZd5 = Chlorobenzene-d5 Area Limit = 60%-140% of internal standard area RT Limit = ± 0.33 minutes of internal standard RT # Column used to flag values outside QC limits FORM VIII TO-15 Page 422 of 478 AIR - GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY Lab Name:Job No.: SDG No.: FORM VIII TestAmerica Burlington 200-40725-1 Sample No.:ICIS 200-122454/9 Date Analyzed:10/23/2017 21:37 Lab File ID (Standard):27547_09.D Instrument ID:CHX.i GC Column:RTX-624 ID:0.32(mm) Heated Purge: (Y/N)N Calibration ID:38271 # RT #RT ## RT ## BCM DFBZ CBNZd5 AREA AREA AREA UPPER LIMIT LOWER LIMIT 441008 189004 951749 2220747 841328 1963100 10.19 12.27 18.60INITIAL CALIBRATION MID-POINT 10.52 9.86 12.60 11.94 18.93 18.27 315006 1586248 1402214 LAB SAMPLE ID CLIENT SAMPLE ID ICV 200-122454/17 307663 1542573 1355169 10.19 12.27 18.60 BCM = Bromochloromethane DFBZ = 1,4-Difluorobenzene CBNZd5 = Chlorobenzene-d5 Area Limit = 60%-140% of internal standard area RT Limit = ± 0.33 minutes of internal standard RT # Column used to flag values outside QC limits FORM VIII TO-15 Page 423 of 478 AIR - GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY Lab Name:Job No.: SDG No.: FORM VIII TestAmerica Burlington 200-40725-1 Sample No.:CCVIS 200-122903/4 Date Analyzed:11/03/2017 12:06 Lab File ID (Standard):27725_04.D Instrument ID:CHX.i GC Column:RTX-624 ID:0.32(mm) Heated Purge: (Y/N)N Calibration ID:38271 # RT #RT ## RT ## BCM DFBZ CBNZd5 AREA AREA AREA UPPER LIMIT LOWER LIMIT 468374 200732 1014620 2367448 903787 2108835 10.19 12.27 18.6012/24 HOUR STD 10.52 9.86 12.60 11.94 18.93 18.27 334553 1691034 1506311 LAB SAMPLE ID CLIENT SAMPLE ID LCS 200-122903/5 331131 1672572 1521875 10.19 12.27 18.60 MB 200-122903/6 332462 1717793 1512641 10.18 12.26 18.60 200-40725-2 4436 300504 1525189 1315337 10.19 12.27 18.60 BCM = Bromochloromethane DFBZ = 1,4-Difluorobenzene CBNZd5 = Chlorobenzene-d5 Area Limit = 60%-140% of internal standard area RT Limit = ± 0.33 minutes of internal standard RT # Column used to flag values outside QC limits FORM VIII TO-15 Page 424 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: 5632 SDG No.: 200-40706-1 Lab Sample ID:200-40706-6 TestAmerica Burlington Matrix:27725_08.DLab File ID: Date Collected:TO-15Analysis Method: Air 10/31/2017 00:00 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:0.2 Level: (low/med)Low 1000(mL) 0.32(mm) Date Analyzed:11/03/2017 15:43 ID:RTX-624 Analysis Batch No.:122903 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLRL 1.0 1.0U115-07-1 Propylene 1.0 0.10 0.10U75-71-8 Dichlorodifluoromethane 0.10 0.10 0.10U75-45-6 Freon 22 0.10 0.040 0.040U76-14-2 1,2-Dichlorotetrafluoroethane 0.040 0.10 0.10U74-87-3 Chloromethane 0.10 0.10 0.10U106-97-8 n-Butane 0.10 0.040 0.040U75-01-4 Vinyl chloride 0.040 0.040 0.040U106-99-0 1,3-Butadiene 0.040 0.040 0.040U74-83-9 Bromomethane 0.040 0.10 0.10U75-00-3 Chloroethane 0.10 0.040 0.040U593-60-2 Bromoethene(Vinyl Bromide)0.040 0.040 0.040U75-69-4 Trichlorofluoromethane 0.040 1.0 1.0U64-17-5 Ethanol 1.0 0.040 0.040U76-13-1 Freon TF 0.040 0.040 0.040U75-35-4 1,1-Dichloroethene 0.040 1.0 1.0U67-64-1 Acetone 1.0 1.0 1.0U67-63-0 Isopropyl alcohol 1.0 0.10 0.10U75-15-0 Carbon disulfide 0.10 0.10 0.10U107-05-1 3-Chloropropene 0.10 0.10 0.10U75-09-2 Methylene Chloride 0.10 1.0 1.0U75-65-0 tert-Butyl alcohol 1.0 0.040 0.040U1634-04-4 Methyl tert-butyl ether 0.040 0.040 0.040U156-60-5 trans-1,2-Dichloroethene 0.040 0.040 0.040U110-54-3 n-Hexane 0.040 0.040 0.040U75-34-3 1,1-Dichloroethane 0.040 1.0 1.0U108-05-4 Vinyl acetate 1.0 1.0 1.0U141-78-6 Ethyl acetate 1.0 0.10 0.10U78-93-3 Methyl Ethyl Ketone 0.10 0.040 0.040U156-59-2 cis-1,2-Dichloroethene 0.040 0.080 0.080U540-59-0 1,2-Dichloroethene, Total 0.080 0.040 0.040U67-66-3 Chloroform 0.040 1.0 1.0U109-99-9 Tetrahydrofuran 1.0 0.040 0.040U71-55-6 1,1,1-Trichloroethane 0.040 0.040 0.040U110-82-7 Cyclohexane 0.040 0.040 0.040U56-23-5 Carbon tetrachloride 0.040 0.040 0.040U540-84-1 2,2,4-Trimethylpentane 0.040 FORM I TO-15 Page 425 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: 5632 SDG No.: 200-40706-1 Lab Sample ID:200-40706-6 TestAmerica Burlington Matrix:27725_08.DLab File ID: Date Collected:TO-15Analysis Method: Air 10/31/2017 00:00 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:0.2 Level: (low/med)Low 1000(mL) 0.32(mm) Date Analyzed:11/03/2017 15:43 ID:RTX-624 Analysis Batch No.:122903 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLRL 0.040 0.040U71-43-2 Benzene 0.040 0.040 0.040U107-06-2 1,2-Dichloroethane 0.040 0.040 0.040U142-82-5 n-Heptane 0.040 0.040 0.040U79-01-6 Trichloroethene 0.040 0.10 0.10U80-62-6 Methyl methacrylate 0.10 0.040 0.040U78-87-5 1,2-Dichloropropane 0.040 1.0 1.0U123-91-1 1,4-Dioxane 1.0 0.040 0.040U75-27-4 Bromodichloromethane 0.040 0.040 0.040U10061-01-5 cis-1,3-Dichloropropene 0.040 0.10 0.10U108-10-1 methyl isobutyl ketone 0.10 0.040 0.040U108-88-3 Toluene 0.040 0.040 0.040U10061-02-6 trans-1,3-Dichloropropene 0.040 0.040 0.040U79-00-5 1,1,2-Trichloroethane 0.040 0.040 0.040U127-18-4 Tetrachloroethene 0.040 0.10 0.10U591-78-6 Methyl Butyl Ketone (2-Hexanone)0.10 0.040 0.040U124-48-1 Dibromochloromethane 0.040 0.040 0.040U106-93-4 1,2-Dibromoethane 0.040 0.040 0.040U108-90-7 Chlorobenzene 0.040 0.040 0.040U100-41-4 Ethylbenzene 0.040 0.10 0.10U179601-23-1 m,p-Xylene 0.10 0.040 0.040U95-47-6 Xylene, o-0.040 0.14 0.14U1330-20-7 Xylene (total)0.14 0.040 0.040U100-42-5 Styrene 0.040 0.040 0.040U75-25-2 Bromoform 0.040 0.040 0.040U98-82-8 Cumene 0.040 0.040 0.040U79-34-5 1,1,2,2-Tetrachloroethane 0.040 0.040 0.040U103-65-1 n-Propylbenzene 0.040 0.040 0.040U622-96-8 4-Ethyltoluene 0.040 0.040 0.040U108-67-8 1,3,5-Trimethylbenzene 0.040 0.040 0.040U95-49-8 2-Chlorotoluene 0.040 0.040 0.040U98-06-6 tert-Butylbenzene 0.040 0.040 0.040U95-63-6 1,2,4-Trimethylbenzene 0.040 0.040 0.040U135-98-8 sec-Butylbenzene 0.040 0.040 0.040U99-87-6 4-Isopropyltoluene 0.040 0.040 0.040U541-73-1 1,3-Dichlorobenzene 0.040 0.040 0.040U106-46-7 1,4-Dichlorobenzene 0.040 FORM I TO-15 Page 426 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: 5632 SDG No.: 200-40706-1 Lab Sample ID:200-40706-6 TestAmerica Burlington Matrix:27725_08.DLab File ID: Date Collected:TO-15Analysis Method: Air 10/31/2017 00:00 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:0.2 Level: (low/med)Low 1000(mL) 0.32(mm) Date Analyzed:11/03/2017 15:43 ID:RTX-624 Analysis Batch No.:122903 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLRL 0.040 0.040U100-44-7 Benzyl chloride 0.040 0.040 0.040U104-51-8 n-Butylbenzene 0.040 0.040 0.040U95-50-1 1,2-Dichlorobenzene 0.040 0.10 0.10U120-82-1 1,2,4-Trichlorobenzene 0.10 0.040 0.040U87-68-3 Hexachlorobutadiene 0.040 0.10 0.10U91-20-3 Naphthalene 0.10 FORM I TO-15 Page 427 of 478 Report Date: 06-Nov-2017 09:07:15 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Target Compound Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHX.i\20171103-27725.b\27725_08.D Lims ID: 200-40706-A-6 Client ID: 5632 Sample Type: Client Inject. Date: 03-Nov-2017 15:43:30 ALS Bottle#: 8 Worklist Smp#: 8 Purge Vol: 200.000 mL Dil. Factor: 0.2000 Sample Info: 200-0027725-008 Misc. Info.: 40706-06 Operator ID: pad Instrument ID: CHX.i Method:\\ChromNA\Burlington\ChromData\CHX.i\20171103-27725.b\TO15_MasterMethod_X.m.m Limit Group: AI_TO15_ICAL Last Update: 06-Nov-2017 09:07:14 Calib Date: 24-Oct-2017 00:08:30 Integrator: RTE ID Type: Deconvolution ID Quant Method: Internal Standard Quant By: Initial Calibration Last ICal File: \\ChromNA\Burlington\ChromData\CHX.i\20171023-27547.b\27547_12.D Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host: XAWRK013 First Level Reviewer: puangmaleek Date:06-Nov-2017 09:07:14 Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response OnCol Amt ppb v/v Flags 1 Propene 41 3.044 ND 2 Dichlorodifluoromethane 85 3.108 ND 3 Chlorodifluoromethane 51 3.156 ND 4 1,2-Dichloro-1,1,2,2-tetra 85 3.354 ND 5 Chloromethane 50 3.493 3.488 0.005 94 1208 0.0489 6 Butane 43 3.670 ND 7 Vinyl chloride 62 3.712 ND 8 Butadiene 54 3.782 ND 10 Bromomethane 94 4.419 ND 11 Chloroethane 64 4.638 ND 13 Vinyl bromide 106 5.007 ND 14 Trichlorofluoromethane 101 5.098 ND 17 Ethanol 45 5.697 5.654 0.043 97 2999 0.2201 20 1,1,2-Trichloro-1,2,2-trif 101 6.120 ND 21 1,1-Dichloroethene 96 6.173 ND 22 Acetone 43 6.425 ND 23 Carbon disulfide 76 6.564 ND 24 Isopropyl alcohol 45 6.762 6.708 0.054 97 3558 0.0782 25 3-Chloro-1-propene 41 6.949 ND 27 Methylene Chloride 49 7.243 ND 28 2-Methyl-2-propanol 59 7.479 ND 29 Methyl tert-butyl ether 73 7.645 ND 31 trans-1,2-Dichloroethene 61 7.677 ND 33 Hexane 57 8.046 ND 34 1,1-Dichloroethane 63 8.565 ND 35 Vinyl acetate 43 8.645 ND S 30 1,2-Dichloroethene, Total 61 9.665 ND 37 cis-1,2-Dichloroethene 96 9.699 ND 38 2-Butanone (MEK) 72 9.768 ND 39 Ethyl acetate 88 9.806 ND * 40 Chlorobromomethane 128 10.186 10.186 0.000 98 313748 10.0 Page 428 of 478 Report Date: 06-Nov-2017 09:07:15 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File: \\ChromNA\Burlington\ChromData\CHX.i\20171103-27725.b\27725_08.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response OnCol Amt ppb v/v Flags 41 Tetrahydrofuran 42 10.202 ND 42 Chloroform 83 10.325 ND 43 Cyclohexane 84 10.560 ND 44 1,1,1-Trichloroethane 97 10.603 ND 45 Carbon tetrachloride 117 10.854 ND 46 Isooctane 57 11.309 ND 47 Benzene 78 11.363 ND 48 1,2-Dichloroethane 62 11.566 ND 49 n-Heptane 43 11.726 ND * 50 1,4-Difluorobenzene 114 12.267 12.267 0.000 95 1594194 10.0 53 Trichloroethene 95 12.759 ND 54 1,2-Dichloropropane 63 13.358 ND 55 Methyl methacrylate 69 13.545 ND 56 1,4-Dioxane 88 13.609 ND 57 Dibromomethane 174 13.625 ND 58 Dichlorobromomethane 83 13.941 ND 60 cis-1,3-Dichloropropene 75 14.920 ND 61 4-Methyl-2-pentanone (MIBK 43 15.241 ND 65 Toluene 92 15.530 ND 66 trans-1,3-Dichloropropene 75 16.177 ND 67 1,1,2-Trichloroethane 83 16.568 ND 68 Tetrachloroethene 166 16.659 ND 69 2-Hexanone 43 17.055 ND 71 Chlorodibromomethane 129 17.365 ND 72 Ethylene Dibromide 107 17.648 ND * 74 Chlorobenzene-d5 117 18.595 18.595 0.000 89 1382833 10.0 75 Chlorobenzene 112 18.660 ND 76 Ethylbenzene 91 18.820 ND 78 m-Xylene & p-Xylene 106 19.088 ND S 73 Xylenes, Total 106 19.600 ND 79 o-Xylene 106 19.981 ND 80 Styrene 104 20.045 ND 81 Bromoform 173 20.511 ND 82 Isopropylbenzene 105 20.741 ND 84 1,1,2,2-Tetrachloroethane 83 21.468 ND 85 N-Propylbenzene 91 21.527 ND 88 4-Ethyltoluene 105 21.730 ND 89 2-Chlorotoluene 91 21.736 ND 90 1,3,5-Trimethylbenzene 105 21.848 ND 92 tert-Butylbenzene 119 22.367 ND 93 1,2,4-Trimethylbenzene 105 22.469 ND 94 sec-Butylbenzene 105 22.709 ND 95 4-Isopropyltoluene 119 22.923 ND 96 1,3-Dichlorobenzene 146 22.950 ND 97 1,4-Dichlorobenzene 146 23.094 ND 98 Benzyl chloride 91 23.303 ND 100 n-Butylbenzene 91 23.517 ND 101 1,2-Dichlorobenzene 146 23.645 ND 103 1,2,4-Trichlorobenzene 180 26.213 ND 104 Hexachlorobutadiene 225 26.401 ND 105 Naphthalene 128 26.711 ND Page 429 of 478 Report Date: 06-Nov-2017 09:07:15 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Reagents: ATTO15XISs_00002 Amount Added: 20.00 Units: mL Run Reagent Page 430 of 478 Report Date: 06-Nov-2017 09:07:15 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHX.i\20171103-27725.b\27725_08.D Injection Date: 03-Nov-2017 15:43:30 Instrument ID: CHX.i Operator ID: pad Lims ID: 200-40706-A-6 Lab Sample ID: 200-40706-6 Worklist Smp#: 8 Client ID: 5632 Purge Vol: 200.000 mL Dil. Factor: 0.2000 ALS Bottle#: 8 Method:TO15_MasterMethod_X.m Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Y Scaling: Method Defined: Scale to the Nth Largest Target: 1 2.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 18.0 20.0 22.0 24.0 26.0 28.0 30.0 Min 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 Y ( X 1 0 0 0 0 0 ) 27725_08[MS SCAN Chro]:Total * C h l o r o b r o m o m e t h a n e ( 1 0 . 1 8 6 ) * 1 ,4- D i f lu o r o b e n z en e ( 1 2 . 2 6 7 ) * C h l o r o b e n z en e - d 5 ( 1 8 . 5 9 5 ) Page 431 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: 4436 SDG No.: 200-40725-1 Lab Sample ID:200-40725-2 TestAmerica Burlington Matrix:27725_10.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/01/2017 00:00 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:0.2 Level: (low/med)Low 1000(mL) 0.32(mm) Date Analyzed:11/03/2017 17:38 ID:RTX-624 Analysis Batch No.:122903 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLRL 1.0 1.0U115-07-1 Propylene 1.0 0.10 0.10U75-71-8 Dichlorodifluoromethane 0.10 0.10 0.10U75-45-6 Freon 22 0.10 0.040 0.040U76-14-2 1,2-Dichlorotetrafluoroethane 0.040 0.10 0.10U74-87-3 Chloromethane 0.10 0.10 0.10U106-97-8 n-Butane 0.10 0.040 0.040U75-01-4 Vinyl chloride 0.040 0.040 0.040U106-99-0 1,3-Butadiene 0.040 0.040 0.040U74-83-9 Bromomethane 0.040 0.10 0.10U75-00-3 Chloroethane 0.10 0.040 0.040U593-60-2 Bromoethene(Vinyl Bromide)0.040 0.040 0.040U75-69-4 Trichlorofluoromethane 0.040 1.0 1.0U64-17-5 Ethanol 1.0 0.040 0.040U76-13-1 Freon TF 0.040 0.040 0.040U75-35-4 1,1-Dichloroethene 0.040 1.0 1.0U67-64-1 Acetone 1.0 1.0 1.0U67-63-0 Isopropyl alcohol 1.0 0.10 0.10U75-15-0 Carbon disulfide 0.10 0.10 0.10U107-05-1 3-Chloropropene 0.10 0.10 0.10U75-09-2 Methylene Chloride 0.10 1.0 1.0U75-65-0 tert-Butyl alcohol 1.0 0.040 0.040U1634-04-4 Methyl tert-butyl ether 0.040 0.040 0.040U156-60-5 trans-1,2-Dichloroethene 0.040 0.040 0.040U110-54-3 n-Hexane 0.040 0.040 0.040U75-34-3 1,1-Dichloroethane 0.040 1.0 1.0U108-05-4 Vinyl acetate 1.0 1.0 1.0U141-78-6 Ethyl acetate 1.0 0.10 0.10U78-93-3 Methyl Ethyl Ketone 0.10 0.040 0.040U156-59-2 cis-1,2-Dichloroethene 0.040 0.080 0.080U540-59-0 1,2-Dichloroethene, Total 0.080 0.040 0.040U67-66-3 Chloroform 0.040 1.0 1.0U109-99-9 Tetrahydrofuran 1.0 0.040 0.040U71-55-6 1,1,1-Trichloroethane 0.040 0.040 0.040U110-82-7 Cyclohexane 0.040 0.040 0.040U56-23-5 Carbon tetrachloride 0.040 0.040 0.040U540-84-1 2,2,4-Trimethylpentane 0.040 FORM I TO-15 Page 432 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: 4436 SDG No.: 200-40725-1 Lab Sample ID:200-40725-2 TestAmerica Burlington Matrix:27725_10.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/01/2017 00:00 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:0.2 Level: (low/med)Low 1000(mL) 0.32(mm) Date Analyzed:11/03/2017 17:38 ID:RTX-624 Analysis Batch No.:122903 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLRL 0.040 0.040U71-43-2 Benzene 0.040 0.040 0.040U107-06-2 1,2-Dichloroethane 0.040 0.040 0.040U142-82-5 n-Heptane 0.040 0.040 0.040U79-01-6 Trichloroethene 0.040 0.10 0.10U80-62-6 Methyl methacrylate 0.10 0.040 0.040U78-87-5 1,2-Dichloropropane 0.040 1.0 1.0U123-91-1 1,4-Dioxane 1.0 0.040 0.040U75-27-4 Bromodichloromethane 0.040 0.040 0.040U10061-01-5 cis-1,3-Dichloropropene 0.040 0.10 0.10U108-10-1 methyl isobutyl ketone 0.10 0.040 0.040U108-88-3 Toluene 0.040 0.040 0.040U10061-02-6 trans-1,3-Dichloropropene 0.040 0.040 0.040U79-00-5 1,1,2-Trichloroethane 0.040 0.040 0.040U127-18-4 Tetrachloroethene 0.040 0.10 0.10U591-78-6 Methyl Butyl Ketone (2-Hexanone)0.10 0.040 0.040U124-48-1 Dibromochloromethane 0.040 0.040 0.040U106-93-4 1,2-Dibromoethane 0.040 0.040 0.040U108-90-7 Chlorobenzene 0.040 0.040 0.040U100-41-4 Ethylbenzene 0.040 0.10 0.10U179601-23-1 m,p-Xylene 0.10 0.040 0.040U95-47-6 Xylene, o-0.040 0.14 0.14U1330-20-7 Xylene (total)0.14 0.040 0.040U100-42-5 Styrene 0.040 0.040 0.040U75-25-2 Bromoform 0.040 0.040 0.040U98-82-8 Cumene 0.040 0.040 0.040U79-34-5 1,1,2,2-Tetrachloroethane 0.040 0.040 0.040U103-65-1 n-Propylbenzene 0.040 0.040 0.040U622-96-8 4-Ethyltoluene 0.040 0.040 0.040U108-67-8 1,3,5-Trimethylbenzene 0.040 0.040 0.040U95-49-8 2-Chlorotoluene 0.040 0.040 0.040U98-06-6 tert-Butylbenzene 0.040 0.040 0.040U95-63-6 1,2,4-Trimethylbenzene 0.040 0.040 0.040U135-98-8 sec-Butylbenzene 0.040 0.040 0.040U99-87-6 4-Isopropyltoluene 0.040 0.040 0.040U541-73-1 1,3-Dichlorobenzene 0.040 0.040 0.040U106-46-7 1,4-Dichlorobenzene 0.040 FORM I TO-15 Page 433 of 478 FORM I AIR - GC/MS VOA ORGANICS ANALYSIS DATA SHEET Client Sample ID: Lab Name:Job No.: 4436 SDG No.: 200-40725-1 Lab Sample ID:200-40725-2 TestAmerica Burlington Matrix:27725_10.DLab File ID: Date Collected:TO-15Analysis Method: Air 11/01/2017 00:00 Sample wt/vol: % Moisture: GC Column:Soil Extract Vol.: Dilution Factor:Soil Aliquot Vol:0.2 Level: (low/med)Low 1000(mL) 0.32(mm) Date Analyzed:11/03/2017 17:38 ID:RTX-624 Analysis Batch No.:122903 ppb v/vUnits: CAS NO.COMPOUND NAME RESULT Q RLRL 0.040 0.040U100-44-7 Benzyl chloride 0.040 0.040 0.040U104-51-8 n-Butylbenzene 0.040 0.040 0.040U95-50-1 1,2-Dichlorobenzene 0.040 0.10 0.10U120-82-1 1,2,4-Trichlorobenzene 0.10 0.040 0.040U87-68-3 Hexachlorobutadiene 0.040 0.10 0.10U91-20-3 Naphthalene 0.10 FORM I TO-15 Page 434 of 478 Report Date: 06-Nov-2017 09:16:48 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Target Compound Quantitation Report Data File: \\ChromNA\Burlington\ChromData\CHX.i\20171103-27725.b\27725_10.D Lims ID: 200-40725-A-2 Client ID: 4436 Sample Type: Client Inject. Date: 03-Nov-2017 17:38:30 ALS Bottle#: 10 Worklist Smp#: 10 Purge Vol: 200.000 mL Dil. Factor: 0.2000 Sample Info: 200-0027725-010 Misc. Info.: 40725-02 Operator ID: pad Instrument ID: CHX.i Method:\\ChromNA\Burlington\ChromData\CHX.i\20171103-27725.b\TO15_MasterMethod_X.m.m Limit Group: AI_TO15_ICAL Last Update: 06-Nov-2017 09:16:46 Calib Date: 24-Oct-2017 00:08:30 Integrator: RTE ID Type: Deconvolution ID Quant Method: Internal Standard Quant By: Initial Calibration Last ICal File: \\ChromNA\Burlington\ChromData\CHX.i\20171023-27547.b\27547_12.D Column 1 : RTX-624 ( 0.32 mm)Det: MS SCAN Process Host: XAWRK013 First Level Reviewer: puangmaleek Date:06-Nov-2017 09:16:46 Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response OnCol Amt ppb v/v Flags 1 Propene 41 3.044 ND 2 Dichlorodifluoromethane 85 3.108 ND 3 Chlorodifluoromethane 51 3.156 ND 4 1,2-Dichloro-1,1,2,2-tetra 85 3.354 ND 5 Chloromethane 50 3.488 ND 6 Butane 43 3.670 ND 7 Vinyl chloride 62 3.712 ND 8 Butadiene 54 3.782 ND 10 Bromomethane 94 4.419 ND 11 Chloroethane 64 4.638 ND 13 Vinyl bromide 106 5.007 ND 14 Trichlorofluoromethane 101 5.098 ND 17 Ethanol 45 5.686 5.654 0.032 99 3286 0.2518 20 1,1,2-Trichloro-1,2,2-trif 101 6.120 ND 21 1,1-Dichloroethene 96 6.173 ND 22 Acetone 43 6.473 6.473 0.048 67 4346 0.1190 7 23 Carbon disulfide 76 6.574 6.564 0.010 98 2797 0.0386 24 Isopropyl alcohol 45 6.762 6.708 0.054 97 3985 0.0914 25 3-Chloro-1-propene 41 6.949 ND 27 Methylene Chloride 49 7.243 ND 28 2-Methyl-2-propanol 59 7.479 ND 29 Methyl tert-butyl ether 73 7.645 ND 31 trans-1,2-Dichloroethene 61 7.677 ND 33 Hexane 57 8.046 ND 34 1,1-Dichloroethane 63 8.565 ND 35 Vinyl acetate 43 8.645 ND S 30 1,2-Dichloroethene, Total 61 9.665 ND 37 cis-1,2-Dichloroethene 96 9.699 ND 38 2-Butanone (MEK) 72 9.768 ND 39 Ethyl acetate 88 9.806 ND * 40 Chlorobromomethane 128 10.186 10.186 0.000 98 300504 10.0 Page 435 of 478 Report Date: 06-Nov-2017 09:16:48 Chrom Revision: 2.2 28-Sep-2017 09:29:16 Data File: \\ChromNA\Burlington\ChromData\CHX.i\20171103-27725.b\27725_10.D Compound Sig RT (min.) Adj RT (min.) Dlt RT (min.)Q Response OnCol Amt ppb v/v Flags 41 Tetrahydrofuran 42 10.202 ND 42 Chloroform 83 10.325 ND 43 Cyclohexane 84 10.560 ND 44 1,1,1-Trichloroethane 97 10.603 ND 45 Carbon tetrachloride 117 10.854 ND 46 Isooctane 57 11.309 ND 47 Benzene 78 11.363 ND 48 1,2-Dichloroethane 62 11.566 ND 49 n-Heptane 43 11.726 ND * 50 1,4-Difluorobenzene 114 12.267 12.267 0.000 95 1525189 10.0 53 Trichloroethene 95 12.759 ND 54 1,2-Dichloropropane 63 13.358 ND 55 Methyl methacrylate 69 13.545 ND 56 1,4-Dioxane 88 13.609 ND 57 Dibromomethane 174 13.625 ND 58 Dichlorobromomethane 83 13.941 ND 60 cis-1,3-Dichloropropene 75 14.920 ND 61 4-Methyl-2-pentanone (MIBK 43 15.241 ND 65 Toluene 92 15.541 15.530 0.011 89 1498 0.0224 66 trans-1,3-Dichloropropene 75 16.177 ND 67 1,1,2-Trichloroethane 83 16.568 ND 68 Tetrachloroethene 166 16.659 ND 69 2-Hexanone 43 17.055 ND 71 Chlorodibromomethane 129 17.365 ND 72 Ethylene Dibromide 107 17.648 ND * 74 Chlorobenzene-d5 117 18.595 18.595 0.000 92 1315337 10.0 75 Chlorobenzene 112 18.660 ND 76 Ethylbenzene 91 18.825 18.820 0.005 88 1848 0.0122 78 m-Xylene & p-Xylene 106 19.087 19.088 -0.001 0 1152 0.0193 S 73 Xylenes, Total 106 0 0.0193 7 79 o-Xylene 106 19.981 ND 80 Styrene 104 20.045 ND 81 Bromoform 173 20.511 ND 82 Isopropylbenzene 105 20.741 ND 84 1,1,2,2-Tetrachloroethane 83 21.468 ND 85 N-Propylbenzene 91 21.527 ND 88 4-Ethyltoluene 105 21.730 ND 89 2-Chlorotoluene 91 21.736 ND 90 1,3,5-Trimethylbenzene 105 21.848 ND 92 tert-Butylbenzene 119 22.367 ND 93 1,2,4-Trimethylbenzene 105 22.469 ND 94 sec-Butylbenzene 105 22.709 ND 95 4-Isopropyltoluene 119 22.923 ND 96 1,3-Dichlorobenzene 146 22.950 ND 97 1,4-Dichlorobenzene 146 23.094 ND 98 Benzyl chloride 91 23.303 ND 100 n-Butylbenzene 91 23.517 ND 101 1,2-Dichlorobenzene 146 23.645 ND 103 1,2,4-Trichlorobenzene 180 26.213 ND 104 Hexachlorobutadiene 225 26.401 ND 105 Naphthalene 128 26.711 ND Page 436 of 478 Report Date: 06-Nov-2017 09:16:48 Chrom Revision: 2.2 28-Sep-2017 09:29:16 QC Flag Legend Processing Flags 7 - Failed Limit of Detection Reagents: ATTO15XISs_00002 Amount Added: 20.00 Units: mL Run Reagent Page 437 of 478 Report Date: 06-Nov-2017 09:16:48 Chrom Revision: 2.2 28-Sep-2017 09:29:16 TestAmerica Burlington Data File: \\ChromNA\Burlington\ChromData\CHX.i\20171103-27725.b\27725_10.D Injection Date: 03-Nov-2017 17:38:30 Instrument ID: CHX.i Operator ID: pad Lims ID: 200-40725-A-2 Lab Sample ID: 200-40725-2 Worklist Smp#: 10 Client ID: 4436 Purge Vol: 200.000 mL Dil. Factor: 0.2000 ALS Bottle#: 10 Method:TO15_MasterMethod_X.m Limit Group: AI_TO15_ICAL Column: RTX-624 ( 0.32 mm)Y Scaling: Method Defined: Scale to the Nth Largest Target: 1 2.0 4.0 6.0 8.0 10.0 12.0 14.0 16.0 18.0 20.0 22.0 24.0 26.0 28.0 30.0 Min 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 Y ( X 1 0 0 0 0 0 ) 27725_10[MS SCAN Chro]:Total * C h l o r o b r o m o m e t h a n e ( 1 0 . 1 8 6 ) * 1 ,4- D i f lu o r o b e n z en e ( 1 2 . 2 6 7 ) * C h l o r o b e n z en e - d 5 ( 1 8 . 5 9 5 ) Page 438 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:GC Column:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-40706-1 CHX.i Analy Batch No.:122454 38271Calibration Start Date:Calibration End Date:10/23/2017 16:35 N 10/24/2017 00:08 0.32(mm)RTX-624 ID: CURVE EVALUATION Calibration Files: LEVEL: LAB SAMPLE ID:LAB FILE ID: 1Level IC 200-122454/3 27547_03.D 2Level IC 200-122454/4 27547_04.D 3Level IC 200-122454/6 27547_06.D 4Level IC 200-122454/8 27547_08.D 5Level ICIS 200-122454/9 27547_09.D 6Level IC 200-122454/10 27547_10.D 7Level IC 200-122454/11 27547_11.D 8Level IC 200-122454/12 27547_12.D ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 #%RSD # MAX %RSD R^2 OR COD # MIN R^2 OR COD MIN RRF LVL 6 LVL 7 LVL 8 Propylene +++++ +++++ +++++ 0.6681 0.6639 Ave 10.3 0.6069 0.5721 0.5215 30.00.6065 Dichlorodifluoromethane +++++ +++++ 2.2330 2.4666 2.5022 Ave 10.5 2.2959 2.0532 1.8970 30.02.2413 Freon 22 +++++ +++++ 1.4326 1.4420 1.4468 Ave 9.1 1.3259 1.2518 1.1503 30.01.3416 1,2-Dichlorotetrafluoroethane +++++ 2.3225 2.3597 2.4932 2.4848 Ave 8.2 2.2915 2.1607 1.9545 30.02.2953 Chloromethane +++++ +++++ 0.8460 0.8453 0.8513 Ave 9.3 0.7745 0.7300 0.6752 30.00.7870 n-Butane +++++ +++++ 1.4856 1.3901 1.3764 Ave 11.5 1.2522 1.1737 1.0873 30.01.2942 Vinyl chloride 0.9285 0.9080 0.9299 1.0031 1.0040 Ave 7.3 0.9181 0.8691 0.7998 30.00.9201 1,3-Butadiene 0.7219 0.7134 0.7023 0.7250 0.7308 Ave 7.5 0.6680 0.6390 0.5851 30.00.6857 Bromomethane +++++ 0.8294 0.8209 0.8623 0.8741 Ave 7.4 0.8010 0.7651 0.6995 30.00.8075 Chloroethane +++++ +++++ 0.4845 0.4847 0.4863 Ave 8.9 0.4478 0.4225 0.3897 30.00.4526 Isopentane +++++ 1.2102 0.9642 0.9718 0.9489 Ave 15.7 0.8672 0.8170 0.7570 30.00.9338 Bromoethene(Vinyl Bromide)+++++ 0.8479 0.8659 0.9318 0.9401 Ave 6.3 0.8793 0.8420 0.7821 30.00.8699 Trichlorofluoromethane +++++ 2.4469 2.4687 2.5727 2.5950 Ave 6.5 2.4123 2.3155 2.1372 30.02.4212 n-Pentane +++++ +++++ 1.6602 1.5865 1.5738 Ave 10.6 1.4359 1.3558 1.2520 30.01.4774 FORM VI TO-15 Note: The M1 coefficient is the same as Ave RRF for an Ave curve type. Page 439 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:GC Column:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-40706-1 CHX.i Analy Batch No.:122454 38271Calibration Start Date:Calibration End Date:10/23/2017 16:35 N 10/24/2017 00:08 0.32(mm)RTX-624 ID: CURVE EVALUATION ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 #%RSD # MAX %RSD R^2 OR COD # MIN R^2 OR COD MIN RRF LVL 6 LVL 7 LVL 8 Ethanol +++++ +++++ 0.5535 0.4952 0.4427 Ave 19.6 0.4320 0.3629 0.3192 30.00.4343 Ethyl ether +++++ 0.6451 0.6298 0.6564 0.6664 Ave 6.9 0.6173 0.5870 0.5435 30.00.6208 Acrolein +++++ +++++ +++++ 0.2574 0.3221 Ave 14.5 0.2730 0.2352 0.2251 30.00.2626 Freon TF +++++ 1.7830 1.8081 1.8759 1.8861 Ave 7.2 1.7399 1.6647 1.5286 30.01.7552 1,1-Dichloroethene +++++ 0.8747 0.8526 0.8926 0.9075 Ave 6.5 0.8343 0.8067 0.7482 30.00.8452 Acetone +++++ +++++ +++++ 1.3834 1.2858 Ave 10.3 1.1941 1.1589 1.0562 30.01.2157 Carbon disulfide +++++ +++++ 2.4855 2.5937 2.5965 Ave 7.9 2.3967 2.2784 2.1105 30.02.4102 Isopropyl alcohol +++++ +++++ +++++ 1.5962 1.5350 Ave 8.1 1.3903 1.4342 1.2993 30.01.4510 3-Chloropropene +++++ 1.0982 0.9790 0.9524 1.1472 Ave 12.7 1.0281 0.8581 0.7968 30.00.9800 Acetonitrile +++++ +++++ +++++ 0.6817 0.6626 Ave 9.3 0.5826 0.5833 0.5503 30.00.6121 Methylene Chloride +++++ +++++ 1.0509 1.0650 1.0553 Ave 9.2 0.9654 0.9132 0.8461 30.00.9827 tert-Butyl alcohol +++++ +++++ +++++ 2.1253 2.0887 Ave 6.3 1.9174 1.9648 1.8196 30.01.9832 Methyl tert-butyl ether +++++ 2.6676 2.7703 2.8831 2.9016 Ave 6.8 2.6948 2.5693 2.3781 30.02.6950 trans-1,2-Dichloroethene +++++ 1.3656 1.3686 1.4771 1.4678 Ave 7.9 1.3464 1.2769 1.1701 30.01.3532 Acrylonitrile +++++ +++++ 0.6778 0.6935 0.7023 Ave 7.4 0.6445 0.6190 0.5769 30.00.6523 n-Hexane +++++ 1.5200 1.5132 1.5330 1.5253 Ave 8.6 1.3956 1.3262 1.2194 30.01.4332 1,1-Dichloroethane 1.6588 1.7944 1.8060 1.8733 1.8701 Ave 7.1 1.7202 1.6396 1.5190 30.01.7352 Vinyl acetate +++++ +++++ +++++ 2.3609 2.3781 Ave 8.4 2.1828 2.0718 1.9499 30.02.1887 cis-1,2-Dichloroethene +++++ 1.0323 1.0402 1.0885 1.1012 Ave 5.5 1.0305 0.9932 0.9337 30.01.0314 Methyl Ethyl Ketone +++++ +++++ 0.6088 0.5397 0.5468 Ave 9.2 0.5092 0.4996 0.4671 30.00.5285 FORM VI TO-15 Note: The M1 coefficient is the same as Ave RRF for an Ave curve type. Page 440 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:GC Column:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-40706-1 CHX.i Analy Batch No.:122454 38271Calibration Start Date:Calibration End Date:10/23/2017 16:35 N 10/24/2017 00:08 0.32(mm)RTX-624 ID: CURVE EVALUATION ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 #%RSD # MAX %RSD R^2 OR COD # MIN R^2 OR COD MIN RRF LVL 6 LVL 7 LVL 8 Ethyl acetate +++++ +++++ +++++ 0.0818 0.0818 Ave 5.5 0.0788 0.0762 0.0715 30.00.0780 Tetrahydrofuran +++++ +++++ +++++ 0.2267 0.2270 Ave 8.5 0.2063 0.1971 0.1872 30.00.2088 Chloroform +++++ 2.1917 2.1373 2.2309 2.2629 Ave 5.3 2.1198 2.0481 1.9332 30.02.1320 Cyclohexane +++++ 0.2658 0.2807 0.2926 0.2990 Ave 5.3 0.2791 0.2686 0.2574 30.00.2776 1,1,1-Trichloroethane +++++ 0.4274 0.4247 0.4562 0.4671 Ave 4.6 0.4371 0.4237 0.4094 30.00.4351 Carbon tetrachloride 0.3979 0.4060 0.4021 0.4570 0.4858 Ave 7.2 0.4531 0.4337 0.4269 30.00.4328 2,2,4-Trimethylpentane +++++ 1.0074 1.0168 1.0580 1.0755 Ave 5.3 0.9971 0.9589 0.9217 30.01.0050 Benzene +++++ 0.6484 0.6293 0.6635 0.6778 Ave 4.6 0.6331 0.6122 0.5928 30.00.6367 1,2-Dichloroethane +++++ 0.2671 0.2686 0.2835 0.2877 Ave 4.8 0.2676 0.2595 0.2509 30.00.2693 n-Heptane +++++ 0.3594 0.3625 0.3621 0.3673 Ave 6.2 0.3395 0.3242 0.3125 30.00.3468 n-Butanol +++++ +++++ +++++ 0.1230 0.1185 Ave 3.5 0.1114 0.1187 0.1181 30.00.1179 Trichloroethene 0.2718 0.2635 0.2651 0.2803 0.2899 Ave 3.2 0.2738 0.2695 0.2681 30.00.2728 1,2-Dichloropropane +++++ 0.2228 0.2190 0.2312 0.2402 Ave 4.1 0.2242 0.2174 0.2131 30.00.2240 Methyl methacrylate +++++ +++++ 0.2018 0.2201 0.2311 Ave 4.5 0.2201 0.2142 0.2135 30.00.2168 1,4-Dioxane +++++ +++++ +++++ 0.1414 0.1370 Ave 4.0 0.1276 0.1383 0.1319 30.00.1352 Dibromomethane +++++ 0.2506 0.2404 0.2643 0.2724 Ave 4.4 0.2617 0.2660 0.2712 30.00.2609 Bromodichloromethane +++++ 0.4016 0.4056 0.4554 0.4863 Ave 6.8 0.4588 0.4404 0.4344 30.00.4404 cis-1,3-Dichloropropene +++++ 0.3205 0.3169 0.3503 0.3682 Ave 5.2 0.3474 0.3375 0.3344 30.00.3393 methyl isobutyl ketone +++++ +++++ 0.4568 0.4512 0.4654 Ave 5.1 0.4354 0.4197 0.4084 30.00.4395 Toluene +++++ 0.5106 0.4959 0.5187 0.5410 Ave 3.5 0.5132 0.4932 0.4901 30.00.5089 FORM VI TO-15 Note: The M1 coefficient is the same as Ave RRF for an Ave curve type. Page 441 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:GC Column:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-40706-1 CHX.i Analy Batch No.:122454 38271Calibration Start Date:Calibration End Date:10/23/2017 16:35 N 10/24/2017 00:08 0.32(mm)RTX-624 ID: CURVE EVALUATION ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 #%RSD # MAX %RSD R^2 OR COD # MIN R^2 OR COD MIN RRF LVL 6 LVL 7 LVL 8 n-Octane +++++ 0.4575 0.4640 0.4897 0.5017 Ave 4.7 0.4680 0.4513 0.4391 30.00.4673 trans-1,3-Dichloropropene +++++ 0.4782 0.4726 0.3679 0.3858 Ave 13.7 0.3644 0.3671 0.3471 30.00.3976 1,1,2-Trichloroethane +++++ 0.2502 0.2470 0.2593 0.2704 Ave 3.8 0.2558 0.2461 0.2426 30.00.2531 Tetrachloroethene 0.3860 0.4167 0.4045 0.4269 0.4487 Ave 4.5 0.4348 0.4250 0.4260 30.00.4211 Methyl Butyl Ketone (2-Hexanone)+++++ +++++ 0.6353 0.4896 0.5109 Ave 13.6 0.4831 0.4547 0.4482 30.00.5036 Dibromochloromethane +++++ 0.4195 0.4326 0.5111 0.5831 Ave 12.0 0.5516 0.4937 0.4773 30.00.4956 1,2-Dibromoethane +++++ 0.4361 0.4389 0.4810 0.5050 Ave 5.3 0.4849 0.4649 0.4650 30.00.4680 Chlorobenzene +++++ 0.6896 0.6873 0.7210 0.7458 Ave 3.6 0.7074 0.6789 0.6762 30.00.7009 Ethylbenzene +++++ 1.1273 1.0984 1.1844 1.2328 Ave 4.1 1.1768 1.1286 1.1184 30.01.1524 n-Nonane +++++ 0.5090 0.5124 0.5462 0.5656 Ave 4.5 0.5370 0.5119 0.5029 30.00.5264 m,p-Xylene +++++ 0.4314 0.4287 0.4656 0.4910 Ave 5.0 0.4717 0.4510 0.4409 30.00.4543 Xylene, o-+++++ 0.4301 0.4116 0.4466 0.4678 Ave 4.0 0.4508 0.4357 0.4338 30.00.4395 Styrene +++++ 0.5692 0.5876 0.6957 0.7516 Ave 10.2 0.7251 0.6877 0.7030 30.00.6743 Bromoform +++++ 0.2955 0.3546 0.4291 0.5787 Ave 24.8 0.5394 0.3911 0.3493 30.00.4197 Cumene +++++ 1.2120 1.1954 1.3317 1.3992 Ave 5.7 1.3448 1.2929 1.2640 30.01.2914 1,1,2,2-Tetrachloroethane +++++ 0.6269 0.6294 0.6816 0.7121 Ave 5.3 0.6776 0.6506 0.6201 30.00.6569 n-Propylbenzene +++++ 1.5044 1.5023 1.6457 1.7406 Ave 6.0 1.6695 1.5909 1.5033 30.01.5938 1,2,3-Trichloropropane +++++ +++++ 0.5292 0.5497 0.5733 Ave 4.8 0.5479 0.5221 0.4999 30.00.5370 n-Decane +++++ +++++ 0.6456 0.7245 0.7604 Ave 10.5 0.7142 0.6388 0.5665 30.00.6750 4-Ethyltoluene +++++ 1.2108 1.2142 1.3899 1.4838 Ave 10.4 1.4159 1.3105 1.1001 30.01.3036 FORM VI TO-15 Note: The M1 coefficient is the same as Ave RRF for an Ave curve type. Page 442 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:GC Column:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-40706-1 CHX.i Analy Batch No.:122454 38271Calibration Start Date:Calibration End Date:10/23/2017 16:35 N 10/24/2017 00:08 0.32(mm)RTX-624 ID: CURVE EVALUATION ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 #%RSD # MAX %RSD R^2 OR COD # MIN R^2 OR COD MIN RRF LVL 6 LVL 7 LVL 8 2-Chlorotoluene +++++ 1.0748 1.0506 1.1735 1.2519 Ave 8.4 1.1933 1.1227 0.9746 30.01.1202 1,3,5-Trimethylbenzene +++++ 1.0111 1.0075 1.1386 1.2094 Ave 7.3 1.1621 1.0848 1.0303 30.01.0920 Alpha Methyl Styrene +++++ 0.4119 0.4271 0.5448 0.5940 Ave 13.6 0.5745 0.5235 0.5130 30.00.5127 tert-Butylbenzene +++++ 0.9574 0.9314 1.0707 1.1282 Ave 7.4 1.0854 1.0054 0.9566 30.01.0193 1,2,4-Trimethylbenzene +++++ 1.0079 1.0038 1.1521 1.2215 Ave 7.9 1.1625 1.0587 1.0342 30.01.0915 sec-Butylbenzene +++++ 1.4597 1.4682 1.6540 1.7413 Ave 7.6 1.6541 1.5038 1.4489 30.01.5614 4-Isopropyltoluene +++++ 1.1690 1.1885 1.3866 1.4751 Ave 9.0 1.3590 1.2408 1.2191 30.01.2912 1,3-Dichlorobenzene +++++ 0.7001 0.7021 0.7782 0.8409 Ave 7.9 0.8094 0.7228 0.6962 30.00.7499 1,4-Dichlorobenzene +++++ 0.6957 0.7022 0.7716 0.8309 Ave 7.3 0.7980 0.6994 0.7197 30.00.7453 Benzyl chloride +++++ 0.7546 0.6218 0.9024 1.1252 Ave 19.5 1.0374 0.8031 0.8576 30.00.8717 n-Butylbenzene +++++ 1.1247 1.1331 1.3046 1.3497 Ave 7.2 1.2172 1.1577 1.1789 30.01.2094 n-Undecane +++++ +++++ +++++ 0.7050 0.6673 Ave 3.6 0.6604 0.6453 0.6485 30.00.6653 1,2-Dichlorobenzene +++++ 0.6556 0.6541 0.7256 0.7821 Ave 7.2 0.7374 0.6554 0.6845 30.00.6992 n-Dodecane +++++ +++++ +++++ 0.5124 0.4842 Ave 18.5 0.4879 0.4196 0.3097 30.00.4428 1,2,4-Trichlorobenzene +++++ +++++ 0.4899 0.4891 0.5398 Ave 7.1 0.5642 0.4907 0.4712 30.00.5075 Hexachlorobutadiene +++++ 0.4515 0.4443 0.4674 0.4811 Ave 7.2 0.4988 0.4898 0.4013 30.00.4620 Naphthalene +++++ +++++ 1.1237 0.9917 1.2361 Ave 10.7 1.2574 1.0025 1.0257 30.01.1062 1,2,3-Trichlorobenzene +++++ +++++ 0.4569 0.4446 0.4762 Ave 11.3 0.5016 0.4377 0.3537 30.00.4451 FORM VI TO-15 Note: The M1 coefficient is the same as Ave RRF for an Ave curve type. Page 443 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-40706-1 CHX.i Analy Batch No.:122454 38271Calibration Start Date:Calibration End Date:10/23/2017 16:35 N 10/24/2017 00:08 GC Column:RTX-624 ID:0.32(mm) RESPONSE AND CONCENTRATION Calibration Files: LEVEL: LAB SAMPLE ID:LAB FILE ID: Level 1 IC 200-122454/3 27547_03.D Level 2 IC 200-122454/4 27547_04.D Level 3 IC 200-122454/6 27547_06.D Level 4 IC 200-122454/8 27547_08.D Level 5 ICIS 200-122454/9 27547_09.D Level 6 IC 200-122454/10 27547_10.D Level 7 IC 200-122454/11 27547_11.D Level 8 IC 200-122454/12 27547_12.D ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (PPB V/V) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 6 LVL 7 LVL 8 Propylene AveBCM +++++ +++++ +++++ 102553 209088 295665 383329 733525 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Dichlorodifluoromethane AveBCM +++++ +++++ 34132 378619 788068 1118396 1375810 2668106 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Freon 22 AveBCM +++++ +++++ 21898 221348 455675 645875 838809 1617809 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 1,2-Dichlorotetrafluoroethane AveBCM +++++ 14311 36069 382702 782560 1116258 1447830 2748966 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Chloromethane AveBCM +++++ +++++ 12931 129755 268108 377289 489178 949589 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 n-Butane AveBCM +++++ +++++ 22707 213381 433493 609985 786455 1529255 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Vinyl chloride AveBCM 1002 5595 14213 153984 316190 447253 582341 1124828 0.0351 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,3-Butadiene AveBCM 779 4396 10735 111292 230152 325381 428200 822928 0.0351 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Bromomethane AveBCM +++++ 5111 12547 132363 275306 390212 512654 983760 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Chloroethane AveBCM +++++ +++++ 7405 74395 153171 218149 283094 548111 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Isopentane AveBCM +++++ 7457 14738 149178 298865 422428 547443 1064662 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Bromoethene(Vinyl Bromide)AveBCM +++++ 5225 13236 143039 296073 428347 564215 1099998 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Trichlorofluoromethane AveBCM +++++ 15078 37735 394919 817285 1175116 1551534 3005949 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Pentane AveBCM +++++ +++++ 25376 243529 495676 699485 908464 1760850 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Ethanol AveBCM +++++ +++++ 84710 152112 209223 281207 486444 1122438 +++++ +++++ 5.01 9.99 15.0 20.0 40.0 100.0 FORM VI TO-15 Page 444 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-40706-1 CHX.i Analy Batch No.:122454 38271Calibration Start Date:Calibration End Date:10/23/2017 16:35 N 10/24/2017 00:08 GC Column:RTX-624 ID:0.32(mm) RESPONSE AND CONCENTRATION ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (PPB V/V) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 6 LVL 7 LVL 8 Ethyl ether AveBCM +++++ 3975 9626 100756 209888 300719 393347 764379 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Acrolein AveBCM +++++ +++++ +++++ 39513 101444 133002 157585 316543 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Freon TF AveBCM +++++ 10987 27637 287954 594002 847569 1115468 2149853 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,1-Dichloroethene AveBCM +++++ 5390 13032 137018 285811 406393 540532 1052382 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Acetone AveBCM +++++ +++++ +++++ 212360 404965 581667 776574 1485543 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Carbon disulfide AveBCM +++++ +++++ 37992 398140 817739 1167488 1526687 2968327 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Isopropyl alcohol AveBCM +++++ +++++ +++++ 245011 483454 677260 961000 1827406 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 3-Chloropropene AveBCM +++++ 6767 14964 146189 361320 500834 574993 1120688 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Acetonitrile AveBCM +++++ +++++ +++++ 104645 208675 283793 390879 773944 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Methylene Chloride AveBCM +++++ +++++ 16064 163475 332375 470285 611891 1190051 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 tert-Butyl alcohol AveBCM +++++ +++++ +++++ 326233 657838 934046 1316584 2559163 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Methyl tert-butyl ether AveBCM +++++ 16438 42344 442553 913845 1312746 1721648 3344671 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 trans-1,2-Dichloroethene AveBCM +++++ 8415 20920 226737 462280 655879 855597 1645639 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Acrylonitrile AveBCM +++++ +++++ 10361 106449 221179 313942 414760 811440 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 n-Hexane AveBCM +++++ 9366 23130 235318 480401 679826 888634 1714976 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,1-Dichloroethane AveBCM 1790 11057 27605 287553 588966 837948 1098640 2136445 0.0351 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Vinyl acetate AveBCM +++++ +++++ +++++ 362399 748981 1063297 1388261 2742463 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 cis-1,2-Dichloroethene AveBCM +++++ 6361 15899 167086 346817 501982 665524 1313245 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Methyl Ethyl Ketone AveBCM +++++ +++++ 9306 82840 172222 248067 334785 656964 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Ethyl acetate AveBCM +++++ +++++ +++++ 12554 25765 38394 51082 100588 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Tetrahydrofuran AveDFBZ +++++ +++++ +++++ 175579 359954 510836 673815 1317270 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 FORM VI TO-15 Page 445 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-40706-1 CHX.i Analy Batch No.:122454 38271Calibration Start Date:Calibration End Date:10/23/2017 16:35 N 10/24/2017 00:08 GC Column:RTX-624 ID:0.32(mm) RESPONSE AND CONCENTRATION ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (PPB V/V) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 6 LVL 7 LVL 8 Chloroform AveBCM +++++ 13505 32669 342441 712688 1032623 1372381 2719039 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Cyclohexane AveDFBZ +++++ 8548 22138 226698 474143 691140 918510 1811063 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,1,1-Trichloroethane AveDFBZ +++++ 13743 33489 353378 740782 1082206 1448598 2880937 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Carbon tetrachloride AveDFBZ 2265 13056 31710 354012 770388 1121989 1482862 3003863 0.0351 0.200 0.500 4.99 10.00 15.0 20.0 40.0 2,2,4-Trimethylpentane AveDFBZ +++++ 32393 80184 819590 1705633 2468728 3278556 6485246 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Benzene AveDFBZ +++++ 20850 49626 513943 1075001 1567657 2093114 4171026 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,2-Dichloroethane AveDFBZ +++++ 8590 21182 219600 456212 662579 887163 1765151 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Heptane AveDFBZ +++++ 11556 28584 280503 582478 840512 1108575 2199085 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Butanol AveDFBZ +++++ +++++ +++++ 95269 188013 275873 405781 831088 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Trichloroethene AveDFBZ 1547 8474 20904 217129 459822 678007 921595 1886228 0.0351 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,2-Dichloropropane AveDFBZ +++++ 7164 17269 179114 380868 555075 743330 1499203 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Methyl methacrylate AveDFBZ +++++ +++++ 15911 170513 366543 544893 732558 1502078 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 1,4-Dioxane AveDFBZ +++++ +++++ +++++ 109497 217341 316031 472869 927989 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Dibromomethane AveDFBZ +++++ 8059 18958 204735 431950 647898 909652 1908419 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Bromodichloromethane AveDFBZ +++++ 12915 31986 352786 771290 1136055 1505805 3056799 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 cis-1,3-Dichloropropene AveDFBZ +++++ 10307 24993 271353 583954 860223 1154046 2353259 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 methyl isobutyl ketone AveDFBZ +++++ +++++ 36019 349498 738112 1077942 1435092 2873471 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Toluene AveCBNZ d5 +++++ 14179 34222 355752 758399 1119474 1514793 3089729 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Octane AveDFBZ +++++ 14711 36592 379330 795715 1158747 1543072 3089403 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 trans-1,3-Dichloropropene AveDFBZ +++++ 15376 37267 284983 611800 902146 1255186 2442595 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,1,2-Trichloroethane AveCBNZ d5 +++++ 6946 17045 177823 379130 557985 755934 1529748 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 FORM VI TO-15 Page 446 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-40706-1 CHX.i Analy Batch No.:122454 38271Calibration Start Date:Calibration End Date:10/23/2017 16:35 N 10/24/2017 00:08 GC Column:RTX-624 ID:0.32(mm) RESPONSE AND CONCENTRATION ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (PPB V/V) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 6 LVL 7 LVL 8 Tetrachloroethene AveCBNZ d5 1912 11571 27911 292834 629100 948589 1305509 2686070 0.0351 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Methyl Butyl Ketone (2-Hexanone)AveCBNZ d5 +++++ +++++ 43837 335774 716248 1053929 1396540 2825866 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Dibromochloromethane AveCBNZ d5 +++++ 11649 29849 350577 817529 1203420 1516624 3009450 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,2-Dibromoethane AveCBNZ d5 +++++ 12109 30283 329937 708037 1057924 1428119 2931683 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Chlorobenzene AveCBNZ d5 +++++ 19147 47429 494516 1045508 1543223 2085187 4263216 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Ethylbenzene AveCBNZ d5 +++++ 31301 75794 812366 1728309 2567163 3466791 7051388 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Nonane AveCBNZ d5 +++++ 14134 35358 374634 792992 1171399 1572372 3170907 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 m,p-Xylene AveCBNZ d5 +++++ 23957 59169 638664 1376844 2058035 2770904 5559936 +++++ 0.401 1.00 9.99 20.0 30.0 40.0 80.0 Xylene, o-AveCBNZ d5 +++++ 11943 28401 306335 655855 983367 1338225 2735040 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Styrene AveCBNZ d5 +++++ 15804 40550 477159 1053703 1581739 2112310 4432021 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Bromoform AveCBNZ d5 +++++ 8204 24470 294330 811246 1176747 1201332 2202241 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Cumene AveCBNZ d5 +++++ 33654 82488 913392 1961615 2933654 3971271 7969390 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,1,2,2-Tetrachloroethane AveCBNZ d5 +++++ 17408 43429 467499 998334 1478298 1998321 3909363 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Propylbenzene AveCBNZ d5 +++++ 41771 103668 1128783 2440180 3642200 4886538 9477791 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,2,3-Trichloropropane AveCBNZ d5 +++++ +++++ 36519 377004 803694 1195200 1603715 3151465 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 n-Decane AveCBNZ d5 +++++ +++++ 44547 496909 1066104 1557969 1962194 3571786 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 4-Ethyltoluene AveCBNZ d5 +++++ 33620 83787 953322 2080218 3088837 4025397 6935560 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 2-Chlorotoluene AveCBNZ d5 +++++ 29843 72493 804876 1755115 2603346 3448505 6144439 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,3,5-Trimethylbenzene AveCBNZ d5 +++++ 28076 69520 780963 1695476 2535147 3332133 6495727 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Alpha Methyl Styrene AveCBNZ d5 +++++ 11436 29470 373692 832783 1253371 1607966 3234283 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 tert-Butylbenzene AveCBNZ d5 +++++ 26585 64273 734383 1581627 2367838 3088186 6030821 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 FORM VI TO-15 Page 447 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-40706-1 CHX.i Analy Batch No.:122454 38271Calibration Start Date:Calibration End Date:10/23/2017 16:35 N 10/24/2017 00:08 GC Column:RTX-624 ID:0.32(mm) RESPONSE AND CONCENTRATION ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (PPB V/V) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 6 LVL 7 LVL 8 1,2,4-Trimethylbenzene AveCBNZ d5 +++++ 27986 69268 790235 1712441 2536126 3251928 6520552 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 sec-Butylbenzene AveCBNZ d5 +++++ 40531 101312 1134465 2441195 3608548 4619126 9134837 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 4-Isopropyltoluene AveCBNZ d5 +++++ 32459 82009 951060 2068038 2964730 3811339 7686123 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,3-Dichlorobenzene AveCBNZ d5 +++++ 19440 48447 533729 1178891 1765738 2220164 4389130 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,4-Dichlorobenzene AveCBNZ d5 +++++ 19316 48457 529230 1164892 1740852 2148311 4537210 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Benzyl chloride AveCBNZ d5 +++++ 20954 42905 618969 1577518 2263180 2466893 5406703 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Butylbenzene AveCBNZ d5 +++++ 31228 78191 894770 1892250 2655419 3556033 7432450 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Undecane AveCBNZ d5 +++++ +++++ +++++ 483539 935471 1440642 1982050 4088785 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 1,2-Dichlorobenzene AveCBNZ d5 +++++ 18205 45133 497647 1096400 1608570 2013126 4315824 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Dodecane AveCBNZ d5 +++++ +++++ +++++ 351478 678767 1064431 1288717 1952757 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 1,2,4-Trichlorobenzene AveCBNZ d5 +++++ +++++ 33805 335494 756763 1230886 1507194 2970534 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Hexachlorobutadiene AveCBNZ d5 +++++ 12537 30662 320613 674435 1088074 1504634 2530367 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Naphthalene AveCBNZ d5 +++++ +++++ 77542 680215 1732883 2743171 3079216 6466475 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 1,2,3-Trichlorobenzene AveCBNZ d5 +++++ +++++ 31527 304974 667593 1094345 1344526 2229929 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Curve Type Legend: Ave = Average ISTD FORM VI TO-15 Page 448 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:GC Column:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-40725-1 CHX.i Analy Batch No.:122454 38271Calibration Start Date:Calibration End Date:10/23/2017 16:35 N 10/24/2017 00:08 0.32(mm)RTX-624 ID: CURVE EVALUATION Calibration Files: LEVEL: LAB SAMPLE ID:LAB FILE ID: 1Level IC 200-122454/3 27547_03.D 2Level IC 200-122454/4 27547_04.D 3Level IC 200-122454/6 27547_06.D 4Level IC 200-122454/8 27547_08.D 5Level ICIS 200-122454/9 27547_09.D 6Level IC 200-122454/10 27547_10.D 7Level IC 200-122454/11 27547_11.D 8Level IC 200-122454/12 27547_12.D ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 #%RSD # MAX %RSD R^2 OR COD # MIN R^2 OR COD MIN RRF LVL 6 LVL 7 LVL 8 Propylene +++++ +++++ +++++ 0.6681 0.6639 Ave 10.3 0.6069 0.5721 0.5215 30.00.6065 Dichlorodifluoromethane +++++ +++++ 2.2330 2.4666 2.5022 Ave 10.5 2.2959 2.0532 1.8970 30.02.2413 Freon 22 +++++ +++++ 1.4326 1.4420 1.4468 Ave 9.1 1.3259 1.2518 1.1503 30.01.3416 1,2-Dichlorotetrafluoroethane +++++ 2.3225 2.3597 2.4932 2.4848 Ave 8.2 2.2915 2.1607 1.9545 30.02.2953 Chloromethane +++++ +++++ 0.8460 0.8453 0.8513 Ave 9.3 0.7745 0.7300 0.6752 30.00.7870 n-Butane +++++ +++++ 1.4856 1.3901 1.3764 Ave 11.5 1.2522 1.1737 1.0873 30.01.2942 Vinyl chloride 0.9285 0.9080 0.9299 1.0031 1.0040 Ave 7.3 0.9181 0.8691 0.7998 30.00.9201 1,3-Butadiene 0.7219 0.7134 0.7023 0.7250 0.7308 Ave 7.5 0.6680 0.6390 0.5851 30.00.6857 Bromomethane +++++ 0.8294 0.8209 0.8623 0.8741 Ave 7.4 0.8010 0.7651 0.6995 30.00.8075 Chloroethane +++++ +++++ 0.4845 0.4847 0.4863 Ave 8.9 0.4478 0.4225 0.3897 30.00.4526 Isopentane +++++ 1.2102 0.9642 0.9718 0.9489 Ave 15.7 0.8672 0.8170 0.7570 30.00.9338 Bromoethene(Vinyl Bromide)+++++ 0.8479 0.8659 0.9318 0.9401 Ave 6.3 0.8793 0.8420 0.7821 30.00.8699 Trichlorofluoromethane +++++ 2.4469 2.4687 2.5727 2.5950 Ave 6.5 2.4123 2.3155 2.1372 30.02.4212 n-Pentane +++++ +++++ 1.6602 1.5865 1.5738 Ave 10.6 1.4359 1.3558 1.2520 30.01.4774 FORM VI TO-15 Note: The M1 coefficient is the same as Ave RRF for an Ave curve type. Page 449 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:GC Column:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-40725-1 CHX.i Analy Batch No.:122454 38271Calibration Start Date:Calibration End Date:10/23/2017 16:35 N 10/24/2017 00:08 0.32(mm)RTX-624 ID: CURVE EVALUATION ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 #%RSD # MAX %RSD R^2 OR COD # MIN R^2 OR COD MIN RRF LVL 6 LVL 7 LVL 8 Ethanol +++++ +++++ 0.5535 0.4952 0.4427 Ave 19.6 0.4320 0.3629 0.3192 30.00.4343 Ethyl ether +++++ 0.6451 0.6298 0.6564 0.6664 Ave 6.9 0.6173 0.5870 0.5435 30.00.6208 Acrolein +++++ +++++ +++++ 0.2574 0.3221 Ave 14.5 0.2730 0.2352 0.2251 30.00.2626 Freon TF +++++ 1.7830 1.8081 1.8759 1.8861 Ave 7.2 1.7399 1.6647 1.5286 30.01.7552 1,1-Dichloroethene +++++ 0.8747 0.8526 0.8926 0.9075 Ave 6.5 0.8343 0.8067 0.7482 30.00.8452 Acetone +++++ +++++ +++++ 1.3834 1.2858 Ave 10.3 1.1941 1.1589 1.0562 30.01.2157 Carbon disulfide +++++ +++++ 2.4855 2.5937 2.5965 Ave 7.9 2.3967 2.2784 2.1105 30.02.4102 Isopropyl alcohol +++++ +++++ +++++ 1.5962 1.5350 Ave 8.1 1.3903 1.4342 1.2993 30.01.4510 3-Chloropropene +++++ 1.0982 0.9790 0.9524 1.1472 Ave 12.7 1.0281 0.8581 0.7968 30.00.9800 Acetonitrile +++++ +++++ +++++ 0.6817 0.6626 Ave 9.3 0.5826 0.5833 0.5503 30.00.6121 Methylene Chloride +++++ +++++ 1.0509 1.0650 1.0553 Ave 9.2 0.9654 0.9132 0.8461 30.00.9827 tert-Butyl alcohol +++++ +++++ +++++ 2.1253 2.0887 Ave 6.3 1.9174 1.9648 1.8196 30.01.9832 Methyl tert-butyl ether +++++ 2.6676 2.7703 2.8831 2.9016 Ave 6.8 2.6948 2.5693 2.3781 30.02.6950 trans-1,2-Dichloroethene +++++ 1.3656 1.3686 1.4771 1.4678 Ave 7.9 1.3464 1.2769 1.1701 30.01.3532 Acrylonitrile +++++ +++++ 0.6778 0.6935 0.7023 Ave 7.4 0.6445 0.6190 0.5769 30.00.6523 n-Hexane +++++ 1.5200 1.5132 1.5330 1.5253 Ave 8.6 1.3956 1.3262 1.2194 30.01.4332 1,1-Dichloroethane 1.6588 1.7944 1.8060 1.8733 1.8701 Ave 7.1 1.7202 1.6396 1.5190 30.01.7352 Vinyl acetate +++++ +++++ +++++ 2.3609 2.3781 Ave 8.4 2.1828 2.0718 1.9499 30.02.1887 cis-1,2-Dichloroethene +++++ 1.0323 1.0402 1.0885 1.1012 Ave 5.5 1.0305 0.9932 0.9337 30.01.0314 Methyl Ethyl Ketone +++++ +++++ 0.6088 0.5397 0.5468 Ave 9.2 0.5092 0.4996 0.4671 30.00.5285 FORM VI TO-15 Note: The M1 coefficient is the same as Ave RRF for an Ave curve type. Page 450 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:GC Column:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-40725-1 CHX.i Analy Batch No.:122454 38271Calibration Start Date:Calibration End Date:10/23/2017 16:35 N 10/24/2017 00:08 0.32(mm)RTX-624 ID: CURVE EVALUATION ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 #%RSD # MAX %RSD R^2 OR COD # MIN R^2 OR COD MIN RRF LVL 6 LVL 7 LVL 8 Ethyl acetate +++++ +++++ +++++ 0.0818 0.0818 Ave 5.5 0.0788 0.0762 0.0715 30.00.0780 Tetrahydrofuran +++++ +++++ +++++ 0.2267 0.2270 Ave 8.5 0.2063 0.1971 0.1872 30.00.2088 Chloroform +++++ 2.1917 2.1373 2.2309 2.2629 Ave 5.3 2.1198 2.0481 1.9332 30.02.1320 Cyclohexane +++++ 0.2658 0.2807 0.2926 0.2990 Ave 5.3 0.2791 0.2686 0.2574 30.00.2776 1,1,1-Trichloroethane +++++ 0.4274 0.4247 0.4562 0.4671 Ave 4.6 0.4371 0.4237 0.4094 30.00.4351 Carbon tetrachloride 0.3979 0.4060 0.4021 0.4570 0.4858 Ave 7.2 0.4531 0.4337 0.4269 30.00.4328 2,2,4-Trimethylpentane +++++ 1.0074 1.0168 1.0580 1.0755 Ave 5.3 0.9971 0.9589 0.9217 30.01.0050 Benzene +++++ 0.6484 0.6293 0.6635 0.6778 Ave 4.6 0.6331 0.6122 0.5928 30.00.6367 1,2-Dichloroethane +++++ 0.2671 0.2686 0.2835 0.2877 Ave 4.8 0.2676 0.2595 0.2509 30.00.2693 n-Heptane +++++ 0.3594 0.3625 0.3621 0.3673 Ave 6.2 0.3395 0.3242 0.3125 30.00.3468 n-Butanol +++++ +++++ +++++ 0.1230 0.1185 Ave 3.5 0.1114 0.1187 0.1181 30.00.1179 Trichloroethene 0.2718 0.2635 0.2651 0.2803 0.2899 Ave 3.2 0.2738 0.2695 0.2681 30.00.2728 1,2-Dichloropropane +++++ 0.2228 0.2190 0.2312 0.2402 Ave 4.1 0.2242 0.2174 0.2131 30.00.2240 Methyl methacrylate +++++ +++++ 0.2018 0.2201 0.2311 Ave 4.5 0.2201 0.2142 0.2135 30.00.2168 1,4-Dioxane +++++ +++++ +++++ 0.1414 0.1370 Ave 4.0 0.1276 0.1383 0.1319 30.00.1352 Dibromomethane +++++ 0.2506 0.2404 0.2643 0.2724 Ave 4.4 0.2617 0.2660 0.2712 30.00.2609 Bromodichloromethane +++++ 0.4016 0.4056 0.4554 0.4863 Ave 6.8 0.4588 0.4404 0.4344 30.00.4404 cis-1,3-Dichloropropene +++++ 0.3205 0.3169 0.3503 0.3682 Ave 5.2 0.3474 0.3375 0.3344 30.00.3393 methyl isobutyl ketone +++++ +++++ 0.4568 0.4512 0.4654 Ave 5.1 0.4354 0.4197 0.4084 30.00.4395 Toluene +++++ 0.5106 0.4959 0.5187 0.5410 Ave 3.5 0.5132 0.4932 0.4901 30.00.5089 FORM VI TO-15 Note: The M1 coefficient is the same as Ave RRF for an Ave curve type. Page 451 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:GC Column:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-40725-1 CHX.i Analy Batch No.:122454 38271Calibration Start Date:Calibration End Date:10/23/2017 16:35 N 10/24/2017 00:08 0.32(mm)RTX-624 ID: CURVE EVALUATION ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 #%RSD # MAX %RSD R^2 OR COD # MIN R^2 OR COD MIN RRF LVL 6 LVL 7 LVL 8 n-Octane +++++ 0.4575 0.4640 0.4897 0.5017 Ave 4.7 0.4680 0.4513 0.4391 30.00.4673 trans-1,3-Dichloropropene +++++ 0.4782 0.4726 0.3679 0.3858 Ave 13.7 0.3644 0.3671 0.3471 30.00.3976 1,1,2-Trichloroethane +++++ 0.2502 0.2470 0.2593 0.2704 Ave 3.8 0.2558 0.2461 0.2426 30.00.2531 Tetrachloroethene 0.3860 0.4167 0.4045 0.4269 0.4487 Ave 4.5 0.4348 0.4250 0.4260 30.00.4211 Methyl Butyl Ketone (2-Hexanone)+++++ +++++ 0.6353 0.4896 0.5109 Ave 13.6 0.4831 0.4547 0.4482 30.00.5036 Dibromochloromethane +++++ 0.4195 0.4326 0.5111 0.5831 Ave 12.0 0.5516 0.4937 0.4773 30.00.4956 1,2-Dibromoethane +++++ 0.4361 0.4389 0.4810 0.5050 Ave 5.3 0.4849 0.4649 0.4650 30.00.4680 Chlorobenzene +++++ 0.6896 0.6873 0.7210 0.7458 Ave 3.6 0.7074 0.6789 0.6762 30.00.7009 Ethylbenzene +++++ 1.1273 1.0984 1.1844 1.2328 Ave 4.1 1.1768 1.1286 1.1184 30.01.1524 n-Nonane +++++ 0.5090 0.5124 0.5462 0.5656 Ave 4.5 0.5370 0.5119 0.5029 30.00.5264 m,p-Xylene +++++ 0.4314 0.4287 0.4656 0.4910 Ave 5.0 0.4717 0.4510 0.4409 30.00.4543 Xylene, o-+++++ 0.4301 0.4116 0.4466 0.4678 Ave 4.0 0.4508 0.4357 0.4338 30.00.4395 Styrene +++++ 0.5692 0.5876 0.6957 0.7516 Ave 10.2 0.7251 0.6877 0.7030 30.00.6743 Bromoform +++++ 0.2955 0.3546 0.4291 0.5787 Ave 24.8 0.5394 0.3911 0.3493 30.00.4197 Cumene +++++ 1.2120 1.1954 1.3317 1.3992 Ave 5.7 1.3448 1.2929 1.2640 30.01.2914 1,1,2,2-Tetrachloroethane +++++ 0.6269 0.6294 0.6816 0.7121 Ave 5.3 0.6776 0.6506 0.6201 30.00.6569 n-Propylbenzene +++++ 1.5044 1.5023 1.6457 1.7406 Ave 6.0 1.6695 1.5909 1.5033 30.01.5938 1,2,3-Trichloropropane +++++ +++++ 0.5292 0.5497 0.5733 Ave 4.8 0.5479 0.5221 0.4999 30.00.5370 n-Decane +++++ +++++ 0.6456 0.7245 0.7604 Ave 10.5 0.7142 0.6388 0.5665 30.00.6750 4-Ethyltoluene +++++ 1.2108 1.2142 1.3899 1.4838 Ave 10.4 1.4159 1.3105 1.1001 30.01.3036 FORM VI TO-15 Note: The M1 coefficient is the same as Ave RRF for an Ave curve type. Page 452 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:GC Column:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-40725-1 CHX.i Analy Batch No.:122454 38271Calibration Start Date:Calibration End Date:10/23/2017 16:35 N 10/24/2017 00:08 0.32(mm)RTX-624 ID: CURVE EVALUATION ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 #%RSD # MAX %RSD R^2 OR COD # MIN R^2 OR COD MIN RRF LVL 6 LVL 7 LVL 8 2-Chlorotoluene +++++ 1.0748 1.0506 1.1735 1.2519 Ave 8.4 1.1933 1.1227 0.9746 30.01.1202 1,3,5-Trimethylbenzene +++++ 1.0111 1.0075 1.1386 1.2094 Ave 7.3 1.1621 1.0848 1.0303 30.01.0920 Alpha Methyl Styrene +++++ 0.4119 0.4271 0.5448 0.5940 Ave 13.6 0.5745 0.5235 0.5130 30.00.5127 tert-Butylbenzene +++++ 0.9574 0.9314 1.0707 1.1282 Ave 7.4 1.0854 1.0054 0.9566 30.01.0193 1,2,4-Trimethylbenzene +++++ 1.0079 1.0038 1.1521 1.2215 Ave 7.9 1.1625 1.0587 1.0342 30.01.0915 sec-Butylbenzene +++++ 1.4597 1.4682 1.6540 1.7413 Ave 7.6 1.6541 1.5038 1.4489 30.01.5614 4-Isopropyltoluene +++++ 1.1690 1.1885 1.3866 1.4751 Ave 9.0 1.3590 1.2408 1.2191 30.01.2912 1,3-Dichlorobenzene +++++ 0.7001 0.7021 0.7782 0.8409 Ave 7.9 0.8094 0.7228 0.6962 30.00.7499 1,4-Dichlorobenzene +++++ 0.6957 0.7022 0.7716 0.8309 Ave 7.3 0.7980 0.6994 0.7197 30.00.7453 Benzyl chloride +++++ 0.7546 0.6218 0.9024 1.1252 Ave 19.5 1.0374 0.8031 0.8576 30.00.8717 n-Butylbenzene +++++ 1.1247 1.1331 1.3046 1.3497 Ave 7.2 1.2172 1.1577 1.1789 30.01.2094 n-Undecane +++++ +++++ +++++ 0.7050 0.6673 Ave 3.6 0.6604 0.6453 0.6485 30.00.6653 1,2-Dichlorobenzene +++++ 0.6556 0.6541 0.7256 0.7821 Ave 7.2 0.7374 0.6554 0.6845 30.00.6992 n-Dodecane +++++ +++++ +++++ 0.5124 0.4842 Ave 18.5 0.4879 0.4196 0.3097 30.00.4428 1,2,4-Trichlorobenzene +++++ +++++ 0.4899 0.4891 0.5398 Ave 7.1 0.5642 0.4907 0.4712 30.00.5075 Hexachlorobutadiene +++++ 0.4515 0.4443 0.4674 0.4811 Ave 7.2 0.4988 0.4898 0.4013 30.00.4620 Naphthalene +++++ +++++ 1.1237 0.9917 1.2361 Ave 10.7 1.2574 1.0025 1.0257 30.01.1062 1,2,3-Trichlorobenzene +++++ +++++ 0.4569 0.4446 0.4762 Ave 11.3 0.5016 0.4377 0.3537 30.00.4451 FORM VI TO-15 Note: The M1 coefficient is the same as Ave RRF for an Ave curve type. Page 453 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-40725-1 CHX.i Analy Batch No.:122454 38271Calibration Start Date:Calibration End Date:10/23/2017 16:35 N 10/24/2017 00:08 GC Column:RTX-624 ID:0.32(mm) RESPONSE AND CONCENTRATION Calibration Files: LEVEL: LAB SAMPLE ID:LAB FILE ID: Level 1 IC 200-122454/3 27547_03.D Level 2 IC 200-122454/4 27547_04.D Level 3 IC 200-122454/6 27547_06.D Level 4 IC 200-122454/8 27547_08.D Level 5 ICIS 200-122454/9 27547_09.D Level 6 IC 200-122454/10 27547_10.D Level 7 IC 200-122454/11 27547_11.D Level 8 IC 200-122454/12 27547_12.D ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (PPB V/V) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 6 LVL 7 LVL 8 Propylene AveBCM +++++ +++++ +++++ 102553 209088 295665 383329 733525 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Dichlorodifluoromethane AveBCM +++++ +++++ 34132 378619 788068 1118396 1375810 2668106 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Freon 22 AveBCM +++++ +++++ 21898 221348 455675 645875 838809 1617809 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 1,2-Dichlorotetrafluoroethane AveBCM +++++ 14311 36069 382702 782560 1116258 1447830 2748966 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Chloromethane AveBCM +++++ +++++ 12931 129755 268108 377289 489178 949589 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 n-Butane AveBCM +++++ +++++ 22707 213381 433493 609985 786455 1529255 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Vinyl chloride AveBCM 1002 5595 14213 153984 316190 447253 582341 1124828 0.0351 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,3-Butadiene AveBCM 779 4396 10735 111292 230152 325381 428200 822928 0.0351 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Bromomethane AveBCM +++++ 5111 12547 132363 275306 390212 512654 983760 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Chloroethane AveBCM +++++ +++++ 7405 74395 153171 218149 283094 548111 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Isopentane AveBCM +++++ 7457 14738 149178 298865 422428 547443 1064662 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Bromoethene(Vinyl Bromide)AveBCM +++++ 5225 13236 143039 296073 428347 564215 1099998 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Trichlorofluoromethane AveBCM +++++ 15078 37735 394919 817285 1175116 1551534 3005949 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Pentane AveBCM +++++ +++++ 25376 243529 495676 699485 908464 1760850 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Ethanol AveBCM +++++ +++++ 84710 152112 209223 281207 486444 1122438 +++++ +++++ 5.01 9.99 15.0 20.0 40.0 100.0 FORM VI TO-15 Page 454 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-40725-1 CHX.i Analy Batch No.:122454 38271Calibration Start Date:Calibration End Date:10/23/2017 16:35 N 10/24/2017 00:08 GC Column:RTX-624 ID:0.32(mm) RESPONSE AND CONCENTRATION ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (PPB V/V) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 6 LVL 7 LVL 8 Ethyl ether AveBCM +++++ 3975 9626 100756 209888 300719 393347 764379 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Acrolein AveBCM +++++ +++++ +++++ 39513 101444 133002 157585 316543 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Freon TF AveBCM +++++ 10987 27637 287954 594002 847569 1115468 2149853 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,1-Dichloroethene AveBCM +++++ 5390 13032 137018 285811 406393 540532 1052382 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Acetone AveBCM +++++ +++++ +++++ 212360 404965 581667 776574 1485543 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Carbon disulfide AveBCM +++++ +++++ 37992 398140 817739 1167488 1526687 2968327 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Isopropyl alcohol AveBCM +++++ +++++ +++++ 245011 483454 677260 961000 1827406 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 3-Chloropropene AveBCM +++++ 6767 14964 146189 361320 500834 574993 1120688 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Acetonitrile AveBCM +++++ +++++ +++++ 104645 208675 283793 390879 773944 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Methylene Chloride AveBCM +++++ +++++ 16064 163475 332375 470285 611891 1190051 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 tert-Butyl alcohol AveBCM +++++ +++++ +++++ 326233 657838 934046 1316584 2559163 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Methyl tert-butyl ether AveBCM +++++ 16438 42344 442553 913845 1312746 1721648 3344671 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 trans-1,2-Dichloroethene AveBCM +++++ 8415 20920 226737 462280 655879 855597 1645639 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Acrylonitrile AveBCM +++++ +++++ 10361 106449 221179 313942 414760 811440 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 n-Hexane AveBCM +++++ 9366 23130 235318 480401 679826 888634 1714976 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,1-Dichloroethane AveBCM 1790 11057 27605 287553 588966 837948 1098640 2136445 0.0351 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Vinyl acetate AveBCM +++++ +++++ +++++ 362399 748981 1063297 1388261 2742463 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 cis-1,2-Dichloroethene AveBCM +++++ 6361 15899 167086 346817 501982 665524 1313245 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Methyl Ethyl Ketone AveBCM +++++ +++++ 9306 82840 172222 248067 334785 656964 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Ethyl acetate AveBCM +++++ +++++ +++++ 12554 25765 38394 51082 100588 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Tetrahydrofuran AveDFBZ +++++ +++++ +++++ 175579 359954 510836 673815 1317270 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 FORM VI TO-15 Page 455 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-40725-1 CHX.i Analy Batch No.:122454 38271Calibration Start Date:Calibration End Date:10/23/2017 16:35 N 10/24/2017 00:08 GC Column:RTX-624 ID:0.32(mm) RESPONSE AND CONCENTRATION ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (PPB V/V) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 6 LVL 7 LVL 8 Chloroform AveBCM +++++ 13505 32669 342441 712688 1032623 1372381 2719039 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Cyclohexane AveDFBZ +++++ 8548 22138 226698 474143 691140 918510 1811063 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,1,1-Trichloroethane AveDFBZ +++++ 13743 33489 353378 740782 1082206 1448598 2880937 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Carbon tetrachloride AveDFBZ 2265 13056 31710 354012 770388 1121989 1482862 3003863 0.0351 0.200 0.500 4.99 10.00 15.0 20.0 40.0 2,2,4-Trimethylpentane AveDFBZ +++++ 32393 80184 819590 1705633 2468728 3278556 6485246 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Benzene AveDFBZ +++++ 20850 49626 513943 1075001 1567657 2093114 4171026 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,2-Dichloroethane AveDFBZ +++++ 8590 21182 219600 456212 662579 887163 1765151 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Heptane AveDFBZ +++++ 11556 28584 280503 582478 840512 1108575 2199085 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Butanol AveDFBZ +++++ +++++ +++++ 95269 188013 275873 405781 831088 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Trichloroethene AveDFBZ 1547 8474 20904 217129 459822 678007 921595 1886228 0.0351 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,2-Dichloropropane AveDFBZ +++++ 7164 17269 179114 380868 555075 743330 1499203 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Methyl methacrylate AveDFBZ +++++ +++++ 15911 170513 366543 544893 732558 1502078 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 1,4-Dioxane AveDFBZ +++++ +++++ +++++ 109497 217341 316031 472869 927989 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 Dibromomethane AveDFBZ +++++ 8059 18958 204735 431950 647898 909652 1908419 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Bromodichloromethane AveDFBZ +++++ 12915 31986 352786 771290 1136055 1505805 3056799 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 cis-1,3-Dichloropropene AveDFBZ +++++ 10307 24993 271353 583954 860223 1154046 2353259 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 methyl isobutyl ketone AveDFBZ +++++ +++++ 36019 349498 738112 1077942 1435092 2873471 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Toluene AveCBNZ d5 +++++ 14179 34222 355752 758399 1119474 1514793 3089729 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Octane AveDFBZ +++++ 14711 36592 379330 795715 1158747 1543072 3089403 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 trans-1,3-Dichloropropene AveDFBZ +++++ 15376 37267 284983 611800 902146 1255186 2442595 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,1,2-Trichloroethane AveCBNZ d5 +++++ 6946 17045 177823 379130 557985 755934 1529748 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 FORM VI TO-15 Page 456 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-40725-1 CHX.i Analy Batch No.:122454 38271Calibration Start Date:Calibration End Date:10/23/2017 16:35 N 10/24/2017 00:08 GC Column:RTX-624 ID:0.32(mm) RESPONSE AND CONCENTRATION ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (PPB V/V) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 6 LVL 7 LVL 8 Tetrachloroethene AveCBNZ d5 1912 11571 27911 292834 629100 948589 1305509 2686070 0.0351 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Methyl Butyl Ketone (2-Hexanone)AveCBNZ d5 +++++ +++++ 43837 335774 716248 1053929 1396540 2825866 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Dibromochloromethane AveCBNZ d5 +++++ 11649 29849 350577 817529 1203420 1516624 3009450 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,2-Dibromoethane AveCBNZ d5 +++++ 12109 30283 329937 708037 1057924 1428119 2931683 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Chlorobenzene AveCBNZ d5 +++++ 19147 47429 494516 1045508 1543223 2085187 4263216 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Ethylbenzene AveCBNZ d5 +++++ 31301 75794 812366 1728309 2567163 3466791 7051388 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Nonane AveCBNZ d5 +++++ 14134 35358 374634 792992 1171399 1572372 3170907 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 m,p-Xylene AveCBNZ d5 +++++ 23957 59169 638664 1376844 2058035 2770904 5559936 +++++ 0.401 1.00 9.99 20.0 30.0 40.0 80.0 Xylene, o-AveCBNZ d5 +++++ 11943 28401 306335 655855 983367 1338225 2735040 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Styrene AveCBNZ d5 +++++ 15804 40550 477159 1053703 1581739 2112310 4432021 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Bromoform AveCBNZ d5 +++++ 8204 24470 294330 811246 1176747 1201332 2202241 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Cumene AveCBNZ d5 +++++ 33654 82488 913392 1961615 2933654 3971271 7969390 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,1,2,2-Tetrachloroethane AveCBNZ d5 +++++ 17408 43429 467499 998334 1478298 1998321 3909363 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Propylbenzene AveCBNZ d5 +++++ 41771 103668 1128783 2440180 3642200 4886538 9477791 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,2,3-Trichloropropane AveCBNZ d5 +++++ +++++ 36519 377004 803694 1195200 1603715 3151465 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 n-Decane AveCBNZ d5 +++++ +++++ 44547 496909 1066104 1557969 1962194 3571786 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 4-Ethyltoluene AveCBNZ d5 +++++ 33620 83787 953322 2080218 3088837 4025397 6935560 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 2-Chlorotoluene AveCBNZ d5 +++++ 29843 72493 804876 1755115 2603346 3448505 6144439 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,3,5-Trimethylbenzene AveCBNZ d5 +++++ 28076 69520 780963 1695476 2535147 3332133 6495727 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Alpha Methyl Styrene AveCBNZ d5 +++++ 11436 29470 373692 832783 1253371 1607966 3234283 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 tert-Butylbenzene AveCBNZ d5 +++++ 26585 64273 734383 1581627 2367838 3088186 6030821 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 FORM VI TO-15 Page 457 of 478 FORM VI Lab Name:Job No.: Calibration ID: SDG No.: Instrument ID:Heated Purge: (Y/N) AIR - GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA TestAmerica Burlington 200-40725-1 CHX.i Analy Batch No.:122454 38271Calibration Start Date:Calibration End Date:10/23/2017 16:35 N 10/24/2017 00:08 GC Column:RTX-624 ID:0.32(mm) RESPONSE AND CONCENTRATION ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (PPB V/V) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 6 LVL 7 LVL 8 1,2,4-Trimethylbenzene AveCBNZ d5 +++++ 27986 69268 790235 1712441 2536126 3251928 6520552 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 sec-Butylbenzene AveCBNZ d5 +++++ 40531 101312 1134465 2441195 3608548 4619126 9134837 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 4-Isopropyltoluene AveCBNZ d5 +++++ 32459 82009 951060 2068038 2964730 3811339 7686123 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,3-Dichlorobenzene AveCBNZ d5 +++++ 19440 48447 533729 1178891 1765738 2220164 4389130 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 1,4-Dichlorobenzene AveCBNZ d5 +++++ 19316 48457 529230 1164892 1740852 2148311 4537210 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Benzyl chloride AveCBNZ d5 +++++ 20954 42905 618969 1577518 2263180 2466893 5406703 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Butylbenzene AveCBNZ d5 +++++ 31228 78191 894770 1892250 2655419 3556033 7432450 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Undecane AveCBNZ d5 +++++ +++++ +++++ 483539 935471 1440642 1982050 4088785 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 1,2-Dichlorobenzene AveCBNZ d5 +++++ 18205 45133 497647 1096400 1608570 2013126 4315824 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 n-Dodecane AveCBNZ d5 +++++ +++++ +++++ 351478 678767 1064431 1288717 1952757 +++++ +++++ +++++ 4.99 10.00 15.0 20.0 40.0 1,2,4-Trichlorobenzene AveCBNZ d5 +++++ +++++ 33805 335494 756763 1230886 1507194 2970534 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Hexachlorobutadiene AveCBNZ d5 +++++ 12537 30662 320613 674435 1088074 1504634 2530367 +++++ 0.200 0.500 4.99 10.00 15.0 20.0 40.0 Naphthalene AveCBNZ d5 +++++ +++++ 77542 680215 1732883 2743171 3079216 6466475 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 1,2,3-Trichlorobenzene AveCBNZ d5 +++++ +++++ 31527 304974 667593 1094345 1344526 2229929 +++++ +++++ 0.500 4.99 10.00 15.0 20.0 40.0 Curve Type Legend: Ave = Average ISTD FORM VI TO-15 Page 458 of 478 FORM VII Lab Name:Job No.: SDG No.: Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID: Calib End Date:GC Column: ID: AIR - GC/MS VOA CONTINUING CALIBRATION DATA 0.32(mm) 200-40706-1 CHX.i 10/24/2017 04:21 10/23/2017 16:35 10/24/2017 00:08 ICV 200-122454/17 RTX-624 TestAmerica Burlington Lab File ID:27547_17.D Heated Purge: (Y/N)NConc. Units:ppb v/v ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNT AMOUNT %D AVE RRF RRF MIN RRF Propylene 0.60440.6065 9.96 10.0 -0.3 30.0Ave Dichlorodifluoromethane 2.3302.241 10.4 10.0 4.0 30.0Ave Freon 22 1.3931.342 10.4 10.0 3.8 30.0Ave 1,2-Dichlorotetrafluoroethan e 2.7492.295 12.0 10.0 19.8 30.0Ave Chloromethane 0.79780.7870 10.1 10.0 1.4 30.0Ave n-Butane 1.3031.294 10.1 10.0 0.7 30.0Ave Vinyl chloride 0.95470.9201 10.4 10.0 3.8 30.0Ave 1,3-Butadiene 0.68880.6857 10.0 10.0 0.5 30.0Ave Bromomethane 0.88130.8075 10.9 10.0 9.1 30.0Ave Chloroethane 0.47820.4526 10.6 10.0 5.7 30.0Ave Isopentane 1.0100.9338 10.8 10.0 8.2 30.0Ave Bromoethene(Vinyl Bromide)0.94340.8699 10.8 10.0 8.5 30.0Ave Trichlorofluoromethane 2.5752.421 10.6 10.0 6.4 30.0Ave n-Pentane 1.6651.477 11.3 10.0 12.7 30.0Ave Ethanol 0.42840.4343 14.8 15.0 -1.3 30.0Ave Ethyl ether 0.72610.6208 11.7 10.0 17.0 30.0Ave Acrolein 0.28980.2626 11.0 10.0 10.4 30.0Ave Freon TF 1.9101.755 10.9 10.0 8.8 30.0Ave 1,1-Dichloroethene 0.90560.8452 10.7 10.0 7.1 30.0Ave Acetone 1.3831.216 11.4 10.0 13.8 30.0Ave Carbon disulfide 2.9652.410 12.3 10.0 23.0 30.0Ave Isopropyl alcohol 1.4091.451 9.71 10.0 -2.9 30.0Ave 3-Chloropropene 0.74620.9800 7.61 10.0 -23.9 30.0Ave Acetonitrile 0.72170.6121 11.8 10.0 17.9 30.0Ave Methylene Chloride 1.0170.9827 10.3 10.0 3.5 30.0Ave tert-Butyl alcohol 2.0391.983 10.3 10.0 2.8 30.0Ave Methyl tert-butyl ether 2.8902.695 10.7 10.0 7.2 30.0Ave trans-1,2-Dichloroethene 1.5291.353 11.3 10.0 13.0 30.0Ave Acrylonitrile 0.72530.6523 11.1 10.0 11.2 30.0Ave n-Hexane 1.6051.433 11.2 10.0 12.0 30.0Ave 1,1-Dichloroethane 1.8711.735 10.8 10.0 7.8 30.0Ave Vinyl acetate 2.4292.189 11.1 10.0 11.0 30.0Ave cis-1,2-Dichloroethene 1.1001.031 10.7 10.0 6.7 30.0Ave Methyl Ethyl Ketone 0.55550.5285 10.5 10.0 5.1 30.0Ave Ethyl acetate 0.09120.0780 11.7 10.0 16.9 30.0Ave Tetrahydrofuran 0.22610.2088 10.8 10.0 8.2 30.0Ave Chloroform 2.2932.132 10.8 10.0 7.5 30.0Ave Cyclohexane 0.30810.2776 11.1 10.0 11.0 30.0Ave 1,1,1-Trichloroethane 0.47920.4351 11.0 10.0 10.1 30.0Ave Carbon tetrachloride 0.49270.4328 11.4 10.0 13.8 30.0Ave FORM VII TO-15 Page 459 of 478 FORM VII Lab Name:Job No.: SDG No.: Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID: Calib End Date:GC Column: ID: AIR - GC/MS VOA CONTINUING CALIBRATION DATA 0.32(mm) 200-40706-1 CHX.i 10/24/2017 04:21 10/23/2017 16:35 10/24/2017 00:08 ICV 200-122454/17 RTX-624 TestAmerica Burlington Lab File ID:27547_17.D Heated Purge: (Y/N)NConc. Units:ppb v/v ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNT AMOUNT %D AVE RRF RRF MIN RRF 2,2,4-Trimethylpentane 1.0631.005 10.6 10.0 5.7 30.0Ave Benzene 0.68860.6367 10.8 10.0 8.1 30.0Ave 1,2-Dichloroethane 0.29000.2693 10.8 10.0 7.7 30.0Ave n-Heptane 0.35830.3468 10.3 10.0 3.3 30.0Ave n-Butanol 0.13860.1179 11.7 10.0 17.5 30.0Ave Trichloroethene 0.31370.2728 11.5 10.0 15.0 30.0Ave 1,2-Dichloropropane 0.23500.2240 10.5 10.0 4.9 30.0Ave Methyl methacrylate 0.23360.2168 10.8 10.0 7.8 30.0Ave 1,4-Dioxane 0.14570.1352 10.8 10.0 7.7 30.0Ave Dibromomethane 0.29340.2609 11.2 10.0 12.4 30.0Ave Bromodichloromethane 0.46440.4404 10.5 10.0 5.5 30.0Ave cis-1,3-Dichloropropene 0.37020.3393 10.9 10.0 9.1 30.0Ave methyl isobutyl ketone 0.44850.4395 10.2 10.0 2.1 30.0Ave Toluene 0.55570.5089 10.9 10.0 9.2 30.0Ave n-Octane 0.49360.4673 10.6 10.0 5.6 30.0Ave trans-1,3-Dichloropropene 0.38080.3976 9.58 10.0 -4.2 30.0Ave 1,1,2-Trichloroethane 0.27790.2531 11.0 10.0 9.8 30.0Ave Tetrachloroethene 0.47780.4211 11.3 10.0 13.5 30.0Ave Methyl Butyl Ketone (2-Hexanone) 0.50000.5036 9.93 10.0 -0.7 30.0Ave Dibromochloromethane 0.48560.4956 9.80 10.0 -2.0 30.0Ave 1,2-Dibromoethane 0.51810.4680 11.1 10.0 10.7 30.0Ave Chlorobenzene 0.76230.7009 10.9 10.0 8.8 30.0Ave Ethylbenzene 1.2571.152 10.9 10.0 9.1 30.0Ave n-Nonane 0.56520.5264 10.7 10.0 7.4 30.0Ave m,p-Xylene 0.49950.4543 22.0 20.0 9.9 30.0Ave Xylene, o-0.47390.4395 10.8 10.0 7.8 30.0Ave Styrene 0.74300.6743 11.0 10.0 10.2 30.0Ave Bromoform 0.31670.4197 7.54 10.0 -24.5 30.0Ave Cumene 1.4131.291 10.9 10.0 9.4 30.0Ave 1,1,2,2-Tetrachloroethane 0.69580.6569 10.6 10.0 5.9 30.0Ave n-Propylbenzene 1.7381.594 10.9 10.0 9.0 30.0Ave 1,2,3-Trichloropropane 0.57360.5370 10.7 10.0 6.8 30.0Ave n-Decane 0.74810.6750 11.1 10.0 10.8 30.0Ave 2-Chlorotoluene 1.2601.120 11.2 10.0 12.5 30.0Ave 4-Ethyltoluene 1.5281.304 11.7 10.0 17.2 30.0Ave 1,3,5-Trimethylbenzene 1.2291.092 11.3 10.0 12.6 30.0Ave Alpha Methyl Styrene 0.59550.5127 11.6 10.0 16.2 30.0Ave tert-Butylbenzene 1.1591.019 11.4 10.0 13.7 30.0Ave 1,2,4-Trimethylbenzene 1.2301.092 11.3 10.0 12.7 30.0Ave sec-Butylbenzene 1.7701.561 11.3 10.0 13.4 30.0Ave FORM VII TO-15 Page 460 of 478 FORM VII Lab Name:Job No.: SDG No.: Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID: Calib End Date:GC Column: ID: AIR - GC/MS VOA CONTINUING CALIBRATION DATA 0.32(mm) 200-40706-1 CHX.i 10/24/2017 04:21 10/23/2017 16:35 10/24/2017 00:08 ICV 200-122454/17 RTX-624 TestAmerica Burlington Lab File ID:27547_17.D Heated Purge: (Y/N)NConc. Units:ppb v/v ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNT AMOUNT %D AVE RRF RRF MIN RRF 4-Isopropyltoluene 1.5061.291 11.7 10.0 16.6 30.0Ave 1,3-Dichlorobenzene 0.83990.7499 11.2 10.0 12.0 30.0Ave 1,4-Dichlorobenzene 0.81050.7453 10.9 10.0 8.7 30.0Ave Benzyl chloride 0.90740.8717 10.4 10.0 4.1 30.0Ave n-Butylbenzene 1.3701.209 11.3 10.0 13.3 30.0Ave n-Undecane 0.69690.6653 10.5 10.0 4.8 30.0Ave 1,2-Dichlorobenzene 0.79530.6992 11.4 10.0 13.7 30.0Ave n-Dodecane 0.53090.4428 12.0 10.0 19.9 30.0Ave 1,2,4-Trichlorobenzene 0.50670.5075 9.98 10.0 -0.2 30.0Ave Hexachlorobutadiene 0.55390.4620 12.0 10.0 19.9 30.0Ave Naphthalene 0.95581.106 8.64 10.0 -13.6 30.0Ave 1,2,3-Trichlorobenzene 0.48170.4451 10.8 10.0 8.2 30.0Ave FORM VII TO-15 Page 461 of 478 FORM VII Lab Name:Job No.: SDG No.: Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID: Calib End Date:GC Column: ID: AIR - GC/MS VOA CONTINUING CALIBRATION DATA 0.32(mm) 200-40706-1 CHX.i 11/03/2017 12:06 10/23/2017 16:35 10/24/2017 00:08 CCVIS 200-122903/4 RTX-624 TestAmerica Burlington Lab File ID:27725_04.D Heated Purge: (Y/N)NConc. Units:ppb v/v ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNT AMOUNT %D AVE RRF RRF MIN RRF Propylene 0.73610.6065 12.1 10.0 21.4 30.0Ave Dichlorodifluoromethane 2.4022.241 10.7 10.0 7.2 30.0Ave Freon 22 1.5641.342 11.7 10.0 16.6 30.0Ave 1,2-Dichlorotetrafluoroethan e 2.4442.295 10.6 10.0 6.5 30.0Ave Chloromethane 0.89670.7870 11.4 10.0 13.9 30.0Ave n-Butane 1.4991.294 11.6 10.0 15.8 30.0Ave Vinyl chloride 1.0190.9201 11.1 10.0 10.7 30.0Ave 1,3-Butadiene 0.75400.6857 11.0 10.0 10.0 30.0Ave Bromomethane 0.82820.8075 10.3 10.0 2.6 30.0Ave Chloroethane 0.49450.4526 10.9 10.0 9.3 30.0Ave Isopentane 1.0310.9338 11.0 10.0 10.4 30.0Ave Bromoethene(Vinyl Bromide)0.87490.8699 10.1 10.0 0.6 30.0Ave Trichlorofluoromethane 2.5562.421 10.6 10.0 5.6 30.0Ave n-Pentane 1.7201.477 11.6 10.0 16.4 30.0Ave Ethanol 0.46660.4343 16.1 15.0 7.4 30.0Ave Ethyl ether 0.68610.6208 11.1 10.0 10.5 30.0Ave Acrolein 0.32100.2626 12.2 10.0 22.3 30.0Ave Freon TF 1.7901.755 10.2 10.0 2.0 30.0Ave 1,1-Dichloroethene 0.84270.8452 9.97 10.0 -0.3 30.0Ave Acetone 1.4121.216 11.6 10.0 16.2 30.0Ave Carbon disulfide 2.5192.410 10.5 10.0 4.5 30.0Ave Isopropyl alcohol 1.6431.451 11.3 10.0 13.2 30.0Ave 3-Chloropropene 1.2450.9800 12.7 10.0 27.0 30.0Ave Acetonitrile 0.71640.6121 11.7 10.0 17.0 30.0Ave Methylene Chloride 1.1260.9827 11.5 10.0 14.6 30.0Ave tert-Butyl alcohol 2.1691.983 10.9 10.0 9.4 30.0Ave Methyl tert-butyl ether 2.9042.695 10.8 10.0 7.8 30.0Ave trans-1,2-Dichloroethene 1.5111.353 11.2 10.0 11.7 30.0Ave Acrylonitrile 0.73160.6523 11.2 10.0 12.1 30.0Ave n-Hexane 1.5811.433 11.0 10.0 10.3 30.0Ave 1,1-Dichloroethane 1.9221.735 11.1 10.0 10.8 30.0Ave Vinyl acetate 2.5432.189 11.6 10.0 16.2 30.0Ave cis-1,2-Dichloroethene 1.0491.031 10.2 10.0 1.7 30.0Ave Methyl Ethyl Ketone 0.53610.5285 10.1 10.0 1.4 30.0Ave Ethyl acetate 0.07920.0780 10.1 10.0 1.4 30.0Ave Tetrahydrofuran 0.24320.2088 11.6 10.0 16.4 30.0Ave Chloroform 2.1992.132 10.3 10.0 3.1 30.0Ave Cyclohexane 0.28280.2776 10.2 10.0 1.9 30.0Ave 1,1,1-Trichloroethane 0.44450.4351 10.2 10.0 2.2 30.0Ave Carbon tetrachloride 0.44860.4328 10.4 10.0 3.6 30.0Ave FORM VII TO-15 Page 462 of 478 FORM VII Lab Name:Job No.: SDG No.: Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID: Calib End Date:GC Column: ID: AIR - GC/MS VOA CONTINUING CALIBRATION DATA 0.32(mm) 200-40706-1 CHX.i 11/03/2017 12:06 10/23/2017 16:35 10/24/2017 00:08 CCVIS 200-122903/4 RTX-624 TestAmerica Burlington Lab File ID:27725_04.D Heated Purge: (Y/N)NConc. Units:ppb v/v ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNT AMOUNT %D AVE RRF RRF MIN RRF 2,2,4-Trimethylpentane 1.0921.005 10.9 10.0 8.7 30.0Ave Benzene 0.64820.6367 10.2 10.0 1.8 30.0Ave 1,2-Dichloroethane 0.29020.2693 10.8 10.0 7.8 30.0Ave n-Heptane 0.38210.3468 11.0 10.0 10.2 30.0Ave n-Butanol 0.11670.1179 9.89 10.0 -1.1 30.0Ave Trichloroethene 0.26720.2728 9.79 10.0 -2.0 30.0Ave 1,2-Dichloropropane 0.23470.2240 10.5 10.0 4.8 30.0Ave Methyl methacrylate 0.21750.2168 10.0 10.0 0.3 30.0Ave 1,4-Dioxane 0.12550.1352 9.27 10.0 -7.2 30.0Ave Dibromomethane 0.22590.2609 8.66 10.0 -13.4 30.0Ave Bromodichloromethane 0.45430.4404 10.3 10.0 3.2 30.0Ave cis-1,3-Dichloropropene 0.34980.3393 10.3 10.0 3.1 30.0Ave methyl isobutyl ketone 0.46970.4395 10.7 10.0 6.9 30.0Ave Toluene 0.48810.5089 9.59 10.0 -4.1 30.0Ave n-Octane 0.51510.4673 11.0 10.0 10.2 30.0Ave trans-1,3-Dichloropropene 0.36300.3976 9.13 10.0 -8.7 30.0Ave 1,1,2-Trichloroethane 0.25280.2531 9.99 10.0 -0.1 30.0Ave Tetrachloroethene 0.37650.4211 8.94 10.0 -10.6 30.0Ave Methyl Butyl Ketone (2-Hexanone) 0.50850.5036 10.1 10.0 1.0 30.0Ave Dibromochloromethane 0.50220.4956 10.1 10.0 1.3 30.0Ave 1,2-Dibromoethane 0.45330.4680 9.68 10.0 -3.1 30.0Ave Chlorobenzene 0.65920.7009 9.40 10.0 -5.9 30.0Ave Ethylbenzene 1.1211.152 9.73 10.0 -2.7 30.0Ave n-Nonane 0.55830.5264 10.6 10.0 6.1 30.0Ave m,p-Xylene 0.43720.4543 19.2 20.0 -3.8 30.0Ave Xylene, o-0.41640.4395 9.47 10.0 -5.2 30.0Ave Styrene 0.64240.6743 9.53 10.0 -4.7 30.0Ave Bromoform 0.47320.4197 11.3 10.0 12.7 30.0Ave Cumene 1.2511.291 9.69 10.0 -3.1 30.0Ave 1,1,2,2-Tetrachloroethane 0.66840.6569 10.2 10.0 1.7 30.0Ave n-Propylbenzene 1.5911.594 9.98 10.0 -0.2 30.0Ave 1,2,3-Trichloropropane 0.54830.5370 10.2 10.0 2.1 30.0Ave n-Decane 0.77040.6750 11.4 10.0 14.1 30.0Ave 4-Ethyltoluene 1.3501.304 10.4 10.0 3.6 30.0Ave 2-Chlorotoluene 1.1711.120 10.5 10.0 4.5 30.0Ave 1,3,5-Trimethylbenzene 1.0801.092 9.89 10.0 -1.1 30.0Ave Alpha Methyl Styrene 0.50200.5127 9.79 10.0 -2.1 30.0Ave tert-Butylbenzene 0.99431.019 9.75 10.0 -2.4 30.0Ave 1,2,4-Trimethylbenzene 1.0881.092 9.97 10.0 -0.3 30.0Ave sec-Butylbenzene 1.5661.561 10.0 10.0 0.3 30.0Ave FORM VII TO-15 Page 463 of 478 FORM VII Lab Name:Job No.: SDG No.: Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID: Calib End Date:GC Column: ID: AIR - GC/MS VOA CONTINUING CALIBRATION DATA 0.32(mm) 200-40706-1 CHX.i 11/03/2017 12:06 10/23/2017 16:35 10/24/2017 00:08 CCVIS 200-122903/4 RTX-624 TestAmerica Burlington Lab File ID:27725_04.D Heated Purge: (Y/N)NConc. Units:ppb v/v ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNT AMOUNT %D AVE RRF RRF MIN RRF 4-Isopropyltoluene 1.3051.291 10.1 10.0 1.0 30.0Ave 1,3-Dichlorobenzene 0.70870.7499 9.45 10.0 -5.5 30.0Ave 1,4-Dichlorobenzene 0.69020.7453 9.26 10.0 -7.4 30.0Ave Benzyl chloride 0.99400.8717 11.4 10.0 14.0 30.0Ave n-Butylbenzene 1.2741.209 10.5 10.0 5.4 30.0Ave n-Undecane 0.69730.6653 10.5 10.0 4.8 30.0Ave 1,2-Dichlorobenzene 0.65720.6992 9.40 10.0 -6.0 30.0Ave n-Dodecane 0.46900.4428 10.6 10.0 5.9 30.0Ave 1,2,4-Trichlorobenzene 0.41220.5075 8.12 10.0 -18.8 30.0Ave Hexachlorobutadiene 0.38890.4620 8.41 10.0 -15.8 30.0Ave Naphthalene 0.98841.106 8.93 10.0 -10.6 30.0Ave 1,2,3-Trichlorobenzene 0.38730.4451 8.70 10.0 -13.0 30.0Ave FORM VII TO-15 Page 464 of 478 FORM VII Lab Name:Job No.: SDG No.: Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID: Calib End Date:GC Column: ID: AIR - GC/MS VOA CONTINUING CALIBRATION DATA 0.32(mm) 200-40725-1 CHX.i 10/24/2017 04:21 10/23/2017 16:35 10/24/2017 00:08 ICV 200-122454/17 RTX-624 TestAmerica Burlington Lab File ID:27547_17.D Heated Purge: (Y/N)NConc. Units:ppb v/v ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNT AMOUNT %D AVE RRF RRF MIN RRF Propylene 0.60440.6065 9.96 10.0 -0.3 30.0Ave Dichlorodifluoromethane 2.3302.241 10.4 10.0 4.0 30.0Ave Freon 22 1.3931.342 10.4 10.0 3.8 30.0Ave 1,2-Dichlorotetrafluoroethan e 2.7492.295 12.0 10.0 19.8 30.0Ave Chloromethane 0.79780.7870 10.1 10.0 1.4 30.0Ave n-Butane 1.3031.294 10.1 10.0 0.7 30.0Ave Vinyl chloride 0.95470.9201 10.4 10.0 3.8 30.0Ave 1,3-Butadiene 0.68880.6857 10.0 10.0 0.5 30.0Ave Bromomethane 0.88130.8075 10.9 10.0 9.1 30.0Ave Chloroethane 0.47820.4526 10.6 10.0 5.7 30.0Ave Isopentane 1.0100.9338 10.8 10.0 8.2 30.0Ave Bromoethene(Vinyl Bromide)0.94340.8699 10.8 10.0 8.5 30.0Ave Trichlorofluoromethane 2.5752.421 10.6 10.0 6.4 30.0Ave n-Pentane 1.6651.477 11.3 10.0 12.7 30.0Ave Ethanol 0.42840.4343 14.8 15.0 -1.3 30.0Ave Ethyl ether 0.72610.6208 11.7 10.0 17.0 30.0Ave Acrolein 0.28980.2626 11.0 10.0 10.4 30.0Ave Freon TF 1.9101.755 10.9 10.0 8.8 30.0Ave 1,1-Dichloroethene 0.90560.8452 10.7 10.0 7.1 30.0Ave Acetone 1.3831.216 11.4 10.0 13.8 30.0Ave Carbon disulfide 2.9652.410 12.3 10.0 23.0 30.0Ave Isopropyl alcohol 1.4091.451 9.71 10.0 -2.9 30.0Ave 3-Chloropropene 0.74620.9800 7.61 10.0 -23.9 30.0Ave Acetonitrile 0.72170.6121 11.8 10.0 17.9 30.0Ave Methylene Chloride 1.0170.9827 10.3 10.0 3.5 30.0Ave tert-Butyl alcohol 2.0391.983 10.3 10.0 2.8 30.0Ave Methyl tert-butyl ether 2.8902.695 10.7 10.0 7.2 30.0Ave trans-1,2-Dichloroethene 1.5291.353 11.3 10.0 13.0 30.0Ave Acrylonitrile 0.72530.6523 11.1 10.0 11.2 30.0Ave n-Hexane 1.6051.433 11.2 10.0 12.0 30.0Ave 1,1-Dichloroethane 1.8711.735 10.8 10.0 7.8 30.0Ave Vinyl acetate 2.4292.189 11.1 10.0 11.0 30.0Ave cis-1,2-Dichloroethene 1.1001.031 10.7 10.0 6.7 30.0Ave Methyl Ethyl Ketone 0.55550.5285 10.5 10.0 5.1 30.0Ave Ethyl acetate 0.09120.0780 11.7 10.0 16.9 30.0Ave Tetrahydrofuran 0.22610.2088 10.8 10.0 8.2 30.0Ave Chloroform 2.2932.132 10.8 10.0 7.5 30.0Ave Cyclohexane 0.30810.2776 11.1 10.0 11.0 30.0Ave 1,1,1-Trichloroethane 0.47920.4351 11.0 10.0 10.1 30.0Ave Carbon tetrachloride 0.49270.4328 11.4 10.0 13.8 30.0Ave FORM VII TO-15 Page 465 of 478 FORM VII Lab Name:Job No.: SDG No.: Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID: Calib End Date:GC Column: ID: AIR - GC/MS VOA CONTINUING CALIBRATION DATA 0.32(mm) 200-40725-1 CHX.i 10/24/2017 04:21 10/23/2017 16:35 10/24/2017 00:08 ICV 200-122454/17 RTX-624 TestAmerica Burlington Lab File ID:27547_17.D Heated Purge: (Y/N)NConc. Units:ppb v/v ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNT AMOUNT %D AVE RRF RRF MIN RRF 2,2,4-Trimethylpentane 1.0631.005 10.6 10.0 5.7 30.0Ave Benzene 0.68860.6367 10.8 10.0 8.1 30.0Ave 1,2-Dichloroethane 0.29000.2693 10.8 10.0 7.7 30.0Ave n-Heptane 0.35830.3468 10.3 10.0 3.3 30.0Ave n-Butanol 0.13860.1179 11.7 10.0 17.5 30.0Ave Trichloroethene 0.31370.2728 11.5 10.0 15.0 30.0Ave 1,2-Dichloropropane 0.23500.2240 10.5 10.0 4.9 30.0Ave Methyl methacrylate 0.23360.2168 10.8 10.0 7.8 30.0Ave 1,4-Dioxane 0.14570.1352 10.8 10.0 7.7 30.0Ave Dibromomethane 0.29340.2609 11.2 10.0 12.4 30.0Ave Bromodichloromethane 0.46440.4404 10.5 10.0 5.5 30.0Ave cis-1,3-Dichloropropene 0.37020.3393 10.9 10.0 9.1 30.0Ave methyl isobutyl ketone 0.44850.4395 10.2 10.0 2.1 30.0Ave Toluene 0.55570.5089 10.9 10.0 9.2 30.0Ave n-Octane 0.49360.4673 10.6 10.0 5.6 30.0Ave trans-1,3-Dichloropropene 0.38080.3976 9.58 10.0 -4.2 30.0Ave 1,1,2-Trichloroethane 0.27790.2531 11.0 10.0 9.8 30.0Ave Tetrachloroethene 0.47780.4211 11.3 10.0 13.5 30.0Ave Methyl Butyl Ketone (2-Hexanone) 0.50000.5036 9.93 10.0 -0.7 30.0Ave Dibromochloromethane 0.48560.4956 9.80 10.0 -2.0 30.0Ave 1,2-Dibromoethane 0.51810.4680 11.1 10.0 10.7 30.0Ave Chlorobenzene 0.76230.7009 10.9 10.0 8.8 30.0Ave Ethylbenzene 1.2571.152 10.9 10.0 9.1 30.0Ave n-Nonane 0.56520.5264 10.7 10.0 7.4 30.0Ave m,p-Xylene 0.49950.4543 22.0 20.0 9.9 30.0Ave Xylene, o-0.47390.4395 10.8 10.0 7.8 30.0Ave Styrene 0.74300.6743 11.0 10.0 10.2 30.0Ave Bromoform 0.31670.4197 7.54 10.0 -24.5 30.0Ave Cumene 1.4131.291 10.9 10.0 9.4 30.0Ave 1,1,2,2-Tetrachloroethane 0.69580.6569 10.6 10.0 5.9 30.0Ave n-Propylbenzene 1.7381.594 10.9 10.0 9.0 30.0Ave 1,2,3-Trichloropropane 0.57360.5370 10.7 10.0 6.8 30.0Ave n-Decane 0.74810.6750 11.1 10.0 10.8 30.0Ave 2-Chlorotoluene 1.2601.120 11.2 10.0 12.5 30.0Ave 4-Ethyltoluene 1.5281.304 11.7 10.0 17.2 30.0Ave 1,3,5-Trimethylbenzene 1.2291.092 11.3 10.0 12.6 30.0Ave Alpha Methyl Styrene 0.59550.5127 11.6 10.0 16.2 30.0Ave tert-Butylbenzene 1.1591.019 11.4 10.0 13.7 30.0Ave 1,2,4-Trimethylbenzene 1.2301.092 11.3 10.0 12.7 30.0Ave sec-Butylbenzene 1.7701.561 11.3 10.0 13.4 30.0Ave FORM VII TO-15 Page 466 of 478 FORM VII Lab Name:Job No.: SDG No.: Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID: Calib End Date:GC Column: ID: AIR - GC/MS VOA CONTINUING CALIBRATION DATA 0.32(mm) 200-40725-1 CHX.i 10/24/2017 04:21 10/23/2017 16:35 10/24/2017 00:08 ICV 200-122454/17 RTX-624 TestAmerica Burlington Lab File ID:27547_17.D Heated Purge: (Y/N)NConc. Units:ppb v/v ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNT AMOUNT %D AVE RRF RRF MIN RRF 4-Isopropyltoluene 1.5061.291 11.7 10.0 16.6 30.0Ave 1,3-Dichlorobenzene 0.83990.7499 11.2 10.0 12.0 30.0Ave 1,4-Dichlorobenzene 0.81050.7453 10.9 10.0 8.7 30.0Ave Benzyl chloride 0.90740.8717 10.4 10.0 4.1 30.0Ave n-Butylbenzene 1.3701.209 11.3 10.0 13.3 30.0Ave n-Undecane 0.69690.6653 10.5 10.0 4.8 30.0Ave 1,2-Dichlorobenzene 0.79530.6992 11.4 10.0 13.7 30.0Ave n-Dodecane 0.53090.4428 12.0 10.0 19.9 30.0Ave 1,2,4-Trichlorobenzene 0.50670.5075 9.98 10.0 -0.2 30.0Ave Hexachlorobutadiene 0.55390.4620 12.0 10.0 19.9 30.0Ave Naphthalene 0.95581.106 8.64 10.0 -13.6 30.0Ave 1,2,3-Trichlorobenzene 0.48170.4451 10.8 10.0 8.2 30.0Ave FORM VII TO-15 Page 467 of 478 FORM VII Lab Name:Job No.: SDG No.: Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID: Calib End Date:GC Column: ID: AIR - GC/MS VOA CONTINUING CALIBRATION DATA 0.32(mm) 200-40725-1 CHX.i 11/03/2017 12:06 10/23/2017 16:35 10/24/2017 00:08 CCVIS 200-122903/4 RTX-624 TestAmerica Burlington Lab File ID:27725_04.D Heated Purge: (Y/N)NConc. Units:ppb v/v ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNT AMOUNT %D AVE RRF RRF MIN RRF Propylene 0.73610.6065 12.1 10.0 21.4 30.0Ave Dichlorodifluoromethane 2.4022.241 10.7 10.0 7.2 30.0Ave Freon 22 1.5641.342 11.7 10.0 16.6 30.0Ave 1,2-Dichlorotetrafluoroethan e 2.4442.295 10.6 10.0 6.5 30.0Ave Chloromethane 0.89670.7870 11.4 10.0 13.9 30.0Ave n-Butane 1.4991.294 11.6 10.0 15.8 30.0Ave Vinyl chloride 1.0190.9201 11.1 10.0 10.7 30.0Ave 1,3-Butadiene 0.75400.6857 11.0 10.0 10.0 30.0Ave Bromomethane 0.82820.8075 10.3 10.0 2.6 30.0Ave Chloroethane 0.49450.4526 10.9 10.0 9.3 30.0Ave Isopentane 1.0310.9338 11.0 10.0 10.4 30.0Ave Bromoethene(Vinyl Bromide)0.87490.8699 10.1 10.0 0.6 30.0Ave Trichlorofluoromethane 2.5562.421 10.6 10.0 5.6 30.0Ave n-Pentane 1.7201.477 11.6 10.0 16.4 30.0Ave Ethanol 0.46660.4343 16.1 15.0 7.4 30.0Ave Ethyl ether 0.68610.6208 11.1 10.0 10.5 30.0Ave Acrolein 0.32100.2626 12.2 10.0 22.3 30.0Ave Freon TF 1.7901.755 10.2 10.0 2.0 30.0Ave 1,1-Dichloroethene 0.84270.8452 9.97 10.0 -0.3 30.0Ave Acetone 1.4121.216 11.6 10.0 16.2 30.0Ave Carbon disulfide 2.5192.410 10.5 10.0 4.5 30.0Ave Isopropyl alcohol 1.6431.451 11.3 10.0 13.2 30.0Ave 3-Chloropropene 1.2450.9800 12.7 10.0 27.0 30.0Ave Acetonitrile 0.71640.6121 11.7 10.0 17.0 30.0Ave Methylene Chloride 1.1260.9827 11.5 10.0 14.6 30.0Ave tert-Butyl alcohol 2.1691.983 10.9 10.0 9.4 30.0Ave Methyl tert-butyl ether 2.9042.695 10.8 10.0 7.8 30.0Ave trans-1,2-Dichloroethene 1.5111.353 11.2 10.0 11.7 30.0Ave Acrylonitrile 0.73160.6523 11.2 10.0 12.1 30.0Ave n-Hexane 1.5811.433 11.0 10.0 10.3 30.0Ave 1,1-Dichloroethane 1.9221.735 11.1 10.0 10.8 30.0Ave Vinyl acetate 2.5432.189 11.6 10.0 16.2 30.0Ave cis-1,2-Dichloroethene 1.0491.031 10.2 10.0 1.7 30.0Ave Methyl Ethyl Ketone 0.53610.5285 10.1 10.0 1.4 30.0Ave Ethyl acetate 0.07920.0780 10.1 10.0 1.4 30.0Ave Tetrahydrofuran 0.24320.2088 11.6 10.0 16.4 30.0Ave Chloroform 2.1992.132 10.3 10.0 3.1 30.0Ave Cyclohexane 0.28280.2776 10.2 10.0 1.9 30.0Ave 1,1,1-Trichloroethane 0.44450.4351 10.2 10.0 2.2 30.0Ave Carbon tetrachloride 0.44860.4328 10.4 10.0 3.6 30.0Ave FORM VII TO-15 Page 468 of 478 FORM VII Lab Name:Job No.: SDG No.: Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID: Calib End Date:GC Column: ID: AIR - GC/MS VOA CONTINUING CALIBRATION DATA 0.32(mm) 200-40725-1 CHX.i 11/03/2017 12:06 10/23/2017 16:35 10/24/2017 00:08 CCVIS 200-122903/4 RTX-624 TestAmerica Burlington Lab File ID:27725_04.D Heated Purge: (Y/N)NConc. Units:ppb v/v ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNT AMOUNT %D AVE RRF RRF MIN RRF 2,2,4-Trimethylpentane 1.0921.005 10.9 10.0 8.7 30.0Ave Benzene 0.64820.6367 10.2 10.0 1.8 30.0Ave 1,2-Dichloroethane 0.29020.2693 10.8 10.0 7.8 30.0Ave n-Heptane 0.38210.3468 11.0 10.0 10.2 30.0Ave n-Butanol 0.11670.1179 9.89 10.0 -1.1 30.0Ave Trichloroethene 0.26720.2728 9.79 10.0 -2.0 30.0Ave 1,2-Dichloropropane 0.23470.2240 10.5 10.0 4.8 30.0Ave Methyl methacrylate 0.21750.2168 10.0 10.0 0.3 30.0Ave 1,4-Dioxane 0.12550.1352 9.27 10.0 -7.2 30.0Ave Dibromomethane 0.22590.2609 8.66 10.0 -13.4 30.0Ave Bromodichloromethane 0.45430.4404 10.3 10.0 3.2 30.0Ave cis-1,3-Dichloropropene 0.34980.3393 10.3 10.0 3.1 30.0Ave methyl isobutyl ketone 0.46970.4395 10.7 10.0 6.9 30.0Ave Toluene 0.48810.5089 9.59 10.0 -4.1 30.0Ave n-Octane 0.51510.4673 11.0 10.0 10.2 30.0Ave trans-1,3-Dichloropropene 0.36300.3976 9.13 10.0 -8.7 30.0Ave 1,1,2-Trichloroethane 0.25280.2531 9.99 10.0 -0.1 30.0Ave Tetrachloroethene 0.37650.4211 8.94 10.0 -10.6 30.0Ave Methyl Butyl Ketone (2-Hexanone) 0.50850.5036 10.1 10.0 1.0 30.0Ave Dibromochloromethane 0.50220.4956 10.1 10.0 1.3 30.0Ave 1,2-Dibromoethane 0.45330.4680 9.68 10.0 -3.1 30.0Ave Chlorobenzene 0.65920.7009 9.40 10.0 -5.9 30.0Ave Ethylbenzene 1.1211.152 9.73 10.0 -2.7 30.0Ave n-Nonane 0.55830.5264 10.6 10.0 6.1 30.0Ave m,p-Xylene 0.43720.4543 19.2 20.0 -3.8 30.0Ave Xylene, o-0.41640.4395 9.47 10.0 -5.2 30.0Ave Styrene 0.64240.6743 9.53 10.0 -4.7 30.0Ave Bromoform 0.47320.4197 11.3 10.0 12.7 30.0Ave Cumene 1.2511.291 9.69 10.0 -3.1 30.0Ave 1,1,2,2-Tetrachloroethane 0.66840.6569 10.2 10.0 1.7 30.0Ave n-Propylbenzene 1.5911.594 9.98 10.0 -0.2 30.0Ave 1,2,3-Trichloropropane 0.54830.5370 10.2 10.0 2.1 30.0Ave n-Decane 0.77040.6750 11.4 10.0 14.1 30.0Ave 4-Ethyltoluene 1.3501.304 10.4 10.0 3.6 30.0Ave 2-Chlorotoluene 1.1711.120 10.5 10.0 4.5 30.0Ave 1,3,5-Trimethylbenzene 1.0801.092 9.89 10.0 -1.1 30.0Ave Alpha Methyl Styrene 0.50200.5127 9.79 10.0 -2.1 30.0Ave tert-Butylbenzene 0.99431.019 9.75 10.0 -2.4 30.0Ave 1,2,4-Trimethylbenzene 1.0881.092 9.97 10.0 -0.3 30.0Ave sec-Butylbenzene 1.5661.561 10.0 10.0 0.3 30.0Ave FORM VII TO-15 Page 469 of 478 FORM VII Lab Name:Job No.: SDG No.: Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID: Calib End Date:GC Column: ID: AIR - GC/MS VOA CONTINUING CALIBRATION DATA 0.32(mm) 200-40725-1 CHX.i 11/03/2017 12:06 10/23/2017 16:35 10/24/2017 00:08 CCVIS 200-122903/4 RTX-624 TestAmerica Burlington Lab File ID:27725_04.D Heated Purge: (Y/N)NConc. Units:ppb v/v ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNT AMOUNT %D AVE RRF RRF MIN RRF 4-Isopropyltoluene 1.3051.291 10.1 10.0 1.0 30.0Ave 1,3-Dichlorobenzene 0.70870.7499 9.45 10.0 -5.5 30.0Ave 1,4-Dichlorobenzene 0.69020.7453 9.26 10.0 -7.4 30.0Ave Benzyl chloride 0.99400.8717 11.4 10.0 14.0 30.0Ave n-Butylbenzene 1.2741.209 10.5 10.0 5.4 30.0Ave n-Undecane 0.69730.6653 10.5 10.0 4.8 30.0Ave 1,2-Dichlorobenzene 0.65720.6992 9.40 10.0 -6.0 30.0Ave n-Dodecane 0.46900.4428 10.6 10.0 5.9 30.0Ave 1,2,4-Trichlorobenzene 0.41220.5075 8.12 10.0 -18.8 30.0Ave Hexachlorobutadiene 0.38890.4620 8.41 10.0 -15.8 30.0Ave Naphthalene 0.98841.106 8.93 10.0 -10.6 30.0Ave 1,2,3-Trichlorobenzene 0.38730.4451 8.70 10.0 -13.0 30.0Ave FORM VII TO-15 Page 470 of 478 Lab Name:Job No.: SDG No.: Instrument ID: Analysis Batch Number: AIR - GC/MS VOA ANALYSIS RUN LOG DILUTION FACTOR COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID TestAmerica Burlington 200-40706-1 CHX.i 122454 Start Date: End Date:10/24/2017 12:30 10/23/2017 14:57 BFB 200-122454/1 RTX-624 0.32(mm)110/23/2017 14:57 27547_01.D VIBLK 200-122454/2 RTX-624 0.32(mm)110/23/2017 15:45 IC 200-122454/3 RTX-624 0.32(mm)110/23/2017 16:35 27547_03.D IC 200-122454/4 RTX-624 0.32(mm)110/23/2017 17:25 27547_04.D ZZZZZ RTX-624 0.32(mm)110/23/2017 18:15 IC 200-122454/6 RTX-624 0.32(mm)110/23/2017 19:06 27547_06.D ZZZZZ RTX-624 0.32(mm)110/23/2017 19:56 IC 200-122454/8 RTX-624 0.32(mm)110/23/2017 20:46 27547_08.D ICIS 200-122454/9 RTX-624 0.32(mm)110/23/2017 21:37 27547_09.D IC 200-122454/10 RTX-624 0.32(mm)110/23/2017 22:27 27547_10.D IC 200-122454/11 RTX-624 0.32(mm)110/23/2017 23:18 27547_11.D IC 200-122454/12 RTX-624 0.32(mm)110/24/2017 00:08 27547_12.D VIBLK 200-122454/13 RTX-624 0.32(mm)110/24/2017 00:59 VIBLK 200-122454/14 RTX-624 0.32(mm)110/24/2017 01:49 VIBLK 200-122454/15 RTX-624 0.32(mm)110/24/2017 02:40 ZZZZZ RTX-624 0.32(mm)110/24/2017 03:30 ICV 200-122454/17 RTX-624 0.32(mm)110/24/2017 04:21 27547_17.D ZZZZZ RTX-624 0.32(mm)110/24/2017 05:12 ZZZZZ RTX-624 0.32(mm)110/24/2017 06:03 ZZZZZ RTX-624 0.32(mm)110/24/2017 09:58 ZZZZZ RTX-624 0.32(mm)110/24/2017 10:48 ZZZZZ RTX-624 0.32(mm)110/24/2017 11:39 ZZZZZ RTX-624 0.32(mm)110/24/2017 12:30 TO-15 Page 471 of 478 Lab Name:Job No.: SDG No.: Instrument ID: Analysis Batch Number: AIR - GC/MS VOA ANALYSIS RUN LOG DILUTION FACTOR COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID TestAmerica Burlington 200-40706-1 CHX.i 122903 Start Date: End Date:11/04/2017 05:32 11/03/2017 09:29 BFB 200-122903/1 RTX-624 0.32(mm)111/03/2017 09:29 27725_01.D CCVIS 200-122903/4 RTX-624 0.32(mm)111/03/2017 12:06 27725_04.D LCS 200-122903/5 RTX-624 0.32(mm)111/03/2017 12:57 27725_05.D MB 200-122903/6 RTX-624 0.32(mm)111/03/2017 13:47 27725_06.D ZZZZZ RTX-624 0.32(mm)0.211/03/2017 14:45 200-40706-6 RTX-624 0.32(mm)0.211/03/2017 15:43 27725_08.D ZZZZZ RTX-624 0.32(mm)0.211/03/2017 16:40 ZZZZZ RTX-624 0.32(mm)0.211/03/2017 17:38 ZZZZZ RTX-624 0.32(mm)0.211/03/2017 18:36 ZZZZZ RTX-624 0.32(mm)1011/03/2017 19:26 ZZZZZ RTX-624 0.32(mm)1011/03/2017 20:17 ZZZZZ RTX-624 0.32(mm)3111/03/2017 21:07 ZZZZZ RTX-624 0.32(mm)111/03/2017 21:57 ZZZZZ RTX-624 0.32(mm)111/03/2017 22:48 ZZZZZ RTX-624 0.32(mm)111/03/2017 23:38 ZZZZZ RTX-624 0.32(mm)211/04/2017 00:29 ZZZZZ RTX-624 0.32(mm)111/04/2017 01:20 ZZZZZ RTX-624 0.32(mm)111/04/2017 02:10 ZZZZZ RTX-624 0.32(mm)111/04/2017 03:01 ZZZZZ RTX-624 0.32(mm)111/04/2017 03:51 ZZZZZ RTX-624 0.32(mm)111/04/2017 04:42 ZZZZZ RTX-624 0.32(mm)511/04/2017 05:32 TO-15 Page 472 of 478 Lab Name:Job No.: SDG No.: Instrument ID: Analysis Batch Number: AIR - GC/MS VOA ANALYSIS RUN LOG DILUTION FACTOR COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID TestAmerica Burlington 200-40725-1 CHX.i 122454 Start Date: End Date:10/24/2017 12:30 10/23/2017 14:57 BFB 200-122454/1 RTX-624 0.32(mm)110/23/2017 14:57 27547_01.D VIBLK 200-122454/2 RTX-624 0.32(mm)110/23/2017 15:45 IC 200-122454/3 RTX-624 0.32(mm)110/23/2017 16:35 27547_03.D IC 200-122454/4 RTX-624 0.32(mm)110/23/2017 17:25 27547_04.D ZZZZZ RTX-624 0.32(mm)110/23/2017 18:15 IC 200-122454/6 RTX-624 0.32(mm)110/23/2017 19:06 27547_06.D ZZZZZ RTX-624 0.32(mm)110/23/2017 19:56 IC 200-122454/8 RTX-624 0.32(mm)110/23/2017 20:46 27547_08.D ICIS 200-122454/9 RTX-624 0.32(mm)110/23/2017 21:37 27547_09.D IC 200-122454/10 RTX-624 0.32(mm)110/23/2017 22:27 27547_10.D IC 200-122454/11 RTX-624 0.32(mm)110/23/2017 23:18 27547_11.D IC 200-122454/12 RTX-624 0.32(mm)110/24/2017 00:08 27547_12.D VIBLK 200-122454/13 RTX-624 0.32(mm)110/24/2017 00:59 VIBLK 200-122454/14 RTX-624 0.32(mm)110/24/2017 01:49 VIBLK 200-122454/15 RTX-624 0.32(mm)110/24/2017 02:40 ZZZZZ RTX-624 0.32(mm)110/24/2017 03:30 ICV 200-122454/17 RTX-624 0.32(mm)110/24/2017 04:21 27547_17.D ZZZZZ RTX-624 0.32(mm)110/24/2017 05:12 ZZZZZ RTX-624 0.32(mm)110/24/2017 06:03 ZZZZZ RTX-624 0.32(mm)110/24/2017 09:58 ZZZZZ RTX-624 0.32(mm)110/24/2017 10:48 ZZZZZ RTX-624 0.32(mm)110/24/2017 11:39 ZZZZZ RTX-624 0.32(mm)110/24/2017 12:30 TO-15 Page 473 of 478 Lab Name:Job No.: SDG No.: Instrument ID: Analysis Batch Number: AIR - GC/MS VOA ANALYSIS RUN LOG DILUTION FACTOR COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID TestAmerica Burlington 200-40725-1 CHX.i 122903 Start Date: End Date:11/04/2017 05:32 11/03/2017 09:29 BFB 200-122903/1 RTX-624 0.32(mm)111/03/2017 09:29 27725_01.D CCVIS 200-122903/4 RTX-624 0.32(mm)111/03/2017 12:06 27725_04.D LCS 200-122903/5 RTX-624 0.32(mm)111/03/2017 12:57 27725_05.D MB 200-122903/6 RTX-624 0.32(mm)111/03/2017 13:47 27725_06.D ZZZZZ RTX-624 0.32(mm)0.211/03/2017 14:45 ZZZZZ RTX-624 0.32(mm)0.211/03/2017 15:43 ZZZZZ RTX-624 0.32(mm)0.211/03/2017 16:40 200-40725-2 RTX-624 0.32(mm)0.211/03/2017 17:38 27725_10.D ZZZZZ RTX-624 0.32(mm)0.211/03/2017 18:36 ZZZZZ RTX-624 0.32(mm)1011/03/2017 19:26 ZZZZZ RTX-624 0.32(mm)1011/03/2017 20:17 ZZZZZ RTX-624 0.32(mm)3111/03/2017 21:07 ZZZZZ RTX-624 0.32(mm)111/03/2017 21:57 ZZZZZ RTX-624 0.32(mm)111/03/2017 22:48 ZZZZZ RTX-624 0.32(mm)111/03/2017 23:38 ZZZZZ RTX-624 0.32(mm)211/04/2017 00:29 ZZZZZ RTX-624 0.32(mm)111/04/2017 01:20 ZZZZZ RTX-624 0.32(mm)111/04/2017 02:10 ZZZZZ RTX-624 0.32(mm)111/04/2017 03:01 ZZZZZ RTX-624 0.32(mm)111/04/2017 03:51 ZZZZZ RTX-624 0.32(mm)111/04/2017 04:42 ZZZZZ RTX-624 0.32(mm)511/04/2017 05:32 TO-15 Page 474 of 478 Shipping and Receiving Documents Page 475 of 478 Page 476 of 478 Page 477 of 478 Login Sample Receipt Checklist Client: AKRF Inc Job Number: 200-41113-1 SDG Number: 200-41113-1 Login Number: 41113 Question Answer Comment Creator: Deason, Barbara N List Source: TestAmerica Burlington List Number: 1 TrueRadioactivity wasn't checked or is </= background as measured by a survey meter. Lab does not accept radioactive samples. TrueThe cooler's custody seal, if present, is intact.461502 TrueSample custody seals, if present, are intact. TrueThe cooler or samples do not appear to have been compromised or tampered with. N/ASamples were received on ice.Thermal preservation not required. TrueCooler Temperature is acceptable. N/ACooler Temperature is recorded.Thermal preservation not required. TrueCOC is present. TrueCOC is filled out in ink and legible. TrueCOC is filled out with all pertinent information. TrueIs the Field Sampler's name present on COC?TM TrueThere are no discrepancies between the containers received and the COC. TrueSamples are received within Holding Time (excluding tests with immediate HTs) TrueSample containers have legible labels. TrueContainers are not broken or leaking. TrueSample collection date/times are provided. TrueAppropriate sample containers are used. N/ASample bottles are completely filled. TrueSample Preservation Verified. TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4"). TrueMultiphasic samples are not present. TrueSamples do not require splitting or compositing. N/AResidual Chlorine Checked. TestAmerica Burlington Page 478 of 478