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QyC DR C £i VILLAGE OF RYE BROOK MAYOR 938 King Street,Rye Brook,N.Y. 10573 ADMINISTRATOR Jason A. Klein (914)939-0668 Christopher J.Bradbury www.ryebrookny.gov TRUSTEES BUILDING&FIRE INSPECTOR Susan R. Epstein Steven E. Fews Stephanie J. Fischer David M. Heiser Salvatore W. Morlino CERTIFICATE OF COMPLIANCE October 17,2024 Enrico Marini&Dome Marini 42 Roanoke Avenue Rye Brook,New York 10573 Re: 42 Roanoke Avenue,Rye Brook,New York 10573 Parcel ID#: 141.35-1-44 This document certifies that the work done under Mechanical Permit #16-123 issued on 9/23/2016 for the installation of a new above-ground oil tank has been satisfactorily completed. Sincerely, Steven E. Fews Building&Fire Inspector /to QyE DR �. o cz. � ti t'l .a a� t� w 4 V�aLC Vey V `C . 19 VILLAGE OF RYE BROOK MAYOR 938 King Street, Rye Brook,N.Y. 10573 ADMINISTRATOR Jason A. Klein (914)939-0668 Christopher J. Bradbury www.ryebrookny.Qov TRUSTEES BUILDING& FIRE INSPECTOR Susan R. Epstein Steven E. Fews Stephanie J. Fischer David M. Heiser Salvatore W. Morhno CERTIFICATE OF COMPLIANCE October 17,2024 Enrico Marini&Dorrie Marini 42 Roanoke Avenue Rye Brook,New York 10573 Re: 42 Roanoke Avenue, Rye Brook,New York 10573 Parcel ID#: 141.35-1-44 As per the Documentation from New York State Department of Environmental Conservation Spill Close Out Record dated January 10, 2017, the removal of an underground oil tank under Mechanical Permit #16-123 issued on 9/23/2016 has been satisfactorily completed. Sincerely, Steven E. Fews Building&Fire Inspector /to QyE BRC��• t7 T 1982•��O BUILDING DEPARTMENT ❑BUILDING INSPECTOR ASSISTANT BUILDING INSPECTOR VILLAGE OF RYE BROOK ❑CODE ENFORCEMENT OFFICER 938 KING STREET • RYE BROOK,NY 10573 (914) 939-0668 FAx (914) 939-5801 www.ryebrook.org - - - - - - - - - - - - - - - - - - - - INSPECTION REPORT - - - - - - - - - - - - - - -- - - - - ADDRESS : 1 I R oA N 0 U- DATE: [ 4) - /S - C.0 L PERMIT# NI? I t' - I Z-,> ISSUED: SECT:_y/ 3y BLOCK: / LOT: y/ LOCATION: EJ A -5 E Ir f iy OCCUPANCY: ❑ VIOLATION NOTED THE WORK IS... ❑ ACCEPTED ❑ REJECTED/ REINSPECTION ❑ SITE INSPECTION REQUIRED ❑ FOOTING ❑ FOOTING DRAINAGE ❑ FOUNDATION ❑ UNDERGROUND PLUMBING NOTES ON INSPECTION: ❑ ROUGH PLUMBING ❑ ROUGH FRAMING ❑ INSULATION ❑ NATURAL GAS _ 7 � L ❑ L.P. GAS 2 FUEL TANK ❑ FIRE SPRINKLER ❑ FINAL PLUMBING ❑ CROSS CONNECTION ❑ FINAL ❑ OTHER 4 i i `! \\� QyE BRC��, cu � '9a2 BUILDING DEPARTMENT ❑BUILDING INSPECTOR QASSISTANT BUILDING INSPECTOR VILLAGE OF RYE BROOK ❑CODE ENFORCEMENT OFFICER 938 KING STREET • RYE BROOK,NY 10573 (914) 939-0668 FAx (914) 939-5801 www.ryebrook.org - - - - - - - - - - - - - - - - - - - - INSPECTION REPORT - - - - - - - - - - - - - - - - - - - - ADDRESS : 1 2 /e o,4Aj o r F 4 ✓c DATE: /0 - 9 - 2021 PERMIT# A) P ISSUED: -13-fib SECT: 1,3." BLOCK: / LOT: 7 LOCATION: OCCUPANCY: ❑ VIOLATION NOTED THE WORK IS... © ACCEPTED ❑ REJECTED/ REINSPECTION ❑ SITE INSPECTION REQUIRED ❑ FOOTING ❑ FOOTING DRAINAGE ❑ FOUNDATION ❑ UNDERGROUND PLUMBING NOTES ON INSPECTION: ❑ ROUGH PLUMBING ❑ ROUGH FRAMING ❑ INSULATION ❑ NATURAL GAS Q # ❑ L.P. GAS ,❑ FUEL TANK ❑ FIRE SPRINKLER ❑ FINAL PLUMBING L 11 ❑ CROSS CONNECTION (� ❑ FINAL -k ❑ OTHER Lo o / DRC�j� w � 193r2 BUILDING DEPARTMENT 0 BUILDING INSPECTOR VILLAGE OF RYE BROOK 0 VILLAGE ENGINEER 938 KING STREET RYE BROOK,NY 10573 O ASSISTANT BUILDING INSPECTOR (914) 939-0668 FAx(914) 939-5801 - - - - - - - - - - - - - - - - - - - - - INSPECTION REPORT - - - - - - - - - - - - - - - - - - - - - ADDRESS: CCJ� � �� DATE: ,U Z PERMIT# ISSUED: SECT: BLOCK: LOT: LOCATION: OCCUPANCY: 0 VIOLATION NOTED 7liE WORK IS... Cl ACCEPTED REJECTED/REINSPECTION 0 Sl IE INSPECTION REQUIRED 0 FOOTING ❑ FOOTING DRAINAGE ❑ FOUNDATION 0 UNDERGROUND PLUMBING NOTES ON INSPECTION: 0 ROUGH PLUMBING 0 ROUGH FYtAmNo 0 INSULATION ❑ NATURAL GAS ❑ L.P. GASc - ❑ FUEL TANK 0 FIRE SPRINKLER ❑ FINAL PLUMBING �^ �h I 1 1 O FINAL O OTHER dOHVEC Hudson Valley Environmental & Construction 462 Lakeview Ave.Valhalla,NY 10595 1-877-811-HVEC etS%awCI` 42 2o.,. k%K_ Rye arc, NY hI I cnJ Z� l�J.O�Lq ? l6C�m'"' w 5 y UST SPILL CLOSURE REPORT MARINI RESIDENCE 42 ROANOKE AVENUE RYE BROOK , NEW YORK NYSDEC SPILL No . 1607332 PREPARED FOR : STATE FARM INSURANCE CLAIM No . 52 -0038- 1 V5 PREPARED BY : HYDROENVIRONMENTAL SOLUTIONS, INC. ENVIRONMENTAL CONSULTANTS ONE DEANS BRIDGE ROAD SOMERS, NEW YORK 10589 (914) 276-2560 sverdibello@hesny.com January 6, 2016 Prepared by: Reviewed by: L -� / .•� Christopher J. LaFonte Steven M. Verdibello Geologist/Hydrogeologist Geologist/Hydrogeologist Junior Project Manager HydroEm ironmental SOL U T I O N S . I N C . INTRODUCTION On behalf of State Farm Insurance (State Farm), HydroEnvironmental Solutions, Inc. (HES) has completed environmental oversight during the removal of one leaking 550- gallon steel fuel oil underground storage tank (UST) and fuel oil impacted soil at the Marini Residence located at 42 Roanoke Avenue in Rye Brook, New York. The site location is shown on Figure 1. The UST closure and soil removal activities were conducted on November 18, 2016. Site activities completed by HES include photographing and inspecting the UST, field screening soil samples with a photoionization detector(PID)for the presence of petroleum vapors, and collection of post-excavation soil samples for laboratory analysis. The field activities and results are presented below. FIELD ACTIVITIES UST and Soil Removal On October 26, 2016, Hudson Valley Environmental & Construction (HVEC) of Valhalla, New York, removed one leaking 550-gallon steel fuel oil UST from the front yard of the subject site. The tank's location prior to removal is shown on Figure 2, a generalized site plan of the subject site. The UST was removed and temporarily staged adjacent to the excavation for visual inspection. The UST was in poor condition with one visible pin-hole. The tank was cleaned and prepared for disposal by HVEC technicians and taken to Brookfield Resource Management in Elmsford, New York for recycling. The manifest for this action is included in Appendix 1. Following UST removal, fuel oil impacted soil was encountered and subsequently excavated by HVEC on November 18, 2016. Photographs taken during spill closure activities and removed UST are included in Figure 3. During soil excavation, a total of five soil samples were collected and screened for petroleum vapors using a MiniRAE' 3000 calibrated PID and the headspace method. Soil samples were collected as excavation end-point samples from the sidewalls and bottom of the excavation. These samples were collected in appropriately labeled sample jars and transported on ice to York Analytical Laboratories, Inc. (York); a New York State certified laboratory located in Stratford, Connecticut, where they were analyzed for the presence of volatile organic compounds (VOCs) using EPA Method 8021 modified to include MTBE (methyl tertiary butyl ether)and for semi-volatile organic compounds (SVOCs) using EPA Method 8270 in accordance with New York State Department of Environmental Conservation (NYSDEC) Commissioner's �\ HydroEnvironmental SOL U T I O N S . I N C . One Deans Bridge Road Somers.New York 10589 (914)276-2560 Fax (914)276-2664 1 Policy No. 51 (CP-51) Guidelines. Soil sampling locations are shown on Figure 2 and the soil sampling laboratory analytical report is included in Appendix 2. Neither bedrock nor groundwater was encountered in the excavation to a completion depth of approximately 8 feet below grade (ftbg). The Marini residence and residences in the area are provided potable water via municipal means. RESULTS Soil Quality During soil removal, PID field screening results indicated that VOC vapors were present in all of the excavation end-point soil samples at concentrations ranging from 2.7 to 32.1 parts per million (ppm). The PID field screening results are summarized on Table 1. The results of PID field screening demonstrate that a significant majority of the accessible fuel oil impacted soil observed beneath and around the UST was removed by excavation. Based on PID field screening results collected during soil removal activities, a total of 7.6 tons of petroleum impacted soil was removed from the UST excavation for off-site disposal. The impacted soil was loaded and transported off-site on November 18, 2016 by HVEC and disposed of at Deep Green of New York, Inc, an approved soil-processing facility located in New Windsor, New York, on November 18, 2016. The Soil Tracking Form and Facility Weight Ticket for soil transportation and disposal are included in Appendix 3. Laboratory analytical results indicate that no VOCs or SVOCs were detected at concentrations above their respective NYSDEC Soil Cleanup Levels (SCLs) in accordance with NYSDEC CP-51 Guidelines in any of the end-point soil samples. The post-excavation soil laboratory results are summarized on Table 2 and the laboratory analytical report is included in Appendix 2. HydroEnvironmental SOL U T I O N S , I N C . / One Deans Bridge Road Somers.New York 10589 /l (914)276-2560 Fax:(914)276-2664 2 DISCUSSION OF RESULTS Soil screening and laboratory analysis completed during UST removal and soil excavation activities at the subject site indicate that a majority of the accessible fuel oil impacted soil has been removed from the former UST area. The fuel oil impacted soil was delineated to the furthest extent practical in the horizontal and vertical directions, as is supported by the results of end-point soil sampling in these areas. The Excavation Bottom end-point soil sample indicates that no fuel oil constituents were detected above laboratory method detection limits (MDLs) at 8 ftbg. Based upon the absence of detectable fuel oil constituents encountered in the excavation end-point soil samples (with the exception of one trace constituent found in the soil sample designated Sidewall-2) and the absence of groundwater encountered during excavation activities, the extent of fuel oil impacted soil does not likely extend beyond the former UST excavation area. RECOMMENDATIONS HES believes that a majority of the fuel oil impacted soil in the vicinity of the former UST area was removed by excavation and that any remaining fuel oil constituents beneath the site do not pose a risk to the environment or human health. In this regard, HES recommends that no further environmental work be completed at the site and that Spill No. 1607332 be formally closed by the NYSDEC Region 3 Office. i V HydroErwironmental SOL U T I O N S , I N C . One Deans Bridge Road Somers.New York 10589 (914)276-2560 Fax:(914)276-2664 3 TABLES TABLE 1 42 ROANOKE AVENUE RYE BROOK, NEW YORK State Farm Claim No. 52-0038-1V5 NYSDEC Spill No. 1607332 Summary of PID Field Screening Results November 18, 2016 Sample No. Depth PID Read n Notes Sidewall-1 6 3.6 SILT and SAND (fine); brown; moist; no fuel oil odor Sidewall-2 7 32.1 SILT and SAND (fine), trace GRAVEL (small, sub-rounded); brown; moist; no fuel oil odor Sidewall-3 7 2.7 SILT and SAND (fine), trace GRAVEL (small, sub-rounded); brown; moist; no fuel oil odor Sidewall-4 7 5.0 SILT and SAND (fine), trace GRAVEL (small, sub-rounded); brown; moist; no fuel oil odor Excavation Bottom 8 7.6 SILT and WEATHERED BEDROCK (schist); brown; moist; no fuel oil odor -PID(photoionization detector)readings in parts per million,calibration gas equivalents -Depth in feet below grade HydroEnvironmental Solutions, Inc. 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C $ c 'S g L o E o G 'o 0 c m!^ c 3 ° O ji v v a LA a E g O y C p a a a G a 7 C a Y N N G O H N u C a C d Y E a o _ a c C U a s w c a N c o c `o c v t v o a O m a of a c o .- p o u C r v G 7 N v a a u O o m 'c� E E c ;; a n X a— C.O a c ~ l' N m 0` L L �>„' O a E G m m a C L n 0 6-6-6-6-6 E Y E W O Ill C y d n > >y) O J a C c L a 0 0 a L G N F N d C c G v W �p O ry M y 0 a m d X - N y 0 T u u C W aci a s a L L J J V N L T C C '- II N I� I� II 11 C vl Y IIR c C O d 0. H X Q Q Q m m m m Call. O W li Z d d 2 Q G 0 ,I 7 m w Z t FIGURES O �74!1 INor 42 Roanoke Avenue Rye Brook, New York M�V� �MJ4 �►�.,,►' �f"sue'•fi`� �a ��'J � � �'�1 287 � �• � j�d'y'.- —is •` ': . I� - ^` toy- I Jr I off + • • 11�1 1 1�1,1 I,I,1 ,I,lil Il�lyl 11 I r .�U �Z Q_ fi 4� Q�eo y 3 Q, LLJ Z [,` :2pZ0 VHpo MWF Q� h s►—v � saw oz b aoo 000 -Anc--I skoLL o LLJ ILJ ILL � Q O < Z W OS �UIU m w U-::s �WQ u S S O ~ 1 � s w ~ � 0 ::N Of z z W LU LU o NQ LU Q °C z LLJ N ; W � Q w 0 z Q Mp W w ° q)a Q W w ZWZ 56� � Q FIGURE 3 42 ROANOKE AVENUE RYE BROOK, NEW YORK 7;f 1 / Photograph taken of subject site Photograph of removed 550-gallon UST Photographs taken during UST spill closure activities on November 18, 2016. HydroEnvironmental Solutions, Inc., One Deans Bridge Road, Somers, New York 10589 FIGURE 3 42 ROANOKE AVENUE RYE BROOK, NEW YORK k Jr K• , �� L Close-up photograph of corrosion hole in UST A ,-TOO Photograph taken during soil excavation activities Photographs taken during UST spill closure activities on November 18, 2016. HydroEnvironmental Solutions, Inc., One Deans Bridge Road, Somers, New York 10589 FIGURE 3 42 ROANOKE AVENUE RYE BROOK, NEW YORK s. k w �1 •� �r� Photograph taken of final excavation area Photographs taken during UST spill closure activities on November 18, 2016. HydroEnvironmental Solutions, Inc., One Deans Bridge Road, Somers, New York 10589 APPENDICES APPENDIX 1 : UST Disposal Receipt PAYMENT RECEIPT Brookfield Resource Management 100 Lamont Street Elmsford, NY 10523 914-592-5250 Receipt: 1127107 Date: 11/21/2016 Customer: 33861 Time: 10:45 HUDSON VALLEY ENVIRONMENTAL 462 LAKE VIEW AVE VALHALL, NY 10595 Ticket: 1260434 Weigh In: 11/21/2016 10:36 Operator: 6 Weigh Out: 11/21/2016 10:45 Description: TRK#77 Commodity Gross Tare Net Price TOTAL_$ #1 Unprepared 19720 18260 1460 2.500/CW 536.50 _........ Ticket Total $36.50 #of Tickets: 1 !Total Paid — .0$3701 Paid by CASH �^� Let Us Know How We're Doing (infoQbrookfioidco.com) APPENDIX 2: Laboratory Analytical Report for Soil 1 ' Technical Report prepared for: Hydro Environmental Solutions One Deans Bridge Road Somers NY, 10589 Attention: Bill Canavan Report Date: 11/29/2016 Client Project ID: 42 Roanoke Avenue, Rye Brook, NY York Project (SDG) No.: 16KO861 CT Ccrt.No.PH-0723 New Jersey Cert.No.CT-005 New York Cert.Nos.10854 and 12058 PA Cert.No.68-04440 60 120 RESEARCH DRIVE STRATFORD,CT 06615 ■ 132-02 89th AVENUE RICHMOND HILL,NY 11418 www.YORKLAB.com (203)325-1371 FAX(203)357-0166 ClientServices@yorklab.com Page 1 of 18 Report Date: 11/29/2016 Client Project ID: 42 Roanoke Avenue, Rye Brook,NY York Project (SDG)No.: 16KO861 Hydro Environmental Solutions One Deans Bridge Road Somers NY, 10589 Attention: Bill Canavan Purpose and Results This report contains the analytical data for the sample(s) identified on the attached chain-of-custody received in our laboratory on November 21,2016 and listed below. The project was identified as your project: 42 Roanoke Avenue,Rye Brook,NY. The analyses were conducted utilizing appropriate EPA, Standard Methods, and ASTM methods as detailed in the data summary tables. All samples were received in proper condition meeting the customary acceptance requirements for environmental samples except those indicated under the Notes section of this report. All analyses met the method and laboratory standard operating procedure requirements except as indicated by any data flags, the meaning of which are explained in the attachment to this report,and case narrative if applicable. The results of the analyses, which are all reported on dry weight basis (soils) unless otherwise noted, are detailed in the following pages. Please contact Client Services at 203.325.1371 with any questions regarding this report. York Sample ID Client Sample ID Matrix Date Collected Date Received 16K0861-01 Sidewall-1 Soil 11/18/2016 11/21/2016 16K0861-02 Sidewall-2 Soil 11/18/2016 11/21/2016 16K0861-03 Sidewall-3 Soil 11/18/2016 11/21/2016 16K0861-04 Sidewal1-4 Soil 11/18/2016 11/21/2016 16K0861-05 Excavation Bottom Soil 11/18/2016 11/21/2016 Page 2 of 18 General Notes for York Project(SDG) No.: 16KO861 1. The RLs and MDLs (Reporting Limit and Method Detection Limit respectively) reported are adjusted for any dilution necessary due to the levels of target and/or non-target analytes and matrix interference. The RL(REPORTING LIMITI is based upon the lowest standard utilized for the calibration where applicable. 2. Samples are retained for a period of thirty days after submittal of report,unless other arrangements are made. 3. York's liability for the above data is limited to the dollar value paid to York for the referenced project. 4. This report shall not be reproduced without the written approval of York Analytical Laboratories,Inc. 5. All samples were received in proper condition for analysis with proper documentation,unless otherwise noted. 6. All analyses conducted met method or Laboratory SOP requirements.See the Qualifiers and/or Narrative sections for further information. 7. It is noted that no analyses reported herein were subcontracted to another laboratory,unless noted in the report. 8. This report reflects results that relate only to the samples submitted on the attached chain-of-custody form(s) received by York. 9. Analyses conducted at York Analytical Laboratories, Inc. Stratford, CT are indicated by NY Cert. No. 10854; those conducted at York Analytical Laboratories,Inc.,Richmond Hill,NY are indicated by NY Cert.No. 12058. Approved By: >- Date: 11/29/2016 Benjamin Gulizia Laboratory Director Page 3 of 18 Sample Information Client Sample ID: Sidewall-1 York Sample ID: 16KO861-01 York Project(SDG)No. Client Project ID Matrix Collection Date/Time Date Received 16KO861 42 Roanoke Avenue,Rye Brook,NY Soil November 18,2016 10:00 am 11/21/2016 Volatile Organics.CP-51(formerly STARS)List Lou-in Notes: Sample Notes: Sample Prepared by Method:EPA 5035A Reported to Date/Time Date/Time CAS No. Parameter Result Flag Units LOD/MDL LOQ Dilution Reference Method Prepared Analyzed Analyst 95-63-6 1,2,4-Trimethylbenzene ND ug/kg dry 2.2 4.3 1 EPA 8260C I1/22/201608:07 1lr=01613:15 SS Certifications: CrDOH,NELAC-NY10854,N)DEP 108-67-8 I,3,5-Trimethylbenzene ND ug/kg dry 2.2 4.3 1 EPA 8260C 11/22/201608:07 1122201613:15 SS Certifications: CfDOH,NELAC-NY 10854,NJDEP 7143-2 Benzene ND ug/kg dry 2.2 4.3 1 EPA 8260C 1122/201608:07 11/=01613:15 SS Ccrtificatioas: CTDOH,NELAC-NY 10854,NJDEP,PADEP 100414 Ethyl Benzene ND ug/kg dry 2.2 4.3 1 EPA 8260C 1122/201608:07 1122201613:15 SS Certifications: CrD0H,NELAC-NY10854,NJDEPPADEP 98-82-8 Isopropylbenzene ND ug/kg dry 2.2 4.3 1 EPA 8260C 1122/201608:07 11f=01613:15 SS Certifications: CTD0H,NELAC-NY10854,NJDEP 1634-04.4 Methyl tert-butyl ether(MTBE) ND ug/kg dry 2.2 4.3 1 EPA 8260C 1122/2016 08:07 11/=01613:15 SS Certifications: CTDOH,NELAC-NY 10854,NJDEP 91-20-3 Naphthalene ND ug/kg dry 2.2 8.6 1 EPA 8260C 1122/201608:07 1122201613:15 SS Certifications: NELAC-NY10854,NJDEP 104-51-8 n-Butylbenzene ND ugAg dry 2.2 4.3 1 EPA 8260C 1122201608:07 1122201613:15 SS Cmificmbons: CTDOH,NELAC-NY10854,NJDEP 103-65-1 n-Propylbenzene ND ug/kg dry 2.2 4.3 1 EPA 8260C 1122201608:07 11/22/201613:15 SS Certifications: CTDOH,NELAC-NY10854,NJDEP 9547-6 o-Xylene ND ug/kg dry 2.2 4.3 1 EPA 8260C 1122201608:07 1122201613:15 SS Certifications: CTDOH,NELAC-NY 10854 179601-23-1 p-&m-Xylenes N D ug/kg dry 4.3 8.6 1 EPA 8260C 11222016 08:07 1122/2016 13:15 SS Certifications: CTDOH,NELAC-NY10854 99-87-6 p4sopropyltoluene ND ug/kg dry 2.2 4.3 1 EPA 8260C Il22/201608:07 1122201613:15 SS Certifications: CTDOH,NELAC-NY10854,NJDEP 135-98-8 sec-Butylbenzene ND ug/kg dry 2.2 4.3 1 EPA 8260C 1122/201608:07 1122/201613:15 SS Certifications: CTDOH,NELAC-NY 10854,NJDEP 98-06.6 tert-Butylbenzene ND ug/kg dry 2.2 4.3 1 EPA 8260C I l22/2016 08:07 1122/2016 13:15 SS Certifications: CTD0H,NELAC-NY10854,NJDEP 108-88-3 Toluene ND ug/kg dry 2.2 4.3 1 EPA 8260C 1122/2016 08:07 I IrMO16 13:15 SS Certifications: CTDOH,NELAC-NY 10854,NJDEP,PADEP 1330-20.7 Xylenes,Total ND ug/kg dry 6.5 13 1 EPA 8260C 1122/201608:07 1122201613:15 SS Certifications: CTDOH,NELAC-NY 10854,NJDEP,PADEP Surrogate Recoveries Result Acceptance Range 17060-07.0 Surrogate:1,2-Dichloroethane-d4 104% 77-125 2037-26-5 Surrogate:Toluene-& 104% 85-110 460-004 Surrogate:p-BromoJluorobenzene 108% 76-130 Semi-Volatiles,CP-51 (formerly STARS)List Lou-in Notes: Sample Notes: 120 RESEARCH DRIVE STRATFORD,CT 06615 ■ 132-02 89th AVENUE RICHMOND HILL,NY 11418 www.YORKLAB.com (203)325-1371 FAX(203)357-0166 ClientServices Page 4 of 18 1 ' Sample Information Client Sample ID: Sidewall-1 York Sample ID: 16KO861-01 York Project(SDG)No. Client Project ID Matrix Collection Date/Time Date Received 16KO861 42 Roanoke Avenue,Rye Brook,NY Soil November 18,2016 10:00 am 11/21/2016 Sunple Prepared by Method:EPA 3550C Reported to Date/"Time Date/Time CAS No. Parameter Result Flag Units LOD/MDL LOQ Dilution Reference Method Prepared Analyzed Analyst 83-32-9 Acenaphthene ND ug/kg dry 50 99 2 EI'A8270D 11/28/201606:13 11/28201621:12 KH Certifications: CTD0H,NELAC-NY10854,NJDEP,PADEP 208-96-8 Acenaphthylene ND ug/kg dry 50 99 2 EPA 8270D 111=01606:13 1128201621:12 KH Certifications: CCD0H,NELAC-NYl0854,NJDEP,PADEP 120-12-7 Anthracene ND ug/kg dry 50 99 2 EPA 8270D 1128201606:13 II28201621:12 KH Certifications: CTD0H,NELAC-NY10854,NJDEP,PADEP 56-55-3 Benzo(a)anthracene ND ug/kg dry 50 99 2 EPA 8270D 1128/201606:13 112820162I:12 KH Certifications: CCD0H,NELAC-NY10854,NJDEP,PADEP 50-32-8 Benzo(a)pyrene ND ug/kg dry 50 99 2 EPA 8270D 1128/201606:13 1128201621:12 KH Certifications: CTD0H,NELAC-NY10854,NJDEPPADEP 205-99-2 Benzo(b)fluoranthene ND ug/kg dry 50 99 2 EPA 8270D 1128201606:13 1128201621:12 KH Certifications: CTD0H,NELAC-NYl0854,NJDEP,PADEP 191-24-2 Benzo(g,h,i)perylene ND ug/kg dry 50 99 2 EPA 8270D 1128201606:13 1128201621:12 KH Certifications: CTDOH,NELAC-NYI0854,NJDEPPADEP 207-08-9 Benzo(k)fluoranthene ND ug/kg dry 50 99 2 EPA 8270D 1128201606:13 1128201621:12 KH Certifications: CTD0H,NE1AC-NY10854,NJDEP,PADEP 218-01-9 Chrysene ND ug/kg dry 50 99 2 EPA 8270D 1128201606:13 I128201621:12 KH Certifications: CTD0H,NELAC-NY10854,NJDEP,PADEP 53-70-3 Dibenzo(a,h)anthracene ND ug/kg dry 50 99 2 EPA 8270D 11282016 06:13 11282016 21:12 KH Certifications: CTD0H,NE1AC-NY10854,NJDEPPADEP 206-44-0 Fluoranthene ND ug/kg dry 50 99 2 EPA 8270D 1128201606:13 1128201621:12 KH Certifications: CTD0H,NELAC-NY10854,NJDEPPADEP 86-73-7 Fluorene ND ug/kg dry 50 99 2 EPA 8270D 1128201606:13 1128201621:12 KH Certifications: NELAC-NY 10854,NJDEP,PADEP 193-39-5 1ndeno(1,2,3-cd)pyrene ND ug/kg dry 50 99 2 EPA 8270D 1128201606:13 1128201621:12 KH Certifications: CTD0H,NELAC-NY10854,NJDEPPADEP 91-20-3 Naphthalene ND ug/kg dry 50 99 2 EPA 8270D 1128201606:13 1129201621:12 KH Certifications: CTD0H,NELAC-NYl0854,NJDERPADEP 85-01-8 Phenanthrene ND ug/kg dry 50 99 2 EPA 8270D 1128201606:13 11282016 21:12 KH Certifications: CTD0H,NELAC-NY10854,NJDEP,PADEP 129-00.0 Pyrene ND ug/kg dry 50 99 2 EPA 8270D 11282016 06:13 11282016 21:12 KH Certifications: CTD01,NELAC-NY10854,NJDEP,PADEP Surrogate Recoveries Result Acceptance Range 4165-60-0 Surrogate:Nitrobenzene45 59.6% 22-108 321-60-8 Surrogate:2-Fhtarobiphenyl 51.2% 21-113 1718-51-0 Surrogate:Terphenv1414 50.8% 14-116 Total Solids Log-in Notes: Sample Notes: Sample Prepared by Method:%Solids Prep Reported to Date/Time Date/Time CAS No. Parameter Result Flag Units LOD/MDL LOQ Dilution Reference Method Prepared Analyzed Analyst solids *%Solids 83.9 % 0.100 0.100 1 SM 254OG 11292016 09:34 I I/29/2016 16:04 DM I Certification.: CTD011 120 RESEARCH DRIVE STRATFORD,CT 06615 ■ 132-02 89th AVENUE RICHMOND HILL,NY 11418 www.YORKLAB.com (203)325-1371 FAX(203)357-0166 ClientServices Page 5 of 18 1 ' Sample Information Client Sample ID: Sidewall-1 lurk Sample ID: 16KO861-01 York Project(SDG)No. Client Project ID Matrix Collection Date/Time Date Received 16KO861 42 Roanoke Avenue,Rye Brook,NY Soil November 18,2016 10:00 am 11/21/2016 Sample Information Client Sample ID: Sidewall-2 York Sample ID: 16KO861-02 York Proiect(SDG)No. Client Proiect ID Matrix Collection Date/Time Date Received 16KO861 42 Roanoke Avenue,Rye Brook,NY Soil November 18,2016 10:00 am 11/21/2016 Volatile Organics,CP-51(formerly STARS)List Loe-in Notes: Sample Notes: Sample Prepared by Method:EPA 5035A Reported to DateJf'lme Date/'1'ime CAS No. Parameter Result Flag Units LOD/blD1, LOQ Dilution Reference Method Prepared Analyzed Analyst 95-63.6 1,2,4-Trimethylbenzene ND ug/kg dry 2.3 4.5 1 EPA 8260C I1/22201608:07 11=01613:50 SS Certifications: CfDOH,NELAC-NY 10854,NJDEP 108-67-8 1,3,5-Trimethylbenzene ND ug/kg dry 2.3 4.5 1 EPA 8260C 11/22201608:07 1122201613:50 SS Certifications: CTDOH,NELAC-NY 10854,NJDEP 7143-2 Bcnzcnc ND ug/kg dry 2.3 4.5 1 EPA 8260C 1122201608:07 11222016 13:50 SS Certifications: CTDOH,NF.LAC-NY 10854,NJDEP,PADF-P 100-414 Ethyl Bcnzcnc ND ug/kg dry 2.3 4.5 1 EPA 8260C 11222016 08:07 1122/2016 13:50 SS Certifications: CTDORNF--LAC-NY 10854,NJDEP,PADEP 98-82.8 Isopropylbenzcne ND ug/kg dry 2.3 4.5 1 EPA 8260C 1122201608:07 11221201613:50 SS Certifications: CTDOH.NELAC-NY 10854,NJDEP 1634-04-4 Methyl tcn-butyl ether(MTBE) ND ug/kg dry 2.3 4.5 1 EPA 8260C II=01608:07 1122/201613:50 SS Certifications: CTDOH,NF.LAC-NY 10854,NJDEP 91-20-3 Naphthalene ND ug/kg dry 2.3 9.1 1 EPA 8260C 11/22201608:07 1122/201613:50 SS Certifications: NELAC-NY 10854,N1DF.P 104-51-8 n-Butylbenzene ND ug/kg dry 2.3 4.5 1 EPA 8260C 1122/201608:07 11 rM01613:50 SS Certifications: CTD0H,NELAC-NYI0854,NJDEP 103-65-1 n-Propylbcnzenc ND ug/kg dry 2.3 4.5 1 EPA 8260C 1122201608:07 11222016 13:50 SS Certifications: CrD0H,NELAC-NY10854,NJDEP 9547-6 o-Xylene ND ug/kg dry 2.3 4.5 1 EPA 8260C 11/22/201608:07 1122201613:50 SS Certifications: CrDOH,NELAC-NY10854 179601-23-1 p-&m-Xylcncs ND ug/kg dry 4.5 9.1 1 EPA 8260C 11/22201608:07 11222016 13:50 SS Ceniftcations: CTDOH.NF.LAC-NY10854 99-87-6 p-Isopropyltolucne ND ug/kg dry 2.3 4.5 1 EPA 8260C 11/22201608:07 11222016 13:50 SS Certifications: CrDOH.NELAC-NY 10854.NJDEP 135-98-8 sec-Butylbenzene ND ug/kg dry 2.3 4.5 1 EPA 8260C 1122/2016 08:07 11222016 13:30 SS Certifications: CrD0H,NF.LAC-NY10854,NJDEP 98-06-6 tert-Butylbcnzene ND ug/kg dry 2.3 4.5 1 EPA 8260C 1122201608:07 1122201613:50 SS Cenifications: CTDOH.NELAC-NY I0854,NJDEP 108-88-3 Toluene ND ug/kg dry 2.3 4.5 1 EPA 8260C 11/22201608:07 1122/201613:50 SS Certifications: CTDOH.NELAC-NY 10854,NJDEP,PADEP 1330-20-7 Xylcncs,Total ND ug/kg dry 6.8 14 1 EPA 8260C 11222016 08:07 11222016 13:50 SS Certifications: CTDOH.NELAC-NY 10854,NJDEP,PADEP Surrogate Recoveries Result Acceptance Range 120 RESEARCH DRIVE STRATFORD,CT 06615 ■ 132-02 89th AVENUE RICHMOND HILL,NY 11418 www.YORKLAB.com (203)325-1371 FAX(203)357-0166 ClientServices ii Page 6 of 18 1 ' Sample Information Client Sample ID: Sidewall-2 York Sample ID: 16KO861-02 York Project(SDG)No. Client Proiect ID Matrix Collection Date/Time Date Received 16KO861 42 Roanoke Avenue,Rye Brook,NY Soil November 18,2016 10:00 am 11/21/2016 Volatile Oreanics,CP-51(formerly STARS)List Loe-in Notes: Sample Notes: Sample Prepared by Method:EPA 5035A Reported to Date/Time Date/Time CAS No. Parameter Result Glag l nits LODAWL LOQ Dilution Reference Method Prepared Analyzed Analyst 17060-07-0 Surrogate:1,2-Dichloroethane-d4 113% 77-125 2037-26-5 Surrogate:Toluened8 99.0% 85-110 460-00-4 Surrogate:p-BromoJluorobenzene 93.7% 76-130 Semi-Volatiles,CP-51 (formerly STARS)List Loe-in Notes: Sample Notes: Sample Prepared by Method:EPA 3550C Reported to Date/Time Date/Time CAS No. Parameter Result Flag Units LOD/MDL LOQ Dilution Reference Method Prepared Analyzed Analyst 83-32-9 Acenaphthene ND ug/kgdry 51 100 2 EPA 8270D 1128/201606:13 1128/201621.45 KH Certifications: CrWH,NE1AC-NY10854,NJDEP,PADEP 208-96-8 Acenaphthylene ND ug/kgdry 51 100 2 EPA 8270D 1128201606:13 1128201621:45 KH Certifications: C`rD0H,NELAC-NY10854,NJDEP,PADEP 120-12-7 Anthracene ND ug/kgdry 51 100 2 EPA 8270D 1128201606:13 1128201621:45 KH Certifications: CI'D0H,NELAC-NY10854,NJDEPPADEP 56-55-3 Benzo(a)anthracene ND ug/kgdry 51 100 2 EPA 8270D 1128201606:13 1128201621.45 KH Ccrtifications: CTD0H,NELAC-NYl0854,NJDEPPADEP 50-32-8 Benzo(a)pyrene ND ug/kgdry 51 100 2 EPA 8270D 112820I606:13 1128201621:45 KH Certifications: CTD0H,NELAC-NY10854,NJDEP,PADEP 205-99-2 Benzo(b)fluoranthene ND ug/kg dry 51 100 2 EPA 8270D 11282016 06:13 11282016 21:45 KH Certifications: CTD0H,NELAC-NY10854,NJDEP,PADEP 191-24-2 Benzo(g,h,i)perylene ND ug/kgdry 51 100 2 EPA 8270D 1128201606:13 1128201621:45 KH Certifications: CCD0H,NELAC-NYl0854,NJDEP,PADEP 207-08-9 Benzo(k)fluoranthene ND ug/kgdry 51 100 2 EPA 8270D 1128201606:13 1128201621:45 KH Certifications: CCD0H,NE1AC-NY10854,NJDEP,PADEP 21841-9 Chrysene ND ug/kgdry 51 100 2 EPA 8270D 1128201606:13 1128201621:45 KH Certifications: CCD0H,NELAC-NY10854,NJDEP,PADEP 53-70-3 Dibenzo(a,h)anthracene ND ug/kgdry 51 100 2 EPA 8270D I128201606:13 1128201621:45 KH Certifications: CTD0H,NELAC-NY10854,NJDEP,PADEP 206-44-0 Fluoranthene ND ug/kgdry 51 100 2 EPA 8270D 1128201606:13 1128201621:45 KH Certifications: CTD0H,NELAC-NY10854,NJDEP,PADEP 86-73-7 Fluorene ND ug/kgdry 51 t00 2 EPA 8270D 1128201606:13 1129201621:45 KH Certifications: NELAC-NY10854,NJDEPPADEP 193-39-5 Indeno(1,2,3-cd)pyrene ND ug/kgdry 51 100 2 EPA 8270D 1128201606:13 1128201621:45 KH Certifications: CTD0N,NELAC-NYl0854,NJDEP,PADEP 91-20-3 Naphthalene ND ug/kgdry 51 100 2 EPA 8270D 1128201606:13 1128201621:45 KH Certifications: CfD0H,NE1AC-NY10854,NJDEP,PADEP 85-01-8 Phenanthrene 63 J ug/kgdry 51 100 2 EPA 8270D 1128201606:13 1128201621:45 KH Certifications: CTD01t,NELAC-NYl0854,NJDEP,PADEP 129-00-0 N ren e ND ug/kg dry 51 100 2 EPA 8270D 11282016 06:13 11282016 21:45 KH Certifications: CfD0H,NELAC-NY10854,NJDEP,PADEP Surrogate Recoveries Result Acceptance Range 4165-60-0 Surrogate:Nitrobenzene-d5 46.4"„ 22-103 120 RESEARCH DRIVE STRATFORD,CT 06615 ■ 132-02 89th AVENUE RICHMOND HILL,NY 11418 www.YORKLAB.com (203)325-1371 FAX(203)357-0166 ClientServices Page 7 of 18 Sample Information ('lient Sample ID: Sideltall-2 fork Sample ID: 16KO861-02 York Proiect(SDG)No. Client Proiect ID Matrix Collection Date/Time Date Received 16KO861 42 Roanoke Avenue,Rye Brook,NY Soil November 18,2016 10:00 am 11/21/2016 Semi-Volatiles.CP-51(formerly STARS)List Loa-in Notes: Sample Notes: Sample Prepared by Method:EPA 3550C Repotted to Date/Time Date/Time CAS No. Parameter Result Flag Units LOD/MDL LOQ Dilution Reference Method Prepared Analyzed Analyst 321.6" Surrogate:2-Fluorobiphenyl 39.4% 21-113 1718-51-0 Surrogate:Terphenyl-dM 46.7% 14-116 Total Solids Loa-in Notes: Sample Notes: Sample Prepared by Method:%Solids Prcp Reponed to Date/Time Date/Time CAS No. Parameter Result Flag Units LOD/MDL LOQ Dilution Reference Method Prepared Analyzed Analyst solids %Solids 81.4 % 0.100 0.100 1 SM 254OG 11/29/201609:34 1129/201616:04 DMI Ccnifications: CrDOH Sample Information Client Sample ID: Sidewall-3 York Sample ID: 16KO861-03 York Proiect(SDG)No. Client Project ID Matrix Collection Date/Time Date Received 16KO861 42 Roanoke Avenue,Rye Brook,NY Soil November 18,2016 10:00 am 11/21/2016 Volatile Oreanics,CP-51(formerly STARS)List I.ot(-in Notes: Sample Notes: Sample Pmparcd by Method:EPA 5035A Rcponcd to Date/Time Date/Time CAS No. Parameter Result Flag Units LOD/MDL LOQ Dilution Reference Method Prepared Analyzed Analyst 95-63.6 1,2,4-Trimethylbenzene ND ug/kg dry 2.1 4.1 1 EPA 8260C 11/22/201609:07 11/22/2016 14:24 ss Certificatims: CPD0H,NE1AC-NY10854,NJDEP 108-67-8 1,3,5-Trimethylbenzene ND ug/kgdry 2.1 4.1 1 EPA 8260C 11/22/201608:07 11/221201614:24 SS Certifications: CrDOH,NELAC-NY10854,NJDEP 71A3.2 Benzene ND ug/kgdry 2.1 4.1 1 EPA 8260C 1122201608:07 11/221201614:24 ss Certifications: CTD0H,NELAC-NY10854,NJDEP,PADEP 100AIA Ethyl Benzene ND ug/kg dry 2.1 4.1 1 EPA 8260C 11/22/201608:07 11/22/201614:24 SS Ccnifications: CfDOH,NELAC-NY10854,NJDEPPADEP 98-82-8 lsopropylbenzene ND ug/kg dry 2.1 4.1 1 EPA 8260C 1122/201608:07 I V22/2016 14:24 ss Certifications: CrD0H,NELAC-NY10854,NJDEP 1634-04-4 Methyl tert-butyl ether(MTBE) ND ug/kg dry 2.1 4.1 1 EPA 8260C 1122/201608:07 1122201614:24 SS Certifications: CrD0H,NELAC-NY10854,NJDEP 91-20-3 Naphthalene ND ug/kg dry 2.1 8.3 1 EPA 8260C 1122201608:07 1122201614:24 SS Ccri ficatioos: NELAC-NY10854,NJDEP 104-51-8 n-Butylbenzene ND ug/kg dry 2.1 4.1 1 EPA 8260C 1122201608:07 1122201614:24 Ss Certifications: C7D0H,NELAC-NY10854,NJDEP 103-65-1 n-Propylbenzene ND ug/kgdry 2.1 4.1 1 EPA 8260C 11/22201608:07 1122/201614:24 SS Ccniftcations: C['D0H,NELAC-NY10854,NJDEP 120 RESEARCH DRIVE STRATFORD,CT 06615 ■ 132-02 89th AVENUE RICHMOND HILL,NY 11418 www,YORKLAB.com (203)325-1371 FAX(203)357-0166 ClientServices Page 8 of 18 1 ' Sample Information Client Sample ID: Sidewall-3 York Sample ID: 16KO861-03 York Project(SDG)No. Client Proiect ID Matrix Collection Date/Time Date Received 16KO861 42 Roanoke Avenue,Rye Brook,NY Soil November 18,2016 10:00 am 11/21/2016 Volatile Organics,CP-51(formerly STARS)List Loa-in Notes: Sample Notes: Sample Prepared by Method:EPA 5035A Reported to Date/Time Date/Time CAS No. Parameter Result Flag Units LODINID1, LOQ Dilution Reference Method Prepared Analyzed Analyst 9547-6 o-Xylene ND ug/kg dry 2.1 4.1 1 EPA 8260C 11/221201608:07 111=01614:24 SS Certifications: CTDOKNELAC-NY10854 179601-23-1 p-&m-Xylenes N D uglkg dry 4.1 8.3 1 EPA 8260C 11222016 08:07 11222016 14:24 SS Certifications: CTDOKNELAC-NY10854 99-87-6 p-Isopropyltoluene ND ug/kg dry 2.1 4.1 1 EPA 8260C 1122201608:07 1122201614:24 SS Certifications: CTD0H,NELAC-NY10854,NJDEP 135-98-8 scc-Butylbcnzenc ND ug/kg dry 2.1 4.1 1 EPA 8260C 1122201608:07 1122201614:24 SS Certifications: CTDOH.NELAC-NY10854,NJDEP 98-06-6 tert-Butylbenzene ND ug/kg dry 2.1 4.1 1 EPA 8260C 1122201608:07 1122/201614:24 SS Certifications: CTDOH,NELAC-NY10854,NJDEP 108-88-3 Toluene ND ug/kg dry 2.1 4.1 1 EPA 8260C 1122201608:07 1122201614:24 SS Certifications: CTII0H.NELAC-NYI0854,NJDEP,PADEP 1330.20-7 Xylenes,Total ND ug/kg dry 6.2 12 1 EPA 8260C 11222016 08:07 11222016 14:24 SS Certifications: CTD0H,NELAC-NY10854,NJDEP,PADEP Surrogate Recoveries Result Acceptance Range 17060-07-0 Surrogate:1,2-Diehloroethane-d4 110% 77-125 2037-26-5 Surrogate:Toluene-d8 98.4% 85-120 460-00-4 Surrogate:p-Bromo/luorobenzene 93.5% 76-130 Semi-Volatiles,CP-51(formerly STARS)List Loa-in Notes: Sample Notes: Sample Prepared by Method:EPA 3550C Reported to Date/Time Date/Time CAS No. Parameter Result Flag Units LOD/MDL LOQ Dilution Reference Method Prepared Analyzed Analyst 8332-9 Acenaphthene ND ug/kg dry 50 99 2 EPA 8270D 1128201606:13 1128201622:17 KH Certifications: CTD0ILNELAC-NY10854,NJDEP,PADEP 208-96-8 Acenaphthylcne ND ug/kg dry 50 99 2 EPA 8270D 1128201606:13 11282016 22:17 KH Certifications: CTD0H,NELAC-NY10854,NJDEP,PADEP 120-12-7 Anthraccnc ND ug/kg dry 50 99 2 EPA 8270D 1128201606:13 1128201622:17 KH Certifications: CTDOH.NELAC-NY 10854,NJDEP.PADEP 56-55-3 Benzo(a)anthracene ND ug/kg dry 50 99 2 EPA 8270D 1129/201606;13 11/=01622:17 KH Certifications: CTDOH,NELAC-NY10854,NJDEP.PADEP 50-32-8 Bcnzo(a)pyrene ND ug/kg dry 50 99 2 EPA 8270D 1128201606:13 1128201622:17 KH Certifications: CTD0H,NELAC-NY10854,NJDEP.PADEP 205-99-2 Benzo(b)fluomnthene ND ug/kg dry 50 99 2 EPA 8270D 1128201606:13 1128201622:17 KH Certifications: CTD0H,NELAC-NY10854,NJDEP,PADEP 191-24-2 Benzo(g,h,i)perylene ND ug/kg dry 50 99 2 EPA 8270D 1128201606:13 1128201622:17 KH certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP 207-08-9 Benzo(k)fluoranthene ND ug/kg dry 50 99 2 EPA 8270D 1128201606:13 1128201622:17 KH Certifications: CTD0H,NELAC-NY10854,NJDEP,PADEP 218-01-9 Chryscnc N D ug/kg dry 50 99 2 EPA 8270D 11282016 06:13 11282016 22:17 KH Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP 120 RESEARCH DRIVE STRATFORD,CT 06615 ■ 132-02 89th AVENUE RICHMOND HILL,NY 11418 www.YORKLAB.com (203)325-1371 FAX(203)357-0166 ClientServices Page 9 of 18 I ' Sample Information Client Sample ID: Sidewall-3 York Sample ID: 16KO861-03 York Proiect(SDG)No. Client Proiect ID Matrix Collection Date/Time Date Received 16KO861 42 Roanoke Avenue,Rye Brook,NY Soil November 18,2016 10:00 am 11/21/2016 Semi-Volatiles,CP-51(formerly STARS)List Log-in Notes: Sample Notes: Sample Prepared by Method:EPA 3550C Reported to Date/Time Date/Time CAS No. Parameter Result Flag Units LOD/NIDL LOQ Dilution Reference Method Prepared Analyzed Analyst 53-70-3 Dibenzo(a,h)anthracene ND ugtkgdry 50 99 2 EPA 8270D 1129/201606:13 11/28/201622:17 KH Certifications: CTD0H,NELAC-NY10854,NJDEP,PADEP 206-44-0 Fluoranthenc ND ug/kg dry 50 99 2 EPA 8270D 11/28/201606:13 1128201622:17 KH Certifications: CTD0H,NELAC-NY10854,NJDEP,PADEP 86-73-7 Fluorcne ND ug/kg dry 50 99 2 EPA 8270D 1128201606:13 11/28/201622:17 KH Certifications: NELAGNY10854,NJDEPPADEP 193-39-5 Indcno(1,2,3cd)pyrcne ND ug/kg dry 50 99 2 EPA 8270D 1128201606:13 1128201622:17 KH Certifications: (7=H,NELAC-NY10854,NJDEP,PADEP 91-20-3 Naphthalene ND ug/kg dry 50 99 2 EPA 8270D 1128201606:13 1128201622:17 KH Certifications: CTD0H,NELAC-NY10854,NJDEP,PADEP 85-01-8 Phenanthrene N D ug/kg dry 50 99 2 EPA 8270D 11282016 06:13 11282016 22:17 KH Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP 1294)0-0 Pyrenc ND ug/kg dry 50 99 2 EPA 8270D 11282016 06:13 11282016 22:17 KH Certifications: CTD0H.NELAC-NY10854,NJDEP,PADEP Surrogate Recoveries Result Acceptance Range 4165-60-0 Surrogate:Nitrobenzene-d5 48.2% 22-108 321-60-8 Surrogate:2-Fluorobiphenyl 44.4% 11-113 1718-51-0 Surrogate:Terpheny6d14 52.4% 24-116 Total Solids Log-in Notes: Sample Notes: Sample Prepared by Method:%Solids Prep Reported to Date/Time Datdnme CAS No. Parameter Result Flag Units LOD/MDL LOQ Dilution Reference Method Prepared Analyzed Analyst solids *%Solids 84.0 % 0.100 0.100 1 SM 25400 1129201609:34 1129201616:04 DMI Cmificalions: CTDOH Sample Information Client Sample ID: Sidewall-4 York Sample ID: 16K0861-W York Project(SDG)No. Client Project ID Matrix Collection Date/Time Date Received 16KO861 42 Roanoke Avenue,Rye Brook,NY Soil November 18,2016 10:00 am 11/21/2016 Volatile Organics,CP-51(formerly STARS)List Log-in Notes: Sample Notes: Sample Prepared by Method:EPA 5035A Reported to Date/Time DateAftme CAS No. Parameter Result Flag Units LODAIDL LOQ Dilution Reference Method Prepared Analyzed Analyst 95-63-6 1,2,4-Trimethylbenzene ND ugtkg dry 2.0 4.1 1 EPA8260C 1122201608:07 1122201614:58 SS Certifications: CTDOH,NELAC-NY10854,NJDEP 120 RESEARCH DRIVE STRATFORD,CT 06615 ■ 132-02 891h AVENUE RICHMOND HILL,NY 11418 www.YORKLAB.com (203)325-1371 FAX(203)357-0166 ClientServices Page 10 of 18 1 ' Sample Information Client Sample ID: Sidewal14 York Sample ID: 16KO861-04 York Project(SDG)No. Client Project ID Matrix Collection Date/Time Date Received 16KO861 42 Roanoke Avenue,Rye Brook,NY Soil November 18,2016 10:00 am 11/21/2016 N olatile Organics.CP-51(formerly STARS)List Loa-in Notes: Sample Notes: Sample 1'repared by Method:EPA 5035A Reported to DatefIime Date/Time CAS No. Parameter Result Flag Units LODMIDL LOQ Dilution Reference Method Prepared Analyzed Analyst 108-67-8 1,3,5-Trimethylbcnzenc ND ug/kg dry 2.0 4.1 1 EPA 8260C 11/22/201608:07 11/22/201614:58 SS Certifications: CTD0H,NELAC-NY10854,NJDEP 7143-2 Benzene ND ug/kg dry 2.0 4.1 1 EPA 8260C 11/22/201608:07 1122/201614:58 SS Certifications: CTD0KNELAC-NY10854,NJDEP,PADEP 100-414 Ethyl Benzene ND ug/kg dry 2.0 4.1 1 EPA 8260C 11222016 08:07 1122/2016 14:58 SS Certifications: CTD0KNELAC-NY10854,NJDEP,PADEP 98-82-8 Isopropylbenzenc ND ug/kg dry 2.0 4.1 1 EPA 8260C I122201608:07 111=01614:58 SS Certifications: CTD0H,NELAC-NY10854,NJDEP 1634-04-4 Methyl tert-butyl ether(MTBE) ND ug/kg dry 2.0 4.1 1 EPA 8260C 1122201608:07 1122201614:58 SS Certifications: CTD0H,NELAC-NY10854,NJDEP 91-20-3 Naphthalene ND ug/kg dry 2.0 8.2 1 EPA 8260C 1122201608:07 1122/201614:58 SS Certifications: NELAC-NY10854,NJDEP 104-51-8 n-Butylbenzene ND ug/kg dry 2.0 4.1 1 EPA 8260C 1122201608:07 1122201614:58 Ss Certifications: CTD0H,NELAC-NY10854,NJDEP 103-65-1 n-Propylbenzene ND ug/kg dry 2.0 4.1 1 EPA 8260C 1122201608:07 1122201614:58 ss Certifications: CfD0H,NELAC-NY10854,NJDEP 9547.6 o-Xylene N D ug/kg dry 2.0 4.1 1 EPA 8260C 11222016 08:07 11222016 14:58 SS Certifications: CrD0H,NELAC-NY10854 179601-23-1 p-&m-Xylenes ND ug/kg dry 4.1 8.2 1 EPA 8260C I1222016 08:07 1122201614:58 SS Certifications: CTDOH,NELAC-NY10854 99-87-6 p-Isopropyltoluene ND ug/kg dry 2.0 4.1 1 EPA 8260C 1122201608:07 1I/=01614:58 ss Certifications: CfD0H.NELAC-NY10854,NJDEP 135-98-8 sec-Butylbenzene ND ug/kg dry 2.0 4.1 1 EPA 8260C Ii22/201608:07 1122/201614:58 SS Certifications: CI'D0H,NELAC-NY10854,NJDEP 98-06-6 tort-Butylbenzene ND ug/kg dry 2.0 4.1 1 EPA 8260C 1122201608:07 1122/201614:58 ss Certifications: CPDOH,NELAC-NY10854,NJDEP 108-88-3 Toluene ND ug/kg dry 2.0 4.1 1 EPA 8260C 1122201608:07 1122201614:58 SS Certifications: CID0H,NELAC-NY10854,NJDEP,PADEP 1330-20-7 Xylenes,Total ND ug/kg dry 6.1 12 1 EPA 8260C 11222016 08:07 l 1222016 14:58 SS Certifications: CrD0H,NELAC-NY10854,NJDEPBADEP Surrogate Recoveries Result Acceptance Range 17060-07-0 Surrogate:1,2-Dichloroethane-d4 104% 77-125 2037-26-5 Surrogate:Toluene-& 103% 85-120 460-00-4 Surrogate:p-BromoJluorobenzene 120% 76-130 Semi-Volatiles.CP-51(formerly STARS)List Lop_-in Notes: Sample Notes: Sample Prepared by Method:EPA 3550C Reported to Date/Time Daterrime CAS No. Parameter Result Flag Units LOWIM, LOQ Dilution Reference Method Prepared Analyzed Analyst 83-32-9 Acenaphthene ND ug/kg dry 50 100 2 EPA 8270D 11282016 06:13 11282016 22:50 KH Cer ifcations: CTD0H,NELAC-NY10854,NJDEP,PADEP 120 RESEARCH DRIVE STRATFORD,CT 06615 ■ 132-02 89th AVENUE RICHMOND HILL,NY 11418 www.YORKLAB.com (203)325-1371 FAX(203)357-0166 ClientServices Page 11 of 18 1 ' Sample Information Client Sample ID: Sidewall4 lurk Sample ID: 16KO861-04 York Project(SDG)No. Client Proiect ID Matrix Collection Date/Time Date Received 16KO861 42 Roanoke Avenue,Rye Brook,NY Soil November 18,2016 10:00 am 11/21/2016 Semi-Volatiles.CP-51(formerly STARS)List LoQ-in Notes: Sample Notes: Sample Prepared by Method:EPA 3550C Rclxncd to Date/Time Date/Time CAS No. Parameter Result Flat; I nits I ODAIDI I uU Dilution Reference Method Prepared Anahzed Analyst 209-96-8 Acenaphthylcnc ND ug/kg dry 50 I00 2 EPA 8270D I I28/2016 06:13 1128/2016 22:50 KH Certifications: CrDOH.NF.LAC-NY 10854,NJDEP.PADEP 120-12-7 Anthraccnc ND ug/kg dry 50 100 2 EPA8270D 1128/201606:13 1128201622:50 Kli Certiftutions: CTDOH.NELAC-NY10854,NJDEP.PADEP 56-55-3 Benzo(a)anlhraccne ND ug/kg dry 50 100 2 EPA 8270D 11282016 06:13 11292016 22:50 Kit Certifications: CTD0H.NF.LAC-NY10854,NJDEP.PADF.P 50-32-8 Benzo(a)pyrenc ND ug/kg dry 50 too 2 EPA8270D 11/28201606:13 1128/201622:50 Kit Certifications: CTDOH.NF.LAC-NY 10854,NJDEP.PADEP 205-99-2 Benzo(b)Iluoranthene ND ug/kg dry 50 100 2 EPA8270D 1128201606:13 112W01622:50 Kli Certifications: CTDOH,NELAC-NY 10854,NJDEP.PADEP 19124-2 Benzo(g,h,i)perylcne ND ug/kg dry 50 100 2 EPA8270D 1128/201606:13 1128201622:50 Kit Certifications: CTDOH,NF,LAC-NY 10854,NJDEP.PADEP 207-08-9 Benzo(k)Ouoranthene ND ug/kg dry 50 100 2 EPA 8270D 1 1/28/201 6 06:13 1129/201622:50 K11 Certifications: CTD0H,NELAC-NY10854,NJDEP,PADEP 218-01-9 Chryscne ND ug/kg dry 50 100 2 EPA8270D 1128201606:13 1128201622:50 Kli Cenifica6ons: CTDOH.NELAC-NY 10854,NJDEP,PADEP 53-70-3 Dibcnzo(a,h)anthraccne ND ug/kg dry 50 100 2 EPA8270D 1128201606:13 1128201622:50 Kit Certifications: CTDOH.NELAC-NY 10854,NJDEP.PADF.P 20644-0 Fluoranthene ND ug/kg dry 50 100 2 EPA8270D 1128201606:13 1128/201622:50 Kit Certifications: CrD0H.NELAC-NY10854,NJDEP.PADEP 86-73-7 Fluorenc ND ug/kg dry 50 100 2 EPA 8270D 1128/201606:13 1128/201622:50 KH Certifications: NELAC-NY10854.NJDEPPADF,P 193-39-5 Indcno(1,2,3-cd)pyrcnc ND ug/kg dry 50 100 2 EPA9270D 11/28201606:13 11/28201622:50 Kit Certifications: CTDOH.NELAC-NY 10854,N1DEP,PADEP 91-20-3 Naphthalene ND ug/kg dry 50 100 2 EPA 8270D 11/28/201606:13 1128201622:50 Klt Certifications: CfDOH.NELAC-NY 10854MDEPTADF.P 85-01-8 Phenanthrcnc ND ug/kg dry 50 100 2 EPA8270D 1128/201606:13 1128/201622:50 Fit Certifications: CTDOH,NELAC-NY 10854,NJDEP,PADF.P 129400.0 Pyrenc ND ug/kg dry 50 100 2 EPA8270D 1128201606:13 1128201622:50 Kit Certifications: CTDOH.NELAC-NY 10854,NJDEP,PADF.P Surrogate Recoveries Result Acceptance Range 4165-60-0 Surrogate:Nitrobenzene-d5 51.6% 22-108 321-60-8 Surrogate:1-Fbrorobiphenyl 47.3% 21-113 1718-51-0 Surrogate:Terphenvl-d14 63.3 o, 24-116 Total Solids Lo¢-in Notes: Sample Notes: Sample Prepared by Method:%Solids Prep RcT,rtcd to Date/Time Date/Time CAS No. Parameter Result Flag Units LOD/MDI, LOQ Dilution Reference Method Prepared Analyzed Analyst solids •%Solids 83.0 0 0.100 0.100 1 SM 254OG 1129201609:34 11292016 16:04 DMI Certifications: CTDOH 120 RESEARCH DRIVE STRATFORD,CT 06615 ■ 132-02 89th AVENUE RICHMOND HILL,NY 11418 www.YORKLAB.com (203)325-1371 FAX(203)357-0166 ClientServices Page 12 of 18 1 ' Sample Information Client Sample ID: Excavation Bottom York Sample m: 16KO861-05 York Project(SDG)No. Client Project ID Matrix Collection Date/Time Date Received 16KO861 42 Roanoke Avenue,Rye Brook,NY Soil November 18,2016 10:00 am 11/21/2016 Volatile Orsanics.CP-51(formerly STARS)List Loa-in Notes: Sample Notes: Sample Prepared by Method:EPA 5035A Reported to Date/Time Date/Time CAS No. Parameter Result Flag Units LOD/MDL LOQ Dilution Reference Method Prepared Analyzed Amdyst 95-63-6 1,2,4-Trimethylbenzene ND ug/kg dry 2.0 4.0 1 EPA 8260C 1 1/22/201 6 08:07 11/22/201615:32 SS Certifications: CTD0H,NELAC-NY10854,NJDEP 108-67-8 1,3,5-Ttimethylbenzene ND ugtkg dry 2.0 4.0 1 EPA 8260C 1122/201608:07 IIFM01615:32 SS Certifications: CTD0H,NELAC-NY10854,NJDEP 71-43-2 Benzene ND ug/kgdry 2.0 4.0 1 EPA 8260C 1122201608:07 1122201615:32 SS Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP 100-41-4 Ethyl Benzene ND ug/kgdry 2.0 4.0 1 EPA 8260C 1122201608:07 ]I/=01615:32 SS Certifications: CTDOH,NELAC-NY 10854,NJDEP,PADEP 98-82-8 lsopropylbenzene ND ug/kgdry 2.0 4.0 1 EPA 8260C 111=01608:07 1122201615:32 SS Cenifications: CTDOH.NELAC-NY10854,NJDEP 1634-04-4 Methyl tert-butyl ether(MTBE) ND ug/kg dry 2.0 4.0 1 EPA 8260C 1122/2016 08:07 11221201615:32 SS Certifications: CTDOH.NELAC-NY10854,NJDEP 91-20-3 Naphthalene ND ug/kgdry 2.0 7.9 1 EPA 8260C 1122201608:07 1122/201615:32 SS Certifications: NELAC-NY10854,NJDEP 104-51-8 n-Butylbenzene ND ug/kgdry 2.0 4.0 1 EPA 8260C 1122201608:07 1122201615:32 SS Certifications: CTD0H,NELAC-NY10854,NJDEP 103-65-1 n-Propylbenzene ND ug/kgdry 2.0 4.0 1 EPA 8260C 1122201608:07 11r=01615:32 SS Cenifications: CTD01i,NELAC-NY10854,NJDEP 95A7-6 o-Xylene ND ug/kgdry 2.0 4.0 1 EPA 8260C 1122201608:07 1122201615:32 SS Certifications: CTDOH,NELAC-NY10854 179601-23.1 p-&m-Xylenes N D ug/kg dry 4.0 7.9 1 EPA 8260C 11222016 08.07 11/=016 15:32 SS Certifications: CTDOILNELAC-NY10854 99-87-6 p-Isopropyltoluene ND ug/kgdry 2.0 4.0 1 EPA 8260C Il22201608:07 111=01615:32 SS Certifications: CTDOH,NELAC-NY 10854,NJDEP 135-98-8 sec-Butylbenzene ND ug/kg dry 2.0 4.0 1 EPA 8260C 1122/2016 08:07 11221201615:32 SS Certifications: CTDOH,NELAC-NY10854,NJDEP 98-06-6 tert-Butylbenzene ND ug/kgdry 2.0 4.0 1 EPA 8260C 11/22201608:07 1122201615:32 SS Certifications: CTD0H,NELAC-NY10854,NJDEP 108-88-3 Toluene ND ug/kg dry 2.0 4.0 1 EPA 8260C 11/221201609:07 I1/=01615:32 SS Certifications: CfDOH,NELAC-NY10854,NJDEP,PADEP 1330-20-7 Xylenes,Total ND ug/kg dry 6.0 12 1 EPA 8260C 1122/2016 08:07 11222016 15:32 SS Certifications: CTDOH,NELAC-NY I0854,NJDEP,PADEP Surrogate Recoveries Result Acceptance Range 17060-07-0 Surrogate:1,1-Dichloroethane-d4 109% 77-115 2037-26-5 Surrogate:Toluene-& 98.7% 85-110 460.)0.4 Surrogate:p-BromoJluorobenzene 93.9% 76-130 Semi-Volatiles,CP-51(formerly STARS)List Lo¢-in Notes: Sample Notes: Sample Prepared by Method:EPA 3550C Reported to Date/Time Datefnme CAS No. Parameter Result Flab, Units LOD/MDL LOQ Dilution Reference Method Prepared Analyzed Analyst 120 RESEARCH DRIVE STRATFORD,CT 06615 ■ 132-02 89th AVENUE RICHMOND HILL,NY 11418 www.YORKLAB.com (203)325-1371 FAX(203)357-0166 ClientServices Page 13 of 18 1 ' Sample Information Client Sample ID: Excavation Bottom York Sample ID: 16KO861-05 York Proiect(SDG)No. Client Proiect ID Matrix Collection Date/Time Date Received 16KO861 42 Roanoke Avenue,Rye Brook,NY Soil November 18,2016 10:00 am 11/21/2016 Semi-Volatiles.CP-51(formerly STARS)List Loe-in Notes: Sample Notes: Sample Prepared by Method:EPA 3550C Reported to Date/Time Date/Time CAS No. Parameter Result Flag Units LODJMDL LOQ Dilution Reference Method Prepared Analyzed Analyst 83-32-9 Acenaphthene ND ug/kg dry 48 96 2 EPA 8270D 11/28/201606:13 1128201623:22 KH Cerifications: CrDOH,NELAC-NY10854,NJDEP,PADEP 208-96-8 Acenaphthylene ND ug/kg dry 48 96 2 EPA 8270D 11282016 06:13 11282016 23:22 KH Certifications: CrD0H,NELAC-NY10854,NJDEP.PADEP 120-12-7 Anlhracene ND ug/kg dry 48 96 2 EPA 8270D 11282016 06:13 11282016 23:22 KH Certifies(ions: CfDOH,NELAC-NY10854,NJDEP,PADEP 56-55-3 Benzo(a)anthracene ND ug/kg dry 48 96 2 EPA 8270D 1128201606:13 1128201623:22 KH Certifications: CTD0H,NELAC-NY10854,NJDEPPADEP 50-32-8 Benzo(a)pyrene ND ug/kg dry 48 96 2 EPA 8270D 1128201606:13 1128201623:22 KH Certifications: CTDOH,NELAC-NY 10854,NJDEP,PADEP 205-99-2 Benzo(b)fluoranthene ND ug/kg dry 48 96 2 EPA 8270D 1128201606d3 1128201623:22 KH Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP 191-24-2 Benzo(g,h,i)perylene ND ug/kg dry 48 96 2 EPA 8270D 1128201606:13 1128/20I623:22 KH Certifications: CTDOH,NELAC-NY 10854,NJDEP,PADEP 207-08-9 Benzo(k)fluoranthene ND ug/kg dry 48 96 2 EPA 8270D 1128201606:13 1128201623:22 KH Certificalions: CTD0H,NELAC-NY10854,NJDEPPADEP 218-01-9 Chrysene ND ug/kg dry 48 96 2 EPA 8270D 11282016 06:13 11282016 23:22 KH Certifications: CTD0H,NELAC-NY10854,NJDEP,PADEP 53-70-3 Dibenzo(a,h)anthracene ND ug/kg dry 48 96 2 EPA 8270D 1128201606:13 11/28201623:22 KH Certificnions: CrDOH,NELAC-NY10854,NJDEPPADEP 20644-0 Fluoranthene ND ug/kg dry 48 96 2 EPA 8270D 1128201606:13 1128201623:22 KH Certifications: C7DOH,NELAC-NY10854,NJDEPPADEP 86-73-7 Fluorene ND ug/kg dry 48 96 2 EPA 8270D 11282016 06:13 11282016 23:22 KH Certifications: NELAGNY10854,NJDEP,PADEP 193-39-5 indeno(1,2,3cd)pyrene ND ug/kg dry 48 96 2 EPA 8270D 1128201606:13 1128201623:22 KH Certifications: CI'DOH,NELAC-NY10854,NJDEP,PADEP 91-20-3 Naphthalene N D ug/kg dry 48 96 2 EPA 8270D 11282016 06:13 11282016 23:22 KH Certifications: CfD0H,NELAC-NY10854,NJDEPPADEP 85-01-8 Phenanthrene ND ug/kg dry 48 96 2 EPA 8270D 1128201606:13 1128201623:22 KH Certifications: CTD0H,NELAC-NY10854,NJDEPPADEP 129-00-0 Pyrene ND ug/kg dry 48 96 2 EPA 8270D 1128201606:13 1128/201623:22 KH Certifications: CTD0H,NELAC-NY10854,NJDEP,PADEP Surrogate Recoveries Result Acceptance Range 4165-60-0 Surrogate:Nitrobenzene-d5 72.9% 21-108 321-60-8 Surrogate:2-Fluorobiphenyl 62.7% 21-113 1718-51-0 Surrogate:Terphenyl-d/4 67.3% 24-116 Total Solids Loe-in Notes: Sample Notes: Sample Prepared by Method:%Solids Prep Reported to Date/Time Date/time CAS No. Parameter Result Flag Units LOD/MDL LOQ Dilution Reference Method Prepared Analyzed Analyst 120 RESEARCH DRIVE STRATFORD,CT 06615 ■ 132-02 89th AVENUE RICHMOND HILL,NY 11418 www.YORKLAB.com (203)325-1371 FAX(203)357-0166 ClientServices Page 14 of 18 1 ' Sample Information Client Sample ID: Excavation Bottom York Sample ID: 16KO861-05 York Project(SDG)No. Client Project ID Matrix Collection Date/Time Date Received 16KO861 42 Roanoke Avenue,Rye Brook,NY Soil November 18,2016 10:00 am 11/21/2016 Total Solids Loa-in Notes: Sample Notes: Sample Prepared by Method:io Solids Prep Reported to Date/Time Date/Time CAS No. Parameter Result Flag Units LOD/MIDI, LOQ Dilution Reference Method Prepared Analyzed Analyst solids *%Solids 86.6 0.100 0.100 1 SM 254OG 11/29201609:34 11129/201616:04 DMI Certifications: CfDOH 120 RESEARCH DRIVE STRATFORD,CT 06615 ■ 132-02 89th AVENUE RICHMOND HILL,NY 11418 www.YORKLAB.com (203)325-1371 FAX(203)357-0166 ClientServices Page 15 of 18 1 ' Volatile Analysis Sample Containers Lab ID Client Sample ID Volatile Sample Container 16KO861-01 Sidewall-I 40mL Vial with Stir Bar-Cool 4°C 16KO861-02 Sidewall-2 40mL Vial with Stir Bar-Cool 4'C 16KO861-03 Sidewall-3 40mL Vial with Stir Bar-Cool 4'C 16KO861-04 Sidewall-4 40mL Vial with Stir Bar-Cool 4°C 16KO861-05 Excavation Bottom 40ml- Vial with Stir Bar-Cool 4°C 120 RESEARCH DRIVE STRATFORD,CT 06615 ■ 132-02 89th AVENUE RICHMOND HILL,NY 11418 www.YORKLAB.com (203)325-1371 FAX(203)357-0166 ClientServices Page 16 of 18 t ' Notes and Definitions J Detected below the Reporting Limit but greater than or equal to the Method Detection Limit(MDL/LOD)or in the case of a TIC,the result is an estimated concentration. Analyte is not certified or the state of the samples origination does not offer certification for the Analyte. ND NOT DETECTED-the analyte is not detected at the Reported to level(LOQ/RL or LOD/MDL) RL REPORTING LIMIT-the minimum reportable value based upon the lowest point in the analyte calibration curve. LOQ LIMIT OF QUANTITATION-the minimum concentration of a target analyte that can be reported within a specified degree of confidence. This is the lowest point in an analyte calibration curve that has been subjected to all steps of the processing/analysis and verified to meet defined criteria.This is based upon NELAC 2009 Standards and applies to all analyses. LOD LIMIT OF DETECTION-a verified estimate of the minimum concentration of a substance in a given matrix that an analytical process can reliably detect. This is based upon NELAC 2009 Standards and applies to all analyses conducted under the auspices of EPA SW-846. MDL METHOD DETECTION LIMIT- a statistically derived estimate of the minimum amount of a substance an analytical system can reliably detect with a 99%confidence that the concentration of the substance is greater than zero. This is based upon 40 CFR Part 136 Appendix B and applies only to EPA 600 and 200 series methods. Reported to This indicates that the data for a particular analysis is reported to either the LOD/MDL,or the LOQ/RL. In cases where the"Reported to"is located above the LOD/MDL,any value between this and the LOQ represents an estimated value which is "J"flagged accordingly.This applies to volatile and semi-volatile target compounds only. NR Not reported RPD Relative Percent Difference Wet The data has been reported on an as-received(wet weight)basis Low Bias Low Bias flag indicates that the recovery of the flagged analyze is below the laboratory or regulatory lower control limit. The data user should take note that this analyte may be biased low but should evaluate multiple lines of evidence including the LCS and site-specific MS/MSD data to draw bias conclusions. In cases where no site-specific MS/MSD was requested,only the LCS data can be used to evaluate such bias. High Bias High Bias flag indicates that the recovery of the flagged analyte is above the laboratory or regulatory upper control limit. The data user should take note that this analyte may be biased high but should evaluate multiple lines of evidence including the LCS and site-specific MS/MSD data to draw bias conclusions. In cases where no site-specific MS/MSD was requested,only the LCS data can be used to evaluate such bias. Non-Dir. Non-dir.flag(Non-Directional Bias)indicates that the Relative Percent Difference(RPD)(a measure of precision)among the MS and MSD data is outside the laboratory or regulatory control limit. This alerts the data user where the MS and MSD are from site-specific samples that the RPD is high due to either non-homogeneous distribution of target analyte between the MS/MSD or indicates poor reproducibility for other reasons. If EPA SW-846 method 8270 is included herein it is noted that the target compound N-nitrosodiphenylamine(NDPA)decomposes in the gas chromatographic inlet and cannot be separated from diphenylamine(DPA). These results could actually represent 100%DPA,100%NDPA or some combination of the two. For this reason,York reports the combined result for n-nitrosodiphenylamine and diphenylamine for either of these compounds as a combined concentration as Diphenylamine. If Total PCBs are detected and the target aroclors reported are"Not detected", the Total PCB value is reported due to the presence of either or both Aooclors 1262 and 1268 which are non-target aroclors for some regulatory lists. 2chloroethylvinyl ether readily breaks down under acidic conditions. Samples that are acid preserved,including standards will exhibit breakdown.The data user should take note. Certification for pH is no longer offered by NYDOH ELAP. Semi-Volatile and Volatile analyses are reported down to the LOD/MDL,with values between the LOD/MDL and the LOQ being"J"flagged as estimated results. For analyses by EPA SW-846-8270D,the Limit of Quantitation(LOQ)reported for benzidine is based upon the lowest standard used for calibration and is not a verified LOQ due to this compound's propensity for oxidative losses during extraction/concentration procedures and non-reproducible chromatographic performance. 120 RESEARCH DRIVE STRATFORD,CT 06615 ■ 132-02 89th AVENUE RICHMOND HILL,NY 11418 www.YORKLAB.com (203)325-1371 FAX(203)357-0166 ClientServices, Page 17 of 18 s _I 0 C y1 ` T X u O U W ? w w NI IJ E n S o — ` E cp a a U p + ~ CJ U O @ N O Q a Q a a a' U a o S C r p w w w N rn m I n` a °a cu a s n. a a a U `n > c c M. Z E M E E w U U cn cn a W a w rc o s E a a a a a o o° Y �, i V O , .. u to O D U Z Z Z IW Z Z w U } L 73 G C X 77 r m > > > m O u a 4va�� Q w 0 F e 1p tp tao F s Cr CO A I Cc Gj n z r a � � G � < 1R c o o = J O r. � v Z U C I, Q z cn � cn <n cn c � 4� gg E a a a a a cn a � � a ,� o � Bt o Q I cn V � xr rro m a PE -�- P- _ U w V o Q ( Fa r .a., bFx. a t7 0. 0. ,c , r�r-j! .�Urj1 li b [ay, w G O J t U '� v: >• F I fD m O — _ O U E c N c ' E v u u O tI1 N U h P_ � � � ,�p_,jj• � _' ppW 0.� (n L � � U C e p 4 C O K+ d O O Vl of $• v� x H td O n '.t• O1 ao 0 a C4 cc Q n a ca •�` Fz Q u c a mcEa a > X j � '� Q W C ti c U Q E mOU ti a (n o o a E G ^ v0 Pn' a`n v " - : .o Z U Q Lli x m a kS LL Cl 0 O -G 0o aro of X �' O .. U) v n I O N E zi m ` ai w n E ll 4t ¢ i`1 Q (O � a PPno (n o o a o a o % Z U c Z N .y Y ❑ U 'O C T O N -\ 4 ¢ ` E 0 t7 L cll E to C Uj U E N O N C .>+ In r w o o `� E _n 4r �'r a -Z. d CL CL Cl) 3 C E o c E % C .q O Page 18 of 18 APPENDIX 3: Non-Hazardous Waste Manifest and Facility Weight Ticket for Soil Transportation and Disposal Deep Green of New York, Inc. SOI ACKING FORM (01V N"Y MOW(lNCGNI DAT F H M RESPONSIBLE FOR PAYMENT PART 364 VEHICLE PLATE NO FACILITY NO. JOB NO. LOAD NO. NvFC B06 DG101991 GENE OR AND BILLING ADDRESS GENERATOR PHONE NO. RICK MARINI GENERATOR CONTACT 42 ROANKE AVENUE Port Chester,10573 GENERATOR FAX NO. CUSTOMER ACCT.NO.WITH DEEP GREEN CONSULTANT NAME AND BILLING ADDRESS CONSULTANT PHONE NO. 914-347.1972 HVEC CONSULTANT CONTACT 462 LAKEVIEW AVE VALHALLA,NY10595 CONSULTANT FAX NO. CUSTOMER ACCT.N0.WITH DEEP GREEN GENERATION SITE(TRANSPORT FROM)NAME AND ADDRESS SIT PHONE NO. RICK MARINI SITE CONTACT 42 ROANKE AVENUE Pon Chester,10573 SITE FAX NUMBER 1 i PCS PROCESSING FACILITY(TRANSPORT TO)NAME AND ADDRESS FACILITY PHONE NO. PART 360 PERMIT NO. ' 845.562-8778 3.334"1 50-0000 1.0 j DEEP GREEN OF NEW YORK,INC. FACILITY CONTACT 1106 RIVER ROAD Amy Kane NEW WINDSOR.NV 12553 FACILITY FAX NO. ! 845-562-9566 TRANSPORTER NAME AND ADDRESS TRANSPORTER PHONE NO. TRANSPORTER PART 384 PERMIT NO. H V EC 914-347-1972 3 A-912 ' 462 LAKEVIEW AVE TRANSPORTER CONTACT TRANSPORTER DOT NO. VALHALLA.NY10595 Permit No.:3A-912 TRANSPORTER FAX NO. CUSTOMER ACCT.NO.WITH DEEP GREEN MATERIALTE8T*6G DESCRIPTION OF DELIVERY GROSS TARE NET (CliECX APPROPRIATE BOXES FOR TESTS CONDUCTED) WEIGHT WEIGHT(TONS) WEIGHT(TONS) (TONS) ❑TOTAL PETROLEUM HYDROCARDONS ❑BENZENE(TOTAL) n BENZENE(TCLP) NONHAZARDOUS ❑LEAD(TOTAL) L)LEAD(TCLP) 7� 0QGNZENEROLUF.NE/ETHY1-BFNZFNFIXYLENE PETROLEUM {(i V ,•((/ ' D METHYL iBUTYL ETHER(MTSE) L]HALOGENATED VOLATILE ORGANICS CONTAMINATED Fl HEAVY METALS(TOTAL) CI HEAVY METALS(TCLP) SOIL ❑OTHER(PLEASE LIST): G DGUTATOR'S AND/OR CONSULTANTS CERTIFICATION: I CERTIFY THAT THE SOIL REFERENCED HEREIN IS TAKEN ENTIRELY FROM THOSE SOILS DESCRIBED IN THE GENERATOR WASTE PROFILE SHEET COMPLETED AND CERTIFIED BY ME FOR THE GENERATION SITE SHOWN ABOVE AND NOTHING HAS BEEN ADDED OR DONE TO SUCH SOIL THAT WOULD ALTER IT IN ANY WAY.1 HEREBY AFFIRM UNDER PENALTY OF PFFUURY THAT INFORMATION PROVIDED ON THIS DOCUMENT IS TRUE TO THE BEST OF MY KNOWLEDGE AND BELIEF,AND THAT I HAVE THE AUTHORITY AB (TITLE)OF (ENTITY)TO SIGN THIS TRACKING DOCUMENT PURSUANT TO 6 NYCRR PART 3W 1 AM AWARE.THAT ANY FALSE STATEMENT MADE HEREIN IS PUNISHABLE AS A CLASS A MI MEANOR PUML4WT TO SECTION 210.45 OF THE PENAL LAW. PRINT OR TYPE,NAME SIQ—�E „ per.E 77) ❑CONBUI0GIENIZ�TANT 1 OR 1' �J ftl TRAN6PORTER'8 CERTIFICATION: 1 ACKNOWLEDGE RECEIPT OF THE SOIL DESCRIBED, E AND CERTIFY THAT SUCH SOIL IS BEING DELIVERED W EXACTLY THE SAME CONDITION AS WHEN RECEIVED I FURTHER CERTIFY THAT THIS SOIL I8 BEING DIRECTLY TRANSPORTED FROM THE GENERATION SITE TO THE PCS PROCESSING FACIIJITY WITHOUT OFF-LOADING. ADDING TO,SUBTRACTING FROM OR IN ANY WAY DELAYING DELIVERY TO SUCH SITE. _ -_ EAR PRINT OR E NAME SIONA MONTHi DATE A 1 ^S7 , f= / /Q TRANSPORTER DISCREPANCY BOX(ANY DISCREPANCIES!N THE TRANSPORTER NAME PCS PROCESSMIK�NAME on LOCA7TON,OR MATERm TESTM OR QLwmTY SHOULD BE NOTED HER PCs VISINO FACIL C! Fl THE RECEIPT OF THE BOIL COVERED by THIS TRACKMiCl FORM EXCEPT As NOTED DlLOW. PRI 3 RE MO- DA k fe�' PROC I F .IL DI S EPANCY BOX(ANY DISCREPANCIES IN ABOVE INFORMATj SHOULD 8E D HEAfJ STRUCTOHS GENERATOR COMASWS ALL ITEMS IN GENERATOR AND/OR CONSULTANT BOXES,RETAINS C OF4 PORTER. s TRANSPORTER C ALL ITEMS IN TRANSPORTER BOXES,RETAINS COPY 03,AND GIVES REMAINING COPIES TO THE P PROCESSING FACILITY COMPLETES ALL ITEMS IN PROCESSING FACILITY BOXES,RETAINS COPY 02.AND RETURNS COPY•1 TO THE GENFRATOR p)WEEKS. DEEP GREEN FACILITY COPY#1 CVCC Q=p..G,een of New York Weig ht Ticket Job # Vcf-� Tons Time in / Date 1� Gross Weight �- `;'°:, t(J 1 (6 Tons rime Out / Date +r ; Tare Weight a 1-13;,'a LO--- NET WEIGHT I�ZD TONS = 7(1 Signature Weiahmaster license # 330154 Soil Processing Facility 1106 River Road•New Windsor, NY 12553 845-562-8776•FAX: 845-562-9566 www.deepgreenofny.com 10/8/24, 11:55 AM Spill Incidents Database Search IWYORK Department of TE OF ORTUNITY Environmental Conservation Spill Incidents Database Search Details Spill Record Administrative Information DEC Region: 3 Spill Number: 1607332 Spill Date/Time Spill Date: 10/26/2016 Spill Time: 01 .10.00 PM Call Received Date: 10/26/2016 Call Received Time: 02:10:00 PM Location Spill Name: MARINI - UST Address: 42 ROANOKE AVENUE City: RYE BROOK County: Westchester Spill Description Material Spilled Amount Spilled Resource Affected #2 fuel oil UNKNOWN Soil Cause: Equipment Failure Source: Private Dwelling Waterbody: Record Close Date Spill Closed: 01/10/2017 "Date Spill Closed" means the date the spill case was closed by the case manager in the Department of Environmental Conservation (the Department). The spill case was closed because either; a) the records and data submitted indicate that the necessary cleanup and removal actions have been completed and no further remedial activities are necessary, or b) the case was closed for administrative reasons (e.g., multiple reports of a single spill consolidated into a single spill number). The Department however reserves the right to require additional remedial work in relation to the spill, if in the future it determines that further action is necessary. If you have questions about this reported incident, please contact the Regional Office where the incident occurred. Refine This Search https://extapps.dec.ny.gov/cfmx/extapps/derexternal/spills/details.cfm?pageid=2 1/1 CERTIFICATE OF COMPLIANCE CERTIFICATE NUMBER: C82200-MH27530 Page 1 of 1 ISSUE DATE: August 22,2000 Issued to: ROTH INDUSTRIES 18DC South Des Plaines avenue Forest Park.IL 00130 Repots Reference: MH27530/OOME 12989 This is to Certify that representative samples of: Dal Series Nonmetallic Tartks for Oil Burner Fuel, Types b_'CL and 1O00L rated for Incloor/Outdoor Use and T-.pes 75OLH and 1CXLH rated for ind(x)r Luse Orth'. Have been investigated by Undem-riters Laboratories Inc.J in accordance with the Standard(s) indicated on this Certificate. Standard(s) for Safes♦: SU2238- Outline of Investigation fur Nlutnnetallic Tanks for Oil Bruner Fuel USE - This category covers nonmetallic tanks of the atmospheric t}pe intended primtril}•for the storage of fuel oil for supplying oil burners and similar egttipment. They-are intended for installation and use in accordance,%ith the Standard for the Installation of Oil Burning Equipment,NFPA 31,of the National Fire Protection Association. Additional Information: L1 MARK- The Listing Nlark of Undem-niters Laboratones Inc. on the product is the only nietbod prmided by LZ to identify products manufactured under its Listutg and Follow-Up Service. The Listing Mark for thesr prtducts includes the L1.symbul together with the word "LISTED",a control number,and the product name "I orinviallic Tank for Oil Burner Fuel". Only those products hearing the UL Listing Mark should be considered as being covered by LL's Listing and Follow-Up Service. 'I}r IT Lining hark rrtrrall.i indides the#dirg kln ekn ilrms:t1r syni-A U u1 a citck.O With tilt Nv,rd"I.I�s.1 I ,,,mtr,.d nuntlxr'mas Ixalpluntu-rru•)a%signed'+s L L:and thr pra:u t categon writ(-r'aincl iJentitierl as iadicued in the aupn yriat:1 1 Dirmton•. E nl itteer. Re%iew Engineer. . R. RIEGEL B. )M-RRI Undemmters Laboratories Inc. Undernriten I.aburatciriu Inc. 1 S'� •9L' •4� '• Y A - WZ�`�-" :+•S• .A 'z?1*. f.^ A -qC= �Yr• A '4 �r. A ML. - +?/s w A /.• V V V 1 V! L V V V 1}r� f � r� ���♦ r� 11..u.0'�'A- '..��TT i ..NI>/ ��ii �1/�r j ju�= �,,���f)1>/h'1 � •Cl/)/)IDS z{{� � ` 1�1>/~ }� � /�)1>IA :'i;�rs'tYi�} �1)1)1y, � :... /l11i��' hll''�:�.:. w «b)> � .�.i .u. .u.t_ �...ss J..u. - _. .u. vim. _. ..u. «d)>•. �4Y c LL N ,.. � 9 a CI Cd Y � ti u o pmo U U R .� �ccoonLO 06 ` w ° H Z a p W1 W77 Q may: "• LLJJ 0 0 Q b > �alow;Jeda� - h..� Wc M LU Y •� d � Q y I.a n .. _ `fly CA a 3 a CA UrA it 00 CN !3r•-% y - i = Y ,�p, ell rll+ s Il/lll `�'w / '' w ♦il A � � �lw )) r w /iAili/lr I � ii� bo I► V .� ^ = A !$. ^ �.,::> ACO® DATE(MMIDWYYYY) C CERTIFICATE OF LIABILITY INSURANCE 5/23/2016 THIS CERTIFICATE IS ISSUED AS A MATTER OF INFORMATION ONLY AND CONFERS NO RIGHTS UPON THE CERTIFICATE HOLDER. THIS CERTIFICATE DOES NOT AFFIRMATIVELY OR NEGATIVELY AMEND, EXTEND OR ALTER THE COVERAGE AFFORDED BY THE POLICIES BELOW. THIS CERTIFICATE OF INSURANCE DOES NOT CONSTITUTE A CONTRACT BETWEEN THE ISSUING INSURER(S), AUTHORIZED REPRESENTATIVE OR PRODUCER,AND THE CERTIFICATE HOLDER. IMPORTANT: If the certificate holder is an ADDITIONAL INSURED, the policy(ies) must be endorsed. If SUBROGATION IS WAIVED, subject to the terms and conditions of the policy,certain policies may require an endorsement. A statement on this certificate does not confer rights to the certificate holder in lieu of such endorsement(s). PRODUCER CONTACT Maria Plasencia NAME: _ Strategic Insurance Partners PHONE (973)667-2600 FNACX No):(973)667-5842 492 Franklin Avenue ADDRESS:mplasencia@siprisk.com INSURE S AFFORDING COVERAGE NAIC A Nutley NJ 07110 INSURERAGreat Divide Insurance Co. 25224 INSURED INSURER B ilarle svill_e Insurance Co 23582 Hudson Valley Environmental & Construction Corp INSURERC: 462 Lakeview Avenue INSURERD: INSURER E: Valhalla NY 10595 INSURER F: COVERAGES CERTIFICATE NUMBER:Kaster Cert REVISION NUMBER: THIS IS TO CERTIFY THAT THE POLICIES OF INSURANCE LISTED BELOW HAVE BEEN ISSUED TO THE INSURED NAMED ABOVE FOR THE POLICY PERIOD INDICATED. NOTWITHSTANDING ANY REQUIREMENT, TERM OR CONDITION OF ANY CONTRACT OR OTHER DOCUMENT WITH RESPECT TO WHICH THIS CERTIFICATE MAY BE ISSUED OR MAY PERTAIN, THE INSURANCE AFFORDED BY THE POLICIES DESCRIBED HEREIN IS SUBJECT TO ALL THE TERMS, EXCLUSIONS AND CONDITIONS OF SUCH POLICIES LIMITS SHOWN MAY HAVE BEEN REDUCED BY PAID CLAIMS. I NSR TYPE OF INSURANCE '.ADDL SUER POLICY NUMBER MM%DIIYYYY MM LICY EXP /DD/Y LIMITS LTR X COMMERCIAL GENERAL LIABILITY EACH OCCURRENCE $ 1,000,000 A CLAIMS-MADE aOCCUR PR MISET EaEoccurrenoe i 100,000 Ali ECP200195215 4/1/2016 4/1/2017 MED EXP(Any one person) S 5,000 PERSONAL&ADV INJURY = 1,000,000 GENT AGGREGATE LIMIT APPLIES PER: GENERAL AGGREGATE s 2,000,000 $ POLICY❑�T LOC PRODUCTS-COMP/OP AGG $ 2,000,000 OTHER Contractors Pollution $ 1,000,000 IT AUTOMOBILE LIABILITY accident IN L LIM Ea accident) $ 1,000,000 B I ANY AUTO BODILY INJURY(Per person) $ ALL OWNED SCHEDULED AUTOS BA 00000052518V 3/20/2016 3/20/2017 BODILY INJURY(Per acadent) S AUTOS NON-OWNED PROPERTY DAMAGE _ HIRED AUTOS AUTOS Per accident LISCH = UMBRELLA LAB OCCUR EACH OCCURRENCE S EXCESS LIAR CLAIMS-MADE AGGREGATE $ DED RETENTION$ $ WORKERS COMPENSATION PER AND EMPLOYERS'LIABILITY Y I N STATUTE ERH ANY PROPR I ETOR/PARTNER/EXECUTIVE E.L.EACH ACCIDENT $ OFFICER/MEMBER EXCLUDED? ❑ N/A (Mandatory In NH) E.L.DISEASE-EA EMPLOYE $ _ If yes,describe under DESCRIPTION OF OPERATIONS below E.L.DISEASE-POLICY LIMB I s DESCRIPTION OF OPERATIONS I LOCATIONS/VEHICLES (ACORD 101,Additional Remarks Schedule,may be attached if more space is required) Coverages are subject to Terms, Conditions and Exclusions on the policy(s) . CERTIFICATE HOLDER CANCELLATION SHOULD ANY OF THE ABOVE DESCRIBED POLICIES BE CANCELLED BEFORE Village of Rye Brook THE EXPIRATION DATE THEREOF, NOTICE WILL BE DELIVERED IN 938 King Street ACCORDANCE WITH THE POLICY PROVISIONS. Rye Brook, NY 10573 AUTHORIZED REPRESENTATIVE Mark Grossbard/MPL ©1988-2014 ACORD CORPORATION. All rights reserved. ACORD 25(2014/01) The ACORD name and logo are registered marks of ACORD INS025.omani e New York State Insurance Fund Workers'Compensation& Disability Benefits Specialists Since 1914 105 CORPORATE PARK DRIVE SUITE 200,WHITE PLAINS,NEW YORK 10604-3814 Phone:(914)253-4861 CERTIFICATE OF WORKERS' COMPENSATION INSURANCE mia� ikf An n Ann 271014843 HUDSON VALLEY ENVIRONMENTAL&CONSTRUCTION CORP 462 LAKEVIEW AVENUE VALHALLA NY 10595 Scan to Validate POLICYHOLDER CERTIFICATE HOLDER HUDSON VALLEY VILLAGE OF RYE BROOK ENVIRONMENTAL&CONSTRUCTION CORP 938 KING STREET 462 LAKEVIEW AVENUE RYE BROOK NY 10573 VALHALLA NY 10595 POLICY NUMBER CERTIFICATE NUMBER PERIOD COVERED BY THIS CERTIFICATE DATE W2097 383-0 443851 04/05/2016 TO 04/05/2017 5/24/2016 THIS IS TO CERTIFY THAT THE POLICYHOLDER NAMED ABOVE IS INSURED WITH THE NEW YORK STATE INSURANCE FUND UNDER POLICY NO. 2097 383-0 UNTIL 04/05/2017, COVERING THE ENTIRE OBLIGATION OF THIS POLICYHOLDER FOR WORKERS' COMPENSATION UNDER THE NEW YORK WORKERS' COMPENSATION LAW WITH RESPECT TO ALL OPERATIONS IN THE STATE OF NEW YORK, EXCEPT AS INDICATED BELOW, AND, WITH RESPECT TO OPERATIONS OUTSIDE OF NEW YORK, TO THE POLICYHOLDER'S REGULAR NEW YORK STATE EMPLOYEES ONLY. IF SAID POLICY IS CANCELLED,OR CHANGED PRIOR TO 04/05/2017 IN SUCH MANNER AS TO AFFECT THIS CERTIFICATE, 10 DAYS WRITTEN NOTICE OF SUCH CANCELLATION WILL BE GIVEN TO THE CERTIFICATE HOLDER ABOVE. NOTICE BY REGULAR MAIL SO ADDRESSED SHALL BE SUFFICIENT COMPLIANCE WITH THIS PROVISION. THE NEW YORK STATE INSURANCE FUND DOES NOT ASSUME ANY LIABILITY IN THE EVENT OF FAILURE TO GIVE SUCH NOTICE. THIS POLICY DOES NOT COVER CLAIMS OR SUITS THAT ARISE FROM BODILY INJURY SUFFERED BY THE OFFICERS OF THE INSURED CORPORATION. JAIME COLEMAN-PRESIDENT DAMIEN COLEMAN-VICE PRESIDENT OF HUDSON VALLEY ENVIRONMENTAL& CONSTRUCTION CORP THIS CERTIFICATE IS ISSUED AS A MATTER OF INFORMATION ONLY AND CONFERS NO RIGHTS NOR INSURANCE COVERAGE UPON THE CERTIFICATE HOLDER. THIS CERTIFICATE DOES NOT AMEND, EXTEND OR ALTER THE COVERAGE AFFORDED BY THE POLICY. NEW YORK STATE INSURANCE FUND DIRECTOR,INSURANCE FUND UNDERWRITING This certificate can be validated on our web site at https://www.nysif.com/cerUcertval.asp or by calling (888)875-5790 VALIDATION NUMBER: 771929919 U-26.3